CN207769264U - A kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid - Google Patents

Abstract

The utility model discloses a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid, return duct surrounds reaction utensil surface tube body；Heater is mounted at left and right sides of reaction utensil on inner wall；Blender is mounted in reaction utensil ware body top inner wall；Screen pipe is located at the outer ware body upper left side of reaction utensil；Exhaust outlet is mounted on ware top center position in reaction utensil, and the pipeline that air pump extends to the external wall of reaction utensil ware with exhaust outlet is connected；Feed inlet is through ware body above reaction utensil；Crystal inlet is located on the right side of feed inlet；Crystal pillar support is installed on ware bottom in reaction utensil ware body；Lens cylinder be mounted on crystal pillar support thread a pipe in；Temperature sensor, acid-base value inductor are mounted on crystal pillar support；The external wall lower center position of its ware is reaction utensil bearing；Controller is located on the left of reaction utensil bearing；The utility model good effect of separating solid from liquid, the rate of departure is high, easy to operate.

Description

A kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid

Technical field

The utility model is related to equipment for separating liquid from solid field, specially a kind of oxalic rare earth precipitates object extraction is separated by solid-liquid separation Device.

Background technology

Solid-liquid separating method：

1, separation of solid and liquid is handled by way of filtering and intercepting；

2, it is detached by solid-liquid two-phase difference in specific gravity：

(1) it centrifuges：The method detached by means of centrifugal force, the substance for keeping proportion different.Due to centrifuge etc. Tailings glass equipment can generate quite high angular speed, and centrifugal force is made to be much larger than gravity, and then the suspended matter in solution is convenient to Precipitation:Again since the centrifugal force suffered by the different substance of proportion is different, to which sinking speed is different, proportion can be made different Substance reach separation osteomyelitis；

(2) gravitational settling：It is the effect by earth gravitational field, and solid-liquid separating equipment utilizes the density of particle and fluid Difference is allowed to that relative motion occurs and settles, i.e. gravitational settling.Gravitational settling is the most simple side that grit is isolated from air-flow Method, only particle are larger, and when gas velocity is smaller, the effect of gravitational settling is just more apparent；

3, other materials and chemical property, as at solid-state, at liquid under high temperature, detached under low temperature.

Utility model content

The purpose of this utility model is to provide a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid, with solid-liquid point Good from effect, the rate of departure is high, it is easy to operate the features such as, solve deficiency in the prior art.

To achieve the above object, the utility model provides the following technical solutions：A kind of oxalic rare earth precipitates object extraction use is solid Liquid separating apparatus, including the induction of return duct, heater, blender, screen pipe, air pump, temperature sensor, feed inlet, acid-base value Device, lens cylinder, crystal pillar support, reaction utensil, reaction utensil bearing, exhaust outlet, crystal inlet, controller；The return duct encloses It is internal for flowing mixture of ice and water around reaction utensil surface tube body；The heater is mounted at left and right sides of reaction utensil on inner wall, Its length is less than liquid height in reaction utensil ware；The blender is mounted in reaction utensil ware body top inner wall, blender paddle Leaf gos deep into reaction utensil liquid internal；The screen pipe is located at the outer ware body upper left side of reaction utensil, and pipeline extends to inside reaction utensil； The exhaust outlet is mounted on ware top center position in reaction utensil, extends on the external wall of ware in horn-like, the air pump with The pipeline that exhaust outlet extends to the external wall of reaction utensil ware is connected；The feed inlet is located at reaction through ware body above reaction utensil In the ware wall of ware upper right side；The crystal inlet is located on the right side of feed inlet, is extended to inside reaction utensil ware body by pipeline, with Crystal pillar support internal pipeline is connected；The crystal pillar support is installed on ware bottom in reaction utensil ware body, and internal distribution is mostly logical Pipeline；The lens cylinder is mounted on interior, the lens cylinder inner hollows of threading a pipe of crystal pillar support more；The temperature sensor, acid Basicity inductor is mounted on crystal pillar support；The reaction utensil is cuboid closed container, ware external wall bottom center position It is set to reaction utensil bearing；The controller is located on the left of reaction utensil bearing, and internal is integrated circuit board, and integrated circuit board passes through Conducting wire is connect with blender, heater, air pump, temperature sensor, soda acid inductor.

Preferably, the screen pipe is in funnel-form, and tubular body is distributed two layers of filter screen, respectively emery cloth filter screen and work Property charcoal filter screen.

Preferably, filling anhydrous cupric sulfate or calcium oxide particle in the pipeline that the air pump is connect with exhaust outlet.

