CN206604414U - Calcium stearate dispersion device for formulating - Google Patents
Calcium stearate dispersion device for formulating Download PDFInfo
- Publication number
- CN206604414U CN206604414U CN201720328663.5U CN201720328663U CN206604414U CN 206604414 U CN206604414 U CN 206604414U CN 201720328663 U CN201720328663 U CN 201720328663U CN 206604414 U CN206604414 U CN 206604414U
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- CN
- China
- Prior art keywords
- calcium stearate
- tank
- surge tank
- feeding pipe
- micelle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The utility model belongs to petrochemical industry, more particularly to a kind of calcium stearate dispersion device for formulating, including calcium stearate preparing tank, the top of calcium stearate preparing tank is respectively communicated with solvent feeding pipe and powder material feeding pipe, bottom connects calcium stearate surge tank, calcium stearate surge tank connects delivery pump, and delivery pump connects calcium stearate surge tank by return duct respectively, calcium stearate glue blender is connected by efferent duct.The utility model improves the dispersion effect of micelle, it is good scattered micelle granularity to be made more moderate uniform, reducing the influence of the solvent loss caused big granularity micelle residual solvent and postprocessing working procedures effusion solvent gas to environment more, the phenomenons such as big granularity micelle is blocked to pipeline and the easy current with removing of small grain size micelle lose are reduced simultaneously, so as to improve the operational stability of device, improve operating environment, product quality, reduction material consumption are improved, environmental pollution is reduced.
Description
Technical field
The utility model is related to a kind of calcium stearate dispersion device for formulating, belongs to petrochemical industry.
Background technology
In halogenated butyl rubber production process, calcium stearate is a kind of very important additive, micelle is risen uniform
Scattered effect, technique is prepared and added to its dispersion liquid influences larger to properties of product.Current halogenated butyl rubber process units
The preparation of middle calcium stearate dispersion and feed postition are that calcium stearate powder is charged first in water and prepared, after the completion of preparation
Calcium stearate dispersion and circulating hot water are mixed into halogenation flash tank, and glue individually enters halogenation flash tank, in flash tank
Calcium stearate is disperseed to micelle.The preparation of this calcium stearate dispersion and feed postition make glue/water of scattered completion
Aqueous phase in mixed system is white, and substantial amounts of calcium stearate, which is present in aqueous phase, causes calcium stearate utilization rate low；Scattered effect
Fruit is also undesirable, and micelle has excessive too small phenomenon to occur, and this adds increased the operation difficulty of postprocessing working procedures, also reduces production
Quality, adds calcium stearate consumption.
Utility model content
The technical problems to be solved in the utility model is：There is provided a kind of calcium stearate utilization rate height, micelle dispersion effect good
Calcium stearate dispersion device for formulating.
Calcium stearate dispersion device for formulating described in the utility model, including calcium stearate preparing tank, calcium stearate are matched somebody with somebody
The top of tank processed is respectively communicated with solvent feeding pipe and powder material feeding pipe, bottom connection calcium stearate surge tank, calcium stearate
Surge tank connects delivery pump, and delivery pump connects calcium stearate surge tank by return duct respectively, stearic acid is connected by efferent duct
Calcium glue blender.
Add suitable solvent in calcium stearate preparing tank to mix with calcium stearate solid powder, calcium stearate preparing tank
Connect calcium stearate surge tank, calcium stearate surge tank connection calcium stearate delivery pump, calcium stearate delivery pump connection stearic acid
Calcium glue blender, calcium stearate glue blender connection halogenation flash tank.
Quantitative solvent is passed through in calcium stearate preparing tank, quantitative calcium stearate solid powder is then added, stirred
It is uniformly after solvent-borne type calcium stearate dispersion, to be discharged into calcium stearate surge tank, delayed calcium stearate by calcium stearate delivery pump
Rush material in tank and send into calcium stearate glue blender, glue and solvent-borne type calcium stearate point in calcium stearate glue blender
Dispersion liquid is sufficiently mixed homogeneous, enters back into halogenation flash tank.
Dispersion liquid material feeding pipe is set at the top of described calcium stearate surge tank, and bottom sets the discharging of dispersion liquid material
Pipe, dispersion liquid material feeding pipe connects the bottom of calcium stearate preparing tank, dispersion liquid material discharge nozzle connection delivery pump.
The junction of described return duct and calcium stearate surge tank is located at the top of calcium stearate surge tank.
It is mixture outlet at the top of described calcium stearate glue blender, bottom is mixture inlet, mixture inlet
Connect efferent duct and glue feeding pipe.
Stirring dress is respectively provided with described calcium stearate preparing tank, calcium stearate surge tank and calcium stearate glue blender
Put.
Described agitating device includes motor, and motor output end connection agitating shaft, agitating shaft is placed, stirred vertically
Mix axle bottom and stirring vane is set.
The beneficial effects of the utility model are：
The arrangement increases the dispersion effect of micelle, it is good it is scattered micelle granularity can be made more moderate uniform, reduce
Influence of the solvent loss and postprocessing working procedures effusion solvent gas caused big granularity micelle residual solvent to environment, subtracts more simultaneously
The phenomenons such as big granularity micelle is blocked to pipeline and the easy current with removing of small grain size micelle lose are lacked, so as to improve the behaviour of device
Make stability, improve operating environment, improve product quality, reduction material consumption, reduce environmental pollution.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
In figure：1st, powder material feeding pipe；2nd, solvent feeding pipe；3rd, calcium stearate preparing tank；4th, calcium stearate surge tank；
5th, delivery pump；6th, glue feeding pipe；7th, stirring vane；8th, mixture outlet；9th, agitating shaft；10th, calcium stearate glue blender.
