CN207605424U - Equipment for separating liquid from solid - Google Patents
Equipment for separating liquid from solid Download PDFInfo
- Publication number
- CN207605424U CN207605424U CN201721627622.2U CN201721627622U CN207605424U CN 207605424 U CN207605424 U CN 207605424U CN 201721627622 U CN201721627622 U CN 201721627622U CN 207605424 U CN207605424 U CN 207605424U
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- sealing cover
- liquid
- storage bottle
- mounting bracket
- liquid storage
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Abstract
The utility model discloses a kind of equipment for separating liquid from solid, including separator ontology, separator ontology includes mounting bracket and the knockout drum that is erected in mounting bracket, liquid storage bottle, knockout drum includes the tank body being erected in mounting bracket, top of the tank is sealedly connected with the first sealing cover that top carries feed inlet, its sealed bottom is connected with the second sealing cover, sealed set has filter plate component between second sealing cover and tank body, second sealing cover bottom is connected to by outlet connector with liquid storage bottle, liquid storage bottle bottom is provided with and communicated with drain pipe, upper part is provided with and communicated with the vacuum adapter with switch valve.The utility model gas tightness is good, filter efficiency is high and knockout drum is convenient for disassembly and assembly, convenient for cleaning；Liquid discharge is convenient, easy to operate without dismantling liquid storage bottle pouring liquid repeatedly, reduces workload, effectively realizes the continuous filtering of brilliant liquid mixture, improve filter efficiency, the pilot scale especially suitable for organic synthesis experiment.
Description
Technical field
The utility model is related to laboratory apparatus, more particularly, to a kind of equipment for separating liquid from solid.
Background technology
Equipment for separating liquid from solid is the usual means that separation of solid and liquid is realized in the scientific research fields such as biology, chemistry and bio-pharmaceuticals.
Existing equipment for separating liquid from solid is mostly negative pressure leaching device comprising negative pressure pump, bottle,suction and Buchner funnel, bottle,suction are leaked with Bu Shi
Bucket is tightly connected, and so that the pressure in bottle,suction is reduced by negative pressure pump, to achieve the purpose that separation of solid and liquid.Above-mentioned apparatus exist with
Lower problem：First, Buchner funnel is constantly in open state in entire filter process, and mixture is easily contaminated；And it crosses
When the mixture of filter crystal and organic solvent, filter paper cannot be fitted closely with Buchner funnel surface, and partial crystals are easy from gap
It enters in bottle,suction, poor filtration effect；Secondly, the treating capacity of existing separator is small, is only applicable to test indoor subtotal
Amount experiment, and need constantly to topple over the liquid of bottle,suction or replace Buchner funnel to meet separation requirement, troublesome in poeration, cleaning
Amount is big；Furthermore it is to be turned off after preventing suck-back from need to pull out the negative tube on bottle,suction after the completion of suction filtration or when replacing bottle,suction
Negative pressure pump, liquid is easy to splash in bottle when tube drawing difficulty is big and tube drawing.Thus, how to design a kind of easy to operate, filtering rate
Fast and big treating capacity equipment for separating liquid from solid is the major issue of those skilled in the art's research.
Invention content
The utility model aim is to provide a kind of installation, unpicks and washes that convenient and filtering rate is fast, treating capacity is big, antipollution
Equipment for separating liquid from solid, the pilot scale which tests especially suitable for organic synthesis.
To achieve the above object, the utility model takes following technical proposals：
Equipment for separating liquid from solid described in the utility model, including separator ontology, the separator ontology include peace
Knockout drum, the liquid storage bottle in the mounting bracket are shelved and are erected at, the knockout drum includes the tank body being erected in mounting bracket, institute
It states top of the tank and the first sealing cover that top carries feed inlet is connected with by the first bolt seal, bottom passes through the second bolt
It is sealedly connected with the second sealing cover, sealed set has filter plate component, the second sealing cover between second sealing cover and tank body
Bottom is connected to setting with the liquid storage bottle by outlet connector, and liquid storage bottle bottom is provided with and communicated with the drain pipe with tapping valve,
Upper part is provided with and communicated with the vacuum adapter with switch valve.
