CN205413054U - Cationic resin separation recovery system - Google Patents

Cationic resin separation recovery system Download PDF

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Publication number
CN205413054U
CN205413054U CN201521084365.3U CN201521084365U CN205413054U CN 205413054 U CN205413054 U CN 205413054U CN 201521084365 U CN201521084365 U CN 201521084365U CN 205413054 U CN205413054 U CN 205413054U
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resin
water washing
washing tower
reactor
waste
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鲁长海
陈相言
卢庆平
白银慧
赵爱华
范炎生
程新生
陈应萍
王磊
鲁贤
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Tangshan Zhonghao Chemical Co ltd
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Abstract

本实用新型涉及化工设备领域,具体涉及一种阳离子树脂分离回收系统。包括用于将好的树脂和破损的树脂清洗分离开的水洗塔、用于将好的树脂输送到树脂反应器的输送加压罐、将破损的树脂进行固液分离的废树脂过滤器以及连接各容器的管道和阀门,所述水洗塔上开设有溢流口,所述溢流口通过管道与所述废树脂过滤器连接,所述输送加压罐的入料口通过管道与所述水洗塔底部的排料口连接。本实用新型结构简单,通过水洗的方式将破损的树脂和完整的树脂分离开,将好的树脂重新放入树脂反应器内,避免的树脂的浪费,水洗后的树脂通过加压后送入树脂反应器,整个过程不用中断,提高了反应效率,节约了能源,减少了人工操作难度,降低了工人的工作强度。

The utility model relates to the field of chemical equipment, in particular to a cationic resin separation and recovery system. Including water washing tower for cleaning and separating good resin and damaged resin, transfer pressurized tank for transferring good resin to resin reactor, waste resin filter for solid-liquid separation of damaged resin and connection The pipelines and valves of each container, the water washing tower is provided with an overflow port, the overflow port is connected with the waste resin filter through a pipeline, and the feed port of the conveying pressurized tank is connected with the water washing tower through a pipeline. The discharge port connection at the bottom of the tower. The utility model has a simple structure. The damaged resin is separated from the complete resin by washing, and the good resin is put back into the resin reactor to avoid waste of the resin. The washed resin is sent into the resin after pressurization. Reactor, the whole process does not need to be interrupted, which improves the reaction efficiency, saves energy, reduces the difficulty of manual operation, and reduces the work intensity of workers.

Description

一种阳离子树脂分离回收系统A cationic resin separation and recovery system

技术领域 technical field

本实用新型涉及一种阳离子树脂分离回收系统。 The utility model relates to a cationic resin separation and recovery system.

背景技术 Background technique

目前,固定床阳离子树脂反应器在工业生产中普遍存在,主要通过离子交换形式用于回收工业尾料(液)中的贵重离子或有毒有害离子(简称目标离子)。树脂通过吸附物料中的高浓度目标离子,用其他物料进行置换后用再生液进行脱附和树脂再生,达到循环使用的目的。相对于其他树脂反应器,固定床具有操作简单、投资和维护成本低的优点,这也是目前很多行业和厂家选择固定床的原因。固定床内树脂经过长时间运行后,部分树脂出现磨损而粉碎,影响了树脂的整体使用性能,通常处理方法是将反应器内的树脂全部排出,重新投入新的树脂。因为使用后的树脂无法实现分离出优劣,造成部分完好的树脂浪费,同时需定时停止装置进行批量更换,人工劳动量大。 At present, fixed-bed cationic resin reactors are widely used in industrial production, and are mainly used to recover precious ions or toxic and harmful ions (referred to as target ions) in industrial tailings (liquid) through ion exchange. The resin absorbs the high-concentration target ions in the material, replaces it with other materials, and then uses the regeneration liquid to perform desorption and resin regeneration, so as to achieve the purpose of recycling. Compared with other resin reactors, fixed beds have the advantages of simple operation, low investment and maintenance costs, which is why many industries and manufacturers choose fixed beds. After the resin in the fixed bed has been running for a long time, part of the resin is worn and crushed, which affects the overall performance of the resin. The usual treatment method is to discharge all the resin in the reactor and put in new resin. Because the used resin cannot be separated into good and bad, resulting in the waste of partially intact resin, and at the same time, it is necessary to stop the device regularly for batch replacement, which requires a large amount of manual labor.

