CN207435359U - 一种6-氯-3-甲基尿嘧啶生产装置 - Google Patents
一种6-氯-3-甲基尿嘧啶生产装置 Download PDFInfo
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- CN207435359U CN207435359U CN201721410352.XU CN201721410352U CN207435359U CN 207435359 U CN207435359 U CN 207435359U CN 201721410352 U CN201721410352 U CN 201721410352U CN 207435359 U CN207435359 U CN 207435359U
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- 238000000034 method Methods 0.000 title claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 47
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 abstract description 21
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 4
- VPLZGVOSFFCKFC-UHFFFAOYSA-N 3-methyluracil Chemical compound 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CN1C(=O)C=CNC1=O VPLZGVOSFFCKFC-UHFFFAOYSA-N 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N chlorine atom Chemical compound 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[Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- -1 reaction mechanism Chemical compound 0.000 abstract 1
- 238000005260 corrosion Methods 0.000 description 4
- 210000003298 Dental Enamel Anatomy 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- SHVCSCWHWMSGTE-UHFFFAOYSA-N 6-methyluracil Chemical compound 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Abstract
本实用新型公开了一种6‑氯‑3‑甲基尿嘧啶生产装置，包括反应机构、冷凝机构及离心机构；所述反应机构包括反应部件、搅拌部件及驱动件；所述搅拌部件设于反应部件内，该搅拌部件包括可正反转的转动件、可上下活动地设于转动件上的第一搅拌件及设于转动件上的第二搅拌件，所述第二搅拌件上设有升温件。本实用新型设置上下活动的第一搅拌件，搅拌时将下层原料带到上层，使原料混合均匀，反应程度一致，并反应充分，提高生产效率；第二搅拌件可持续搅拌下层原料，加速原料混合，且升温件可对中部原料加热，提高升温速率，保证内外层原料温度一致，使反应充分，生产效率高。
Description
一种6-氯-3-甲基尿卩密陡生产装置
技术领域
[0001]本实用新型属于生物制药设备技术领域，尤其是涉及一种6-氯-3—甲基尿嘧啶生 产装置。
背景技术
[0002] 6-氯-3-甲基尿嘧啶为阿格列汀中间体，制造时需放入至反应釜内加热并搅拌以 保证反应充分，但市场上现有的反应釜内搅拌件为浆形搅拌件，该搅拌件于转动时仅能对 反应釜底部搅拌，反应釜上部的原料无法得到充分的搅拌，造成搅拌不匀，原料反应不充 分；同时因现有的反应釜加热时通过设在侧壁上的加热管道对原料加热，但加热期间外壁 的温度过高，但中间原料无法均匀受热，致使反应不充分。 实用新型内容
[0003] 本实用新型为了克服现有技术的不足，提供一种搅拌均匀并加热充分的6-氯-3 -甲基尿嘧啶生产装置。
[0004] 为了实现上述目的，本实用新型采用以下技术方案:一种6-氯-3-甲基尿嘧啶生产 装置，包括反应机构、冷凝机构及离心机构;所述反应机构包括反应部件、搅拌部件及驱动 件;所述搅拌部件设于反应部件内，该搅拌部件包括可正反转的转动件、可上下活动地设于 转动件上的第一搅拌件及设于转动件上的第二搅拌件，所述第二搅拌件上设有升温件。本 实用新型设置可上下活动的第一搅拌件，搅拌时将下层的原料带到上层;使上下层原料混 合均匀，反应程度一致，反应充分，生产效率高;第二搅拌件可持续搅拌下层原料，加速原料 间混合，且升温件可对中间原料加热，提高升温速率，保证内外层原料温度一致，使反应充 分，生产效率高。
[0005] 进一步的，所述第一搅拌件包括套设于所述转动件上的套管和固设于所述套管上 的搅拌叶;设置套管可沿转动件上下活动，带动搅拌叶上下活动，且搅拌叶固设套管上，结 构稳定，不易发生损坏。
[0006] 进一步的，所述搅拌叶包括倾斜设置的第一叶片和与所述第一叶片对称设置的第 二叶片；第一叶片和第二叶片倾斜设置，进而成V形，第一搅拌件向上活动时可将下层原料 至上层;第一搅拌件向下活动时可减阻力，便于向下活动。
[0007] 进一步的，所述第一叶片和第二叶片具有漏液间隙；漏液间隙避免液体集聚于第 一搅拌件上，便于第二壳体内液体从第二搅拌件上流出。
[0008] 进一步的，所述转动件上设有与所述套管相配合的限位部件；限位部件可限制第 一搅拌件活动范围，避免第一搅拌件与第二搅拌件和第二壳体碰撞。
