CN209237406U - A kind of Chemical Manufacture continuous crystallisation device - Google Patents
A kind of Chemical Manufacture continuous crystallisation device Download PDFInfo
- Publication number
- CN209237406U CN209237406U CN201822156848.XU CN201822156848U CN209237406U CN 209237406 U CN209237406 U CN 209237406U CN 201822156848 U CN201822156848 U CN 201822156848U CN 209237406 U CN209237406 U CN 209237406U
- Authority
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- China
- Prior art keywords
- stirring
- main body
- described device
- chemical manufacture
- cross bar
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- 238000002425 crystallisation Methods 0.000 title claims abstract description 42
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 22
- 239000000126 substance Substances 0.000 title claims abstract description 15
- 238000003756 stirring Methods 0.000 claims abstract description 71
- 238000001035 drying Methods 0.000 claims description 12
- 238000010521 absorption reaction Methods 0.000 claims description 5
- 238000005070 sampling Methods 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- 230000008025 crystallization Effects 0.000 abstract description 26
- 239000002994 raw material Substances 0.000 abstract description 12
- 239000012452 mother liquor Substances 0.000 abstract description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000000243 solution Substances 0.000 description 5
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 239000011259 mixed solution Substances 0.000 description 3
- 239000004115 Sodium Silicate Substances 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000019353 potassium silicate Nutrition 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 235000019795 sodium metasilicate Nutrition 0.000 description 2
- 229910052911 sodium silicate Inorganic materials 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- HQAITFAUVZBHNB-UHFFFAOYSA-N sodium;pentahydrate Chemical compound O.O.O.O.O.[Na] HQAITFAUVZBHNB-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model discloses a kind of Chemical Manufacture continuous crystallisation devices, including apparatus main body, the upper end outer surface middle of described device main body is fixedly installed with stirring motor, the lower end of the stirring motor is provided with three-dimensional stirring-head, the three-dimensional stirring-head is made of stirring cross bar with stirring sheet, the outer surface upper end side of described device main body is provided with the first feed pipe, and the outer surface upper end other side of apparatus main body is provided with the second feed pipe, the outside of described device main body is provided with collet, is provided with centrifugal chamber below described device main body.The utility model makes the present apparatus that can stir more abundant by raw material in use by being provided with a series of structure, make to react quicker between raw material, be conducive to improve the efficiency of crystallization work, and the mother liquor after crystallization can be made full use of, keep crystallization work more thorough, also reduces the production cost of user.
Description
Technical field
The utility model relates to crystallization apparatus field, specially a kind of Chemical Manufacture continuous crystallisation device.
Background technique
Crystallization apparatus is the device that a kind of pair of target solution carries out crystallization work, generally reaction kettle or crystallizer etc.,
In the production preparation process of metasilicate pentahydrate sodium, continuous crystallisation device is commonly used；Existing aqueous sodium metasilicate production connects
The majority that continuous crystallization apparatus uses is anchor formula agitating paddle, just can not stir raw material more abundant in this way, can reduce crystallization
The efficiency of work, and the mother liquor after crystallization can not be made full use of, crystallization work can not be made more thorough, also increasing makes
The production cost of user.
Utility model content
The purpose of this utility model is to provide a kind of Chemical Manufacture continuous crystallisation devices, to solve above-mentioned background technique
The problem of middle proposition.
To achieve the above object, the utility model provides the following technical solutions: a kind of Chemical Manufacture continuous crystallisation device,
Including apparatus main body, the upper end outer surface middle of described device main body is fixedly installed with stirring motor, the stirring motor
Lower end is provided with three-dimensional stirring-head, and the three-dimensional stirring-head is made of stirring cross bar with stirring sheet, described device main body
Outer surface upper end side is provided with the first feed pipe, and the outer surface upper end other side of apparatus main body is provided with the second feed pipe,
The outside of described device main body is provided with collet, and centrifugal chamber, the lower end of the centrifugal chamber are provided with below described device main body
Outer surface is fixedly installed with drying box, and the side outer surface thread of drying box is connected with collecting chamber.