实用新型内容 Utility model content

本实用新型所要解决的技术问题是提供一种既能节约树脂又能降低人工劳动强度的阳离子树脂分离回收系统。 The technical problem to be solved by the utility model is to provide a cationic resin separation and recovery system that can save resin and reduce labor intensity.

本实用新型采用如下技术方案: The utility model adopts the following technical solutions:

一种阳离子树脂分离回收系统,包括用于将好的树脂和破损的树脂清洗分离开的水洗塔、用于将好的树脂输送到树脂反应器的输送加压罐、将破损的树脂进行固液分离的废树脂过滤器以及连接各容器的管道和阀门,所述水洗塔上开设有溢流口,所述溢流口通过管道与所述废树脂过滤器连接,所述输送加压罐的入料口通过管道与所述水洗塔底部的排料口连接,所述废树脂过滤器底部开设有排水口。 A cationic resin separation and recovery system, including a water washing tower for cleaning and separating good resin from damaged resin, a delivery pressurized tank for delivering good resin to the resin reactor, and separating damaged resin into solid-liquid The separated waste resin filter and the pipes and valves connecting each container, the water washing tower is provided with an overflow port, the overflow port is connected with the waste resin filter through a pipe, and the inlet of the conveying pressurized tank The feed port is connected to the discharge port at the bottom of the water washing tower through a pipeline, and a drain port is opened at the bottom of the waste resin filter.

作为本实用新型进一步改进,其还包括有用于向树脂反应器送料的树脂添加高位槽,所述树脂添加高位槽的入口通过管道与所述输送加压罐的出口接通,所述树脂添加高位槽的出口通过管道与树脂反应器的加料口接通,且所述树脂添加高位槽安装位置高于树脂反应器的加料口。 As a further improvement of the utility model, it also includes a resin adding high-level tank for feeding materials to the resin reactor, the inlet of the resin adding high-level tank is connected with the outlet of the delivery pressurized tank through a pipeline, and the resin adding high-level tank The outlet of the tank is connected to the feeding port of the resin reactor through a pipeline, and the installation position of the resin adding high-level tank is higher than the feeding port of the resin reactor.

作为本实用新型进一步改进,所述水洗塔和废树脂过滤器之间还安装有树脂沉降罐,所述树脂沉降罐的入口通过管道与水洗塔的溢流口接通,所述树脂沉降罐的出口与废树脂过滤器的入口连接,所述树脂沉降罐上部开设有溢流口。 As a further improvement of the utility model, a resin settling tank is also installed between the water washing tower and the waste resin filter, the inlet of the resin settling tank is connected with the overflow port of the water washing tower through a pipeline, and the resin settling tank The outlet is connected with the inlet of the waste resin filter, and an overflow port is opened on the upper part of the resin settling tank.

本实用新型的积极效果如下: The positive effect of the utility model is as follows:

本实用新型结构简单,通过水洗的方式将破损的树脂和完整的树脂分离开,将好的树脂重新放入树脂反应器内,避免的树脂的浪费,同时将新的树脂添加到水洗塔内,可以将其表面的杂志去除,水洗后的树脂通过加压后送入树脂反应器,整个过程不用中断,提高了反应效率,节约了能源,减少了人工操作难度,降低了工人的工作强度。 The utility model has a simple structure. The damaged resin is separated from the complete resin by washing, and the good resin is put back into the resin reactor to avoid the waste of resin. At the same time, new resin is added to the washing tower. The impurities on the surface can be removed, and the washed resin is sent to the resin reactor after being pressurized. The whole process does not need to be interrupted, which improves the reaction efficiency, saves energy, reduces the difficulty of manual operation, and reduces the work intensity of workers.

附图说明 Description of drawings

附图1为本实用新型结构示意图。 Accompanying drawing 1 is the structural representation of the utility model.

在附图中:1水洗塔、2输送加压罐、3树脂添加高位槽、4树脂沉降罐、5废树脂过滤器、6收集池。 In the attached drawings: 1. Water washing tower, 2. Conveying pressurized tank, 3. Resin adding head tank, 4. Resin settling tank, 5. Waste resin filter, 6. Collection pool.

具体实施方式 detailed description

下面结合附图和具体实施方式对本实用新型作进一步详细的描述。 The utility model will be further described in detail below in conjunction with the accompanying drawings and specific embodiments.

