CN204964324U - Microwave buoyancy method spot test device - Google Patents
Microwave buoyancy method spot test device Download PDFInfo
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- CN204964324U CN204964324U CN201520785771.6U CN201520785771U CN204964324U CN 204964324 U CN204964324 U CN 204964324U CN 201520785771 U CN201520785771 U CN 201520785771U CN 204964324 U CN204964324 U CN 204964324U
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Abstract
Description
技术领域technical field
本实用新型涉及谷物水分测定领域,具体涉及一种微波浮力法快速测定装置。The utility model relates to the field of grain moisture measurement, in particular to a microwave buoyancy method rapid measurement device.
背景技术Background technique
水分含量是谷物质量标准中一项重要的限制性项目,对谷物的加工、储藏、运输和销售都有重要的影响。确定一种快速、准确、便捷地粮食水分测定方法具有重大意义。虽然现在测定粮食水分的方法很多,但是都存在诸多不足,例如:我国国家标准方法(烘干法),虽然检测精度很高,但是费时、耗能大、效率低,不能实现快速在线检测;电容法虽然具有结构简单、成本低、检测速度快等优点,但测量精度低,易受干扰;电阻法不适合高水分、大颗粒粮食的测定;红外线加热法虽然测量快,但是容易造成干物质损失,精度低,近红外法虽然速度快,但是样品的品种、大小、密度、环境温度、震动等对测量结果均有影响,稳定性差、适用面小;其他方法如微波和无线电法、核磁共振法、中子法、声学法等等,均由于成本高,条件要求高等诸多因素无法广泛使用。在谷物水分含量测测定领域,我国在测试方法和基础理论研究方面相比其他科技比较发达的国家还显得比较薄弱。Moisture content is an important restrictive item in grain quality standards, which has an important impact on grain processing, storage, transportation and sales. It is of great significance to determine a fast, accurate and convenient method for grain moisture determination. Although there are many methods for measuring grain moisture, there are many deficiencies, for example: my country's national standard method (drying method), although the detection accuracy is very high, it is time-consuming, energy-consuming, and inefficient, and cannot achieve fast online detection; Although the method has the advantages of simple structure, low cost, and fast detection speed, it has low measurement accuracy and is susceptible to interference; the resistance method is not suitable for the determination of high-moisture and large-grain grains; although the infrared heating method is fast in measurement, it is easy to cause dry matter loss. , low precision, although the near-infrared method is fast, but the variety, size, density, ambient temperature, vibration, etc. of the sample will affect the measurement results, the stability is poor, and the applicable area is small; other methods such as microwave and radio method, nuclear magnetic resonance method , neutron method, acoustic method, etc., are all unable to be widely used due to many factors such as high cost and high condition requirements. In the field of grain moisture content measurement, our country is still relatively weak in terms of testing methods and basic theoretical research compared with other countries with relatively developed science and technology.
在先申请“浮力法谷物水分快速测定方法及其测定仪”专利号为:CN200810050625.3,公开了利用浮力法对谷物水分的快速检测,该专利在一定程度上实现了操作简便、快速、测定数据准确等目的,但是由于测定过程中需要样品粉碎、注水打压等工序,操作不方便,同时在测量的过程中不稳定,自动化水平低,需要人工做操的较繁琐,并且,在背景文件中,该装置体型较大,在移动、运输也存在不便捷的问题。The patent number of the "rapid determination of grain moisture by buoyancy method and its measuring instrument" was first applied for: CN200810050625.3, which discloses the rapid detection of grain moisture by using the buoyancy method. Data accuracy and other purposes, but due to the need for sample crushing, water injection and pressure during the measurement process, the operation is inconvenient, and at the same time, the measurement process is unstable, the automation level is low, and manual operations are more cumbersome, and, in the background file , the device is relatively large in size, and there are inconvenient problems in moving and transporting.
实用新型内容Utility model content
本实用新型设计开发了一种微波浮力法快速测定装置,目的就是根据“阿基米德浮力定律”原理,提供一种测试数据的波动性小,测试结果准确稳定测试装置。The utility model designs and develops a microwave buoyancy method rapid measuring device, the purpose of which is to provide a test device with small fluctuation of test data and accurate and stable test results according to the principle of "Archimedes' buoyancy law".
