CN208082476U - A kind of mashing refining kettle of p-phenoxyphenol crude product - Google Patents
A kind of mashing refining kettle of p-phenoxyphenol crude product Download PDFInfo
- Publication number
- CN208082476U CN208082476U CN201820356807.2U CN201820356807U CN208082476U CN 208082476 U CN208082476 U CN 208082476U CN 201820356807 U CN201820356807 U CN 201820356807U CN 208082476 U CN208082476 U CN 208082476U
- Authority
- CN
- China
- Prior art keywords
- stirring rod
- retort
- phenoxyphenol
- crude product
- mashing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- ZSBDGXGICLIJGD-UHFFFAOYSA-N 4-phenoxyphenol Chemical compound C1=CC(O)=CC=C1OC1=CC=CC=C1 ZSBDGXGICLIJGD-UHFFFAOYSA-N 0.000 title claims abstract description 68
- 239000012043 crude product Substances 0.000 title claims abstract description 38
- 238000005360 mashing Methods 0.000 title claims abstract description 19
- 238000007670 refining Methods 0.000 title claims abstract description 17
- 238000003756 stirring Methods 0.000 claims abstract description 81
- 239000002904 solvent Substances 0.000 claims abstract description 20
- 239000007788 liquid Substances 0.000 claims abstract description 13
- 238000004891 communication Methods 0.000 claims abstract description 4
- 238000004140 cleaning Methods 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 2
- 238000010009 beating Methods 0.000 abstract description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 4
- -1 Phenoxy phenyl Chemical group 0.000 description 3
- YAVVGPBYBUYPSR-UHFFFAOYSA-N benzene;oxygen Chemical compound [O].C1=CC=CC=C1 YAVVGPBYBUYPSR-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 125000001820 oxy group Chemical group [*:1]O[*:2] 0.000 description 2
- 239000005927 Pyriproxyfen Substances 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001802 infusion Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- NHDHVHZZCFYRSB-UHFFFAOYSA-N pyriproxyfen Chemical compound C=1C=CC=NC=1OC(C)COC(C=C1)=CC=C1OC1=CC=CC=C1 NHDHVHZZCFYRSB-UHFFFAOYSA-N 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
Landscapes
- Extraction Or Liquid Replacement (AREA)
Abstract
The utility model discloses a kind of mashing refining kettles of p-phenoxyphenol crude product, belong to field of pharmaceutical equipment.A kind of mashing refining kettle of p-phenoxyphenol crude product includes crushing tank, retort, crush the bottom wall of tank, the bottom wall of retort funnel-form with a narrow upper and lower width, the first discharge port for crushing pot bottom passes through the inlet communication at the top of delivery pipe and retort, the center of retort is equipped with rotatable second stirring rod, the inside of second stirring rod is cavity, and second the top of stirring rod be connected to woven hose by rotary joint, the outer wall of second stirring rod is equipped with multiple controllable opening and closing along its length, and the liquid outlet being connected to cavity inner wall, second stirring rod is equipped with the first stirring sheet along its length, it is equipped with V-arrangement stirring sheet compatible with retort bottom wall positioned at the second stirring rod bottom.A kind of mashing refining kettle of p-phenoxyphenol crude product disclosed by the utility model, can realize that p-phenoxyphenol crude product is uniformly mixed with solvent, beating results are good.
Description
Technical field
The utility model is related to refining kettle technical fields, and in particular to a kind of mashing of p-phenoxyphenol crude product is refined
Kettle.
Background technology
P-phenoxyphenol is for efficient, low-toxin farm chemicals shuangweiwei, pyriproxyfen synthesis, wide market.To improve
The quality of p-phenoxyphenol usually requires in production process to carry out mashing to its crude product refined.It is beaten to reach relatively good
Effect is starched, is usually beaten in presence of organic solvent, there are p-phenoxyphenol mashing pair for existing tank reactor
Phenoxy phenyl crude product mixes non-uniform problem.
Utility model content
It is a kind of to benzene oxygen the technical problem to be solved by the utility model is to propose in order to overcome the deficiencies of existing technologies
The mashing refining kettle of base phenol crude product can realize that p-phenoxyphenol crude product is uniformly mixed with solvent, and beating results are good.
