CN209405746U - A kind of oil water separator for rectification under vacuum - Google Patents
A kind of oil water separator for rectification under vacuum Download PDFInfo
- Publication number
- CN209405746U CN209405746U CN201821631584.2U CN201821631584U CN209405746U CN 209405746 U CN209405746 U CN 209405746U CN 201821631584 U CN201821631584 U CN 201821631584U CN 209405746 U CN209405746 U CN 209405746U
- Authority
- CN
- China
- Prior art keywords
- tank body
- hydraulic fluid
- port
- fluid port
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 239000012530 fluid Substances 0.000 claims abstract description 20
- 230000002706 hydrostatic effect Effects 0.000 claims description 11
- 239000006260 foam Substances 0.000 claims description 5
- 238000004804 winding Methods 0.000 claims description 2
- 235000019198 oils Nutrition 0.000 abstract description 15
- 238000000926 separation method Methods 0.000 abstract description 10
- 238000004821 distillation Methods 0.000 abstract description 5
- 235000019476 oil-water mixture Nutrition 0.000 abstract description 4
- 238000000746 purification Methods 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 238000009510 drug design Methods 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 description 6
- FSEUPUDHEBLWJY-HWKANZROSA-N diacetylmonoxime Chemical compound CC(=O)C(\C)=N\O FSEUPUDHEBLWJY-HWKANZROSA-N 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- CDCMMFMDDMEKSC-UHFFFAOYSA-N n-butan-2-ylidenehydroxylamine;hydrochloride Chemical compound Cl.CCC(C)=NO CDCMMFMDDMEKSC-UHFFFAOYSA-N 0.000 description 2
- 239000005046 Chlorosilane Substances 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical compound Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 125000005646 oximino group Chemical group 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Removal Of Floating Material (AREA)
Abstract
The utility model belongs to purification technique field, discloses a kind of oil water separator for rectification under vacuum, comprising: tank body, it is the vertical tank body with the mouth of a river, hydraulic fluid port and port, the mouth of a river is located at tank base, and the hydraulic fluid port is located in the middle part of tank body, and the port is located at tank body top；And inlet tube, the tank body is protruded into water outlet, and its water outlet is lower than the hydraulic fluid port.The beneficial effects of the utility model, which include: 1, vertical tank body, provides sufficient separated space for oil-water mixture separation；2, the mouth of a river of vertical tank body and rational design, hydraulic fluid port, port match, and realize oil, water individual shunt；3, the real-time continuous separation during low-pressure distillation is realized.
Description
Technical field
The utility model relates to purification technique fields, more particularly, to a kind of water-oil separating for rectification under vacuum
Device.
Background technique
When preparing butanone oximino silane, diacetylmonoxime and chlorosilane are mainly subjected to hybrid reaction, excessive diacetylmonoxime
Byproduct hydrogen chloride can be adsorbed in the reaction, generate butanone oxime hydrochloride.The butanone oxime hydrochloride is recycled (usually
It is washed with water) it can get diacetylmonoxime crude product, wherein a large amount of water can be contained, it is therefore desirable to carry out purification point by rectification under vacuum
From.
Rectification under vacuum (being also known as evaporated in vacuo) is a kind of important method of separation and purification compound, is particularly suitable for high boiling
Point substance and those not up to the boiling point separation of compound that has just been thermally decomposed, aoxidized or polymerize and mentioned in air-distillation
It is pure.
Common oil water separator is generally unsuitable for rectification under vacuum, and is used for the gas-liquid separator of rectification under vacuum usually only
One port and a liquid mouth cannot achieve the real-time separation in distillation process and can only intermittently separate.
Utility model content
The purpose of the utility model is to overcome above-mentioned technical deficiencies, propose a kind of water-oil separating for rectification under vacuum
Device, the technical issues of solving to cannot achieve the real-time continuous separation during low-pressure distillation in the prior art.
To reach above-mentioned technical purpose, the technical solution of the utility model provides a kind of water-oil separating for rectification under vacuum
Device, comprising:
Tank body is the vertical tank body with the mouth of a river, hydraulic fluid port and port, and the mouth of a river is located at tank base, the hydraulic fluid port
In the middle part of tank body, the port is located at tank body top；And
Inlet tube, the tank body is protruded into water outlet, and its water outlet is lower than the hydraulic fluid port.
Compared with prior art, it is that oil-water mixture separation mentions that the beneficial effects of the utility model, which include: 1, vertical tank body,
For sufficient separated space；2, the mouth of a river of vertical tank body and rational design, hydraulic fluid port, port match, and realize that oil, water independently divide
Stream；3, the real-time continuous separation during low-pressure distillation is realized.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model；
Fig. 2 is the structural schematic diagram of hydrostatic plate.