本实用新型另一个实用新型目的是,使称量测试能够在同一装置中一体化完成,并且装置设计结构紧凑,移动方便,自动化程度高。Another purpose of the utility model is to enable the weighing test to be integrated in the same device, and the design of the device is compact, easy to move, and highly automated.
同时,本实用新型还具有另一个实用新型目的是在测试之前通过微波的作用能够使样品充分润湿,增加了样品在水中进行浮力测试时的柔顺性、稳定性及准确性,同时,微波操作简单、灵活、便捷,无需人工繁琐操作即可达到目的。At the same time, the utility model also has another utility model purpose, which is to fully wet the sample through the action of microwaves before the test, which increases the flexibility, stability and accuracy of the buoyancy test of the sample in water. At the same time, microwave operation Simple, flexible and convenient, the goal can be achieved without manual cumbersome operations.
本实用新型提供的技术方案为:The technical scheme provided by the utility model is:
一种微波浮力法快速测定装置,包括:A microwave buoyancy method rapid determination device, comprising:
样品杯容器,其杯身均匀分布小孔;所述样品杯容器为不锈钢材质;The sample cup container has small holes evenly distributed on the cup body; the sample cup container is made of stainless steel;
电子称,其包括用于测量重量的刚性细线,所述刚性细线悬挂所述样品杯容器;an electronic scale comprising a rigid thin wire for measuring weight, the rigid thin wire suspending the sample cup container;
水箱,其为上端开口的容器,设置在所述样品杯容器下方;A water tank, which is a container with an open upper end, is arranged below the sample cup container;
升降台,其设置在所述水箱下方,驱动所述水箱升降;Lifting platform, which is arranged under the water tank and drives the water tank to go up and down;
其中,当所述升降台升至最高处时,驱动所述水箱能够将所述样品杯容器完全浸入水中测试数据;当所述升降台下降至最低处时,驱动所述水箱下降至能够使所述样品杯容器完全脱离所述水箱。Wherein, when the lifting table rises to the highest point, driving the water tank can completely immerse the sample cup container in water to test data; The sample cup container was completely disengaged from the water tank.
优选的是,还包括:Preferably, it also includes:
支架,其包括电子称托盘、弧形支撑架及底座;其中,所述电子称托盘用于放置所述电子称,其中心处设置为开孔结构,所述底座用于放置所述电升降台,所述弧形支撑架上端连接所述电子秤托盘后边缘,下端连接所述底座前边缘,所述弧形支撑架上部分为中空结构,其能够用于将所述升降台驱动所述水箱升降时从中空结构中穿过;所述电子秤托盘、所述弧形支撑架及所述底座焊接成为一体。The bracket includes an electronic scale tray, an arc-shaped support frame and a base; wherein, the electronic scale tray is used to place the electronic scale, and its center is provided with a hole structure, and the base is used to place the electric lifting platform , the upper end of the arc-shaped support frame is connected to the rear edge of the electronic scale tray, and the lower end is connected to the front edge of the base. The upper part of the arc-shaped support frame is a hollow structure, which can be used to drive the lifting platform to the water tank Pass through the hollow structure when lifting; the electronic scale tray, the arc-shaped support frame and the base are welded into one.
优选的是,还包括:外壳,其焊接固定在所述底座上,且穿过所述弧形支撑架,所述升降台置于所述外壳内部。Preferably, it also includes: an outer shell, which is welded and fixed on the base, and passes through the arc-shaped support frame, and the lifting platform is placed inside the outer shell.
优选的是,所述水箱及所述升降台之间设置水箱稳定装置,其用于在水箱升降过程中稳定水箱。Preferably, a water tank stabilizing device is provided between the water tank and the lifting platform, which is used to stabilize the water tank during the lifting process of the water tank.
优选的是,所述升降台还包括用于限定升降高度的上限位器及下限位器。Preferably, the lifting platform further includes an upper limiter and a lower limiter for limiting the lifting height.
优选的是,所述刚性细线系有挂钩,所述挂钩能够穿过所述电子秤托盘的开孔结构用于悬挂所述样品杯容器。Preferably, the rigid thin wire is tied with a hook, and the hook can pass through the opening structure of the electronic scale tray for hanging the sample cup container.