Preferably, the return duct uses copper material.

Preferably, the liquid of the crystal inlet injection is high concentration oxalic rare earth precipitates object crystalloid fluid.

Part is not directed in the device to be the same as those in the prior art or can be realized by using the prior art.

Compared with prior art, the beneficial effects of the utility model are as follows：A kind of oxalic rare earth precipitates object extraction solid-liquid Separator, built-in two pieces of heaters, reaction utensil internal liquid heating rate is very fast, and copper is wrapped on ware wall on the outside of reaction utensil The return duct of material, return duct is interior to flow mixture of ice and water, and the cooling of reaction utensil internal liquid is very fast, oxalic rare earth precipitates object crystal Crystallization is very fast, while return duct is easy to disassemble；Two machine blenders inside simultaneous reactions ware solve fluid temperature liter in reaction utensil High-moisture evaporates the problem of leading to Density inhomogeneity, and the double-layer filtering net in screen pipe carries out first layer to oxalic rare earth precipitates object It is separated by solid-liquid separation, and anhydrous cupric sulfate or calcium oxide particle accelerate have detaching for moisture inside reaction utensil, are added in lens cylinder high Precision rare-earth precipitation object crystal, adds the precipitation of rare-earth precipitation object crystal in block solution.

Description of the drawings

Fig. 1 is that gear teeth meshing is illustrated at a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid cross bar of the utility model Figure.

Figure label explanation:1 it is return duct, 2 be blender, 3 be heater, 4 be screen pipe, 5 be lens cylinder, 6 is gas Pump, 7 be soda acid inductor, 8 be feed inlet, 9 be crystal inlet, 10 be temperature inductor, 11 be crystal pillar support, 12 be anti- It is the device in order to control of exhaust outlet, 14 to answer ware bearing, 13.

Specific implementation mode

The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment is based on the embodiments of the present invention, and those of ordinary skill in the art are without making creative work The every other embodiment obtained, shall fall within the protection scope of the present invention.

In the description of the present invention, it should be understood that term "upper", "lower", "front", "rear", "left", "right", The orientation or positional relationship of the instructions such as "top", "bottom", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, and is only The utility model and simplifying describes for ease of description, do not indicate or imply the indicated device or element must have it is specific Orientation, with specific azimuth configuration and operation, therefore should not be understood as limiting the present invention.

Referring to Fig. 1, a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid, including 1 it is return duct, 2 is stirring Device, 3 be heater, 4 be screen pipe, 5 be lens cylinder, 6 be air pump, 7 be soda acid inductor, 8 be feed inlet, 9 be crystal injection Mouthful, 10 be temperature inductor, 11 be crystal pillar support, 12 be reaction utensil bearing, 13 be the device in order to control of exhaust outlet, 14；Return duct 1 surrounds reaction utensil surface tube body, and internal to flow mixture of ice and water, return duct 1 is made of copper material, easy to disassemble, It is fast to reduce fluid temperature speed in reaction utensil simultaneously；Heater 3 is mounted at left and right sides of reaction utensil on inner wall, and length is less than anti- Liquid height in ware ware, two pieces of heaters 3 is answered to keep the heating of the liquid in reaction utensil efficient；Blender 2 is mounted on reaction utensil ware In body top inner wall, 2 blade of blender gos deep into reaction utensil liquid internal, solves in reaction utensil that moisture evaporation leads to ingredient in liquid The problem of uneven concentration, while keeping heated liquid in reaction utensil uniform；Screen pipe 4 is located at the outer ware body upper left side of reaction utensil, Pipeline extends to inside reaction utensil, has filtered through gauze net and activated charcoal strainer in 4 pipeline of screen pipe, to rare earth oxalate solution into Row initial gross separation；Exhaust outlet 13 is mounted on ware top center position in reaction utensil, is extended on the external wall of ware in horn-like；Gas Pump 6 with exhaust outlet 13 extend to the external wall of reaction utensil ware pipeline connect, the two connect pipeline in filling anhydrous cupric sulfate with Calcium oxide particle accelerates the absorption to vapor in reaction utensil；Feed inlet 8 is located at reaction utensil through ware body above reaction utensil In the ware wall of upper right side；Crystal inlet 9 is located at 8 right side of feed inlet, is extended to inside reaction utensil ware body by pipeline, with crystal 11 internal pipeline of pillar support is connected；Crystal pillar support 11 is installed on ware bottom in reaction utensil ware body, and internal distribution threads a pipe； Lens cylinder 5 is mounted on interior, 5 inner hollows of lens cylinder of threading a pipe of crystal pillar support 11 more, injects high-precision in crystal inlet 9 Rare-earth precipitation object crystal is accelerated crystal in rare earth oxalate solution and is precipitated；Temperature sensor, acid-base value inductor are mounted on lens cylinder On bearing, the temperature and pH value of solution in reaction utensil are detected；Reaction utensil is cuboid closed container, the external wall bottom center of ware Position is reaction utensil bearing 12；Controller 14 is located at 12 left side of reaction utensil bearing, and internal is integrated circuit board, integrated circuit board It is connect with blender 2, heater 3, air pump 6, temperature sensor 10, soda acid inductor 7 by conducting wire.

