CN207044464U - A kind of high-pressure atomization injection apparatus - Google Patents
A kind of high-pressure atomization injection apparatus Download PDFInfo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
- B29B7/76—Mixers with stream-impingement mixing head
- B29B7/7615—Mixers with stream-impingement mixing head characterised by arrangements for controlling, measuring or regulating, e.g. for feeding or proportioning the components
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
- B29B7/7404—Mixing devices specially adapted for foamable substances
- B29B7/7409—Mixing devices specially adapted for foamable substances with supply of gas
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
- B29B7/7404—Mixing devices specially adapted for foamable substances
- B29B7/7409—Mixing devices specially adapted for foamable substances with supply of gas
- B29B7/7419—Mixing devices specially adapted for foamable substances with supply of gas with static or injector mixer elements
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
- B29B7/7476—Systems, i.e. flow charts or diagrams; Plants
- B29B7/7495—Systems, i.e. flow charts or diagrams; Plants for mixing rubber
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/80—Component parts, details or accessories; Auxiliary operations
- B29B7/801—Valves
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Abstract
本实用新型属于橡胶湿法混炼设备技术领域,具体涉及一种高压雾化喷射装置,主体结构包括支座、液体分散罐、填料乳胶入口管、填料乳胶出口管、左端压力罐、中间压力罐、右端压力罐、连接管、连接管架、输液管、喷嘴、输气管、空气管道、空气入口管、液体调节器、液体过滤器、液体关闭阀、液体压力表、气体调节器、气体过滤器、气体关闭阀和气体压力表,采用压力式空气雾化喷嘴,通过液体压力和气体压力将液体输送到喷嘴口,液体和气体在压力雾化喷嘴的液体帽里面混合后通过压力式雾化喷嘴的喷嘴孔喷射出来;其结构简单,使用环境友好,能够有效减少粉尘污染,填料在乳胶中的分散性好,因而生产出的混炼胶均匀性好、质量高,综合性能高。
The utility model belongs to the technical field of rubber wet mixing equipment, and in particular relates to a high-pressure atomizing injection device. The main structure includes a support, a liquid dispersion tank, a filler latex inlet pipe, a filler latex outlet pipe, a pressure tank at the left end, and a middle pressure tank , right end pressure tank, connecting pipe, connecting pipe holder, infusion pipe, nozzle, air pipe, air pipe, air inlet pipe, liquid regulator, liquid filter, liquid shut-off valve, liquid pressure gauge, gas regulator, gas filter , Gas shut-off valve and gas pressure gauge, using a pressure-type air atomizing nozzle, the liquid is delivered to the nozzle opening through liquid pressure and gas pressure, and the liquid and gas are mixed in the liquid cap of the pressure atomizing nozzle and then pass through the pressure-type atomizing nozzle The nozzle hole is sprayed out; its structure is simple, the use environment is friendly, and it can effectively reduce dust pollution. The dispersion of the filler in the latex is good, so the produced mixed rubber has good uniformity, high quality and high comprehensive performance.
Description
技术领域:Technical field:
本实用新型属于橡胶湿法混炼设备技术领域,具体涉及一种高压雾化喷射装置,利用骤温破碎技术对填料乳胶进行高压喷射雾化,实现填料在乳胶中均匀分散与分布的目的,制备得到力学性能优良,综合力学性能和动态力学性能显著提高的橡胶复合材料。The utility model belongs to the technical field of rubber wet mixing equipment, and in particular relates to a high-pressure atomization injection device, which utilizes sudden temperature crushing technology to carry out high-pressure injection atomization on filler latex, so as to realize the purpose of uniform dispersion and distribution of filler in latex. A rubber composite material with excellent mechanical properties and significantly improved comprehensive mechanical properties and dynamic mechanical properties is obtained.