Preferably, the stirring sheet is fixedly mounted on the outside of stirring cross bar, and the quantity of the stirring cross bar is four groups, often
Group has several, wherein the outer end for stirring cross bar described in two groups is movably installed with brush head, several stirring cross bars are in different
Plane, the quantity of the stirring sheet are several groups, and the quantity of stirring sheet described in stirring sheet is in different planes.
Preferably, a side external surface of the centrifugal chamber is fixedly installed with micropump, and micropump and the first feed pipe it
Between be provided with circulation pipe.
Preferably, the inner wall of the collecting chamber is movably installed with moisture-absorption box, and be provided at the internal edge of collecting chamber every
Hot plate is provided with connecting rod and connecting tube between the collecting chamber and drying box.
Preferably, discharge nozzle is provided between the centrifugal chamber and apparatus main body, the external activity of discharge nozzle, which is equipped with, to be put
Pellet valve.
Preferably, one side position of outer surface lower end of described device main body is provided with sampling observation mouth, and the lower end of apparatus main body
Outer surface side is fixedly installed with thermometer.
In conclusion the utility model has the following beneficial effects:
1, three-dimensional stirring-head is provided with by the lower end in stirring motor, three-dimensional stirring-head is by stirring cross bar and stirring
Piece composition, stirring sheet are fixedly mounted on the outside of stirring cross bar, and the quantity for stirring cross bar is four groups, and every group has several, wherein
The outer end of two groups of stirring cross bars is movably installed with brush head, several stirring cross bars are in different planes, and the quantity of stirring sheet is
Several groups, the quantity of stirring sheet stirring sheet are in different planes, in use, firstly, powering on to device, at this time
Stirring motor is just in energized state, by waterglass raw material by the first feed pipe adding apparatus, by sodium hydroxide solution by
In two feed pipe adding apparatus, start stirring motor, stirring motor will drive three-dimensional stirring-head to rotate, stirred
Cheng Zhong needs to be passed through the temperature inside steam raising device into collet, since each stirring cross bar is not at stirring sheet
In same plane, can raw material be stirred more abundant in stirring in this way, make to react quicker between raw material, favorably
In the efficiency for improving crystallization work；
2, by being provided with centrifugal chamber below apparatus main body, a side external surface of centrifugal chamber is fixedly installed with miniature
Pump, and it is provided with circulation pipe between micropump and the first feed pipe, secondly, being checked by sampling observation mouth molten after being stirred
Liquid component, meets the requirements, and stops inputting steam into collet, starts to be passed through cooling water and cools down to it, carries out crystallization work,
The mixed solution of initial crystallization is reached in centrifugal chamber by discharge nozzle, by obtaining mother liquor and crystallization wet feed, mother liquor after centrifuge chamber
It is entered in the first feed pipe under the action of micropump by circulation pipe, sufficiently benefit can be carried out to the mother liquor after crystallization in this way
With, make crystallize work it is more thorough, also reduce the production cost of user.
Detailed description of the invention
Fig. 1 is the overall structure diagram of the utility model；
Fig. 2 is the interior views of the collecting chamber of the utility model；
Fig. 3 is the partial view of the three-dimensional stirring-head of the utility model.
In figure: 1, apparatus main body；2, stirring motor；3, three-dimensional stirring-head；31, cross bar is stirred；32, stirring sheet；33, it brushes
Head；4, the first feed pipe；5, the second feed pipe；6, mouth is inspected by random samples；7, centrifugal chamber；71, micropump；72, circulation pipe；8, drying box；
9, collecting chamber；91, thermal insulation board；92, moisture-absorption box；93, moisture-absorption box；94, connecting rod；10, collet.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
In the description of the present invention, it should be noted that term " on ", "lower", "inner", "outside" " front end ", " after
The orientation or positional relationship of the instructions such as end ", " both ends ", " one end ", " other end " is that orientation based on the figure or position are closed
System, is merely for convenience of describing the present invention and simplifying the description, rather than the device or element of indication or suggestion meaning are necessary
It with specific orientation, is constructed and operated in a specific orientation, therefore should not be understood as limiting the present invention.In addition,
Term " first ", " second " are used for descriptive purposes only and cannot be understood as indicating or suggesting relative importance.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " is pacified
Dress ", " being provided with ", " connection " etc., shall be understood in a broad sense, such as " connection ", may be a fixed connection, be also possible to detachably connect
It connects, or is integrally connected；It can be mechanical connection, be also possible to be electrically connected；It can be directly connected, intermediate matchmaker can also be passed through
Jie is indirectly connected, and can be the connection inside two elements.It for the ordinary skill in the art, can be with concrete condition
Understand the concrete meaning of above-mentioned term in the present invention.
