CN208097466U - It is used to prepare the macroporous resin enrichment device of matrine - Google Patents

It is used to prepare the macroporous resin enrichment device of matrine Download PDF

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Publication number
CN208097466U
CN208097466U CN201820244490.3U CN201820244490U CN208097466U CN 208097466 U CN208097466 U CN 208097466U CN 201820244490 U CN201820244490 U CN 201820244490U CN 208097466 U CN208097466 U CN 208097466U
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CN
China
Prior art keywords
tank
macroporous resin
rack
matrine
resin enrichment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201820244490.3U
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Chinese (zh)
Inventor
魏硕
郭继昌
李桂菊
孟庆苓
王秀珍
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cangzhou Zheng Xing Biological Pesticide Co Ltd
Original Assignee
Cangzhou Zheng Xing Biological Pesticide Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cangzhou Zheng Xing Biological Pesticide Co Ltd filed Critical Cangzhou Zheng Xing Biological Pesticide Co Ltd
Priority to CN201820244490.3U priority Critical patent/CN208097466U/en
Application granted granted Critical
Publication of CN208097466U publication Critical patent/CN208097466U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model relates to a kind of macroporous resin enrichment devices for being used to prepare matrine, it includes rack, the tank body being rotatably erected in the rack, and the driving mechanism for driving the tank body reciprocating rotation in the rack, and the guide holder being sheathed on outside the tank body is equipped in the rack;It further include that top is fixed on the rack and the intracorporal hollow agitating shaft of tank is inserted into bottom end, and the hollow agitating paddle in the tank body is connected on the hollow agitating shaft, the hollow agitating paddle is connected to the hollow agitating shaft and offers multiple liquid distributing holes on the hollow agitating paddle.Operation is extracted in the enrichment that the macroporous resin enrichment device for being used to prepare matrine of the utility model can carry out matrine, also can be avoided the complicated sealing structure of setting, can overcome deficiency in the prior art, and has preferable practicability.