For this purpose, the utility model uses following technical scheme：
The utility model provides a kind of mashing refining kettle of p-phenoxyphenol crude product, including crushes tank, retort, institute
State crush the bottom wall of tank, the retort bottom wall funnel-form with a narrow upper and lower width, the crushings tank top sets that there are two passes
In the symmetrical first charging aperture in the crushing tank center, first discharge port for crushing pot bottom by delivery pipe with it is described
Inlet communication at the top of retort, first discharge port is connected to the lowest point for crushing tank bottom wall, in the delivery pipe
Equipped with delivery pump, the first stirring rod is equipped in the crushing tank, first stirring rod is driven by first motor, and described first stirs
It mixes bar and is from top to bottom equipped with the first helical blade and the second helical blade, the diameter edge of second helical blade along its length
It is gradually reduced close to the direction of first discharge port；The center of the retort is equipped with the second stirring rod, second stirring
Bar is connect with driving mechanism, and the inside of second stirring rod is cavity, and the top of second stirring rod is connect by rotation
Head is connected to woven hose, and the outer wall of second stirring rod goes out liquid equipped with multiple controllable opening and closing along its length
Mouthful, and the liquid outlet is uniformly arranged for one week around the outer wall of second stirring rod, the liquid outlet in the cavity
Wall is connected to, and the second discharge port of the reaction pot bottom is connected to the lowest point of the retort bottom wall, second stirring rod
It is from top to bottom equipped with the first stirring sheet along its length, is located at second stirring rod bottom and is equipped with and the retort bottom wall phase
It is equipped with through-hole in the V-arrangement stirring sheet of adaptation, first stirring sheet and the V-arrangement stirring sheet.
In the preferable embodiment of the utility model, the woven hose by three-way pipe respectively with solvent pipe, cleaning pipe
It is connected to, motor-driven valve is equipped in the solvent pipe, the cleaning pipe.
In the preferable embodiment of the utility model, the end of first stirring sheet is equipped with scraper plate, and the scraper plate is in
Arc.
In the preferable embodiment of the utility model, the driving mechanism includes rack, in the rack
It two motors, the driving shaft being connect with second motor output shaft, the drive bevel gear on the driving shaft and is set to
The driven wheel of differential of second stirring rod upper end, the drive bevel gear are meshed with the driven wheel of differential, the active
Axis is vertical with second stirring rod, and the both ends of the driving shaft are separately mounted in bearing block, and the bearing block is set to described
Frame top.
In the preferable embodiment of the utility model, the woven hose is equipped with metering pump.
The beneficial effects of the utility model are：
The crushing tank is arranged to benzene in a kind of mashing refining kettle of p-phenoxyphenol crude product provided by the utility model
Oxygroup phenol crude product crushes break up in advance, increases the mobility of p-phenoxyphenol crude product, advantageously ensures that toward the retort
Continuous uniform conveys p-phenoxyphenol crude product, and under the action of the delivery pump, p-phenoxyphenol crude product is from the crushing
First discharge port of tank can smoothly enter into along the delivery pump in the retort；Solvent enters the stirring rod from the woven hose
Cavity in, with the rotation of second stirring rod, solvent sprays outward from multiple liquid outlets, improve solvent with to benzene
The touch opportunity of oxygroup phenol crude product, first stirring sheet, V-arrangement stirring sheet stir p-phenoxyphenol crude product and solvent
Mixing is mixed, solvent is made to be uniformly mixed with p-phenoxyphenol crude product, beating results are good.
Description of the drawings
Fig. 1 is that a kind of structure of the mashing refining kettle of the p-phenoxyphenol crude product provided in the utility model embodiment is shown
It is intended to.
In figure：
100, tank is crushed；101, first charging aperture；102, the first discharge port；103, delivery pipe；104, delivery pump；110,
One stirring rod；111, the first helical blade；112, the second helical blade；120, first motor；200, retort；201, second goes out
Material mouth；210, the second stirring rod；211, rotary joint；212, woven hose；213, cavity；214, liquid outlet；215, the first stirring
Piece；215a, scraper plate；216, V-arrangement stirring sheet；217, solvent pipe；218, cleaning pipe；219, motor-driven valve；220, driving mechanism；221,
Rack；222, the second motor；223, driving shaft；224, drive bevel gear；225, driven wheel of differential；226, bearing block；227, it counts
Amount pump.
Specific implementation mode
Further illustrate the technical solution of the utility model below with reference to the accompanying drawings and specific embodiments.