优选的是,所述水箱内部贯穿设置竖直分隔板,其上边缘与所述水箱上边缘齐平,所述分隔板与所述水箱侧壁分割出所述水箱1/4体积,所述分隔板距离上边缘处开设溢水孔。Preferably, a vertical partition plate is provided through the interior of the water tank, the upper edge of which is flush with the upper edge of the water tank, and the partition plate and the side wall of the water tank divide 1/4 of the volume of the water tank, so An overflow hole is provided at the distance from the upper edge of the dividing plate.
优选的是,所述样品杯容器包括杯体、杯盖和提梁;所述杯体、所述杯盖及杯底均匀分布小孔,所述杯盖可拆卸的连接所述杯体,所述杯盖侧面上端设置有提梁,提梁中部设置有凹槽,其用于与所述挂钩配合悬挂所述样品杯容器。Preferably, the sample cup container includes a cup body, a cup cover and a handle; small holes are evenly distributed on the cup body, the cup cover and the bottom of the cup, the cup cover is detachably connected to the cup body, the A handle is provided on the upper end of the side of the cup cover, and a groove is provided in the middle of the handle, which is used to cooperate with the hook to hang the sample cup container.
本实用新型所述的有益效果:Beneficial effects described in the utility model:
1、通过本实用新型提供的测试装置,克服了传统“烘干法”操作时间长,指导不及时和其他快速水分测定仪误差偏大的缺点,能够方便、快速、准确、环保的对样品中含水量进行测试,对样品无需进行粉碎,注水打压等繁琐操作,同时采用电动升降平台,增加浮力测量的稳定性和测量过程的自动化水平;1. Through the test device provided by the utility model, it overcomes the shortcomings of the traditional "drying method" such as long operation time, untimely guidance and large error of other rapid moisture analyzers, and can conveniently, quickly, accurately and environmentally friendly test the moisture in the sample. The water content is tested, and the sample does not need to be pulverized, water injection and pressure and other cumbersome operations. At the same time, the electric lifting platform is used to increase the stability of the buoyancy measurement and the automation level of the measurement process;
2、在样品称量后,进行在水中测试之前,进行微波操作,使样品得到充分的润湿之后再将样品装入样品杯中,使其能够更柔顺的进入水中,使测量更稳定准确;2. After the sample is weighed and before the test in water, perform microwave operation to make the sample fully wet and then put the sample into the sample cup so that it can enter the water more smoothly and make the measurement more stable and accurate;
3、本实用新型的设备采用一体化支架设计,使称量测试能够在同一装置中一体化完成,装置设计结构紧凑,移动方便,自动化程度高,并且方便移动及运输,外壳焊接在一体化支架上,升降台及水箱设置在外壳内部安装并且穿过支架主体的设计,使测试结果受外界环境影响小,测试稳定。3. The equipment of this utility model adopts an integrated bracket design, so that the weighing test can be integrated in the same device. The design of the device is compact, easy to move, high in automation, and convenient to move and transport. The shell is welded on the integrated bracket In addition, the lifting platform and water tank are installed inside the shell and pass through the design of the main body of the bracket, so that the test results are less affected by the external environment and the test is stable.
附图说明Description of drawings
图1为本实用新型所述的微波浮力法谷物水分快速测定装置剖视图;Fig. 1 is the cross-sectional view of the microwave buoyancy method grain moisture fast measuring device described in the utility model;
图2为本实用新型所述的微波浮力法谷物水分快速测定装置主视图;Fig. 2 is the front view of the microwave buoyancy method grain moisture fast measuring device described in the utility model;
图3为本实用新型所述的微波浮力法谷物水分快速测定装置左视图;Fig. 3 is the left view of the microwave buoyancy method grain moisture fast measuring device described in the utility model;
图4为本实用新型所述的微波浮力法谷物水分快速测定装置俯视图;Fig. 4 is the top view of the microwave buoyancy method grain moisture fast measuring device described in the utility model;
图5为本实用新型所述的微波浮力法谷物水分快速测定装置立体图;Fig. 5 is a three-dimensional view of the microwave buoyancy method grain moisture fast measuring device described in the utility model;
图6为本实用新型所述的样品杯;Fig. 6 is the sample cup described in the utility model;
图7为本实用新型所述的水箱;Fig. 7 is the water tank described in the utility model;
图8为本实用新型所述的支架立体图;Fig. 8 is a three-dimensional view of the bracket described in the utility model;
具体实施方式detailed description
下面结合附图对本实用新型做进一步的详细说明,以令本领域技术人员参照说明书文字能够据以实施。The utility model will be described in further detail below in conjunction with the accompanying drawings, so that those skilled in the art can implement it by referring to the description.
