CN206549402U - A kind of collection of diphenyl sulphone (DPS) sublimate and retracting device - Google Patents
A kind of collection of diphenyl sulphone (DPS) sublimate and retracting device Download PDFInfo
- Publication number
- CN206549402U CN206549402U CN201720250498.6U CN201720250498U CN206549402U CN 206549402 U CN206549402 U CN 206549402U CN 201720250498 U CN201720250498 U CN 201720250498U CN 206549402 U CN206549402 U CN 206549402U
- Authority
- CN
- China
- Prior art keywords
- casing
- sublimate
- air inlet
- collecting box
- collection device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- KZTYYGOKRVBIMI-UHFFFAOYSA-N diphenyl sulfone Chemical compound C=1C=CC=CC=1S(=O)(=O)C1=CC=CC=C1 KZTYYGOKRVBIMI-UHFFFAOYSA-N 0.000 title claims abstract description 36
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000007921 spray Substances 0.000 claims abstract description 16
- 238000004140 cleaning Methods 0.000 claims description 9
- 238000005507 spraying Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- 238000004821 distillation Methods 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 5
- 239000000178 monomer Substances 0.000 abstract description 4
- 230000009172 bursting Effects 0.000 abstract description 2
- 238000001311 chemical methods and process Methods 0.000 abstract description 2
- 239000003344 environmental pollutant Substances 0.000 abstract description 2
- 238000012423 maintenance Methods 0.000 abstract description 2
- 231100000719 pollutant Toxicity 0.000 abstract description 2
- 230000002265 prevention Effects 0.000 abstract description 2
- 239000007789 gas Substances 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 6
- 238000000889 atomisation Methods 0.000 description 3
- 238000004064 recycling Methods 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 238000012824 chemical production Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 230000000505 pernicious effect Effects 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Landscapes
- Treating Waste Gases (AREA)
Abstract
The utility model provides collection and the retracting device of a kind of diphenyl sulphone (DPS) sublimate, is made up of collecting box and spray collection device two parts；The two ends of casing are respectively equipped with air inlet and exhaust outlet, deflection plate in casing in up and down serrated vertical layout, by casing be separated into above and below S-shaped air channel, spray collection device, secondary air inlet, atomizing sprayer are respectively equipped with the top of sprayed tank, bottom is provided with collecting pit and discharge outlet；Sprayed tank is connected by exhaust duct with activated carbon adsorber；The bottom of activated carbon adsorber is exhaust outlet.Using collecting box and spray collection device structure, the monomer material of distillation is reclaimed to greatest extent, is realized that the Matter Transfer of production process is utilized, is reduced production cost；The problem of a large amount of sublimates that solution is produced in the chemical process of part effectively can not be collected and reclaimed, can be distilled with prevention and control sublimate high temperature, and workshop can be made to reach clean dustless requirement；The utility model is simple to operate, and cost is relatively low, meets bursting problem maintenance and changes quick；Realize the zero-emission that gas pollutant is realized in production process.
Description
Technical field
The utility model belongs to chemical production equipment field, discloses a kind of collection of diphenyl sulphone (DPS) sublimate and reclaims dress
Put, be related in high-temperature reaction process, there is distillation monomer in reaction system, the discharge to such material can be controlled effectively, and
Sublimate can be reclaimed to greatest extent, accomplish sublimate zero-emission and can be with cycling and reutilization.
Background technology
In chemical production field, substantial amounts of easy distillation material is as reaction monomers or reaction dissolvent, such as in polyethers ether
In the building-up process of ketone resin, diphenyl sulphone (DPS) will be used as reaction dissolvent.Diphenyl sulphone (DPS) extensively should as a kind of solvent easily distilled
For Polymer Synthesizing field, because its boiling point is relatively low and easy distillation, substantial amounts of reaction dissolvent is caused to be distilled during blowing,
It how to be then a great problem of production field by its efficient recycling.
Existing to collect easy sublimate and mainly use special sublimate collection device, the device avoids sublimate to big
Gas discharge has remarkable result, but such equipment cost is higher, and unsuitable medium-sized and small enterprises use, and the kind equipment is only capable of to rising
Magnificent thing is obstructed, it is impossible to effective to carry out recycling to sublimate.
