CN206045978U - A kind of sulfur dioxide liquid automatic feeding system - Google Patents

A kind of sulfur dioxide liquid automatic feeding system Download PDF

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CN206045978U
CN206045978U CN201620711943.XU CN201620711943U CN206045978U CN 206045978 U CN206045978 U CN 206045978U CN 201620711943 U CN201620711943 U CN 201620711943U CN 206045978 U CN206045978 U CN 206045978U
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sulfur dioxide
liquid level
feeding
metering tank
liquid
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范忠雷
种煜晖
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Zhengzhou University
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Abstract

本实用新型涉及一种液体二氧化硫自动加料系统。该系统由二氧化硫储罐、进料泵、高位计量槽、搪瓷反应釜、带程序段的智能仪表、液位压差变送器、调节阀和电磁阀等部件构成。所述系统的高位计量槽通过进料泵和带有电磁阀的管线与二氧化硫储罐相连,其底部出料口通过设有调节阀的管线与搪瓷反应釜相连。备料时,压差变送器检测计量槽二氧化硫的液位信号,液位达到给定值时智能仪表控制进料泵和电磁阀的启闭。程序加料时,利用液位压差信号与二氧化硫加料量之间的对应关系,通过计量槽液位信号来控制二氧化硫的程序加料。所述系统通过计量槽液位信号来控制二氧化硫程序加料量,简化了控制方案,提高了加料量的控制精度。

The utility model relates to an automatic liquid sulfur dioxide feeding system. The system consists of sulfur dioxide storage tanks, feed pumps, high-level metering tanks, enamel reactors, intelligent instruments with program segments, liquid level differential pressure transmitters, regulating valves and solenoid valves. The high-level metering tank of the system is connected to the sulfur dioxide storage tank through a feed pump and a pipeline with a solenoid valve, and its bottom outlet is connected to an enamel reaction kettle through a pipeline with a regulating valve. When preparing materials, the differential pressure transmitter detects the liquid level signal of sulfur dioxide in the metering tank, and when the liquid level reaches a given value, the intelligent instrument controls the opening and closing of the feed pump and solenoid valve. During program feeding, the program feeding of sulfur dioxide is controlled by the liquid level signal of the metering tank by using the corresponding relationship between the liquid level pressure difference signal and the sulfur dioxide feeding amount. The system controls the programmed feeding amount of sulfur dioxide through the liquid level signal of the metering tank, which simplifies the control scheme and improves the control precision of the feeding amount.

Description

一种液体二氧化硫自动加料系统A liquid sulfur dioxide automatic feeding system

技术领域technical field

本实用新型涉及一种液体物料自动加料系统,具体涉及糖精钠生产过程中将液体二氧化硫添加到反应釜的系统。The utility model relates to an automatic feeding system for liquid materials, in particular to a system for adding liquid sulfur dioxide to a reaction kettle during the production process of sodium saccharin.