In summary：A kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid, by rare earth oxalate solution from screen pipe 4 It inside pours into inside reaction utensil, preliminary separation of solid and liquid is carried out to solution, when temperature sensor 10 in reaction utensil and soda acid inductor 7 It is sent data in the integrated circuit board in controller 14 after the temperature and pH value of induction solution, integrated circuit board is heating Device 3 is powered with blender 2, and heating is boiled after one hour to solution, and air pump 6 is started to work, and the water slowly detached in reaction utensil steams High precision rare earth crystal is added in gas out of crystal inlet 9 at this time, injects mixture of ice and water in return duct 1 at this time, is reaction utensil The cooling of interior liquid removes return duct 1,3 intermittent heat of heater is kept for 80 degrees Celsius, gradually when temperature is reduced to 80 degrees Celsius Oxalic acid is added from feed inlet 8, separation of solid and liquid can be completed in reciprocating operation twice.

The advantages of basic principles and main features and the utility model of the utility model have been shown and described above, one's own profession The technical staff of industry is it should be appreciated that the present utility model is not limited to the above embodiments, described in above embodiments and description Only illustrate the principles of the present invention, on the premise of not departing from the spirit and scope of the utility model, the utility model is also It will have various changes and improvements, these various changes and improvements fall within the scope of the claimed invention, the utility model Claimed range is defined by the appending claims and its equivalent thereof.

Claims (5)

1. a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid, including return duct, heater, blender, screen pipe, gas Pump, temperature sensor, feed inlet, acid-base value inductor, lens cylinder, crystal pillar support, reaction utensil, reaction utensil bearing, exhaust outlet, Crystal inlet, controller；It is characterized in that:The return duct surrounds reaction utensil surface tube body, internal to be mixed for flowing ice water Close object；The heater is mounted at left and right sides of reaction utensil on inner wall, and length is less than liquid height in reaction utensil ware；It is described to stir Device is mixed in reaction utensil ware body top inner wall, propeller-blade gos deep into reaction utensil liquid internal；The screen pipe is located at The outer ware body upper left side of reaction utensil, pipeline extend to inside reaction utensil；The exhaust outlet is mounted on ware center of top in reaction utensil Position is extended in horn-like on the external wall of ware；The pipeline that the air pump extends to the external wall of reaction utensil ware with exhaust outlet connects It is logical；The feed inlet is located at through ware body above reaction utensil in the ware wall of reaction utensil upper right side；The crystal inlet be located at into It on the right side of material mouth, is extended to inside reaction utensil ware body by pipeline, is connected with crystal pillar support internal pipeline；The lens cylinder branch Seat is installed on ware bottom in reaction utensil ware body, and internal distribution threads a pipe；The lens cylinder is mounted on the more of crystal pillar support In threading a pipe, lens cylinder inner hollow；The temperature sensor, acid-base value inductor are mounted on crystal pillar support；It is described anti- It is cuboid closed container to answer ware, and the external wall lower center position of ware is reaction utensil bearing；The controller is located at reaction utensil On the left of bearing, internal is integrated circuit board, and integrated circuit board passes through conducting wire and blender, heater, air pump, temperature sensing Device, the connection of soda acid inductor.

2. a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid according to claim 1, it is characterised in that：It is described Screen pipe is in funnel-form, and tubular body is distributed two layers of filter screen, respectively emery cloth filter screen and activated charcoal strainer.

3. a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid according to claim 1, it is characterised in that：It is described Filling anhydrous cupric sulfate or calcium oxide particle in the pipeline that air pump is connect with exhaust outlet.

4. a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid according to claim 1, it is characterised in that：It is described Return duct uses copper material.

5. a kind of oxalic rare earth precipitates object extraction equipment for separating liquid from solid according to claim 1, it is characterised in that：It is described The liquid of crystal inlet injection is high concentration oxalic rare earth precipitates object crystalloid fluid.