背景技术:Background technique:
在橡胶复合材料的制备过程中,混炼是最关键的工序,混炼过程的本质就是将各种配合剂混入生胶中以制成质量均匀的混炼胶的过程,也就是橡胶与各种配合剂的混合与分散过程;因为混炼胶质量的好坏,直接影响到橡胶制品的质量、性能及其使用寿命,所以,混炼是橡胶制品加工过程中第一道也是最重要的一道工序;目前,橡胶工业传统混炼工艺多采用密炼机多段式混炼方法,由于高聚物高弹特性,导致混炼过程是一个不断生热升温的过程,为防止胶料焦烧破坏胶料的性能,同时达到配合剂均匀分散的目的,混炼过程不得不反复进行。为了提高混炼效率,新的混炼方法和工艺层出不穷,低温一次法、串联式混炼和连续混炼等先进的混炼方式逐渐开始使用,新的混炼技术在混炼效率和混炼质量上有很好的均衡效果,但是这些机械混炼技术只能使填料的分散等级达到一定程度,即使延长混炼时间,胶料的混炼质量也不会获得提高。为了获得更好的混炼质量,人们尝试将新能量(超声波和固体干冰等)注入到混炼过程中,通过新能量的输入打破填料的聚集体,提高橡胶混炼质量。研究发现这些新的技术手段只是在一定程度上改善了填料的微观分散程度,其与高端橡胶制品的要求仍存在一定的差距。In the preparation process of rubber composite materials, mixing is the most critical process. The essence of the mixing process is to mix various compounding ingredients into raw rubber to make a uniform quality of mixed rubber, that is, rubber and various The mixing and dispersing process of the compounding agent; because the quality of the rubber compound directly affects the quality, performance and service life of the rubber product, mixing is the first and most important process in the rubber product processing process ; At present, the traditional mixing process of the rubber industry mostly adopts the multi-stage mixing method of the internal mixer. Due to the high elasticity of the polymer, the mixing process is a process of continuous heat generation and heating. In order to prevent the rubber from being scorched and damaged performance, while achieving the purpose of uniform dispersion of compounding agents, the mixing process has to be repeated. In order to improve the mixing efficiency, new mixing methods and processes emerge in an endless stream. Advanced mixing methods such as low-temperature one-shot method, serial mixing and continuous mixing are gradually used. There is a very good equalization effect, but these mechanical mixing techniques can only make the dispersion level of the filler reach a certain level. Even if the mixing time is prolonged, the mixing quality of the rubber compound will not be improved. In order to obtain better mixing quality, people try to inject new energy (ultrasonic wave and solid dry ice, etc.) into the mixing process, and break the aggregates of fillers through the input of new energy to improve the quality of rubber mixing. Studies have found that these new technical means have only improved the microscopic dispersion of fillers to a certain extent, and there is still a certain gap between them and the requirements of high-end rubber products.
现有技术中的橡胶纳米复合材料的湿法制备主要采用化学方法处理新材料与胶乳乳液,利用搅拌的方式实现纳米填料在胶乳中的均匀分散,然后絮凝制得湿法混炼胶,这种方法和工艺加入了化学试剂,对胶料性能产生了很大影响,降低了橡胶制品的质量和使用寿命。中国专利201110064299.3公开的湿法混炼天然橡胶料的制备方法包括:首先配制浆料,将15-40%白炭黑干料浸泡在60-85%的去离子水中,加入偶联剂、表面活性剂混合均匀,再依次研磨、制取胶乳混合液、取天然胶乳和将白炭黑水分散体加入到胶乳中,然后搅拌混合成胶乳混合液,絮凝,在混合液中加入醋酸,经洗胶机进行洗胶和脱水,送至橡胶造粒机造粒,最后将胶料粒送入箱式干燥柜中进行干燥,其是对传统混炼技术的改进,制取胶乳溶液后在混合溶液中加入醋酸絮凝,经洗胶机洗胶和脱水,再在干燥箱中干燥4h-6h,干燥后的即为天然橡胶的混炼胶料。然而传统的强酸絮凝存在难以避免的缺陷,不仅会影响操作人员的身体健康,设备腐蚀,絮凝后的烘干阶段时间长,容易产生酸性气体影响环境,如果强酸清洗不干净还会影响后续的硫化时间,酸性环境下硫化会导致硫化时间滞后。新的工艺需要相配套的高压雾化喷射装置,中国专利201220110946.X公开的一种高压雾化喷射系统冷却装置包括雾化喷嘴,设于风冷室外机的冷凝器进风口处,用于喷射水雾,高压输水管,与所述雾化喷嘴连接,用于向所述雾化喷嘴供水,雾化网罩,设于风冷室外机的冷凝器进风口侧,并覆盖冷凝器进风口和所述雾化喷嘴;高压水泵,与所述高压输水管连接,控制系统,与所述高压水泵连接,用于控制所述高压水泵的运行;中国专利201510745426.4公开的一种高压雾化喷射头包括连接法兰、密封套、锥形引槽、喷射头外套、旋流芯、多通道喷嘴,喷射头上端设有连接法兰,连接法兰连接外高压水泵,喷射头外套与连接法兰之间设有密封套密封,密封套紧贴在喷射头外套内壁上,喷射头内设有旋流芯,旋流芯一端连接锥形引槽,另一端通向喷射头的多通道喷嘴;中国专利201510815009.2公开的一种高压雾化喷射油烟处理设备包括烟道、抽烟口和集油池,抽烟口安装在烟道入口端,集油池设置在烟道出口端下方,烟道的中段设置有高压喷头,高压喷头通过高压水管与高压水泵连接,高压喷头能够朝向烟道出口端喷射高压雾化水流;以上专利产品不适用于橡胶复合材料的制备。因此,研发一种提高湿法混炼过程中填料分散程度的高压雾化喷射装置,使填料达到均匀分散的效果,能够阻止填料分散后的重聚,缩短生产周期,提高橡胶的性能强度,很有科学和应用价性,也具有良好的社会和应用前景。The wet preparation of rubber nanocomposites in the prior art mainly uses chemical methods to process new materials and latex emulsions, and realizes the uniform dispersion of nano fillers in latex by stirring, and then flocculates to obtain wet mixed rubber. The method and process add chemical reagents, which have a great impact on the properties of the rubber compound and reduce the quality and service life of the rubber product. The preparation method of the wet mixing natural rubber material disclosed in Chinese patent 201110064299.3 includes: first preparing the slurry, soaking 15-40% white carbon black dry material in 60-85% deionized water, adding coupling agent, surface active Mix the agent evenly, then grind in turn, prepare the latex mixed solution, take the natural latex and add the white carbon black water dispersion into the latex, then stir and mix to form the latex mixed solution, flocculate, add acetic acid to the mixed solution, wash the rubber Machine for washing and dehydration, sent to the rubber granulator for granulation, and finally the rubber granules are sent to the box-type drying cabinet for drying, which is an improvement on the traditional mixing technology. After the latex solution is prepared, it is mixed in the mixed solution Add acetic acid for flocculation, wash and dehydrate the rubber by a rubber washing machine, and then dry it in a drying oven for 4h-6h, and the dried rubber is the natural rubber compound. However, the traditional strong acid flocculation has unavoidable defects, not only will affect the health of operators, equipment corrosion, long drying period after flocculation, easy to produce acid gas and affect the environment, if the strong acid cleaning is not clean, it will also affect the subsequent vulcanization Time, vulcanization in an acidic environment will cause a lag in the vulcanization time. The new process requires a matching high-pressure atomizing injection device. Chinese patent 201220110946.X discloses a high-pressure atomizing injection system cooling device including an atomizing nozzle, which is located at the air inlet of the condenser of the air-cooled outdoor unit for spraying Water mist, high-pressure water delivery pipe, connected with the atomizing nozzle, used to supply water to the atomizing nozzle, atomizing net cover, arranged on the air inlet side of the condenser of the air-cooled outdoor unit, and covering the air inlet of the condenser and The atomizing nozzle; a high-pressure water pump connected to the high-pressure water pipe; a control system connected to the high-pressure water pump for controlling the operation of the high-pressure water pump; a high-pressure atomizing nozzle disclosed in Chinese patent 201510745426.4 includes Connecting flange, sealing sleeve, tapered guide groove, spray head casing, swirl core, multi-channel nozzle, the upper end of the spray head is provided with a connecting flange, the connecting flange is connected to the external high-pressure water pump, and the gap between the spray head casing and the connecting flange There is a sealing sleeve for sealing, and the sealing sleeve is tightly attached to the inner wall of the spray head jacket. There is a swirl core inside the spray head. One end of the swirl core is connected to the tapered guide groove, and the other end leads to the multi-channel nozzle of the spray head; Chinese patent 201510815009.2 A disclosed high-pressure atomization spray oil fume treatment equipment includes a flue, a smoke outlet and an oil collection tank, the smoke outlet is installed at the inlet end of the flue, the oil collection tank is arranged below the outlet end of the flue, and a high-pressure nozzle is arranged in the middle of the flue , the high-pressure nozzle is connected to the high-pressure water pump through a high-pressure water pipe, and the high-pressure nozzle can spray high-pressure atomized water toward the outlet of the flue; the above patented products are not suitable for the preparation of rubber composite materials. Therefore, research and development of a high-pressure atomization injection device that improves the degree of dispersion of fillers in the wet mixing process can achieve uniform dispersion of fillers, prevent the reunion of fillers after dispersion, shorten the production cycle, and improve the performance and strength of rubber. It has scientific and practical value, and also has good social and application prospects.
发明内容:Invention content:
本实用新型的目的在于克服现有技术存在的缺点,研发设计一种提高湿法混炼过程中填料分散程度的高压雾化喷射装置,使填料达到均匀分散的效果,能够阻止填料分散后的重聚,缩短生产周期,提高橡胶的性能强度。The purpose of this utility model is to overcome the shortcomings of the existing technology, to develop and design a high-pressure atomization spraying device that improves the dispersion degree of the filler in the wet mixing process, so that the filler can be uniformly dispersed, and can prevent the filler from re-dispersing. poly, shorten the production cycle, improve the performance strength of rubber.
为了实现上述目的,本实用新型涉及的高压雾化喷射装置的主体结构包括支座、液体分散罐、填料乳胶入口管、填料乳胶出口管、左端压力罐、中间压力罐、右端压力罐、连接管、连接管架、输液管、喷嘴、输气管、空气管道、空气入口管、液体调节器、液体过滤器、液体关闭阀、液体压力表、气体调节器、气体过滤器、气体关闭阀和气体压力表;内空式矩形框架结构的支座的内部设置有内空式灯笼形结构的液体分散罐,液体分散罐的顶部与圆形管状结构的填料乳胶入口管连通,液体分散罐的底部与圆形管状结构的填料乳胶出口管连通,支座的两个平行的长边外侧分别设置有内空式圆形结构的左端压力罐、中间压力罐和右端压力罐,左端压力罐与中间压力罐之间和中间压力罐与右端压力罐之间均设置有内空式圆柱形结构的连接管,左端压力罐、中间压力罐和右端压力罐通过连接管连接成为弧形结构,两个中间压力罐之间设置有内空式结构的连接管架,填料乳胶入口管与连接管架的中心连通,左端压力罐、中间压力罐和右端压力罐的上表面中心处均设置有内空式圆柱形结构的输液管,输液管与喷嘴的一端连接,喷嘴的另一端与内空式圆柱形结构的输气管连接,输气管与圆弧形管状结构的空气管道连通,空气管道的中部与圆弧形管状结构的空气入口管连通,输液管上从靠近喷嘴的一端到远离喷嘴的一端依次设置有液体调节器、液体过滤器和液体关闭阀,液体调节器上设置有液体压力表,输气管上从靠近喷嘴的一端到远离喷嘴的一端依次设置有气体调节器、气体过滤器和气体关闭阀,气体调节器上设置有气体压力表。In order to achieve the above object, the main structure of the high-pressure atomizing injection device involved in the utility model includes a support, a liquid dispersion tank, a filler latex inlet pipe, a filler latex outlet pipe, a left end pressure tank, a middle pressure tank, a right end pressure tank, and a connecting pipe , connection tube holder, infusion tube, nozzle, air tube, air pipe, air inlet tube, liquid regulator, liquid filter, liquid shut-off valve, liquid pressure gauge, gas regulator, gas filter, gas shut-off valve and gas pressure Table; the inside of the support of the hollow rectangular frame structure is provided with a liquid dispersion tank with a hollow lantern-shaped structure, the top of the liquid dispersion tank communicates with the filler latex inlet pipe of the circular tubular structure, and the bottom of the liquid dispersion tank connects The filler latex outlet pipe in the tubular structure is connected. The two parallel long sides of the support are respectively provided with a left-end pressure tank, a middle pressure tank and a right-end pressure tank with an inner hollow circular structure. There are connecting pipes with hollow cylindrical structure between the middle and middle pressure tanks and the right end pressure tank. The left end pressure tank, the middle pressure tank and the right end pressure tank are connected by connecting pipes to form an arc structure. There is a connecting pipe frame with an inner hollow structure in between, the filler latex inlet pipe communicates with the center of the connecting pipe frame, and the center of the upper surface of the left end pressure tank, the middle pressure tank and the right end pressure tank are all equipped with an inner hollow cylindrical structure. The infusion tube, the infusion tube is connected to one end of the nozzle, the other end of the nozzle is connected to the air tube of the hollow cylindrical structure, the air tube is connected to the air tube of the arc-shaped tubular structure, and the middle part of the air tube is connected to the arc-shaped tubular structure The air inlet pipe is connected with the air inlet pipe. A liquid regulator, a liquid filter and a liquid shut-off valve are arranged on the infusion pipe from the end close to the nozzle to the end far away from the nozzle. The liquid regulator is provided with a liquid pressure gauge. A gas regulator, a gas filter and a gas shut-off valve are arranged in sequence from one end of the nozzle to the end far away from the nozzle, and a gas pressure gauge is arranged on the gas regulator.
本实用新型与现有技术相比,采用压力式空气雾化喷嘴,通过液体压力和气体压力将液体输送到喷嘴口,液体和气体在压力雾化喷嘴的液体帽里面混合后通过压力式雾化喷嘴的喷嘴孔喷射出来,空气帽能够控制雾化喷嘴的喷雾形状,填料乳胶和压缩空气由喷嘴喷出,起到对天然乳胶混合液的雾化作用,在喷射时,填料乳胶液柱与压缩空气之间有很大的速度差,填料乳胶液柱由于压缩空气的扰动而发生分裂和破碎,使混合液到达雾化效果;其结构简单,使用环境友好,能够有效减少粉尘污染,实现混炼胶的连续性生产,提高生产效率,显著降低生产成本,填料在乳胶中的分散性好,因而生产出的混炼胶均匀性好、质量高,综合性能高。Compared with the prior art, the utility model adopts a pressure-type air atomizing nozzle to transport the liquid to the nozzle mouth through liquid pressure and gas pressure, and the liquid and gas are mixed in the liquid cap of the pressure atomizing nozzle and then atomized by pressure The nozzle hole of the nozzle is sprayed out, and the air cap can control the spray shape of the atomizing nozzle. The filler latex and compressed air are sprayed out from the nozzle to atomize the natural latex mixture. When spraying, the filler latex liquid column and the compression There is a large speed difference between the air, and the filler latex liquid column is split and broken due to the disturbance of the compressed air, so that the mixed liquid reaches the atomization effect; its structure is simple, the use of the environment is friendly, and it can effectively reduce dust pollution and realize mixing The continuous production of rubber improves production efficiency and significantly reduces production costs. The dispersion of fillers in latex is good, so the produced mixed rubber has good uniformity, high quality and high comprehensive performance.
附图说明:Description of drawings:
图1为本实用新型的主体结构原理示意图。Fig. 1 is the principle schematic diagram of the main structure of the utility model.
图2为本实用新型的局部结构放大原理示意图。Fig. 2 is a schematic diagram of a partial structure enlarged principle of the present invention.
图3为本实用新型涉及的喷嘴的主体结构原理示意图。Fig. 3 is a schematic diagram of the principle of the main structure of the nozzle involved in the present invention.
图4为本实用新型涉及的喷嘴的喷射雾化原理示意图。Fig. 4 is a schematic diagram of the jet atomization principle of the nozzle involved in the present invention.
具体实施方式:detailed description:
下面通过实施例并结合附图对本实用新型做进一步描述。Below through embodiment and in conjunction with accompanying drawing, the utility model is further described.
实施例1:Example 1:
本实施例涉及的高压雾化喷射装置的主体结构包括支座1、液体分散罐2、填料乳胶入口管3、填料乳胶出口管4、左端压力罐5、中间压力罐6、右端压力罐7、连接管8、连接管架9、输液管10、喷嘴11、输气管12、空气管道13、空气入口管14、液体调节器15、液体过滤器16、液体关闭阀17、液体压力表18、气体调节器19、气体过滤器20、气体关闭阀21和气体压力表22;内空式矩形框架结构的支座1的内部设置有内空式灯笼形结构的液体分散罐2,液体分散罐2的顶部与圆形管状结构的填料乳胶入口管3连通,液体分散罐2的底部与圆形管状结构的填料乳胶出口管4连通,支座1的两个平行的长边外侧分别设置有内空式圆形结构的左端压力罐5、中间压力罐6和右端压力罐7,左端压力罐5与中间压力罐6之间和中间压力罐6与右端压力罐7之间均设置有内空式圆柱形结构的连接管8,左端压力罐5、中间压力罐6和右端压力罐7通过连接管8连接成为弧形结构,两个中间压力罐6之间设置有内空式结构的连接管架9,填料乳胶入口管3与连接管架9的中心连通,左端压力罐5、中间压力罐6和右端压力罐7的上表面中心处均设置有内空式圆柱形结构的输液管10,输液管10与喷嘴11的一端连接,喷嘴11的另一端与内空式圆柱形结构的输气管12连接,输气管12与圆弧形管状结构的空气管道13连通,空气管道13的中部与圆弧形管状结构的空气入口管14连通,输液管10上从靠近喷嘴11的一端到远离喷嘴11的一端依次设置有液体调节器15、液体过滤器16和液体关闭阀17,液体调节器15上设置有液体压力表18,输气管12上从靠近喷嘴11的一端到远离喷嘴11的一端依次设置有气体调节器19、气体过滤器20和气体关闭阀21,气体调节器19上设置有气体压力表22。The main structure of the high-pressure atomizing injection device involved in this embodiment includes a support 1, a liquid dispersion tank 2, a filler latex inlet pipe 3, a filler latex outlet pipe 4, a left end pressure tank 5, an intermediate pressure tank 6, a right end pressure tank 7, Connecting pipe 8, connecting pipe holder 9, infusion pipe 10, nozzle 11, air pipe 12, air pipe 13, air inlet pipe 14, liquid regulator 15, liquid filter 16, liquid shut-off valve 17, liquid pressure gauge 18, gas Regulator 19, gas filter 20, gas shut-off valve 21 and gas pressure gauge 22; The inside of the support 1 of hollow type rectangular frame structure is provided with the liquid dispersion tank 2 of hollow formula lantern-shaped structure, the liquid dispersion tank 2 The top is connected with the filler latex inlet pipe 3 of the circular tubular structure, the bottom of the liquid dispersion tank 2 is connected with the filler latex outlet pipe 4 of the circular tubular structure, and the two parallel long sides of the support 1 are provided with inner hollow type respectively. The left end pressure tank 5, the middle pressure tank 6 and the right end pressure tank 7 of the circular structure are provided with an inner hollow cylinder between the left end pressure tank 5 and the middle pressure tank 6 and between the middle pressure tank 6 and the right end pressure tank 7. The connecting pipe 8 of the structure, the left end pressure tank 5, the middle pressure tank 6 and the right end pressure tank 7 are connected to form an arc structure through the connecting pipe 8, and a connecting pipe frame 9 of an inner hollow structure is arranged between the two middle pressure tanks 6, The filler latex inlet pipe 3 communicates with the center of the connecting pipe frame 9, and the center of the upper surface of the left end pressure tank 5, the middle pressure tank 6 and the right end pressure tank 7 is provided with an infusion tube 10 of an inner hollow cylindrical structure, and the infusion tube 10 It is connected to one end of the nozzle 11, and the other end of the nozzle 11 is connected to the air delivery pipe 12 of the hollow cylindrical structure. The air inlet pipe 14 of the structure communicates, and the infusion tube 10 is provided with a liquid regulator 15, a liquid filter 16 and a liquid shut-off valve 17 sequentially from one end close to the nozzle 11 to an end far away from the nozzle 11, and the liquid regulator 15 is provided with a liquid A pressure gauge 18, a gas regulator 19, a gas filter 20 and a gas shut-off valve 21 are arranged in sequence from the end close to the nozzle 11 to the end far away from the nozzle 11 on the gas delivery pipe 12, and a gas pressure gauge 22 is arranged on the gas regulator 19.
本实施例涉及的支座1作为液体分散罐2的安装支架并为液体分散罐2提供支撑力;液体分散罐2作为填料乳胶的分散雾化场所;填料乳胶入口管3作为填料乳胶的入口通道;填料乳胶出口管4作为填料乳胶的出口通道;左端压力罐5、中间压力罐6和右端压力罐7收集填料乳胶并受到空气压力的作用为填料乳胶加压;连接管8作为左端压力罐5与中间压力罐6和中间压力罐6与右端压力罐7之间的连接通道;连接管架9作为中间压力罐6的连接通道并将支座1两侧的左端压力罐5、中间压力罐6和右端压力罐7连接成为一体;输液管10作为液态填料乳胶进入喷嘴11的输送通道;喷嘴11为压力式空气雾化喷嘴,压力式空气雾化喷嘴的工作原理是通过液体压力或气体压力将液体输送到喷嘴口,液体和气体在压力雾化喷嘴的液体帽里面混合后通过压力式雾化喷嘴的喷嘴孔喷射出来,空气帽能够控制雾化喷嘴的喷雾形状,喷嘴11作为填料乳胶的喷射口将乳液喷射成雾状,实现填料在乳胶中的分散目的;输气管12、空气管道13和空气入口管14共同作用作为空气进入喷嘴11的通道;液体调节器15用于调节液态填料乳胶的流速;液体过滤器16用于滤除液态填料乳胶中的固态物质;液体关闭阀17的用途是开闭输液管10;液体压力表18用于监测输液管10的压力;气体调节器19用于调节气体的流速;气体过滤器20用于滤除气体中的固态和液态物质;气体关闭阀21用于开闭输气管12;气体压力表22用于监测输气管12的压力。The support 1 involved in this embodiment is used as the mounting bracket of the liquid dispersion tank 2 and provides support for the liquid dispersion tank 2; the liquid dispersion tank 2 is used as the dispersion and atomization place of the filler latex; the filler latex inlet pipe 3 is used as the inlet channel of the filler latex The filler latex outlet pipe 4 is used as the outlet passage of the filler latex; the left end pressure tank 5, the middle pressure tank 6 and the right end pressure tank 7 collect the filler latex and are subjected to the effect of air pressure to pressurize the filler latex; the connecting pipe 8 is used as the left end pressure tank 5 The connection channel between the middle pressure tank 6 and the middle pressure tank 6 and the right end pressure tank 7; the connecting pipe frame 9 is used as the connection channel of the middle pressure tank 6 and the left end pressure tank 5 and the middle pressure tank 6 on both sides of the support 1 It is connected with the pressure tank 7 at the right end; the infusion tube 10 is used as the delivery channel for the liquid filler latex to enter the nozzle 11; the nozzle 11 is a pressure-type air atomizing nozzle, and the working principle of the pressure-type air atomizing nozzle is to use liquid pressure or gas pressure to The liquid is sent to the nozzle mouth, the liquid and the gas are mixed in the liquid cap of the pressure atomizing nozzle and sprayed out through the nozzle hole of the pressure atomizing nozzle. The air cap can control the spray shape of the atomizing nozzle, and the nozzle 11 is used as the injection of filler latex The mouth sprays the emulsion into a mist to realize the dispersion of the filler in the latex; the air pipe 12, the air pipe 13 and the air inlet pipe 14 work together as the channel for the air to enter the nozzle 11; the liquid regulator 15 is used to adjust the liquid filler latex Flow rate; Liquid filter 16 is used to filter out the solid matter in the liquid filler latex; The purpose of liquid shut-off valve 17 is to open and close infusion tube 10; Liquid pressure gauge 18 is used for monitoring the pressure of infusion tube 10; Gas regulator 19 is used for Adjust the flow rate of the gas; the gas filter 20 is used to filter out solid and liquid substances in the gas; the gas shut-off valve 21 is used to open and close the gas pipeline 12; the gas pressure gauge 22 is used to monitor the pressure of the gas pipeline 12.
本实施例涉及的喷嘴11的工作流程为填料乳胶和压缩空气由喷嘴11喷出,起到对天然乳胶混合液的雾化作用;在喷射时,填料乳胶液柱与压缩空气之间有很大的速度差,填料乳胶液柱由于压缩空气的扰动而发生分裂和破碎,使混合液到达雾化效果。以白炭黑/天然橡胶混合液为例,混合液在高压作用下急剧雾化,白炭黑团聚体会被充分打散,使白炭黑颗粒更加细化,乳胶粒子表面的保护膜在气体振动波的作用下以及其与气体的摩擦作用下被破坏,进而白炭黑粒子与橡胶烃分子接触,填充到橡胶分子链中,与橡胶分子结合;由于雾化是在瞬间完成,橡胶烃分子链的体积瞬间增大,被释放出来的橡胶烃分子链充分伸展,大量的白炭黑颗粒完全填充进橡胶烃分子链之间,最大限度的提高白炭黑在天然橡胶中的填充量,得到高填充量的白炭黑胶料,同时,雾化之后天然胶乳/白炭黑浆料混合液更加均匀,白炭黑填料在其中的分散性能得到进一步优化。The working process of the nozzle 11 that the present embodiment involves is that the filler latex and the compressed air are sprayed out by the nozzle 11, which plays the role of atomizing the natural latex mixture; when spraying, there is a large gap between the filler latex liquid column and the compressed air Due to the speed difference, the filler latex liquid column is split and broken due to the disturbance of compressed air, so that the mixed liquid can reach the atomization effect. Taking the silica/natural rubber mixture as an example, the mixture is sharply atomized under high pressure, and the silica aggregates will be fully dispersed, making the silica particles more refined, and the protective film on the surface of the latex particles is vibrated in the gas. Under the action of the wave and the friction between it and the gas, it is destroyed, and then the silica particles are in contact with the rubber hydrocarbon molecules, filled into the rubber molecular chains, and combined with the rubber molecules; because the atomization is completed in an instant, the rubber hydrocarbon molecular chains The volume of the rubber increases instantaneously, the released rubber hydrocarbon molecular chains are fully stretched, and a large number of silica particles are completely filled between the rubber hydrocarbon molecular chains, so as to maximize the filling amount of silica in natural rubber and obtain high At the same time, the natural latex/silica slurry mixture is more uniform after atomization, and the dispersion performance of the silica filler in it is further optimized.
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| CN201720996475.XU CN207044464U (en) | 2017-08-10 | 2017-08-10 | A kind of high-pressure atomization injection apparatus |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107253296A (en) * | 2017-08-10 | 2017-10-17 | 青岛科技大学 | A kind of high-pressure atomization injection apparatus |
| CN109940776A (en) * | 2019-03-21 | 2019-06-28 | 青岛科技大学 | Open mill is used in a kind of GO/NR composite material and preparation method thereof and its preparation |
| CN111844502A (en) * | 2020-07-17 | 2020-10-30 | 中国科学院长春应用化学研究所 | Synthetic rubber continuous wet mixing method and device |
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2017
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107253296A (en) * | 2017-08-10 | 2017-10-17 | 青岛科技大学 | A kind of high-pressure atomization injection apparatus |
| CN107253296B (en) * | 2017-08-10 | 2023-06-02 | 青岛科技大学 | High-pressure atomizing and spraying device |
| CN109940776A (en) * | 2019-03-21 | 2019-06-28 | 青岛科技大学 | Open mill is used in a kind of GO/NR composite material and preparation method thereof and its preparation |
| CN111844502A (en) * | 2020-07-17 | 2020-10-30 | 中国科学院长春应用化学研究所 | Synthetic rubber continuous wet mixing method and device |
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