The filter plate component includes that top carries the deflector of circular groove and buckles the ring being placed in the circular groove
Shape top board is folded with the filter plate with micropore, with the filter plate pair between the deflector and the annular top board
Multiple deflector holes are offered on the deflector that should locate.
It is provided with Gask-O-Seal between the tank body and first sealing cover；The deflector upper and lower surface
Edge be both provided with O-ring seals.
The bottom of the mounting bracket is provided with traveling wheel.
The vacuum adapter at least two.
The utility model advantage is that knockout drum is matched with liquid storage bottle, and gas tightness is good, filter efficiency is high and detaches
Tank is convenient for disassembly and assembly, is convenient for cleaning, passes through the feed inlet at the top of knockout drum and feeds；Liquid discharge in liquid storage bottle is convenient, without anti-
Liquid storage bottle pouring liquid is dismantled again, it is easy to operate, reduce workload, effectively realizes the continuous filtering of brilliant liquid mixture, carry
High filter efficiency, the pilot scale especially suitable for organic synthesis experiment.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model.
Fig. 2 is the enlarged structure schematic diagram in the portions A in Fig. 1.
Specific implementation mode
As shown in Figure 1, equipment for separating liquid from solid described in the utility model, including separator ontology, separator ontology
Including mounting bracket 1 and the knockout drum, the liquid storage bottle 2 that are erected in mounting bracket 1,1 bottom of mounting bracket is provided with traveling wheel 19, convenient for turning
It moves；Knockout drum is arranged by holder on 1 top of mounting bracket, and liquid storage bottle 2 is erected at 1 lower part of mounting bracket by Support bracket；Separation
Tank includes the tank body 3 being erected in mounting bracket 1, and 3 top of tank body is sealedly connected with top by the first bolt 4 and carries feed inlet 5
The first sealing cover 6, be provided with Gask-O-Seal 17 between tank body 3 and the first sealing cover 6, it is ensured that leakproofness；In 3 bottom of tank body
It is sealedly connected with the second sealing cover 8 by the second bolt 7, sealed set has filtering board group between the second sealing cover 8 and tank body 3
Part, filter plate component include that top carries the deflector 13 of circular groove and buckles the annular top board 14 being placed in circular groove,
It is folded with the filter plate 15 with micropore between deflector 13 and annular top board 14, the deflector 13 with 15 corresponding position of filter plate
On offer multiple deflector holes 16, deflector 13 is used to support and protects filter plate 15；13 upper and lower surface of deflector
Edge is both provided with O-ring seals 18, it is ensured that the leakproofness between the second sealing cover 8 and tank body 3；Second sealing cover, 8 bottom is logical
It crosses outlet connector and is connected to setting with liquid storage bottle 2,2 bottom of liquid storage bottle is provided with and communicated with the drain pipe 10 with tapping valve 9, upper part
Interval is provided with and communicated with two vacuum adapters 12 for carrying switch valve 11.
When practical manufacture, knockout drum is made of high-boron-silicon glass, and deflector 13 and annular top board 14 are by polytetrafluoroethylene (PTFE)
Material is made, for protecting filter plate 15 made of glass material.