如图1、图5、图6所示,本实用新型提供一种微波浮力法快速测定装置,其主体包括电子称100、水箱200及电动升降台300;其中,在电子称100的正下方通过“S”型挂钩110悬挂均匀分布小孔的不锈钢样品杯容器500,样品杯容器500为圆柱体,在电子称100下称的秤钩上系上刚性细线,在细线的另一端系上“S”型挂钩110;水箱200为上端开口的容器,设置在样品杯容器500的下方,并且放置在电动升降台300上,当样品杯容器500挂在电子称100下称的秤钩的“S”型挂钩110上时,电动升降台300能够托着水箱200升至最高处,将样品杯容器500全部浸入水中,从而测定样品杯容器的皮重、毛重,进而计算被测样品水分值,当电动升降台300下降至最低处时,驱动水箱200下降至能够使样品杯容器500完全脱离水箱200的位置。As shown in Figure 1, Figure 5, and Figure 6, the utility model provides a microwave buoyancy method rapid measurement device, the main body of which includes an electronic scale 100, a water tank 200 and an electric lifting platform 300; The "S" type hook 110 hangs the stainless steel sample cup container 500 with small holes evenly distributed. "S" type hook 110; the water tank 200 is a container with an open upper end, which is arranged below the sample cup container 500 and placed on the electric lifting platform 300, when the sample cup container 500 is hung on the " When the S”-shaped hook 110 is on, the electric lifting platform 300 can lift the water tank 200 to the highest point, and immerse the sample cup container 500 in water, so as to measure the tare weight and gross weight of the sample cup container, and then calculate the moisture value of the sample to be tested , when the electric lifting platform 300 descends to the lowest point, the water tank 200 is driven down to a position where the sample cup container 500 can be completely separated from the water tank 200 .
在另一种实施例中,如图1、图5、图8所示,还包括:能够将电子称100、水箱200及自动升降台300整体放置的支架400,其整体为一体化设计,其中,支架400包括电子称托盘410、底座420及弧形支撑架430,在电子称托盘410上放置电子称100,在电子秤托盘的中心处开设有直径10cm的孔,“S”型挂钩110能够从这个孔中穿过来悬挂样品杯容器500,在底座420上放置电动升降台300,弧形支撑架430的上端焊接在电子秤托盘410的后边缘,弧形支撑架430的下端焊接在底座420的前边缘,同时,弧形支撑架430上部为中空结构,当电动升降台300驱动水箱200升降时,能够从该中空结构中穿过;并且,这种方式只是一种较佳实例的说明,但并不局限于此,作为一种优选,电子秤托盘410及弧形支撑架430还能够通过螺接的方式连接,弧形支撑架430及底座420同样通过螺接的方式连接,从而使电子秤托盘410、底座420及弧形支撑架430可拆卸,方便更换清洗。In another embodiment, as shown in Fig. 1, Fig. 5 and Fig. 8, it also includes: a support 400 capable of placing the electronic scale 100, the water tank 200 and the automatic lifting platform 300 as a whole, and the whole is an integrated design, wherein , the bracket 400 includes an electronic scale tray 410, a base 420 and an arc support frame 430, an electronic scale 100 is placed on the electronic scale tray 410, and a hole with a diameter of 10 cm is opened at the center of the electronic scale tray, and the "S" type hook 110 can Pass through this hole to hang the sample cup container 500, place the electric lifting platform 300 on the base 420, the upper end of the arc support frame 430 is welded on the rear edge of the electronic scale tray 410, and the lower end of the arc support frame 430 is welded on the base 420 At the same time, the upper part of the arc-shaped support frame 430 is a hollow structure, and when the electric lifting platform 300 drives the water tank 200 to go up and down, it can pass through the hollow structure; and this method is only a description of a better example, But it is not limited thereto. As a preference, the electronic scale tray 410 and the arc-shaped support frame 430 can also be connected by a screw connection, and the arc-shaped support frame 430 and the base 420 are also connected by a screw connection, so that the electronic scale The scale tray 410, the base 420 and the arc support frame 430 are detachable for easy replacement and cleaning.