如附图1所示的一种阳离子树脂分离回收系统,包括用于将好的树脂和破损的树脂清洗分离开的水洗塔1,用于将好的树脂输送到树脂反应器的输送加压罐2,用于向树脂反应器送料的树脂添加高位槽3,将破损的树脂进行固液分离的废树脂过滤器5,安装在所述水洗塔1和废树脂过滤器5之间的树脂沉降罐4以及连接各容器的管道和阀门,树脂在树脂反应器内反应一段时间后,将树脂排放一部分到水洗塔1内,树脂经过水洗塔后,破碎的树脂在水洗塔内水的作用下漂浮在水的表面,然后通过所述水洗塔1上开设的溢流口流出,好树脂在重力的作用下沉到水洗塔1的底部,所述输送加压罐2的入料口通过管道与所述水洗塔1底部的排料口连接,好的树脂就直接排到输送加压罐2内加压后到达树脂添加高位槽3。 A kind of cationic resin separation and recovery system as shown in accompanying drawing 1, comprises the water washing tower 1 that is used to clean and separate good resin and damaged resin, is used to deliver good resin to the delivery pressurized tank of resin reactor 2. A high level tank 3 for adding resin to the resin reactor, a waste resin filter 5 for solid-liquid separation of damaged resin, and a resin settling tank installed between the water washing tower 1 and the waste resin filter 5 4 and the pipes and valves connecting each container. After the resin reacts in the resin reactor for a period of time, part of the resin is discharged into the water washing tower 1. After the resin passes through the water washing tower, the broken resin floats in the water under the action of water in the water washing tower. The surface of the water flows out through the overflow port offered on the water washing tower 1, and the good resin sinks to the bottom of the water washing tower 1 under the action of gravity, and the feed inlet of the delivery pressurized tank 2 passes through the pipeline and the The discharge port at the bottom of the water washing tower 1 is connected, and the good resin is directly discharged into the conveying pressurized tank 2 and then pressurized to reach the resin adding head tank 3.

所述树脂添加高位槽3的入口通过管道与所述输送加压罐2的出口接通,所述树脂添加高位槽3的出口通过管道与树脂反应器的加料口接通,且所述树脂添加高位槽3安装位置高于树脂反应器的加料口,在树脂反应器内的树脂量少的时候,打开树脂添加高位槽3下游的阀门将树脂添加到树脂反应器内参加反应。 The inlet of the resin adding head tank 3 is connected with the outlet of the conveying pressurized tank 2 through a pipeline, the outlet of the resin adding head tank 3 is connected with the feeding port of the resin reactor through a pipeline, and the resin adding The installation position of the head tank 3 is higher than the feeding port of the resin reactor. When the amount of resin in the resin reactor is small, open the valve downstream of the resin addition head tank 3 to add resin to the resin reactor to participate in the reaction.

所述树脂沉降罐4的入口通过管道与水洗塔1的溢流口接通,水洗塔1内漂浮的破碎的树脂随着水进入到树脂沉降罐4内,树脂在这里经过时间沉淀后,破碎的树脂沉淀到底部,沉淀后的水通过其顶部的溢流口流出树脂沉降罐4,然后通过管道通入到水洗塔1内,所述树脂沉降罐4的出口与废树脂过滤器5的入口连接,在沉淀一段时间后打开所述树脂沉降罐4的出口的阀门,沉淀后的树脂通过管道达到废树脂过滤器5。 The inlet of the resin settling tank 4 is connected with the overflow port of the water washing tower 1 through a pipeline, and the broken resin floating in the water washing tower 1 enters in the resin settling tank 4 along with the water, and the resin is broken after settling over time here. The resin of the resin settles to the bottom, and the water after the precipitation flows out of the resin settling tank 4 through the overflow port at the top, and then passes into the water washing tower 1 through the pipeline, and the outlet of the resin settling tank 4 and the inlet of the waste resin filter 5 Connect, open the valve of the outlet of the resin settling tank 4 after settling for a period of time, and the resin after settling reaches the waste resin filter 5 through the pipeline.