The suction filtration process of the utility model is as follows：First negative pressure pump and one of vacuum adapter 12 are connected as with rubber tube
One, the switch valve 11 on another vacuum head is closed, the tapping valve 9 of 2 bottom of liquid storage bottle is simultaneously closed off, passes through feed inlet 5
Solidliquid mixture is injected into knockout drum, liquid storage bottle can be enabled its flow by the extraction of the liquid in knockout drum by then starting negative pressure pump
In 2；When liquid is excessive in liquid storage bottle 2, the switch valve 11 being connected with negative pressure pump is closed, tapping valve 9 is opened, by liquid storage bottle 2
Interior liquid discharge, above-mentioned switch valve 11 is reopened after liquid is completely exhausted out, closes tapping valve 9, continues to filter；It takes out
Mixture to be separated can be supplemented during filter by feed inlet 5；After the completion of suction filtration, valve 11 is turned off the switch, vacuum adapter is pulled out
Negative pressure pump is closed after negative tube on 12, the first sealing cover 6 is unloaded, filtered crystal cake is taken out.The utility model
Filter device realize the continuous filtering of solidliquid mixture, easy to operate and filter efficiency is high, especially suitable for organic synthesis
The pilot plant test of experiment.
Claims (5)
1. a kind of equipment for separating liquid from solid, including separator ontology, it is characterised in that：The separator ontology includes mounting bracket
（1）Be erected at the mounting bracket（1）Interior knockout drum, liquid storage bottle（2）, the knockout drum includes being erected at mounting bracket（1）It is interior
Tank body（3）, the tank body（3）Top passes through the first bolt（4）It is sealedly connected with top and carries feed inlet（5）First sealing
Lid（6）, bottom passes through the second bolt（7）It is sealedly connected with the second sealing cover（8）, second sealing cover（8）With tank body（3）
Between sealed set have filter plate component, the second sealing cover（8）Bottom passes through outlet connector and the liquid storage bottle（2）Connection is set
It sets, liquid storage bottle（2）Bottom is provided with and communicated with tapping valve（9）Drain pipe（10）, upper part, which is provided with and communicated with, carries switch
Valve（11）Vacuum adapter（12）.
2. equipment for separating liquid from solid according to claim 1, it is characterised in that：The filter plate component includes top with circle
The deflector of connected in star（13）The annular top board being placed on button in the circular groove（14）, the deflector（13）With it is described
Annular top board（14）Between be folded with the filter plate with micropore（15）, with the filter plate（15）The deflector of corresponding position
（13）On offer multiple deflector holes（16）.
3. equipment for separating liquid from solid according to claim 2, it is characterised in that：The tank body（3）With first sealing cover
（6）Between be provided with Gask-O-Seal（17）；The deflector（13）The edge of upper and lower surface is both provided with the sealing of O shapes
Circle（18）.
4. equipment for separating liquid from solid according to claim 1, it is characterised in that：The mounting bracket（1）Bottom be provided with row
Walk wheel（19）.
5. equipment for separating liquid from solid according to claim 1, it is characterised in that：The vacuum adapter（12）At least two.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721627622.2U CN207605424U (en) | 2017-11-29 | 2017-11-29 | Equipment for separating liquid from solid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721627622.2U CN207605424U (en) | 2017-11-29 | 2017-11-29 | Equipment for separating liquid from solid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207605424U true CN207605424U (en) | 2018-07-13 |
Family
ID=62796495
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721627622.2U Active CN207605424U (en) | 2017-11-29 | 2017-11-29 | Equipment for separating liquid from solid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207605424U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111839135A (en) * | 2020-07-13 | 2020-10-30 | 金情芬 | PLA degradation tableware |
| CN115246788A (en) * | 2021-12-24 | 2022-10-28 | 连云港贵科药业有限公司 | Preparation method and preparation device of regorafenib |
-
2017
- 2017-11-29 CN CN201721627622.2U patent/CN207605424U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111839135A (en) * | 2020-07-13 | 2020-10-30 | 金情芬 | PLA degradation tableware |
| CN115246788A (en) * | 2021-12-24 | 2022-10-28 | 连云港贵科药业有限公司 | Preparation method and preparation device of regorafenib |
| CN115246788B (en) * | 2021-12-24 | 2023-08-11 | 连云港贵科药业有限公司 | Preparation method and preparation device of regorafenib |
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