Description

It is used to prepare the macroporous resin enrichment device of matrine
Technical field
The utility model belongs to pesticide Preparation equipment technical field more particularly to a kind of macropore tree for being used to prepare matrine Rouge enriching apparatus.
Background technique
Currently, having removed deimpurity matrine pesticide production technology using macroreticular resin as adsorbent adsorption of effective component Start to be applied.In the prior art, such as one kind disclosed in Chinese utility model patent CN201231149Y can be used for The macroporous resin adsorption column that the enrichment of biological pesticide effective component is extracted, by the way that mechanical stirring device is designed as hollow agitating shaft The cooperation that cloth liquid paddle is stirred with hollow pipe, to also reach preferable cloth liquid effect while agitating.But, this macropore tree Rouge adsorption column the deficiencies of there is also the sealing structure at stirring cloth liquid structure is complex, and maintenance is inconvenient.
Utility model content
For above description, the purpose of this utility model is to provide a kind of macroporous resin enrichments for being used to prepare matrine Device is extracted with can be used for the enrichment of matrine, and can overcome the shortcomings of existing stirring cloth liquid form.
The technical solution of the utility model is achieved in the following ways:
A kind of macroporous resin enrichment device being used to prepare matrine comprising rack is rotatably erected in the machine Tank body on frame, and the driving mechanism for driving the tank body reciprocating rotation in the rack, and in the rack Equipped with the guide holder being sheathed on outside the tank body;It further include that top is fixed on the rack and in the bottom end insertion tank body Hollow agitating shaft, and the hollow agitating paddle in the tank body is connected on the hollow agitating shaft, it is described hollow to stir Paddle is mixed to be connected to the hollow agitating shaft and offer multiple liquid distributing holes on the hollow agitating paddle;
The top of the hollow agitating shaft be equipped with liquor inlet and eluent import, the top of the tank body be equipped with into Expect population, water inlet, acid solution import and lye import, be equipped with waste liquid outlet, eluent outlet in the bottom of the tank body and go out Material mouth, the water inlet, the acid solution import, the lye import and the waste liquid outlet and eluent outlet pass through soft Pipe is connected to outside, and is equipped with filter in the waste liquid outlet and the eluent exit, is equipped in the tank body Temperature sensor is provided with heating unit in the peripheral side of the tank body.
As the restriction to aforesaid way, the eluent outlet is connected with concentrated freeze-dried machine by hose.
As the restriction to aforesaid way, the driving mechanism includes the motor being installed in the rack, with the electricity Mechatronics have controller;Further include the speed reducer being connect with the motor drive, and is set to the speed reducer and the tank Gear unit between body.
As the restriction to aforesaid way, the gear unit includes the gear ring being set on the tank body periphery wall, with And it is connected on the speed reducer and engages connected gear with the gear ring.
As the restriction to aforesaid way, maintenance population is provided on the periphery wall of the tank body.
As the restriction to aforesaid way, it is equipped on the periphery wall of the tank body and arranges along the tank body short transverse Observe visor.
As the restriction to aforesaid way, the heating unit is the steam jacket being set on the tank body periphery wall, Steam inlet and condensation-water drain are respectively arranged in the top and bottom of the steam jacket.
As the restriction to aforesaid way, the heating unit is the electric heating cover being set in outside the tank body.
The advantages of macroporous resin enrichment device for being used to prepare matrine of the utility model, is:
The macroporous resin enrichment device for being used to prepare matrine of the utility model, by loading macroreticular resin in tank body Material is first cleaned by acid solution and lye, then is successively passed through feed liquid and eluent, and by heating unit to the intracorporal temperature of tank Degree is controlled, and extracts operation so as to carry out the enrichment of matrine.Meanwhile by making tank body rotation arrangement on the rack, And setting driving mechanism drives tank body reciprocating rotation, and the mechanical stirring device of feed liquid and eluent cloth liquid can be carried out and set to be fixed It sets on the rack, while realizing stirring, can be avoided the complicated sealing structure of setting, also so as to overcome the prior art In deficiency, and have preferable practicability.
Detailed description of the invention
Fig. 1 is that the structure for the macroporous resin enrichment device for being used to prepare matrine in specific embodiment of the present invention is shown It is intended to;
In figure:1- rack, 2- tank body, 3- gear ring, 4- motor, 5- speed reducer, the hollow agitating shaft of 6-, the hollow agitating paddle of 7-, 8- liquor inlet, 9- eluent import, 10- lye import, 11- acid solution import, 12- feed population, 13- water inlet, 14- guiding Seat, 15- maintenance population, 16- heating unit, 17- temperature sensor, 18- discharge port, 19- waste liquid outlet, the outlet of 20- eluent, 21- filter, 22- hose, the concentrated freeze-dried machine of 23-.
Specific embodiment
In the description of the present invention, it should be noted that the orientation of the instructions such as term " on ", "lower", "inner", " back " Or positional relationship is to be based on the orientation or positional relationship shown in the drawings, and is merely for convenience of description the utility model and simplification is retouched It states, rather than the device or element of indication or suggestion meaning must have a particular orientation, be constructed and operated in a specific orientation, Therefore it should not be understood as limiting the present invention.In addition, term " first ", " second " are used for description purposes only, and cannot It is interpreted as indication or suggestion relative importance.The utility model will be described in detail below with reference to the accompanying drawings and embodiments.