在另一种实施例中,如图1、图5所示,还包括:焊接固定在底座420上的外壳440,其穿过弧形支撑架430;水箱200及电动升降台300置于外壳440内部,使其在测量时,降低外界对测量的干扰,使测量更为稳定准确;并且,这种方式只是一种较佳实例的说明,但并不局限于此,最为一种优选,外壳440还能够通过螺接的方式可拆卸的固定在底座420上,使外壳440方便更换拆卸。In another embodiment, as shown in Fig. 1 and Fig. 5, it also includes: a shell 440 welded and fixed on the base 420, which passes through the arc support frame 430; the water tank 200 and the electric lifting platform 300 are placed in the shell 440 Internally, it reduces external interference to the measurement during measurement, making the measurement more stable and accurate; and, this method is only a description of a better example, but it is not limited thereto. The most preferred case is the housing 440 It can also be detachably fixed on the base 420 by screwing, so that the shell 440 can be easily replaced and disassembled.
在另一种实施例中,如图1所示,水箱200及电动升降台300之间还设置了水箱稳定装置450,水箱稳定装置450用于在水箱升降过程中使水箱200更为平稳的升降;在本实施例中,水箱稳定装置450为表面平整的木板,并且,这种方式只是一种较佳实例的说明,但并不局限于此,作为一种优选,水箱稳定装置450还能够为缓冲泡沫垫,使水箱200在升降过程中更为平稳,水箱200内的水减少晃动。In another embodiment, as shown in FIG. 1 , a water tank stabilizing device 450 is also provided between the water tank 200 and the electric lifting platform 300. The water tank stabilizing device 450 is used to make the water tank 200 more stable in the lifting process. ; In the present embodiment, the water tank stabilizing device 450 is a plank with a flat surface, and this mode is only a description of a preferred example, but is not limited thereto. As a preference, the water tank stabilizing device 450 can also be The buffer foam pad makes the water tank 200 more stable during the lifting process, and the water in the water tank 200 reduces shaking.
在另一种实施例中,如图1所示,电动升降台300还包括用于限定升降高度的上限位器310及下限位器320,电动升降台300内部设有限位开关,升降最高点及最低点分别由上限位器310及下限位器320控制,通过上限位器310及下限位器320的对升降高度的限定,使电动升降台300及水箱200的每次升降的高度固定,增加测试的准确性。In another embodiment, as shown in FIG. 1 , the electric lifting platform 300 also includes an upper limiter 310 and a lower limiter 320 for limiting the lifting height, and a limit switch is arranged inside the electric lifting platform 300. The lowest point is controlled by the upper limiter 310 and the lower limiter 320 respectively. Through the limitation of the lifting height of the upper limiter 310 and the lower limiter 320, the height of each lifting of the electric lifting platform 300 and the water tank 200 is fixed, and the test is increased. accuracy.
在另一种实施例中,如图7所示,在水箱200的体积1/4处内部贯穿焊接与水箱200等高的竖直分隔板441,其上边缘与所述水箱上边缘齐平,分隔板441与水箱200侧壁分割出所述水箱1/4体积,在分隔板441距离上边缘2厘米处开设溢水孔,通过开设溢水孔以保持试验过程中水的液面总是位于溢水孔处,提高试验的准确度;在本实施例中,开设小孔的数量为1个,作为一种优选,可以根据实施者的需求,开设不同数量的小孔,使其高度平齐即可。In another embodiment, as shown in FIG. 7 , a vertical partition plate 441 equal in height to the water tank 200 is penetrated and welded inside the volume 1/4 of the water tank 200 , and its upper edge is flush with the upper edge of the water tank. The partition plate 441 and the side wall of the water tank 200 are divided into 1/4 of the volume of the water tank, and an overflow hole is opened at a distance of 2 cm from the upper edge of the partition plate 441, and the liquid level of the water in the test process is always maintained by opening the overflow hole. Located at the overflow hole to improve the accuracy of the test; in this embodiment, the number of small holes is 1, as a preference, different numbers of small holes can be opened according to the needs of the implementer, so that the height is even That's it.
