CN207002609U - A kind of Isosorbide-5-Nitrae butanediol purifying plant - Google Patents

A kind of Isosorbide-5-Nitrae butanediol purifying plant Download PDF

Info

Publication number
CN207002609U
CN207002609U CN201720879915.3U CN201720879915U CN207002609U CN 207002609 U CN207002609 U CN 207002609U CN 201720879915 U CN201720879915 U CN 201720879915U CN 207002609 U CN207002609 U CN 207002609U
Authority
CN
China
Prior art keywords
equipment
fluid reservoir
purifying
purification tank
bdo
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720879915.3U
Other languages
Chinese (zh)
Inventor
陈剑华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Three Hui (fujian) Industry & Trade Co Ltd
Original Assignee
Three Hui (fujian) Industry & Trade Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Three Hui (fujian) Industry & Trade Co Ltd filed Critical Three Hui (fujian) Industry & Trade Co Ltd
Priority to CN201720879915.3U priority Critical patent/CN207002609U/en
Application granted granted Critical
Publication of CN207002609U publication Critical patent/CN207002609U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The utility model discloses one kind 1,4 butanediol purifying plants, including equipment for purifying body, the bottom of equipment for purifying body is provided with firing equipment, the top of firing equipment is provided with fluid reservoir, the side of fluid reservoir is provided with liquid level gauge, the opposite side of fluid reservoir is provided with refluxing opening, the bottom of refluxing opening is provided with liquid inlet opening, the top of fluid reservoir is provided with reaction purification tank, the side of reaction purification tank is provided with return duct, and the top of reaction purification tank is provided with separating and filtering mouth, and the top of separating and filtering mouth is provided with purification liquid outlet.The device is one kind 1,4 butanediol purifying plants, the device can effectively solve the problems, such as Isosorbide-5-Nitrae butanediol equipment for purifying, and the equipment can effectively improve 1, the operating efficiency of 4 butanediols purification, easy to use simple, refining effect is preferable, while the function that there is recovery to purify, Material Cost is saved, it is very convenient.