沉淀后的树脂在所述废树脂过滤器5内经过过滤将树脂和水彻底分离开,所述废树脂过滤器5底部开设有排水口,水通过排水口排到收集池内,然后送去处理,过滤出来的树脂收集到一起后统一处理。 The precipitated resin is filtered in the waste resin filter 5 to completely separate the resin and water, and the bottom of the waste resin filter 5 is provided with a drain, and the water is discharged into the collection tank through the drain, and then sent for processing. The filtered resins are collected together and processed uniformly.

Claims (3)

1.一种阳离子树脂分离回收系统,其特征在于:包括用于将好的树脂和破损的树脂清洗分离开的水洗塔(1)、用于将好的树脂输送到树脂反应器的输送加压罐(2)、将破损的树脂进行固液分离的废树脂过滤器(5)以及连接各容器的管道和阀门,所述水洗塔(1)上开设有溢流口,所述溢流口通过管道与所述废树脂过滤器(5)连接,所述输送加压罐(2)的入料口通过管道与所述水洗塔(1)底部的排料口连接,所述废树脂过滤器(5)底部开设有排水口。 1. A cationic resin separation and recovery system, characterized in that: it includes a water washing tower (1) for cleaning and separating good resin and damaged resin, and a delivery pressurization unit for delivering good resin to the resin reactor. tank (2), a waste resin filter (5) for solid-liquid separation of the damaged resin, and pipes and valves connecting each container, and an overflow port is opened on the water washing tower (1), and the overflow port passes through The pipeline is connected to the waste resin filter (5), the feed port of the conveying pressurized tank (2) is connected to the discharge port at the bottom of the water washing tower (1) through a pipeline, and the waste resin filter ( 5) There is a drainage port at the bottom. 2.根据权利要求1所述的一种阳离子树脂分离回收系统,其特征在于:其还包括有用于向树脂反应器送料的树脂添加高位槽(3),所述树脂添加高位槽(3)的入口通过管道与所述输送加压罐(2)的出口接通,所述树脂添加高位槽(3)的出口通过管道与树脂反应器的加料口接通,且所述树脂添加高位槽(3)安装位置高于树脂反应器的加料口。 2. A cationic resin separation and recovery system according to claim 1, characterized in that: it also includes a resin adding head tank (3) for feeding to the resin reactor, and the resin adding head tank (3) The inlet is connected to the outlet of the conveying pressurized tank (2) through a pipeline, the outlet of the resin adding head tank (3) is connected to the feeding port of the resin reactor through a pipe, and the resin adding head tank (3) ) The installation position is higher than the feeding port of the resin reactor. 3.根据权利要求1或2所述的一种阳离子树脂分离回收系统,其特征在于:所述水洗塔(1)和废树脂过滤器(5)之间还安装有树脂沉降罐(4),所述树脂沉降罐(4)的入口通过管道与水洗塔(1)的溢流口接通,所述树脂沉降罐(4)的出口与废树脂过滤器(5)的入口连接,所述树脂沉降罐(4)上部开设有溢流口。 3. A cationic resin separation and recovery system according to claim 1 or 2, characterized in that: a resin settling tank (4) is also installed between the water washing tower (1) and the waste resin filter (5), The inlet of the resin settling tank (4) is connected to the overflow port of the water washing tower (1) through a pipeline, the outlet of the resin settling tank (4) is connected to the inlet of the waste resin filter (5), and the resin The upper part of the settling tank (4) is provided with an overflow port.
CN201521084365.3U 2015-12-23 2015-12-23 Cationic resin separation recovery system Expired - Lifetime CN205413054U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107694613A (en) * 2017-11-29 2018-02-16 洛阳市天誉环保工程有限公司 The technique and device of phenol impurity in a kind of removal doctor solution
CN111841666A (en) * 2020-07-14 2020-10-30 江苏核电有限公司 Movable resin bed external flushing device and flushing method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107694613A (en) * 2017-11-29 2018-02-16 洛阳市天誉环保工程有限公司 The technique and device of phenol impurity in a kind of removal doctor solution
CN111841666A (en) * 2020-07-14 2020-10-30 江苏核电有限公司 Movable resin bed external flushing device and flushing method thereof

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Denomination of utility model: A cation resin separation and recovery system

Effective date of registration: 20201026

Granted publication date: 20160803

Pledgee: Bank of Cangzhou Limited by Share Ltd. Tangshan branch

Pledgor: TANGSHAN ZHONGHAO CHEMICAL Co.,Ltd.

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