Specific embodiment
In order to make the purpose of the utility model, technical solutions and advantages more clearly understood, below in conjunction with attached drawing and implementation
Example, the present invention will be further described in detail.It should be appreciated that specific embodiment described herein is only used to explain
The utility model is not used to limit the utility model.
The utility model provides a kind of oil water separator for rectification under vacuum, as shown in Figure 1, comprising: tank body 1 and into
Liquid pipe 2.
Tank body 1 is the vertical tank body with the mouth of a river 11, hydraulic fluid port 12 and port 13, and the mouth of a river 11 is located at 1 bottom of tank body, institute
It states hydraulic fluid port 12 and is located at 2 middle part of tank body, the port 13 is located at 1 top of tank body.
The tank body 1 is protruded into 2 water outlet 21 of inlet tube, and its water outlet 21 is lower than the hydraulic fluid port 12.
When work, the port 13 of tank body 1 connects external negative pressure device (such as air pump, vacuum chamber etc.), so as to be formed in tank body 1
Environment under low pressure.Oil-water mixture enters tank body 1 by inlet tube 2, and in a low pressure environment, passes through the long channel of vertical tank body 1
Gradually grease is layered, and grease can be sufficiently separated and come, and water is located in the middle grease to floating to 1 bottom of tank body, oil is sunk to
Mixed liquor is always positioned between hydraulic fluid port and the mouth of a river and will not be entrained away.Finally, exporting separation by the hydraulic fluid port 12 at 1 middle part of tank body
Oil out exports the water isolated by the mouth of a river 11 of 1 bottom of tank body.
Preferably, further including the hydrostatic plate 3 in the tank body 1, which is lower than the hydraulic fluid port 12.It is quiet
The oil-water mixture that liquid plate 3 is used to help enter tank body 1 is quickly tranquil, to improve the efficiency of oil liquid separation.
Preferably, being distributed several through-holes 31 on the hydrostatic plate 3, which is convenient for the oil droplet isolated upward
Floating, hydrostatic plate 3 at this time can be made covering 1 intracavity section of tank body, increase hydrostatic area.
Preferably, as shown in Fig. 2, the lower end surface of the hydrostatic plate 3 is equipped with gathered trough 32, the gathered trough 32 series winding institute
State through-hole 31.The oil droplet assembled at hydrostatic plate 3 is further collected by gathered trough 32 and is gathered, and forms bigger oil group, then passes through
Through-hole 31 is crossed to floating.Gathered trough 32 intervenes gathering for oil droplet, improves oil liquid separative efficiency.Gathered trough 32 can use
A variety of arrangements, such as radiant type arrangement, concentric ring type arrangement etc..
Preferably, further including the foam removal silk screen 4 in the tank body 1, which is lower than the port 13
And it is higher than the hydraulic fluid port 12.Foam removal silk screen 4 avoids oil or water by the gas of tank body 1 for removing the foam being likely to form in tank body 1
Mouth 13 is escaped, and external negative pressure device is polluted.
Specific embodiment of the present utility model described above does not constitute the restriction to scope of protection of the utility model.
Any other various changes and modifications that any technical concept according to the present utility model is made should be included in practical
In novel scope of protection of the claims.
Claims (5)
1. a kind of oil water separator for rectification under vacuum, characterized by comprising:
Tank body is the vertical tank body with the mouth of a river, hydraulic fluid port and port, and the mouth of a river is located at tank base, and the hydraulic fluid port is located at
In the middle part of tank body, the port is located at tank body top；And
Inlet tube, the tank body is protruded into water outlet, and its water outlet is lower than the hydraulic fluid port.
2. oil water separator according to claim 1, it is characterised in that: it further include being set to the intracorporal hydrostatic plate of the tank,
The hydrostatic plate is lower than the hydraulic fluid port.
3. oil water separator according to claim 2, it is characterised in that: be distributed several through-holes on the hydrostatic plate.
4. oil water separator according to claim 3, it is characterised in that: the lower end surface of the hydrostatic plate is equipped with gathered trough,
The gathered trough series winding through-hole.
5. oil water separator according to claim 1, it is characterised in that: further include being set to the intracorporal foam removal silk of the tank
Net, the foam removal silk screen is lower than the port and is higher than the hydraulic fluid port.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821631584.2U CN209405746U (en) | 2018-10-08 | 2018-10-08 | A kind of oil water separator for rectification under vacuum |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821631584.2U CN209405746U (en) | 2018-10-08 | 2018-10-08 | A kind of oil water separator for rectification under vacuum |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209405746U true CN209405746U (en) | 2019-09-20 |
Family
ID=67931506
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821631584.2U Active CN209405746U (en) | 2018-10-08 | 2018-10-08 | A kind of oil water separator for rectification under vacuum |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209405746U (en) |
-
2018
- 2018-10-08 CN CN201821631584.2U patent/CN209405746U/en active Active
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