CN204946944U - A kind of polarization device of temperature-controllable - Google Patents

A kind of polarization device of temperature-controllable Download PDF

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Publication number
CN204946944U
CN204946944U CN201520487115.8U CN201520487115U CN204946944U CN 204946944 U CN204946944 U CN 204946944U CN 201520487115 U CN201520487115 U CN 201520487115U CN 204946944 U CN204946944 U CN 204946944U
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China
Prior art keywords
insulation board
conductive pole
conductive
conductive plate
polarization
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Expired - Fee Related
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CN201520487115.8U
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Chinese (zh)
Inventor
李慧
张洋洋
王博
张金平
高景霞
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Huanghe Science and Technology College
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Huanghe Science and Technology College
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Abstract

The utility model provides a kind of polarization device of temperature-controllable, comprise high-voltage DC power supply, top crown, bottom crown, polarization clamp, integrated heating device, the time relay, top crown comprises insulation board I, insulation board I fixes thin conductive plate, insulation board I has the through hole through thin conductive plate, be set with conductive pole IV in through hole, the upper end of conductive pole IV contacts with the positive pole of high-voltage DC power supply; Bottom crown comprises insulation board II, and insulation board II fixes conductive plate, conductive plate connects the lower end of conductive pole II, and the lower end of conductive pole II contacts with the ground wire of high-voltage DC power supply; Polarization clamp comprises the conductive pole IV and bottom crown that are set with in top crown, top crown through hole, and integrated heating device comprises integrated heating device pedestal and container, and insulation board II and conductive plate to be dipped in container in silicone oil or transformer oil.That the utility model structure is simple, poling temperature is adjustable is controlled, the polarization time can accurately control, in polarization process with air insulated.