在另一种实施例中,如图6所示,样品杯容器500包括杯体510、杯盖520及提梁530;杯体510、杯盖520及杯底均匀分布小孔,杯体510及杯盖520通过螺纹连接,杯盖520侧面上端设置有提梁530,在提梁530中部设置有凹槽,通过凹槽与“S”型挂钩110配合提拉样品杯容器500,通过凹槽的设置使“S”型挂钩110每次挂住样品杯容器500的提梁530时均在同一位置。In another embodiment, as shown in Figure 6, the sample cup container 500 includes a cup body 510, a cup cover 520 and a handle 530; The cover 520 is connected by threads, and the upper end of the side of the cup cover 520 is provided with a lifting beam 530, and a groove is arranged in the middle of the lifting beam 530, and the sample cup container 500 is lifted through the groove and the "S"-shaped hook 110, and the " The S"-shaped hook 110 is at the same position every time it hangs on the handle 530 of the sample cup container 500.
如图1所示,通过使用本实用新型提供的微波浮力法快速测定装置进行测试,包括如下操作步骤:As shown in Figure 1, by using the microwave buoyancy method quick measuring device provided by the utility model to test, comprising the following steps:
步骤一:样品重称量:用称样器皿称取样品99.00~99.10克,记录样品重;Step 1: Sample weighing: Weigh 99.00-99.10 grams of sample with a weighing vessel, and record the sample weight;
步骤二:微波处理:将样品倒入干净的容器中,加入定量的水,水的体积大约是样品体积的2倍,盖上容器盖,容器盖上有孔,利于水蒸汽逸出,将容器放入微波炉中,高火加热10分钟,取出样品;Step 2: Microwave treatment: Pour the sample into a clean container, add a certain amount of water, the volume of the water is about twice the volume of the sample, cover the container cover, there are holes in the container cover, which is conducive to the escape of water vapor, and the container Put it in a microwave oven, heat it on high heat for 10 minutes, and take out the sample;
步骤三:样品杯皮重称量:将电动升降台300升至最高处时,电子称100清“0”;然后将电动升降台300降至最低处,将样品杯容器500挂在电子称100下秤钩的“S”型挂钩110上,而后将电动升降台300升至最高处,此时样品杯容器500全部浸入水中,待天平数据稳定后,记录皮重数据;Step 3: Sample cup tare weighing: When the electric lifting platform 300 is raised to the highest point, the electronic scale 100 clears "0"; then the electric lifting platform 300 is lowered to the lowest point, and the sample cup container 500 is hung on the electronic scale 100 Lower the "S" hook 110 of the weighing hook, and then raise the electric lifting platform 300 to the highest point. At this time, the sample cup container 500 is completely immersed in water. After the balance data is stable, record the tare weight data;
步骤四:微波处理后的毛重称量:将样品从微波炉中取出后,放在水中冷却10分钟,然后放入样品杯容器500中;将电动升降台300升至最高处时,电子称100清“0”;然后将电动升降台300降至最低处,将盛有样品的样品杯容器500挂在电子称下秤钩的“S”型挂钩110上,而后将电动升降台300升至最高处,此时样品杯容器500全部浸入水中,待天平数据稳定后,记录毛重数据;Step 4: Gross weight weighing after microwave treatment: take the sample out of the microwave oven, cool it in water for 10 minutes, and then put it into the sample cup container 500; "0"; then lower the electric lifting platform 300 to the lowest point, hang the sample cup container 500 containing the sample on the "S" type hook 110 of the electronic weighing scale hook, and then lift the electric lifting platform 300 to the highest point , at this time, the sample cup container 500 is completely immersed in water, and after the balance data is stable, record the gross weight data;
步骤五:结果计算:根据样品重、样品杯皮重、毛重,计算被测样品水分值;利用“阿基米德浮力定律”原理,将样品浸入水中悬浮称量,样品中的水分失重为“0”的同时,称量出干物质在水中的重量,再换算出干物质的百分率,导出谷物含水率;Step 5: Calculation of results: Calculate the moisture value of the tested sample according to the sample weight, sample cup tare weight, and gross weight; use the principle of "Archimedes buoyancy law" to immerse the sample in water for suspension weighing, and the water weight loss in the sample is At the same time as "0", weigh the weight of dry matter in water, and then convert the percentage of dry matter to derive the moisture content of the grain;