Description

A kind of BDO purifying plant
Technical field
It the utility model is related to a kind of purifying plant, and in particular to a kind of BDO purifying plant.
Background technology
Purification refers to separate the impurity in mixture improves its purity with this, purifies as a kind of important chemistry Method, not only play an important roll in chemical research, similarly had a very important role in Chemical Manufacture, Bu Shaochong The chemical research and Chemical Manufacture wanted, all it is to purify, the purification of material is that the impurity in mixture is removed, with Obtain the process of pure material.Filtering is the dissolubility gap using material, and liquid and the solid insoluble in liquid are separated Method;Crystallization to being purified the different solubility of material and impurity, can make to be purified material molten from supersaturation using solvent Separated out in liquid, and allow impurity wholly or largely to remain in solution, so as to reach the purpose of purification;Distillation utilizes the liquid to dissolve each other The boiling point of each component is different in body mixture, the heating of liquid mixture, a certain component therein is become steam and is condensed into again Liquid, so as to reach the purpose of separating-purifying;Extraction utilizes different solubility of certain solute in immiscible solvent, with one Extracted in the solution that kind of solvent forms solute with another solvent from it, recycle liquid separation principle and method by they Separate;Chromatography is to utilize the difference of each component physicochemical properties in mixture, such as absorption affinity, molecular shape and big Small, molecule affinity, distribution coefficient etc., make each component in two-phase, a phase is fixed, and referred to as stationary phase, another phase flow through solid Determine phase, the distributed degrees referred to as in mobile phase are different, so that each component moves and reaches the purpose of separation at different rates.
On the basis of the technical conditions of existing equipment for purifying, the convenience that is used in BDO purifying plant and Still there are many weak points in feature, the refining effect of most BDO purifying plant is general, can waste big The Material Cost of amount, do not reach preferable refining effect, while during equipment use, lack one kind always and suitably carry Pure equipment is purified, and operating efficiency is undesirable, is inconvenient.
Utility model content
Therefore, in view of the above-mentioned problems, the utility model provides a kind of BDO purifying plant, so as to solve above-mentioned ask Topic.
To reach above-mentioned purpose, the utility model is achieved through the following technical solutions:The utility model provides one Kind BDO purifying plant, including equipment for purifying body, the bottom of the equipment for purifying body are provided with firing equipment, institute The top for stating firing equipment is provided with fluid reservoir, and the side of the fluid reservoir is provided with liquid level gauge, the opposite side of the fluid reservoir Refluxing opening is provided with, the bottom of the refluxing opening is provided with liquid inlet opening, and the top of the fluid reservoir is provided with reaction purification Tank, the side of the reaction purification tank are provided with return duct, and the top of the reaction purification tank is provided with separating and filtering mouth, described The top of separating and filtering mouth is provided with purification liquid outlet.
As a kind of optimal technical scheme of the present utility model, the side of the reaction purification tank is provided with material addition Mouthful.
As a kind of optimal technical scheme of the present utility model, the fluid reservoir is connected with reaction purification tank by return duct It is logical.
As a kind of optimal technical scheme of the present utility model, the bottom of the firing equipment is provided with heating valve, described Heating valve is connected with firing equipment.
By using preceding solution, the beneficial effects of the utility model are:
The device is a kind of BDO purifying plant, and the device can effectively solve BDO equipment for purifying Problem, the equipment can effectively improve the operating efficiency of BDO purification, and easy to use simple, refining effect is preferable, together When with recovery purification function, save Material Cost, it is very convenient.
Brief description of the drawings
Accompanying drawing is used for providing further understanding to of the present utility model, and a part for constitution instruction, with this practicality New embodiment is used to explain the utility model together, does not form to limitation of the present utility model.In the accompanying drawings:
Fig. 1 is overall structure diagram of the present utility model;
In figure:1st, equipment for purifying body;2nd, firing equipment;3rd, fluid reservoir;4th, liquid level gauge;5th, heating valve;6th, refluxing opening;7、 Liquid inlet opening;8th, reaction purification tank;9th, return duct;10th, separating and filtering mouth;11st, liquid outlet is purified;12nd, material adding mouth.
Embodiment
Describe embodiment of the present utility model in detail below with reference to specific embodiment, whereby to the utility model such as What application technology means solves technical problem, and the implementation process for reaching technique effect can fully understand and implement according to this.
Embodiment of the present utility model is:
With reference to figure 1, the utility model provides a kind of BDO purifying plant, including equipment for purifying body 1, and purification is set The bottom of standby body 1 is provided with firing equipment 2, and the top of firing equipment 2 is provided with fluid reservoir 3, and the side of fluid reservoir 3 is provided with Liquid level gauge 4, the opposite side of fluid reservoir 3 are provided with refluxing opening 6, and the bottom of refluxing opening 6 is provided with liquid inlet opening 7, fluid reservoir 3 Top is provided with reaction purification tank 8, and the side of reaction purification tank 8 is provided with return duct 9, and the top of reaction purification tank 8 is provided with Separating and filtering mouth 10, the top of separating and filtering mouth 10 are provided with purification liquid outlet 11.
The side of reaction purification tank 8 is provided with material adding mouth 12, can be facilitated by the material adding mouth 12 of setting and carried Reactant is added in pure process, lifts convenience.Fluid reservoir 3 is connected with reaction purification tank 8 by return duct 9, can The inside of the equipment is carried out by return duct 9 to repeat recovery purification, it is cost-effective, improve operating efficiency.
The bottom of firing equipment 2 is provided with heating valve 5, and heating valve 5 is connected with firing equipment 2, can be square by heating valve 5 Just temperature control is carried out to the equipment, reaches more preferably refining effect.
The device is a kind of BDO purifying plant, including equipment for purifying body 1, can when using the device Conveying material is carried out by liquid inlet opening 7, the internal liquid capacity of fluid reservoir 3 can be understood by liquid level gauge 4, passes through bottom Firing equipment 2 is heated, and temperature adjustment can be carried out by heating valve 5, and purification liquid carries out anti-inside reaction purification tank 8 Should, material is added by material adding mouth 12, after ion exchange resin removes metal ion, then obtained through distilation pure Product, enter at separating and filtering mouth 10, the waste material filtered will carry out recovery purification again by return duct 9, and purification liquid leads to Purification liquid outlet 11 is crossed to be discharged.
The device is a kind of BDO purifying plant, and the device can effectively solve BDO equipment for purifying Problem, the equipment can effectively improve the operating efficiency of BDO purification, and easy to use simple, refining effect is preferable, together When with recovery purification function, save Material Cost, it is very convenient.
Although specifically showing and describing the utility model with reference to preferred embodiment, those skilled in the art should This is understood, is not departing from the spirit and scope of the present utility model that appended claims are limited, in form and details On the utility model can be made a variety of changes, be the scope of protection of the utility model.