Fig. 1-3 is please referred to, a kind of embodiment provided by the utility model: a kind of Chemical Manufacture continuous crystallisation device, packet
Apparatus main body 1 is included, the upper end outer surface middle of apparatus main body 1 is fixedly installed with stirring motor 2,2 model of stirring motor
Y80M1-4, the lower end of stirring motor 2 are provided with three-dimensional stirring-head 3, and three-dimensional stirring-head 3 is by stirring cross bar 31 and stirring sheet
32 compositions, the outer surface upper end side of apparatus main body 1 is provided with the first feed pipe 4, and the outer surface upper end of apparatus main body 1 is another
Side is provided with the second feed pipe 5, and the outside of apparatus main body 1 is provided with collet 10, and the lower section of apparatus main body 1 is provided with centrifugal chamber 7,
The lower end outer surface of centrifugal chamber 7 is fixedly installed with drying box 8, and the side outer surface thread of drying box 8 is connected with collecting chamber 9,
Chemical Manufacture continuous crystallisation device can stir raw material more abundant in use, make to react between raw material
Must be quicker, be conducive to the efficiency for improving crystallization work, and can make full use of to the mother liquor after crystallization, make to crystallize work more
Add thoroughly, also reduces the production cost of user.
Further, stirring sheet 32 is fixedly mounted on the outside of stirring cross bar 31, and the quantity of stirring cross bar 31 is four groups, every group
There are several, wherein the outer end of two groups of stirring cross bars 31 is movably installed with brush head 33, several stirring cross bars 31 are in different
Plane, the quantity of stirring sheet 32 are several groups, and the quantity of 32 stirring sheet 32 of stirring sheet is in different planes, stirring sheet 32 with stir
It mixes cross bar 31 and is interspersed and raw material can be mixed more abundant.
Further, a side external surface of centrifugal chamber 7 is fixedly installed with micropump 71, and micropump 71 and the first feed pipe 4
Between be provided with circulation pipe 72, the mother liquor after being centrifuged is passed through circulation by the model MP-10RN of the micropump 71, micropump 71
Pipe 72 is transported in the first feed pipe 4.
Further, the inner wall of collecting chamber 9 is movably installed with moisture-absorption box 92, and be provided at the internal edge of collecting chamber 9 every
Hot plate 91 is provided with connecting rod 94 and connecting tube 93 between collecting chamber 9 and drying box 8, thermal insulation board 91 is for preventing crystallization siccative
It is heated to melt.
Further, discharge nozzle is provided between centrifugal chamber 7 and apparatus main body 1, the external activity of discharge nozzle is equipped with blowing
Ball valve, emptying ball valve are used to release the mixed solution of initial crystallization.
Further, one side position of outer surface lower end of apparatus main body 1 is provided with sampling observation mouth 6, and outside the lower end of apparatus main body 1
Surface side is fixedly installed with thermometer, and thermometer is for the temperature inside detection device main body 1.
It should be noted that the utility model is a kind of Chemical Manufacture continuous crystallisation device, mainly for the preparation of five water
Sodium metasilicate, in use, firstly, powering on to device, stirring motor 2 is just in energized state at this time, by water glass
Glass raw material is by 4 adding apparatus of the first feed pipe, by sodium hydroxide solution by 5 adding apparatus of the second feed pipe, starting stirring
Motor 2, stirring motor 2 will drive three-dimensional stirring-head 3 to rotate, and in whipping process, need to be passed through into collet 10
Steam improves the temperature inside device, since each stirring cross bar 31 is not in same plane with stirring sheet 32, exists in this way
Raw material can be stirred more abundant when stirring, make to react quicker between raw material, be conducive to improve crystallization work
Efficiency, secondly, checking solution component after being stirred by inspecting mouth 6 by random samples, meeting the requirements, stop inputting into collet 10
Steam, starts to be passed through cooling water and cools down to it, carries out crystallization work, the mixed solution of initial crystallization by discharge nozzle reach from
In ventricle 7, mother liquor and crystallization wet feed are obtained after being centrifuged by centrifugal chamber 7, mother liquor passes through circulation pipe 72 under the action of micropump 71
It enters in the first feed pipe 4, the mother liquor after crystallization can be made full use of in this way, keep crystallization work more thorough,
The production cost of user is reduced, finally, crystallization wet feed enters in drying box 8 by after drying, reaches and is stored in collecting chamber 9,
It is more practical.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and
And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new
The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in
All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting
Related claim.