The content of the invention
The utility model discloses a kind of collection of diphenyl sulphone (DPS) sublimate and retracting device, to solve in part Chemical Manufacture
During a large amount of sublimates for producing the problem of effectively can not collect and reclaim, while the covering device also have it is easy to operate, into
The advantages such as this low, sublimate zero-emission.
This collection for using a kind of new described diphenyl sulphone (DPS) sublimate and retracting device, dress is collected by collecting box and spray
Put two parts composition；
Described collecting box, including casing, air inlet, deflection plate, cleaning door, exhaust outlet；The two ends of casing are respectively equipped with
Air inlet and exhaust outlet, deflection plate in casing in up and down serrated vertical layout, by casing be separated into above and below S-shaped air channel, increase
Atmospheric passes through the stroke in casing；The bottom of casing is provided with multiple cleaning doors, the air channel for clearing up collecting box；Casing
Exhaust outlet is connected with spraying the secondary air inlet pipeline of collection device, and centre sets blower unit；
The spray collection device, including sprayed tank, secondary air inlet, atomizing sprayer, collecting pit, discharge outlet, row
Airduct, activated carbon adsorber, exhaust outlet；Secondary air inlet, atomizing sprayer are respectively equipped with the top of sprayed tank, bottom is provided with
Collecting pit and discharge outlet；Sprayed tank is connected by exhaust duct with activated carbon adsorber；The bottom of activated carbon adsorber is exhaust outlet.
Good effect of the present utility model is：Using collecting box and spray collection device structure, reclaim rise to greatest extent
The monomer material of China, realizes that the Matter Transfer of production process is utilized, reduces production cost；Solve in part chemical process
The problem of a large amount of sublimates of middle generation effectively can not be collected and reclaimed, can be distilled with prevention and control sublimate high temperature, can make production
Workshop reaches clean dustless requirement；The utility model is simple to operate, and cost is relatively low, meets bursting problem maintenance and changes quick；It is real
The zero-emission that gas pollutant is realized in production process is showed.
Brief description of the drawings
Fig. 1 is the utility model sublimate collecting box structural representation；
Fig. 2 is that the utility model sublimate sprays collection device structural representation；
In figure：1 air inlet, 2 deflection plates, 3 cleaning doors, 4 exhaust outlets, 5 secondary air inlets, 6 atomizing sprayers, 7 are collected
Pond, 8 discharge outlet, 9 exhaust ducts, 10 activated carbon adsorbers, 11 exhaust outlets, 12 sprayed tanks, 13 casings.
Embodiment
One embodiment of the present utility model is described in detail below in conjunction with accompanying drawing.
The utility model embodiment as shown in Figure 1, 2, is made up of collecting box and spray collection device two parts；Described receipts
Header, including casing 13, air inlet 1, deflection plate 2, cleaning door 3, exhaust outlet 4；The two ends of casing 13 are respectively equipped with the He of air inlet 1
Exhaust outlet 4, deflection plate 2 in casing 13 in up and down serrated vertical layout, by casing 13 be separated into above and below S-shaped air channel, increase
Gas passes through the stroke in casing 13；The bottom of casing 13 is provided with multiple cleaning doors 3, the air channel for clearing up collecting box；Case
The exhaust outlet 4 of body 13 is connected with spraying the pipeline of secondary air inlet 5 of collection device, and centre sets blower unit；
The spray collection device, including sprayed tank 12, secondary air inlet 5, atomizing sprayer 6, collecting pit 7, draining
Mouth 8, exhaust duct 9, activated carbon adsorber 10, exhaust outlet 11；The top of sprayed tank 12 is respectively equipped with secondary air inlet 5, atomization spray
Shower device 6, bottom is provided with collecting pit 7 and discharge outlet 8；Sprayed tank 12 is connected by exhaust duct 9 with activated carbon adsorber 10；Activity
The bottom of charcoal adsorption tower 10 is exhaust outlet 11.