Claims (4)

1. a kind of BDO purifying plant, including equipment for purifying body (1), it is characterised in that the equipment for purifying body (1) bottom is provided with firing equipment (2), and the top of the firing equipment (2) is provided with fluid reservoir (3), the fluid reservoir (3) Side be provided with liquid level gauge (4), the opposite side of the fluid reservoir (3) is provided with refluxing opening (6), the bottom of the refluxing opening (6) Portion is provided with liquid inlet opening (7), and the top of the fluid reservoir (3) is provided with reaction purification tank (8), the reaction purification tank (8) side is provided with return duct (9), and the top of the reaction purification tank (8) is provided with separating and filtering mouth (10), the separation The top of filtering mouth (10) is provided with purification liquid outlet (11).
A kind of 2. BDO purifying plant according to claim 1, it is characterised in that:The reaction purification tank (8) Side be provided with material adding mouth (12).
A kind of 3. BDO purifying plant according to claim 1, it is characterised in that:The fluid reservoir (3) with it is anti- Tank (8) should be purified by return duct (9) to be connected.
A kind of 4. BDO purifying plant according to claim 1, it is characterised in that:The firing equipment (2) Bottom is provided with heating valve (5), and the heating valve (5) is connected with firing equipment (2).
CN201720879915.3U 2017-07-19 2017-07-19 A kind of Isosorbide-5-Nitrae butanediol purifying plant Expired - Fee Related CN207002609U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720879915.3U CN207002609U (en) 2017-07-19 2017-07-19 A kind of Isosorbide-5-Nitrae butanediol purifying plant

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720879915.3U CN207002609U (en) 2017-07-19 2017-07-19 A kind of Isosorbide-5-Nitrae butanediol purifying plant

Publications (1)

Publication Number Publication Date
CN207002609U true CN207002609U (en) 2018-02-13

Family

ID=61454214

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720879915.3U Expired - Fee Related CN207002609U (en) 2017-07-19 2017-07-19 A kind of Isosorbide-5-Nitrae butanediol purifying plant

Country Status (1)

Country Link
CN (1) CN207002609U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113527063A (en) * 2021-08-12 2021-10-22 南京朗碧源化工科技有限公司 An energy-saving acetylenic aldehyde BDO rectification process

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113527063A (en) * 2021-08-12 2021-10-22 南京朗碧源化工科技有限公司 An energy-saving acetylenic aldehyde BDO rectification process

Similar Documents

Publication Publication Date Title
CN204219812U (en) A kind of device of purification of organic acid
CN211445385U (en) Contain organic solvent's salt waste water evaporation equipment
CN208454853U (en) A kind of benzene acetonitrile continuous rectification apparatus
CN207002609U (en) A kind of Isosorbide-5-Nitrae butanediol purifying plant
CN112374967A (en) System and method for recovering ethanol from organic waste liquid
CN101780343B (en) Dynamic purification regenerator of harmful solvent and application thereof
CN106977409A (en) A kind of separation method of triethylamine and water
CN102001924A (en) Technology for reclaiming low-concentration formaldehyde from pesticide wastewater through ionic liquid supported liquid membrane pervaporation-distillation coupling technology
CN215609428U (en) Device for purifying propane and propylene
CN205759788U (en) Energy-saving single-action concentrates rectifier unit
CN205965074U (en) Accurate separator of high -purity n -heptane
CN210012777U (en) Azeotropic distillation separation device for mixed solvent
CN103304398B (en) A kind of method of purification of carboxylic acid aqueous solution
CN205412296U (en) Continuous rectification plant of nitromethane
CN212024963U (en) Solvent recovery system to pharmaceutical chemical industry high solvent waste water
CN204147584U (en) A kind of vapour-liquid hybrid extraction system fast
CN103274922B (en) Side rectification and azeotropic rectification integrated acetone-acetic acid-water separation method
CN107955038A (en) Catalyst mother liquor comprehensive reutilization method and device in a kind of propenecarbonyl
CN209662649U (en) Phenylacetic acid recyclable device
CN208865214U (en) One kind being used for supercritical CO2The mass transfer system of extracting rectifying
CN207645990U (en) The device of extraction saturation saline solution in a kind of industrial wastewater
CN206887263U (en) A chrome-free roughening chemical solution purification and reuse system for electroplating
CN106316793A (en) Alcohol preparing device and method based on the double rectification column and six-column and four-effect distillation
CN207537369U (en) A kind of ethylene glycol multi-effect distillation system
CN204543612U (en) A kind of methanol fractionation system

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180213

Termination date: 20190719