背景技术Background technique

糖精钠生产过程中需要添加各种原料,其中置换反应工段需要在不同的时间间隔内按照不同流速添加液体二氧化硫。该工段二氧化硫加料为间歇式操作,操作压力约0.4MPa,每5分钟调节一次加料速度,总计加料量610公斤,70分钟一个循环。为保证生产过程操作稳定,产品质量可靠,现有的生产中多采用人工投料的方式,操作工人根据要求通过手动阀门来调节二氧化硫的进料流量,通过现场二氧化硫计量罐的液位来估算不同时间点所添加的物料总量。该方式不但操作工作量大,而且进料量的偏差也大,对产品的质量会造成很大影响。后来,采用流量变送器测定二氧化硫加料的瞬时体积流量和累积体积流量,通过单片机控制方式实现二氧化硫加料。然而该方式在加料中、后期存在二氧化硫加料总量累积误差大,尤其小流量加料操作时,控制不及时,流速偏差大等缺陷。因此,需要开发一种操作简单,加料准确,适用于糖精钠生产的二氧化硫程序加料系统,以提高置换工段生产效率和操作可靠性。Various raw materials need to be added in the production process of sodium saccharin, and the replacement reaction section needs to add liquid sulfur dioxide at different flow rates at different time intervals. The sulfur dioxide feeding in this section is intermittent operation, the operating pressure is about 0.4MPa, and the feeding speed is adjusted every 5 minutes. The total feeding amount is 610 kg, and the cycle is 70 minutes. In order to ensure stable operation of the production process and reliable product quality, manual feeding is mostly used in the existing production. Operators adjust the feed flow of sulfur dioxide through manual valves according to requirements, and estimate different times based on the liquid level of the sulfur dioxide metering tank on site. Point the total amount of material added. This method not only has a large workload, but also has a large deviation in the amount of feed, which will have a great impact on the quality of the product. Later, the flow transmitter was used to measure the instantaneous volume flow and cumulative volume flow of sulfur dioxide feeding, and the sulfur dioxide feeding was realized through the control mode of single-chip microcomputer. However, this method has defects such as a large cumulative error in the total amount of sulfur dioxide feeding during and at the later stage of feeding, especially when the feeding operation is performed at a small flow rate, the control is not timely, and the flow rate deviation is large. Therefore, it is necessary to develop a sulfur dioxide program feeding system suitable for the production of sodium saccharin with simple operation and accurate feeding, so as to improve the production efficiency and operational reliability of the replacement section.

发明内容Contents of the invention

针对现有技术存在的缺陷,本实用新型目的是提供一种液体物料自动加料系统,尤其用于糖精钠生产中按程序要求将液体二氧化硫定量添加到反应釜的系统。Aiming at the defects in the prior art, the purpose of this utility model is to provide an automatic feeding system for liquid materials, especially a system for quantitatively adding liquid sulfur dioxide to the reactor in the production of saccharin sodium according to the program requirements.

本实用新型所采用的技术方案是:The technical scheme adopted in the utility model is:

本实用新型的液体二氧化硫自动加料系统包括二氧化硫备料系统和程序自动进料系统,由二氧化硫储罐、进料泵、高位计量槽、搪瓷反应釜、带程序段的智能仪表、液位压差变送器、调节阀和电磁阀等部件构成,具备备料、程序进料、加料复位和结束等功能。所述系统的二氧化硫高位计量槽顶部设有二氧化硫备料口、恒压平衡管接口和溢流口,下部设有二氧化硫出料口。计量槽备料口通过加料泵和带有电磁阀的管线与二氧化硫储罐相连。搪瓷反应釜顶部设有搅拌电机、搅拌器和尾气出口,底部设有二氧化硫进料口和物料出料口。计量槽下部的出料口通过带有调节阀的二氧化硫加料管线与反应釜的二氧化硫进料口相连。备料时高位槽的初始液位和终止液位信号、电磁阀和加料泵的启闭信号,程序加料时二氧化硫加料量所对应的液位信号、自动调节阀的开度,以及复位及结束信号均与带程序段的智能仪表相连接。The liquid sulfur dioxide automatic feeding system of the utility model includes a sulfur dioxide material preparation system and a program automatic feeding system, which consists of a sulfur dioxide storage tank, a feed pump, a high-level metering tank, an enamel reaction kettle, an intelligent instrument with a program segment, and a liquid level differential pressure transmitter. It is composed of components such as controller, regulating valve and solenoid valve, and has functions such as material preparation, program feeding, feeding reset and end. The top of the high-level sulfur dioxide metering tank of the system is provided with a sulfur dioxide preparation port, a constant pressure balance pipe interface and an overflow port, and a sulfur dioxide discharge port is provided at the bottom. The material preparation port of the metering tank is connected with the sulfur dioxide storage tank through a feed pump and a pipeline with a solenoid valve. The top of the enamel reaction kettle is equipped with a stirring motor, agitator and tail gas outlet, and the bottom is equipped with a sulfur dioxide inlet and a material outlet. The discharge port at the lower part of the metering tank is connected with the sulfur dioxide feed port of the reactor through a sulfur dioxide feed pipeline with a regulating valve. The initial liquid level and end liquid level signal of the high level tank, the opening and closing signal of the solenoid valve and the feeding pump during material preparation, the liquid level signal corresponding to the sulfur dioxide feeding amount during program feeding, the opening degree of the automatic regulating valve, and the reset and end signals are all Connect with smart meter with program segment.