Description

A kind of polarization device of temperature-controllable
Technical field
The utility model relates to polarization field, particularly relates to a kind of polarization device to the temperature-controllable that leadless piezoelectric ceramics sheet, lead-free piezoelectric thin film or lead-free piezoelectric thick film polarize.
Background technology
Piezoelectric ceramic has direct piezoelectric effect and inverse piezoelectric effect.The effect being electric energy by changes mechanical energy is direct piezoelectric effect, and the effect being mechanical energy by electric energy conversion is inverse piezoelectric effect.Piezoelectric ceramic is simple owing to making, with low cost and conversion efficiency high, and development is at home and abroad very rapid, and is widely used in electronics, light, heat, and the fields such as acoustics, become national defense industry, functional material important in civilian industry and daily life.But traditional piezoelectric ceramic is lead base piezoelectric ceramic, its main component is that PbO(is up to more than 60% ~ 70%), because PbO is a kind of volatile noxious substance, serious volatilization can be produced when high temperature sintering, not only make the stoichiometric proportion generation deviation of PZT pottery, performance is difficult to stability contorting, and causes the lead contamination to environment, brings very large harm to human health.Some lead base piezoelectric ceramic is discarded in the Nature because of mismanagement after going out of use in addition, brings serious harm to the mankind and biological environment, and the sustainable development of this and human society is runed counter to.The environmentally harmful material of possibility is being prepared, using and do not produced in discarded last handling process to leadless piezoelectric ceramics, and the preparation technology of material has power consumption feature such as environment compatibility such as grade less, replace leaded piezoelectric ceramic devices and will have important scientific meaning, can great social profit be produced.
So-called polarization, adds a strong dc electric field or voltage exactly on piezoelectric ceramic, makes electricdomain in pottery along direction of an electric field orientations.Before the process of polarization operation, in pottery, the distribution in the spontaneous polarization direction of each electricdomain is chaotic, so the polarization intensity in pottery is zero, pottery is without piezoelectric effect.After polarization process process, the spontaneous polarization of each electricdomain is to a certain extent by external electric field orientations, so the polarization intensity in pottery is being not zero, pottery just occurs piezoelectric effect.Make the polarization that piezoelectric ceramic improves, give full play to its piezoelectric property, just reasonably must select polarization condition, be i.e. polarized electric field (polarizing voltage in sample unit length), poling temperature and polarization time.
But, current existing polarization device function singleness, use heating furnace as corollary apparatus, poling temperature can not be realized adjustable controlled, and piezoelectric ceramic piece is exposed polarizes in atmosphere, not only easily causes piezoelectric ceramic to puncture, product qualified rate is reduced, and be absolutely unsafe in operation engineering, the requirement in the places such as inapplicable laboratory and Corporation R & D.Therefore need to provide a kind of poling temperature adjustable controlled, in the process of polarization, pottery and air insulated can be made to puncture probability to reduce, be easy to operation, large-scale production requirement can be adapted to, go for again the polarization device of the Ya electricity Tao Ci ∕ Bao Mo ∕ thick film in the place such as laboratory and Corporation R & D.
Summary of the invention
The technical problems to be solved in the utility model is the polarization device providing a kind of temperature and polarization time controllable precise, in order to solve polarization device function singleness in prior art, non-adjustable uncontrollable, the exposed shortcoming that poor stability rate of finished products is low, can not be used for the place such as laboratory and Corporation R & D etc. that polarizes in atmosphere of temperature.
For solving the problems of the technologies described above, the utility model by the following technical solutions:
A polarization device for temperature-controllable, comprises high-voltage DC power supply, top crown, bottom crown, integrated heating device, polarization clamp;
Described top crown comprises insulation board I 1 and conductive pole I 3-1, insulation board I 1 is fixed thin conductive plate 2, insulation board I 1 has the through hole 4 through thin conductive plate 2, conductive pole IV 4-1 is set with in through hole 4, thin conductive plate 2 connects the upper end of conductive pole I 3-1, conductive pole I 3-1) upper end be connected with the positive pole of high-voltage DC power supply simultaneously;
Described bottom crown comprises insulation board II 6 and conductive pole II 3-2, insulation board II 6 is fixed conductive plate 5, conductive plate 5 connects the lower end of conductive pole II 3-2, and the upper end of conductive pole II 3-2 is connected with the ground wire of high-voltage DC power supply;
The lower end of described conductive pole I 3-1 is connected with insulation board II 6, and the upper end of described conductive pole II 3-2 is connected with insulation board I 1 simultaneously;
Described polarization clamp comprises conductive pole IV 4-1 and the bottom crown of suit in the through hole 4 of top crown;