The utility model is in use, collecting box is connected with reactor first, the air inlet 1 of collecting box and the air draft of reactor
Mouth is directly connected to, and the deflection plate 2 in collecting box is in alternate layout up and down, and the quantity of deflection plate is 20, and the height of deflection plate 2 is less than
Collecting box height, it is ensured that the gas containing sublimate is released in reactor by being S-shaped up and down during collecting box, due to containing distillation
The gas of thing can be begun to cool down when passing through collecting box, and gas sets deflection plate to collect the sublimate cooled down on a small quantity by every section.
Multiple cleaning doors 3 of collecting box are in closure state in utility model works.The remaining gas containing sublimate is with air draft
Mouth 4 is directly entered sublimate spray collection device.This step reclaims for a step of sublimate, if sublimate is excessive, easily causes
Blocked in sublimate collecting box, cleaning door 3 can be opened, cleared up in time compared with multiposition separating out, it is ensured that sublimate is collected
S-shaped air channel is unimpeded in case.
The exhaust outlet 3 of casing 13 is joined directly together with secondary air inlet 5, and centre sets blower unit, contains by preliminary treatment
The gas for having sublimate enters sublimate spray system by secondary air inlet 5.The sprayed tank 12 is provided with atomization spray on top
Mist device 6, gas carries out spray process after entering by atomisation device 6, and sublimate is carried out condensing after heat exchange with water, sunk
Enter collecting pit 7, sublimate elutes clean from gas after this step.Residual gas enters charcoal absorption by exhaust duct 9
Tower 10, further adsorption treatment is carried out to other pernicious gases or impurity, after exclude no sublimate and harmful from exhaust outlet 11
The gas of material.The bottom of collecting pit 7 is provided with discharge outlet 8, sublimate/water mixed liquid of collection can be detached into collecting pit 7, be returned
Receive recycling processing.
Claims (1)
1. collection and the retracting device of a kind of diphenyl sulphone (DPS) sublimate, it is characterised in that by collecting box and spray collection device two parts
Composition；
Described collecting box, including casing, air inlet, deflection plate, cleaning door, exhaust outlet；The two ends of casing are respectively equipped with air intake
Mouthful and exhaust outlet, deflection plate in casing in up and down serrated vertical layout, by casing be separated into above and below S-shaped air channel, increase gas
Body passes through the stroke in casing；The bottom of casing is provided with multiple cleaning doors, the air channel for clearing up collecting box；The air draft of casing
Mouth is connected with spraying the secondary air inlet pipeline of collection device, and centre sets blower unit；
The spray collection device, including sprayed tank, secondary air inlet, atomizing sprayer, collecting pit, discharge outlet, exhaust duct,
Activated carbon adsorber, exhaust outlet；Secondary air inlet, atomizing sprayer are respectively equipped with the top of sprayed tank, bottom is provided with collection
Pond and discharge outlet；Sprayed tank is connected by exhaust duct with activated carbon adsorber；The bottom of activated carbon adsorber is exhaust outlet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720250498.6U CN206549402U (en) | 2017-03-15 | 2017-03-15 | A kind of collection of diphenyl sulphone (DPS) sublimate and retracting device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720250498.6U CN206549402U (en) | 2017-03-15 | 2017-03-15 | A kind of collection of diphenyl sulphone (DPS) sublimate and retracting device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206549402U true CN206549402U (en) | 2017-10-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720250498.6U Active CN206549402U (en) | 2017-03-15 | 2017-03-15 | A kind of collection of diphenyl sulphone (DPS) sublimate and retracting device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206549402U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108479343A (en) * | 2018-06-08 | 2018-09-04 | 威海涌鑫环保工程有限公司 | A kind of Intelligentized control method based on three warehouse formula organic waste gas treatment equipments |
-
2017
- 2017-03-15 CN CN201720250498.6U patent/CN206549402U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108479343A (en) * | 2018-06-08 | 2018-09-04 | 威海涌鑫环保工程有限公司 | A kind of Intelligentized control method based on three warehouse formula organic waste gas treatment equipments |
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