本实用新型的备料系统由二氧化硫储罐、进料泵、高位计量槽、和二氧化硫备料控制系统组成。所述二氧化硫备料控制系统由液位压差变送器与智能仪表相连,利用仪表上下限报警实现进料泵和电磁阀的启闭。The material preparation system of the utility model is composed of a sulfur dioxide storage tank, a feed pump, a high-level metering tank, and a sulfur dioxide material preparation control system. The sulfur dioxide stock preparation control system is connected by a liquid level differential pressure transmitter and an intelligent instrument, and realizes the opening and closing of the feed pump and the electromagnetic valve by using the upper and lower limit alarms of the instrument.

本实用新型的程序自动进料系统由高位计量槽、搪瓷反应釜、智能仪表、液位压差变送器、自动调节阀等部件构成。程序加料时二氧化硫加料量所对应的液位信号、自动调节阀的开度,以及复位及结束信号均与带程序段的智能仪表控制箱相连。The program automatic feeding system of the utility model is composed of a high-level metering tank, an enamel reaction kettle, an intelligent instrument, a liquid level differential pressure transmitter, an automatic regulating valve and other components. The liquid level signal corresponding to the amount of sulfur dioxide added during program feeding, the opening degree of the automatic regulating valve, and the reset and end signals are all connected to the intelligent instrument control box with program segments.

本实用新型的工作原理是利用计量槽中二氧化硫压差信号与加料量之间的对应关系,通过控制计量槽中二氧化硫的液位来实现对应时间的加料量。该装置通过自动给定液位值来控制二氧化硫高位槽不同时间的液位,实现二氧化硫程序加料。The working principle of the utility model is to use the corresponding relationship between the pressure difference signal of sulfur dioxide in the metering tank and the feeding amount, and realize the feeding amount corresponding to the time by controlling the liquid level of the sulfur dioxide in the metering tank. The device controls the liquid level of the sulfur dioxide high-level tank at different times by automatically setting the liquid level value, and realizes the sulfur dioxide program feeding.

所述的液体二氧化硫自动加料系统通过计量槽的二氧化硫液位来控制生产过程的加料量,有利于工艺过程的操作。相比累计流量加料控制技术,所述系统简化了加料过程的控制方案,提高了过程加料量的控制精度,而且操作系统自动化程度也得到了提高。The liquid sulfur dioxide automatic feeding system controls the feeding amount in the production process through the sulfur dioxide liquid level in the metering tank, which is beneficial to the operation of the process. Compared with the cumulative flow feeding control technology, the system simplifies the control scheme of the feeding process, improves the control accuracy of the feeding amount in the process, and the automation degree of the operating system is also improved.

附图说明:Description of drawings:

图1是本实用新型液体二氧化硫自动加料系统的结构示意图。Fig. 1 is the structural representation of the utility model liquid sulfur dioxide automatic feeding system.

具体实施方式:detailed description:

本实用新型所描述的实施例也适用于其它液体的程序加料,由此所获得的其它实施例,也属于本实用新型保护的范围。The embodiments described in the utility model are also applicable to the programmed feeding of other liquids, and other embodiments obtained thereby also belong to the protection scope of the utility model.