在本实施例中,假设样品中的水分重量为W=V×d1,其中,V为样品中水分的体积,单位为mL,d1为样品中水的密度,单位g/mL,由于样品是完全浸入水中称量,那么样品中水分在水中所受浮力为F=V×d2,其中,V为样品中水分的体积,单位为mL,d1为水箱中水的密度,单位g/mL,由于样品杯杯身有孔,而且样品杯在水箱中操作,这样样品中的水与水箱中的水就达到了温度平衡,即d1=d2,因此,W-F=Vd1-Vd2=0,所以,样品浸入水中悬浮称量时,样品中的水分就失重为“0”,样品中的水分在水中失重为“0”时,电子称100上称量出来的就是干物质在水中的重量,利用公式即可换算得出干物质百分率,最终确定水分百分率;其中,水分公式导出如下:In this embodiment, it is assumed that the weight of water in the sample is W=V×d 1 , wherein, V is the volume of water in the sample, in mL, and d 1 is the density of water in the sample, in g/mL, because the sample If it is completely immersed in water and weighed, then the buoyancy of the water in the sample in the water is F=V×d 2 , where V is the volume of water in the sample, in mL, and d 1 is the density of water in the water tank, in g/ mL, because the sample cup body has a hole, and the sample cup is operated in the water tank, so the water in the sample and the water in the water tank have reached temperature equilibrium, that is, d 1 =d 2 , therefore, WF=Vd 1 -Vd 2 = 0, so when the sample is immersed in water and suspended for weighing, the water in the sample will lose weight as "0", and when the water in the sample loses weight in water as "0", what is weighed on the electronic scale 100 is the dry matter in water The weight of the weight can be converted by using the formula to obtain the percentage of dry matter, and finally determine the percentage of moisture; among them, the moisture formula is derived as follows:
W0=Wg+Ws=ρg×Vg+ρs×Vs…………………………………(1)W 0 =W g +W s =ρ g ×V g +ρ s ×V s …………………………(1)
W1=(ρg-ρs)×Vg……………………………………………………(2)W 1 =(ρ g -ρ s )×V g ………………………………………………(2)
(1)-(2)得,(1)-(2) get,
W0-W1=ρs×(Vs+Vg)………………………………………………(3)W 0 -W 1 =ρ s ×(V s +V g )…………………………………………………(3)
由(2)得,From (2),
综合(3)、(4)得,Comprehensive (3), (4) get,
其中,W0为样品重,g;W1干物质在水中重,g;M样品水分含量,%;Vs样品所含水的体积,mL;Vg样品干物质的体积,mL;ρs水的密度,g/mL;ρg样品中干物质的密度,g/mL;设为换算系数A,将(6)简化为即可得到样品中水分含量。Among them, W 0 is the weight of the sample, g; W 1 is the weight of dry matter in water, g; M is the water content of the sample, %; V s is the volume of water contained in the sample, mL; V g is the volume of dry matter in the sample, mL; ρ s Density of water, g /mL; density of dry matter in ρg sample, g/mL; Set as the conversion factor A, simplify (6) to The moisture content in the sample can be obtained.
尽管本实用新型的实施方案已公开如上,但其并不仅仅限于说明书和实施方式中所列运用,它完全可以被适用于各种适合本实用新型的领域,对于熟悉本领域的人员而言,可容易地实现另外的修改,因此在不背离权利要求及等同范围所限定的一般概念下,本实用新型并不限于特定的细节和这里示出与描述的图例。Although the embodiment of the present utility model has been disclosed as above, it is not limited to the use listed in the specification and implementation, it can be applied to various fields suitable for the present utility model, and for those familiar with the art, Further modifications can be readily effected, so the invention is not limited to the specific details and examples shown and described herein without departing from the general concept defined by the claims and their equivalents.
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