The present embodiment is related to a kind of macroporous resin enrichment device for being used to prepare matrine, is used to carry out the richness of matrine Collection extracts, and belongs to more small-sized absorption rod structure, and as shown in Figure 1, which includes rack 1, rotatable perpendicular The tank body 2 in rack 1 is stood on, and the driving mechanism for driving 1 reciprocating rotation of tank body being arranged in rack 1, and in rack 1 It is additionally provided with the guide holder 14 being set in outside tank body 2.
The adsorbing and extracting device of the present embodiment further further includes that top is fixed in rack 1, and tank is inserted into its bottom end Hollow agitating shaft 6 in body 2, and be connected on the hollow agitating shaft 6 multiple along hollow 6 axis of agitating shaft in tank body 2 To spaced apart hollow agitating paddle 7.It is connected between hollow agitating paddle 6 and hollow agitating shaft 7, and is opened on hollow agitating paddle 7 Equipped with multiple liquid distributing holes, meanwhile, the top of hollow agitating shaft 6 is provided with liquor inlet 8 and eluent import 9.
In the present embodiment, tank body 2 can specifically be realized by being located at its Large-scale Thrust Bearings between rack 1 in rack 1 On smooth rotation.Above-mentioned driving mechanism specifically includes the motor 4 being installed in rack 1, and subtracts with the motor 4 transmission connection Fast machine 5 is also sequentially connected with gear unit between speed reducer 5 and tank body 2.Wherein, it is electrically connected with controller on motor 4, it should PLC for example can be used in controller, to control the reciprocal positive and negative rotation of motor 4, and the transmission list between speed reducer 5 and tank body 2 Member specifically includes the gear ring 3 being sleeved on 2 periphery wall of tank body, and be connected to speed reducer 5 power output end and with gear ring 3 The connected gear of engagement.As a result, under control of the controller, it is driven via the positive and negative rotation of motor 4, and then can leading in guide holder 14 To under support, realize tank body 2 in the reciprocating rotation in rack 1.
In the present embodiment, charging population 3 and water inlet 13, acid solution import 11 and lye are additionally provided at the top of tank body 2 Import 10 is provided with waste liquid outlet 19, eluent outlet 20 and discharge port 18 in the bottom of tank body 2.Wherein, in waste liquid outlet 19, valve is provided at eluent outlet 20 and discharge port 18, water inlet 13, acid solution import 10, lye import 11 and useless Liquid outlet 19 and eluent outlet 20 are to be connected to by hose with external corresponding component, are exported in waste liquid outlet 19 and eluent It is also respectively provided with filter 21 at 20, and the filter 21 can be by removing the flange of waste liquid outlet 19 or eluent outlet 20 Disk is replaced in turn.
Concentrated freeze-dried machine 23 is connected with especially by hose 22 at eluent outlet 20, and concentrated freeze-dried machine 23 is used for washing Eluent after de- is handled, with the kuh-seng alkali composition purified.In addition, the present embodiment is additionally provided with temperature in tank body 2 Sensor 17 is spent, temperature sensor 17 is to be inserted into tank body 2 by the side wall of tank body 2, corresponds to temperature sensor 17, in tank body 2 Peripheral side be also equipped with heating unit 16.
The above-mentioned heating unit 16 of the present embodiment may be, for example, the steam jacket being set on 2 periphery wall of tank body, in the steam Steam inlet and condensation-water drain is respectively set in the top and bottom of collet, is realized inside to tank body 2 with that can pass through injection steam Heating.Certainly, in addition to for steam heat form, which can also be the electric heating cover being set in outside tank body 2, phase Compared with steam jacket, electric heating cover structure is more simple, and is easy to carry out temperature control.
In the present embodiment, it is further also equipped with maintenance population 15 on the periphery wall of tank body 2, and for the benefit of observes tank body Situation in 2 is additionally provided with the observation visor not shown in the figure along 2 short transverse of tank body arrangement on the periphery wall of tank body 2, The emissive plastic glazing that the observation visor is fixed on 2 side wall of tank body using sealing.
The matrine enriching apparatus of the present embodiment is put into tank body 2 by charging population 12 when in use, by macroreticular resin, Then it by water inlet 13, acid solution import 10 and lye import 11, successively injects acid solution and lye rushes macroreticular resin It washes, flushing waste is discharged from waste liquid outlet 19.Then the feed liquid to be extracted of proper temperature, injection material are injected by liquor inlet 8 While liquid, motor 4 drives 2 reciprocating rotation of tank body, and rotational angle is advisable between 45 ~ 90 °, not only can reach stirring cloth liquid with this Effect to promote absorption of the macroreticular resin to feed liquid effective component, while will not be influenced through hose and external material pot etc. Connection.
In adsorption process, according to the detection of temperature sensor 17, can real-time control heating unit 16 work, to guarantee The temperature of tank body 2 is within the required range.After reaching setting time, it is again turned on waste liquid outlet 19, the feed liquid discharge after making absorption, Then eluent is injected by eluent import 9 again to be eluted, be equally stirred in elution process, and temperature is controlled System, elution time open eluent outlet 20 after again, so that eluent is entered concentrated freeze-dried machine 23 and carry out subsequent processing.
Finally, the macroreticular resin after the completion of the discharge absorption of openable discharge port 18, when discharge, can be such that tank body 2 rotates, thus Be conducive to discharge.After macroreticular resin discharges, is intake by water inlet 13 to being cleaned in tank body 2, then can be carried out down Primary enrichment operation.
The foregoing is merely the preferred embodiment of the utility model, but the protection scope of the utility model is not limited to This, anyone skilled in the art within the technical scope disclosed by the utility model, technology according to the present utility model Design is subject to the resulting technical solution of equivalent substitution or change, should all be covered by the protection scope of the utility model.