The container that described integrated heating device comprises the adjustable integrated heating device pedestal of temperature 9 and is attached thereto, container content has silicone oil or transformer oil 7, insulation board II 6 and conductive plate 5 are dipped in silicone oil or transformer oil 7, polarized sample 8 is placed on conductive plate 5, is pressed into completely in silicone oil or transformer oil 7 by sample by conductive pole IV 4-1 of suit in through hole 4.
Connect hours relay 10 between the upper end of described conductive pole I 3-1 and the positive pole of high-voltage DC power supply.
Also be provided with conductive pole III 3-3 described in conductive pole III 3-3 for supporting top crown and bottom crown between described top crown and bottom crown and be no less than 1, and the two ends of conductive pole III 3-3 are separately fixed on insulation board I 1 and insulation board II 6, and do not contact with thin conductive plate 2 and conductive plate 5.
Described through hole 4 is no less than 1, and conductive pole IV 4-1 supporting with through hole 4 is quite a few in one.
Described thin conductive plate 2 is screwed in insulation board I 1, and described conductive plate 5 is screwed in insulation board II 6.
Described insulation board I 1 and insulation board II 6 are heat resistance insulating sheet.
The material of described thin conductive plate 2, conductive plate 5, conductive pole I 3-1, conductive pole IV 4-1, conductive pole II 3-2 is copper.
The material of described conductive pole III 3-3 is copper.
Described polarized sample 8 is leadless piezoelectric ceramics sheet, lead-free piezoelectric thin film or lead-free piezoelectric thick film.
When polarized sample not being polarized in silicone oil or transformer oil during the utility model polarization, poling temperature not only can be made to keep constant, and polarization time and air exclusion can be made, not only avoid polarized sample to polarize in atmosphere and easily puncture but also unsafe shortcoming, the coefficient of safety that both improve operating environment turn improves rate of finished products.
Accompanying drawing explanation
Fig. 1 is the utility model top crown schematic diagram.
Fig. 2 is the utility model bottom crown schematic diagram.
Fig. 3 is utility model works state front view.
Fig. 4 is utility model works state rearview.
Fig. 5 is utility model works state left view.
Embodiment
Below in conjunction with accompanying drawing 1 ~ 5 and embodiment, the utility model is described in further detail.
The utility model provides a kind of temperature and polarization time controlled controlled polarization device, is mainly used in polarizing to leadless piezoelectric ceramics sheet, lead-free piezoelectric thin film or lead-free piezoelectric thick film.Polarization device comprises high-voltage DC power supply, top crown, bottom crown, polarization clamp, integrated heating device.
Top crown comprises insulation board I 1 and conductive pole I 3-1, insulation board I 1 is fixed thin conductive plate 2, fixed form can be adopted and to be screwed or alternate manner is fixed, insulation board I 1 has the through hole 4 through thin conductive plate 2, conductive pole IV 4-1 is set with in through hole 4, conductive pole IV 4-1 connects the upper end of conductive pole I 3-1 by thin conductive plate 2, and the upper end of conductive pole I 3-1 contacts with the positive pole of high-voltage DC power supply simultaneously.
Bottom crown comprises insulation board II 6, insulation board II 6 is fixed conductive plate 5, fixed form can be adopted and to be screwed or alternate manner is fixed, and conductive plate 5 connects the lower end of conductive pole II 3-2, the upper end of conductive pole II 3-2 contacts with the ground wire of high-voltage DC power supply.The lower end of conductive pole I 3-1 is connected with insulation board II 6, and the upper end of conductive pole II 3-2 is connected with insulation board I 1.
The container that integrated heating device comprises the adjustable integrated heating device pedestal of temperature 9 and is attached thereto, container content has silicone oil or transformer oil 7, insulation board II 6 and conductive plate 5 are dipped in silicone oil or transformer oil 7, polarized sample 8 is positioned on conductive plate 5, is pressed into completely in silicone oil or transformer oil 7 by conductive pole IV 4-1 of suit in through hole 4.The through hole 4 of top crown is no less than 1, conductive pole IV 4-1 supporting with through hole 4 is quite a few in one, in practice, select the through hole of varying number and the conductive pole supporting with through hole according to the actual needs of polarized sample, meet device in the general object in laboratory and factory.Can connect hours relay 10 on connecting line between the upper end of conductive pole I 3-1 simultaneously in polarization device and the positive pole of high-voltage DC power supply, accurate control can be carried out by the time of the time relay 10 to plan.
Above-mentioned polarization clamp comprises conductive pole IV and the bottom crown of suit in through hole 4, and this polarization clamp not only serves the effect of fixing leadless piezoelectric ceramics sheet, and the upper and lower surface of returning leadless piezoelectric ceramics sheet provides voltage.
Conductive pole III 3-3 for supporting top crown and bottom crown is also provided with between top crown and bottom crown, conductive pole III 3-3 is no less than 1, and the two ends of conductive pole III 3-3 are separately fixed on insulation board I 1 and insulation board II 6, and do not contact with thin conductive plate 2 and conductive plate 5.
In above-mentioned top crown and bottom crown, insulation board I 1 and insulation board II 6 select heat-resisting quantity insulation board.