Embodiment
The utility model is described further below in conjunction with the accompanying drawings：
As shown in figure 1, calcium stearate dispersion device for formulating described in the utility model, including calcium stearate preparing tank 3,
The top of calcium stearate preparing tank 3 is respectively communicated with solvent feeding pipe 2 and powder material feeding pipe 1, and bottom connection calcium stearate delays
Tank 4 is rushed, the connection delivery pump 5 of calcium stearate surge tank 4, delivery pump 5 connects calcium stearate surge tank 4 by return duct respectively, led to
Cross efferent duct connection calcium stearate glue blender 10.The top of calcium stearate surge tank 4 sets dispersion liquid material feeding pipe, bottom
Dispersion liquid material discharge nozzle, the bottom of dispersion liquid material feeding pipe connection calcium stearate preparing tank 3, the discharging of dispersion liquid material are set
Pipe connects delivery pump 5.The junction of return duct and calcium stearate surge tank 4 is located at the top of calcium stearate surge tank 4.Stearic acid
The top of calcium glue blender 10 is mixture outlet 8, and bottom is mixture inlet, and mixture inlet connection efferent duct and glue enter
Expects pipe 6.Agitating device is all provided with calcium stearate preparing tank 3, calcium stearate surge tank and calcium stearate glue blender 10.Stir
Mixing device includes motor, and motor output end connection agitating shaft 9, agitating shaft 9 is placed vertically, and the bottom of agitating shaft 9 is set
Stirring vane 7.
The direction of arrow is the direction that process fluid flows in diagram.
Quantitative solvent is added by solvent feeding pipe 2 in calcium stearate preparing tank 3, then passes through powder material pan feeding
Pipe 1 adds quantitative calcium stearate solid powder, stirs and is mixed into solvent-borne type calcium stearate dispersion, and material passes through gravity flow
Calcium stearate surge tank 4 is discharged into, by calcium stearate delivery pump 5 by a part of solvent-borne type calcium stearate in calcium stearate surge tank 4
In dispersion liquid feeding calcium stearate glue blender 10, a part of circulating reflux to calcium stearate surge tank 4.Calcium stearate glue
Blender 10 carries agitator, and material uses the form of bottom in and top out, makes calcium stearate dispersion with glue in special container
In fully contact, mixing, homogeneous in advance, form homogeneous system, be conducive to the scattered of follow-up phase.Mixed by calcium stearate glue
The solvent-borne type calcium stearate dispersion that the top of clutch 10 is sent out enters halogenation flash tank with glue mixture and further disperses flash distillation.
The calcium stearate dispersion prepared is added into glue/water mixed system and tested.By calcium stearate
Dispersion liquid is added in this mixed system, and profit is mutually layered quickly, and aqueous phase is totally transparent, and oil phase is white, it is seen that the present apparatus is matched somebody with somebody
The calcium stearate dispersion utilization rate of system is higher.
Claims (6)
1. a kind of calcium stearate dispersion device for formulating, it is characterised in that：Including calcium stearate preparing tank (3), calcium stearate is matched somebody with somebody
The top of tank (3) processed is respectively communicated with solvent feeding pipe (2) and powder material feeding pipe (1), bottom connection calcium stearate surge tank
(4), calcium stearate surge tank (4) connection delivery pump (5), delivery pump (5) connects calcium stearate surge tank by return duct respectively
(4) calcium stearate glue blender (10), is connected by efferent duct.
2. calcium stearate dispersion device for formulating according to claim 1, it is characterised in that：Calcium stearate surge tank (4)
Top sets dispersion liquid material feeding pipe, and bottom sets dispersion liquid material discharge nozzle, dispersion liquid material feeding pipe connection stearic acid
The bottom of calcium preparing tank (3), dispersion liquid material discharge nozzle connection delivery pump (5).
3. calcium stearate dispersion device for formulating according to claim 1, it is characterised in that：Return duct delays with calcium stearate
The junction for rushing tank (4) is located at the top of calcium stearate surge tank (4).
4. calcium stearate dispersion device for formulating according to claim 1, it is characterised in that：Calcium stearate glue blender
(10) top is mixture outlet (8), and bottom is mixture inlet, mixture inlet connection efferent duct and glue feeding pipe (6).
5. calcium stearate dispersion device for formulating according to claim 1, it is characterised in that：Calcium stearate preparing tank (3),
Agitating device is all provided with calcium stearate surge tank (4) and calcium stearate glue blender (10).
6. calcium stearate dispersion device for formulating according to claim 5, it is characterised in that：Agitating device includes driving electricity
Machine, motor output end connection agitating shaft (9), agitating shaft (9) is placed vertically, and agitating shaft (9) bottom sets stirring vane
(7)。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720328663.5U CN206604414U (en) | 2017-03-30 | 2017-03-30 | Calcium stearate dispersion device for formulating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720328663.5U CN206604414U (en) | 2017-03-30 | 2017-03-30 | Calcium stearate dispersion device for formulating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206604414U true CN206604414U (en) | 2017-11-03 |
Family
ID=60173361
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720328663.5U Active CN206604414U (en) | 2017-03-30 | 2017-03-30 | Calcium stearate dispersion device for formulating |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206604414U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106823905A (en) * | 2017-03-30 | 2017-06-13 | 山东齐鲁石化工程有限公司 | Calcium stearate dispersion preparing process and device |
-
2017
- 2017-03-30 CN CN201720328663.5U patent/CN206604414U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106823905A (en) * | 2017-03-30 | 2017-06-13 | 山东齐鲁石化工程有限公司 | Calcium stearate dispersion preparing process and device |
| CN106823905B (en) * | 2017-03-30 | 2023-06-30 | 山东齐鲁石化工程有限公司 | Process and device for preparing calcium stearate dispersion liquid |
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