Claims (6)
1. a kind of Chemical Manufacture continuous crystallisation device, including apparatus main body (1), it is characterised in that: described device main body (1)
Upper end outer surface middle is fixedly installed with stirring motor (2), and the lower end of the stirring motor (2) is provided with three-dimensional stirring-head
(3), the three-dimensional stirring-head (3) is made of stirring cross bar (31) and stirring sheet (32), the outer surface of described device main body (1)
Upper end side is provided with the first feed pipe (4), and the outer surface upper end other side of apparatus main body (1) is provided with the second feed pipe
(5), the outside of described device main body (1) is provided with collet (10), and centrifugal chamber (7) are provided with below described device main body (1),
The lower end outer surface of the centrifugal chamber (7) is fixedly installed with drying box (8), and the side outer surface thread connection of drying box (8)
There are collecting chamber (9).
2. a kind of Chemical Manufacture continuous crystallisation device according to claim 1, it is characterised in that: the stirring sheet (32)
It is fixedly mounted on the outside of stirring cross bar (31), the quantity of stirring cross bar (31) is four groups, and every group there are several, wherein two
The outer end of group stirring cross bar (31) is movably installed with brush head (33), several stirrings cross bar (31) are in different planes,
The quantity of the stirring sheet (32) is several groups, and the quantity of stirring sheet (32) stirring sheet (32) is in different planes.
3. a kind of Chemical Manufacture continuous crystallisation device according to claim 1, it is characterised in that: the centrifugal chamber (7)
A side external surface be fixedly installed with micropump (71), and be provided with circulation pipe between micropump (71) and the first feed pipe (4)
(72).
4. a kind of Chemical Manufacture continuous crystallisation device according to claim 1, it is characterised in that: the collecting chamber (9)
Inner wall be movably installed with moisture-absorption box (92), and thermal insulation board (91), the collecting chamber are provided at the internal edge of collecting chamber (9)
(9) connecting rod (94) and connecting tube (93) are provided between drying box (8).
5. a kind of Chemical Manufacture continuous crystallisation device according to claim 1, it is characterised in that: the centrifugal chamber (7)
Discharge nozzle is provided between apparatus main body (1), the external activity of discharge nozzle is equipped with emptying ball valve.
6. a kind of Chemical Manufacture continuous crystallisation device according to claim 1, it is characterised in that: described device main body
(1) one side position of outer surface lower end is provided with sampling observation mouth (6), and the lower end outer surface side of apparatus main body (1) is fixedly mounted
There is thermometer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822156848.XU CN209237406U (en) | 2018-12-21 | 2018-12-21 | A kind of Chemical Manufacture continuous crystallisation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201822156848.XU CN209237406U (en) | 2018-12-21 | 2018-12-21 | A kind of Chemical Manufacture continuous crystallisation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN209237406U true CN209237406U (en) | 2019-08-13 |
Family
ID=67533923
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201822156848.XU Expired - Fee Related CN209237406U (en) | 2018-12-21 | 2018-12-21 | A kind of Chemical Manufacture continuous crystallisation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN209237406U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116492958A (en) * | 2023-04-23 | 2023-07-28 | 江苏欧克动物药业有限公司 | Efficient type device and process for preparing ivermectin special for antiparasitic |
-
2018
- 2018-12-21 CN CN201822156848.XU patent/CN209237406U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116492958A (en) * | 2023-04-23 | 2023-07-28 | 江苏欧克动物药业有限公司 | Efficient type device and process for preparing ivermectin special for antiparasitic |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190813 Termination date: 20201221 |