本实用新型的液体二氧化硫自动加料系统由二氧化硫储罐1、进料泵2、高位计量槽3、搪瓷反应釜4、带程序段智能仪表5、液位压差变送器6、电磁阀7、自动调节阀8、恒压平衡管9以及相关管线构成。其中高位计量槽3设有玻璃管液位计301,计量槽3顶部设有二氧化硫备料口31、恒压平衡管接口32和溢流口33,下部设有二氧化硫出料口34。搪瓷反应釜4为带夹套反应器,其顶部设有搅拌电机401、搅拌器402和尾气出口43,底部设有二氧化硫进料口41和物料出料口42。The liquid sulfur dioxide automatic feeding system of the utility model consists of a sulfur dioxide storage tank 1, a feed pump 2, a high-level metering tank 3, an enamel reaction kettle 4, an intelligent instrument with a program segment 5, a liquid level differential pressure transmitter 6, a solenoid valve 7, An automatic regulating valve 8, a constant pressure balance pipe 9 and related pipelines are formed. Among them, the high-level metering tank 3 is provided with a glass tube liquid level gauge 301, the top of the metering tank 3 is provided with a sulfur dioxide preparation port 31, a constant pressure balance pipe interface 32 and an overflow port 33, and the bottom part is provided with a sulfur dioxide discharge port 34. The enamel reaction kettle 4 is a jacketed reactor with a stirring motor 401 , an agitator 402 and an exhaust gas outlet 43 at the top, and a sulfur dioxide feed port 41 and a material discharge port 42 at the bottom.

本实用新型所述系统的二氧化硫储罐1经由进料泵2的输送管线,经过电磁阀7和备料口31,与高位计量槽3相连;计量槽3二氧化硫出料口34经设有调节阀8的管线和二氧化硫进料口41与搪瓷反应釜4连接。所述带程序段智能仪表5的输入端与高位计量槽3上的液位压差变送器6相连,输出端分别与电磁阀7和调节阀8相连。The sulfur dioxide storage tank 1 of the system described in the utility model is connected to the high-level metering tank 3 through the delivery pipeline of the feed pump 2, the electromagnetic valve 7 and the material preparation port 31; the sulfur dioxide outlet 34 of the metering tank 3 is provided with a regulating valve 8 The pipeline and the sulfur dioxide feed port 41 are connected with the enamel reactor 4. The input end of the smart meter 5 with program segments is connected to the liquid level differential pressure transmitter 6 on the high-level metering tank 3 , and the output end is connected to the solenoid valve 7 and the regulating valve 8 respectively.

本实用新型所述计量槽3的恒压平衡管接口32与恒压平衡管9相连。The constant pressure balance pipe interface 32 of the metering tank 3 of the utility model is connected with the constant pressure balance pipe 9 .

本实用新型的备料系统包括二氧化硫储罐1、进料泵2、高位计量槽3、带程序段的智能仪表5、液位压差变送器6和电磁阀7,其中液位压差变送器6、电磁阀7和进料泵2的启闭信号与智能仪表5相连。备料时,压差变送器6检测计量槽3中二氧化硫的液位信号,液位达到给定值时智能仪表5给出信号实现进料泵2和电磁阀7的启闭。The material preparation system of the utility model includes a sulfur dioxide storage tank 1, a feed pump 2, a high-level metering tank 3, an intelligent instrument 5 with a program segment, a liquid level differential pressure transmitter 6 and an electromagnetic valve 7, wherein the liquid level differential pressure transmitter The opening and closing signals of the device 6, the solenoid valve 7 and the feed pump 2 are connected with the smart meter 5. When preparing materials, the differential pressure transmitter 6 detects the liquid level signal of sulfur dioxide in the metering tank 3, and when the liquid level reaches a given value, the intelligent instrument 5 gives a signal to realize the opening and closing of the feed pump 2 and the solenoid valve 7.

本实用新型的程序自动进料系统包括高位计量槽3、搪瓷反应釜4、智能仪表5、液位压差变送器6、自动调节阀8,其中程序控制部分由液位压差变送器6、智能仪表5和自动调节阀8依次相连构成。程序加料时,高位计量槽3的液位信号通过液位压差变送器6检测二氧化硫计量槽3的液位信号,利用二氧化硫液位的压差信号与加料量之间的对应关系,通过设定智能仪表5各程序段的给定值来调节调节阀8的开度,实现通过二氧化硫液位信号来控制二氧化硫加料量的工艺操作。The program automatic feeding system of the utility model includes a high-level metering tank 3, an enamel reaction kettle 4, an intelligent instrument 5, a liquid level differential pressure transmitter 6, and an automatic regulating valve 8, wherein the program control part is controlled by the liquid level differential pressure transmitter 6. The smart instrument 5 and the automatic regulating valve 8 are connected in sequence to form. When the program feeds, the liquid level signal of the high-level metering tank 3 is detected by the liquid level differential pressure transmitter 6. The opening of the regulating valve 8 is adjusted by setting the given value of each program segment of the intelligent instrument 5, and the technological operation of controlling the amount of sulfur dioxide feeding is realized through the sulfur dioxide liquid level signal.