As shown in Figure 1, a kind of mashing refining kettle of p-phenoxyphenol crude product includes crushing tank 100, retort 200, institute
It states and crushes the bottom wall of tank 100, the bottom wall funnel-form with a narrow upper and lower width of the retort 200 effectively avoids pair convenient for discharging
Phenoxy phenyl crude product is accumulated, the top of the crushings tank 100 set there are two about 100 centers of the crushing tank symmetrical first
Feed inlet 101, first discharge port 102 for crushing 100 bottom of tank pass through 200 top of delivery pipe 103 and the retort
Inlet communication, first discharge port 102 are connected to the lowest point for crushing 100 bottom wall of tank, and the delivery pipe 103 is equipped with
Delivery pump 104, the crushing tank 100 is interior to be equipped with the first stirring rod 110, and first stirring rod 110 is driven by first motor 120
Dynamic, first stirring rod 110 is from top to bottom equipped with the first helical blade 111 and the second helical blade 112, institute along its length
The diameter for stating the second helical blade 112 is gradually reduced along close to the direction of first discharge port 102；The retort 200
Center is equipped with the second stirring rod 210, and second stirring rod 210 is connect with driving mechanism 220, second stirring rod 210
Inside is cavity 213, and the top of second stirring rod 210 is connected to by rotary joint 211 with woven hose 212, described the
The outer wall of two stirring rods 210 is equipped with the liquid outlet 214 of multiple controllable opening and closing, and the liquid outlet along its length
214 outer walls for surrounding second stirring rod 210 are uniformly arranged for one week, and the liquid outlet 214 connects with 213 inner wall of the cavity
Logical, the second discharge port 201 of 200 bottom of the retort is connected to the lowest point of 200 bottom wall of the retort, and described second stirs
It mixes bar 210 and is from top to bottom equipped with the first stirring sheet 215 along its length, be located at 210 bottom of the second stirring rod and be equipped with and institute
The compatible V-arrangement stirring sheet 216 of 200 bottom wall of retort is stated, is all provided in first stirring sheet 215 and the V-arrangement stirring sheet 216
There is through-hole.
It is thick to p-phenoxyphenol that the crushing tank is arranged in a kind of mashing refining kettle of above-mentioned p-phenoxyphenol crude product
Product crush break up in advance, and the first stirring rod 110, the first helical-blade on first stirring rod 110 are set in the crushing tank 100
Piece 111 and the second helical blade 112 are stirred the p-phenoxyphenol crude product in the crushing tank 100, increase to benzene oxygen
The mobility of base phenol crude product avoids p-phenoxyphenol crude product from luming, and advantageously ensures that toward 200 continuous uniform of the retort
P-phenoxyphenol crude product is conveyed, under the action of the delivery pump 104, p-phenoxyphenol crude product is from the crushing tank 100
The first discharge port 102 can smoothly enter into the retort 200 along the delivery pump 104；Solvent enters from the woven hose 212
In the cavity 213 of the stirring rod, with the rotation of second stirring rod 210, solvent is outside from multiple liquid outlets 214
Injection improves the touch opportunity of solvent and p-phenoxyphenol crude product, and first stirring sheet 215, V-arrangement stirring sheet 216 are to right
Phenoxy phenyl crude product and solvent are stirred mixing, and solvent is made to be uniformly mixed with p-phenoxyphenol crude product, and beating results are good.
Further, the woven hose 212 is connected to solvent pipe 217, cleaning pipe 218 respectively by three-way pipe, described molten
It is equipped with motor-driven valve 219 on agent pipe 217, the cleaning pipe 218；When the retort 200 is completed to be beaten, the cleaning is opened
Motor-driven valve on pipe 218, under the rotation on second stirring rod 210, cleaning agent passes through on second stirring rod 210
Each infusion port is sprayed to the inner wall of the retort 200, is cleaned to the retort 200.
Further, it is arc-shaped to be equipped with scraper plate 215a, the scraper plate 215a for the end of first stirring sheet 215；It is described
Scraper plate 215a removes the residue being adhered on 200 inner wall of the retort.
Further, the driving mechanism 220 include rack 221, the second motor 222 in the rack 221, with
Second motor 222 exports the driving shaft 223 of axis connection, the drive bevel gear 224 on the driving shaft 223 and sets
Driven wheel of differential 225 in 210 upper end of the second stirring rod, the drive bevel gear 224 and 225 phase of the driven wheel of differential
Engagement, the driving shaft 223 is vertical with second stirring rod 210, and the both ends of the driving shaft 223 are separately mounted to bearing block
In 226, the bearing block 226 is set to 221 top of the rack；The laterally setting, and the driving shaft 223 of the driving shaft 223
Both ends are separately mounted on bearing block 226, so that the driving shaft 223 is moved more stable, to make second stirring rod 210 transport
It is dynamic steady, it is not easy to shake.
Further, the woven hose 212 is equipped with metering pump 227；Lead in second stirring rod 210 convenient for controlling
The flow of the solvent entered is conducive to that p-phenoxyphenol crude product is made to be uniformly mixed with solvent.