Claims (8)

1. a kind of macroporous resin enrichment device for being used to prepare matrine, it is characterised in that:
The macroporous resin enrichment device for being used to prepare matrine includes rack, the tank being rotatably erected in the rack Body, and the driving mechanism for driving the tank body reciprocating rotation in the rack, and be equipped with and be arranged in the rack Guide holder outside the tank body;It further include that top is fixed on the rack and bottom end is inserted into that the tank is intracorporal hollow to be stirred Axis is mixed, and is connected with the hollow agitating paddle in the tank body on the hollow agitating shaft, the hollow agitating paddle and institute Hollow agitating shaft is stated to be connected to and offer multiple liquid distributing holes on the hollow agitating paddle;
It is equipped with liquor inlet and eluent import on the top of the hollow agitating shaft, is equipped with charging people at the top of the tank body Mouth, water inlet, acid solution import and lye import are equipped with waste liquid outlet, eluent outlet and discharge port in the bottom of the tank body, The water inlet, the acid solution import, the lye import and the waste liquid outlet and the eluent outlet by hose with Outside connection, and it is equipped with filter in the waste liquid outlet and the eluent exit, temperature is equipped in the tank body Sensor is provided with heating unit in the peripheral side of the tank body.
2. the macroporous resin enrichment device according to claim 1 for being used to prepare matrine, it is characterised in that:The elution Liquid outlet is connected with concentrated freeze-dried machine by hose.
3. the macroporous resin enrichment device according to claim 1 for being used to prepare matrine, it is characterised in that:The driving Mechanism includes the motor being installed in the rack, is electrically connected with controller with the motor;Further include and the motor drive The speed reducer of connection, and the gear unit between the speed reducer and the tank body.
4. the macroporous resin enrichment device according to claim 3 for being used to prepare matrine, it is characterised in that:The transmission Unit includes the gear ring being set on the tank body periphery wall, and is connected on the speed reducer and engages with the gear ring Connected gear.
5. the macroporous resin enrichment device according to claim 1 for being used to prepare matrine, it is characterised in that:In the tank Maintenance population is provided on the periphery wall of body.
6. the macroporous resin enrichment device according to claim 1 for being used to prepare matrine, it is characterised in that:In the tank The periphery wall of body is equipped with the observation visor arranged along the tank body short transverse.
7. the macroporous resin enrichment device according to any one of claim 1 to 6 for being used to prepare matrine, feature exist In:The heating unit is the steam jacket being set on the tank body periphery wall, in the top and bottom of the steam jacket It is respectively arranged with steam inlet and condensation-water drain.
8. the macroporous resin enrichment device according to any one of claim 1 to 6 for being used to prepare matrine, feature exist In:The heating unit is the electric heating cover being set in outside the tank body.
CN201820244490.3U 2018-02-11 2018-02-11 It is used to prepare the macroporous resin enrichment device of matrine Expired - Fee Related CN208097466U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820244490.3U CN208097466U (en) 2018-02-11 2018-02-11 It is used to prepare the macroporous resin enrichment device of matrine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820244490.3U CN208097466U (en) 2018-02-11 2018-02-11 It is used to prepare the macroporous resin enrichment device of matrine

Publications (1)

Publication Number Publication Date
CN208097466U true CN208097466U (en) 2018-11-16

Family

ID=64124142

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201820244490.3U Expired - Fee Related CN208097466U (en) 2018-02-11 2018-02-11 It is used to prepare the macroporous resin enrichment device of matrine

Country Status (1)

Country Link
CN (1) CN208097466U (en)

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GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20181116

Termination date: 20200211

CF01 Termination of patent right due to non-payment of annual fee