Claims (4)

1.一种液体二氧化硫自动加料系统,其特征在于该系统由二氧化硫储罐(1)、进料泵(2)、高位计量槽(3)、搪瓷反应釜(4)、带程序段智能仪表(5)、液位压差变送器(6)、电磁阀(7)、调节阀(8)和恒压平衡管(9)组成,所述高位计量槽(3)通过进料泵(2)和具有电磁阀(7)的管线与二氧化硫储罐(1)相连,其底部出料口(34)通过设有调节阀(8)的管线与搪瓷反应釜(4)相连,所述带程序段智能仪表(5)的输入端与高位计量槽(3)上的液位压差变送器(6)相连,输出端分别与电磁阀(7)和调节阀(8)相连。1. An automatic liquid sulfur dioxide feeding system, characterized in that the system consists of a sulfur dioxide storage tank (1), a feed pump (2), a high-level metering tank (3), an enamel reaction kettle (4), and an intelligent instrument with a program ( 5), liquid level differential pressure transmitter (6), solenoid valve (7), regulating valve (8) and constant pressure balance pipe (9), the high-level metering tank (3) passes through the feed pump (2) It is connected with the sulfur dioxide storage tank (1) through the pipeline with the solenoid valve (7), and its bottom outlet (34) is connected with the enamel reaction kettle (4) through the pipeline with the regulating valve (8). The input end of the smart instrument (5) is connected to the liquid level differential pressure transmitter (6) on the high-level metering tank (3), and the output end is respectively connected to the solenoid valve (7) and the regulating valve (8). 2.根据权利要求1所述的系统,其特征在于计量槽(3)的恒压平衡管接口(32)与恒压平衡管(9)相连。2. The system according to claim 1, characterized in that the constant pressure balance pipe interface (32) of the metering tank (3) is connected to the constant pressure balance pipe (9). 3.根据权利要求1所述的系统,其特征在于二氧化硫备料时,进料泵(2)和电磁阀(7)的启闭由高位计量槽(3)中二氧化硫的液位信号来控制。3. The system according to claim 1, characterized in that when the sulfur dioxide is being prepared, the opening and closing of the feed pump (2) and the solenoid valve (7) are controlled by the liquid level signal of the sulfur dioxide in the high-level metering tank (3). 4.根据权利要求1所述的系统,其特征在于程序加料时,通过二氧化硫高位计量槽(3)的液位压差信号控制调节阀(8)开度来实现液体加料。4. The system according to claim 1, characterized in that during program feeding, liquid feeding is realized by controlling the opening of the regulating valve (8) through the liquid level pressure difference signal of the sulfur dioxide high-level metering tank (3).
CN201620711943.XU 2016-07-08 2016-07-08 A kind of sulfur dioxide liquid automatic feeding system Expired - Fee Related CN206045978U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111921267A (en) * 2020-07-23 2020-11-13 华友新能源科技(衢州)有限公司 A kind of method for stably separating mother liquor in precursor synthesis
CN113464846A (en) * 2021-07-02 2021-10-01 金川集团股份有限公司 Method for adding liquid sulfur dioxide in copper-cobalt wet leaching process

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111921267A (en) * 2020-07-23 2020-11-13 华友新能源科技(衢州)有限公司 A kind of method for stably separating mother liquor in precursor synthesis
CN113464846A (en) * 2021-07-02 2021-10-01 金川集团股份有限公司 Method for adding liquid sulfur dioxide in copper-cobalt wet leaching process

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