[0009] 进一步的，所述限位部件包括固设于所述转动件上的第一限位件和第二限位件， 所述套管设于第一限位件和第二限位件之间。
[0010] 进一步的，所述转动件为丝杆;丝杠可有效带动第一搅拌件上下活动，其传动效率 高，传动能力强。 Lum ^进一步的，所述第二冗体为搪瓷层;搪瓷层具有耐酸、耐碱及耐腐蚀，性质稳定。 [0012]综上所述，本实用新型设置可上下活动第一搅拌件，搅拌时将下层原料带到上层， 使原料混合均匀，反应程度一致，并反应充分，提高生产效率;第二搅拌件可持续搅拌下层 原料，加速原料混合，且升温件可对中部原料加热，提高升温速率，保证内外层原料温度一 致，使反应充分，生产效率高。
附图说明
[0013]图1为本实用新型的结构示意图。
[00M]图2为本实用新型的反应机构的结构示意图。
[0015]图3为本实用新型的第一搅拌件的结构示意图。
具体实施方式
[0016]为了使本技术领域的人员更好的理解本实用新型方案，下面将结合本实用新型实 施例中的附图，对本实用新型实施例中的技术方案进行清楚、完整的描述。
[0017]如图1_3所示，一种6_氯-3-甲基尿嘧啶生产装置，包括反应机构1、冷凝机构2及离 心机构3;其中所述的冷凝机构2为市场上现有的冷凝器，所述离心机构3为市场上现有的离 心机，因此不再单独对两机构进行赘述;所述的反应机构1包括反应部件11、搅拌部件12及 驱动件I3;具体的，所述的反应部件11包括第一壳体111、第二壳体112及加热件113,所述的 第一壳体111为金属制成的外壳，第二壳体U2设在该第一壳体m内，并且两壳体间具有间 隙，该间隙为抽真空设置;所述第二壳体112为搪瓷材质制成的内壳，加热件113沿着第二壳 体112的内壁呈螺旋状排列，该加热件113为外层包裹有陶瓷材质的电阻丝;进一步的，所述 的搅拌部件I2设在第二壳体112内，且位于第二壳体112中间，该搅拌部件12包括了转动件 123、第一搅拌件121及第二搅拌件122,且在第二搅拌件122上还设有升温件124;第一壳体 111提高反应机构外层强度，延长反应机构的使用寿命;第二壳体112具有耐酸、耐碱及耐腐 蚀性，避免原料腐蚀反应机构，保证原料反应顺利;加热件113可对原料外层加热，升温速度 快，环形设置的加热件的长度长，加热性能好，升温速度快。
[0018]具体的，所述的转动件123为丝杆，该丝杆通过一行星齿轮组与驱动件13相连，所 述驱动件13为伺服电机;所述的第一搅拌件121套设在丝杆上，且随着丝杆来回正反转而上 下活动;此处来回正反转是指丝杆于伺服电机驱动下先顺时针转动，然后逆时针转动，再顺 时针转动，如此反复;实现第一搅拌件的上下运动;进一步的，所述第一搅拌件121包括套管 125和搅拌叶126;所述的套管125套设在传动件123上，且该套管125为内壁具有与丝杆相配 合的内螺纹;所述的搅拌叶126固设在套管125的侧壁上，该搅拌叶126的数量为两个，且分 别位于套管125两侧;搅拌叶126包括第一叶片127和第二叶片128,第一叶片127为倾斜固定 于套管125侧壁的板体，第二叶片128为与第一叶片127对称设置的板体;第一叶片127和第 二叶片128间具有漏液间隙129。
[0019]进一步的，在所述传动杆123上设有一限位部件14,该限位部件14包括设于传动件 123上端的第一限位件141和设于传动件123下端的第二限位件142,所述第一限位件141和 所述第二限位件142分别为一方形块，且第一搅拌件121设在第一限位件141和第二限位件 142之间;所述的第二搅拌件122固设在转动件123的下端，且该第二搅拌件122为金属桨;所 述的升温件124固定在该第二搅拌件122的上端面上，且该升温件124为外部设有陶瓷的电 热丝，该电热丝的电线经过设在传动件i 23内部的空腔通向外部，与外部电源相连。
[002°]显然，所描述的实施例仅仅是本实用新型的一部分实施例，而不是全部的实施例。 基于本实用新型中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的 所有其他实施例，都应当属于本实用新型保护的范围。
Claims (7)
- i .一种6-氯-3-甲基尿嘧啶生产装置，包括反应机构（1)、冷凝机构⑵及离心机构(3); 所述反应机构（1)包括反应部件（11)、搅拌部件（12)及驱动件（13);其特征在于:所述搅拌 部件（12)设于反应部件（11)内，该搅拌部件（1¾包括可正反转的转动件(123)、可上下活动 地设于转动件（123)上的第一搅拌件（121)及设于转动件(123)上的第二搅拌件（122)，所述 第二搅拌件(122)上设有升温件(124)。
- 2. 根据权利要求1所述的一种6_氯-3-甲基尿嘧啶生产装置，其特征在于:所述第一搅 拌件（121)包括套设于所述转动件（123)上的套管（125)和固设于所述套管（125)上的搅拌 叶（126)。
- 3. 根据权利要求2所述的一种6-氯-3-甲基尿嘧啶生产装置，其特征在于:所述搅拌叶 (126)包括倾斜设置的第一叶片(127)和与所述第一叶片(127)对称设置的第二叶片(128)。
- 4. 根据权利要求3所述的一种6-氯-3-甲基尿嘧啶生产装置，其特征在于:所述第一叶 片（127)和第二叶片（128)间具有漏液间隙（129)。
- 5. 根据权利要求2所述的一种6-氯-3-甲基尿嘧啶生产装置，其特征在于:所述转动件 (123)上设有与所述套管(125)相配合的限位部件（14)。
- 6. 根据权利要求5所述的一种6-氯-3-甲基尿嘧啶生产装置，其特征在于:所述限位部 件（14)包括分别固设于所述转动件（123)上的第一限位件（141)和第二限位件（142)，所述 套管(125)设于第一限位件(141)和第二限位件(142)之间。
- 7. 根据权利要求1所述的一种6-氯-3-甲基尿嘧啶生产装置，其特征在于:所述转动件 (123)为丝杆。
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