The utility model is described with reference to the preferred embodiments, and those skilled in the art know, is not departing from this reality
In the case of with novel spirit and scope, various changes or equivalence replacement can be carried out to these features and embodiment.This reality
It is not limited to the particular embodiment disclosed with novel, other embodiments fallen into claims hereof all belong to
In the range of the utility model protection.
Claims (5)
1. a kind of mashing refining kettle of p-phenoxyphenol crude product, it is characterised in that：
Including crushing tank (100), retort (200), bottom wall, the bottom wall of the retort (200) for crushing tank (100) is equal
Funnel-form with a narrow upper and lower width, sets that there are two symmetrical about crushing tank (100) center at the top of the crushing tank (100)
First charging aperture (101), first discharge port (102) for crushing tank (100) bottom are reacted by delivery pipe (103) with described
Inlet communication at the top of tank (200), first discharge port (102) are connected to the lowest point for crushing tank (100) bottom wall, institute
It states delivery pipe (103) and is equipped with delivery pump (104), equipped with the first stirring rod (110) in the crushings tank (100), described first
Stirring rod (110) is driven by first motor (120), and first stirring rod (110) is from top to bottom equipped with first along its length
The diameter of helical blade (111) and the second helical blade (112), second helical blade (112) goes out along close to described first
The direction of material mouth (102) is gradually reduced；
The center of the retort (200) is equipped with the second stirring rod (210), second stirring rod (210) and driving mechanism
(220) it connects, the inside of second stirring rod (210) is cavity (213), and the top of second stirring rod (210) is logical
It crosses rotary joint (211) to be connected to woven hose (212), the outer wall of second stirring rod (210) is along its length equipped with multiple
The controllable liquid outlet (214) opened and closed, and the liquid outlet (214) is around the outer wall of second stirring rod (210)
It being uniformly arranged within one week, the liquid outlet (214) is connected to the cavity (213) inner wall, and the of retort (200) bottom
Two discharge ports (201) are connected to the lowest point of the retort (200) bottom wall, and second stirring rod (210) is along its length
It is from top to bottom equipped with the first stirring sheet (215), is located at the second stirring rod (210) bottom and is equipped with and the retort (200)
The compatible V-arrangement stirring sheet (216) of bottom wall is equipped on first stirring sheet (215) and the V-arrangement stirring sheet (216) logical
Hole.
2. a kind of mashing refining kettle of p-phenoxyphenol crude product according to claim 1, it is characterised in that：
The woven hose (212) is connected to solvent pipe (217), cleaning pipe (218) respectively by three-way pipe, the solvent pipe
(217), it is equipped with motor-driven valve (219) on the cleaning pipe (218).
3. a kind of mashing refining kettle of p-phenoxyphenol crude product according to claim 1, it is characterised in that：
The end of first stirring sheet (215) is equipped with scraper plate (215a), and the scraper plate (215a) is arc-shaped.
4. a kind of mashing refining kettle of p-phenoxyphenol crude product according to claim 1, it is characterised in that：
The driving mechanism (220) include rack (221), be set to the rack (221) on the second motor (222), with it is described
Second motor (222) export axis connection driving shaft (223), be set to the driving shaft (223) on drive bevel gear (224) with
And set on the second stirring rod (210) upper end driven wheel of differential (225), the drive bevel gear (224) with it is described driven
Bevel gear (225) is meshed, and the driving shaft (223) is vertical with the second stirring rod (210), the driving shaft (223)
Both ends are separately mounted in bearing block (226), and the bearing block (226) is set at the top of the rack (221).
5. a kind of mashing refining kettle of p-phenoxyphenol crude product according to claim 1, it is characterised in that：
The woven hose (212) is equipped with metering pump (227).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820356807.2U CN208082476U (en) | 2018-03-15 | 2018-03-15 | A kind of mashing refining kettle of p-phenoxyphenol crude product |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201820356807.2U CN208082476U (en) | 2018-03-15 | 2018-03-15 | A kind of mashing refining kettle of p-phenoxyphenol crude product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208082476U true CN208082476U (en) | 2018-11-13 |
Family
ID=64059128
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820356807.2U Expired - Fee Related CN208082476U (en) | 2018-03-15 | 2018-03-15 | A kind of mashing refining kettle of p-phenoxyphenol crude product |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208082476U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113145045A (en) * | 2021-02-04 | 2021-07-23 | 江苏金桐表面活性剂有限公司 | Linear alkylbenzene production equipment and production method thereof |
-
2018
- 2018-03-15 CN CN201820356807.2U patent/CN208082476U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113145045A (en) * | 2021-02-04 | 2021-07-23 | 江苏金桐表面活性剂有限公司 | Linear alkylbenzene production equipment and production method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181113 Termination date: 20190315 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |