CN207025317U - A kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate - Google Patents
A kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate Download PDFInfo
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- CN207025317U CN207025317U CN201720655869.9U CN201720655869U CN207025317U CN 207025317 U CN207025317 U CN 207025317U CN 201720655869 U CN201720655869 U CN 201720655869U CN 207025317 U CN207025317 U CN 207025317U
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- Prior art keywords
- fractionation
- producing
- tetrabutyl titanate
- reactor
- reacting kettle
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- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
Abstract
The utility model belongs to chemical production equipment, and in particular to a kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate.A kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate, including reactor, reactor is provided with charging aperture and discharging opening, it is horizontal in the reactor to be provided with rotary shaft, one end of the rotary shaft is connected with motor, and the rotary shaft is provided with agitating paddle, and the adjacent agitating paddle is on the rotating shaft in reversely installation, the inside of the agitating paddle is provided with heating rod, and the both sides of the agitating paddle are provided with wing stirrer gear；This fractionation horizontal reacting kettle, single reaction volume is on the one hand added, multiple agitating paddles are set inside simultaneous reactions kettle, add mixing effect during reaction；Unreacted monomer is reclaimed by condenser pipe, not only increases the purity of product, while unreacted monomer is recycled, meets the environmental protection concept that resource is recycled, made the best use of everything again.
Description
Technical field
The utility model belongs to chemical production equipment, and in particular to a kind of fractionation horizontal reacting for producing tetrabutyl titanate
Kettle.
Background technology
Tetrabutyl titanate be it is a kind of colourless to light yellow liquid, it is inflammable, less toxic, be widely used in polymerization, condensation reaction
Catalyst, in recent years, tetrabutyl titanate have also obtained wider application in terms of coating is manufactured；It is modified using tetrabutyl titanate
The resins such as polyester, epoxy, phenolic aldehyde have excellent heat resistance, fire resistance, anti-corrosive properties.The synthetic route of tetrabutyl titanate has more
Kind, one of which is that titanium and n-butanol synthesize tetrabutyl titanate in polymerization reaction kettle, the conversion ratio of n-butanol in course of reaction
It is different, there is remaining n-butanol to need to be recycled, not only increase the extent of purification of tetrabutyl titanate, while to original
The recycling of material has certain contribution.
Utility model content
The purpose of this utility model can meet single to design a kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate
The requirement of the big volume of reaction, while unreacted monomer can be recycled.
The technical solution of the utility model is：A kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate, including reactor,
Reactor is provided with charging aperture and discharging opening, and level is provided with rotary shaft in the reactor, and one end of the rotary shaft is connected with electricity
Machine, the rotary shaft are provided with agitating paddle, and the adjacent agitating paddle is on the rotating shaft in reversely installation, the inside of the agitating paddle
Provided with heating rod, the both sides of the agitating paddle are provided with wing stirrer gear；The number of the agitating paddle is at least 4, the wing
The length of stirrer gear.
The top of the agitating paddle, which is additionally provided with, scrapes wall oar, and the section for scraping wall oar is engaged with the section of reactor, is scraped
The reaction material that wall oar is accumulated to reactor inner surface side wall scrapes, and disengages it from reactor side wall.
The upper surface of the reactor is additionally provided with pressure regulating hole, and acting as adjusting inside reactor for pressure regulating hole is pressed
Power, to ensure the work safety of reactor.
The upper surface of the reactor is additionally provided with condenser pipe, and MONOMER RECOVERY tank is additionally provided with below the condenser pipe；When anti-
At the end of answering, reaction monomers can be reclaimed using condenser pipe according to the difference of product and reaction monomers boiling point.
The motor and heating rod have power controller controls.
The beneficial effects of the utility model are：This fractionation horizontal reacting kettle, on the one hand adds single reaction volume, simultaneously
Multiple agitating paddles are set inside reactor, add mixing effect during reaction；Unreacted monomer is returned by condenser pipe
Receive, not only increase the purity of product, while unreacted monomer is recycled, meet resource and reclaim profit again
With, the environmental protection concept made the best use of everything.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Wherein, 1 is reactor, and 2 be charging aperture, and 3 be rotary shaft, and 4 be motor, and 5 be agitating paddle, and 6 be wing stirrer gear, 7
To scrape wall oar, 8 be heating rod, and 9 be pressure regulating hole, and 10 be discharging opening, and 11 be condenser pipe, and 12 be MONOMER RECOVERY tank.
Embodiment
Below in conjunction with the accompanying drawings, the technical solution of the utility model is described in detail.
A kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate, including reactor 1, reactor 1 be provided with charging aperture 2 and
Discharging opening 10, horizontal in the reactor 1 to be provided with rotary shaft 3, one end of the rotary shaft 3 is connected with motor 4, the rotary shaft 3
Agitating paddle 5 is provided with, the adjacent agitating paddle 5 is provided with heating in rotary shaft 3 in reversely installation, the inside of the agitating paddle 5
Rod 8, the both sides of the agitating paddle 5 are provided with wing stirrer gear 6；The number of the agitating paddle 5 is at least four, the wing stirring
The length of tooth 6.
The top of the agitating paddle 5, which is additionally provided with, scrapes wall oar 7, and the section for scraping wall oar 7 and the section of reactor 1 match
Close, scrape the reaction material that wall oar 7 is accumulated to the inner surface side wall of reactor 1 and scrape, disengage it from the side wall of reactor 1.
The upper surface of the reactor 1 is additionally provided with pressure regulating hole 9, and pressure regulating hole 9 act as adjusting in reactor 1
Portion's pressure, to ensure the work safety of reactor 1.
The upper surface of the reactor 1 is additionally provided with condenser pipe 11, and the lower section of the condenser pipe 11 is additionally provided with MONOMER RECOVERY tank
12；When the reaction is finished, reaction monomers can be carried out using condenser pipe 11 according to the difference of product and reaction monomers boiling point
Recovery.
The motor 4 and heating rod 8 have power controller controls.
Claims (7)
1. a kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate, including reactor（1）, reactor（1）It is provided with charging aperture
（2）And discharging opening（10）, it is characterised in that：The reactor（1）Interior level is provided with rotary shaft（3）, the rotary shaft（3）One
End is connected with motor（4）, the rotary shaft（3）It is provided with agitating paddle（5）, the adjacent agitating paddle（5）In rotary shaft（3）Upper is in anti-
To installation, the agitating paddle（5）Inside be provided with heating rod（8）, the agitating paddle（5）Both sides be provided with wing stirrer gear（6）.
A kind of 2. fractionation horizontal reacting kettle for producing tetrabutyl titanate according to claim 1, it is characterised in that：It is described to stir
Mix oar（5）Top be additionally provided with and scrape wall oar（7）, it is described to scrape wall oar（7）Section and reactor（1）Section be engaged.
A kind of 3. fractionation horizontal reacting kettle for producing tetrabutyl titanate according to claim 1, it is characterised in that：The institute
State reactor（1）Upper surface be additionally provided with pressure regulating hole（9）.
A kind of 4. fractionation horizontal reacting kettle for producing tetrabutyl titanate according to claim 1, it is characterised in that：It is described anti-
Answer kettle（1）Upper surface be additionally provided with condenser pipe（11）, the condenser pipe（11）Lower section be additionally provided with MONOMER RECOVERY tank（12）.
A kind of 5. fractionation horizontal reacting kettle for producing tetrabutyl titanate according to claim 1, it is characterised in that：It is described to stir
Mix oar（5）Number be at least 4.
A kind of 6. fractionation horizontal reacting kettle for producing tetrabutyl titanate according to claim 1, it is characterised in that：The wing
Type stirrer gear（6）Length.
A kind of 7. fractionation horizontal reacting kettle for producing tetrabutyl titanate according to claim 1, it is characterised in that：The electricity
Machine（4）And heating rod（8）There are power controller controls.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720655869.9U CN207025317U (en) | 2017-06-07 | 2017-06-07 | A kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720655869.9U CN207025317U (en) | 2017-06-07 | 2017-06-07 | A kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207025317U true CN207025317U (en) | 2018-02-23 |
Family
ID=61470751
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720655869.9U Expired - Fee Related CN207025317U (en) | 2017-06-07 | 2017-06-07 | A kind of fractionation horizontal reacting kettle for producing tetrabutyl titanate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207025317U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116983941A (en) * | 2023-09-27 | 2023-11-03 | 南通北风橡塑制品有限公司 | A horizontal reation kettle for polyurethane production |
-
2017
- 2017-06-07 CN CN201720655869.9U patent/CN207025317U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116983941A (en) * | 2023-09-27 | 2023-11-03 | 南通北风橡塑制品有限公司 | A horizontal reation kettle for polyurethane production |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180223 Termination date: 20190607 |