And in top crown, bottom crown, polarization clamp, identical electric conducting material selected by electric conducting material, the material of electric conducting material can be any material that can conduct electricity, but in concrete enforcement, because the cost performance of copper is the highest, therefore, preferably copper is as conductive material.The material of namely above-mentioned thin conductive plate 2, conductive plate 5, conductive pole I 3-1, conductive pole IV 4-1, conductive pole II 3-2, conductive pole III 3-3 is copper.
As shown in Fig. 1 ~ Fig. 5, as a kind of execution mode, selection copper is conductive material, selects top crown and bottom crown to be rectangle, the number of copper post III 3-3 is two, together with copper post II 3-2, copper post I 3-1, be distributed in four angles of top crown and bottom crown, well support top crown and bottom crown, simultaneously in the present embodiment, the number selecting through hole 4 is 5, accordingly when polarizing shown in Fig. 3, Fig. 4, Fig. 5, selects 5 copper post IV 4-1.
In above-mentioned polarization device, when connecting high-voltage DC power supply, sheet copper 2 on top crown is connected with the positive pole of high-voltage DC power supply by copper post I 3-1, therefore electromotive force is just, copper post II 3-2 upper end is connected with the ground wire of high-voltage DC power supply by wire, when connecting high-voltage DC power supply, electromotive force on bottom crown on copper foil 5 is zero, therefore, copper post I 3-1 and copper post II 3-2 not only plays the effect supporting top crown and bottom crown, provide electrical potential difference for top crown and bottom crown, i.e. voltage simultaneously.And copper post III 3-3 is not connected with any one copper coin, only play the effect of pillar.Through hole 4 is set to the certain circular hole of radius, when needs polarize to polarized sample, actual conditions per sample and quantity, select copper post IV 4-1 of suitable number, the diameter of copper post IV 4-1 is close with the diameter of through hole 4, utilizes the gravity of copper post IV 4-1 self to be firmly pressed on bottom crown by leadless piezoelectric thin slice.Because copper post IV 4-1 inserted in through hole 4 contacts with the sheet copper 2 on top crown, so the electromotive force of the upper surface of leadless piezoelectric thin slice 8 can be made equal with the positive electrode potential of high-voltage DC power supply.For bottom crown, when polarized sample, because the lower surface of sample contacts with copper coin 5, so the electromotive force of polarized sample lower surface is also zero.
When specifically polarizing, first will the sample 8 of polarization be needed to be placed on copper coin 5, then copper post identical with through hole 4 for diameter is pressed in the upper surface of polarized sample through the through hole 4 on top crown, due to the Action of Gravity Field of copper post self, need the polarized sample of polarization can be fixed on firmly between copper post and bottom crown.When connecting high-voltage DC power supply, the upper surface of polarized sample is communicated with the positive pole of power supply by pressure copper post thereon, electromotive force be on the occasion of, lower surface is connected with ground wire by contact bottom crown, electromotive force is zero, there is electrical potential difference up and down like this in polarized sample between two surfaces, by regulating the magnitude of voltage of high-voltage DC power supply, change and be added in upper and lower two the surperficial magnitudes of voltage of polarized sample, it is polarized.Bottom crown is placed in silicone oil or transformer oil 7 with needing the polarized sample polarized simultaneously.By regulating integrated heating device, the temperature of silicone oil or transformer oil in adjustable integrated heating apparatus container, and then controlling the poling temperature of polarized sample, being controlled by the time of the time relay 10 to polarization simultaneously.When improving poling temperature, can the polarization time be shortened, enhance productivity.
When leadless piezoelectric ceramics sheet, lead-free piezoelectric thin film or lead-free piezoelectric thick film are polarized, when they are not polarized in silicone oil or transformer oil, poling temperature not only can be made to keep constant, and leadless piezoelectric ceramics sheet, lead-free piezoelectric thin film or lead-free piezoelectric thick film and air exclusion can be made, not only avoid exposed the polarization in atmosphere of leadless piezoelectric ceramics sheet, lead-free piezoelectric thin film or lead-free piezoelectric thick film easily to puncture but also unsafe shortcoming, the coefficient of safety that both improve operating environment turn improves rate of finished products.
In the use procedure of equipment, can according to the quantity of the sheet number that once polarizes, the quantity of adjustment through hole 4 and the copper post through through hole 4, this apparatus structure is simple, be easy to operation, poling temperature and polarization time adjustable controlled, the place such as laboratory and Corporation R & D can be used for can be used for again the places such as factory mass production, lead piezoelectric ceramics sheet, lead-free piezoelectric thin film or lead-free piezoelectric thick film and air insulated can be accomplished in polarization process, not only increase the fail safe of operation, turn improve rate of finished products.

Claims (9)

1. a polarization device for temperature-controllable, is characterized in that: comprise high-voltage DC power supply, top crown, bottom crown, integrated heating device, polarization clamp;
Described top crown comprises insulation board I (1) and conductive pole I (3-1), at the upper fixing thin conductive plate (2) of insulation board I (1), insulation board I (1) has the through hole (4) through thin conductive plate (2), conductive pole IV (4-1) is set with in through hole (4), thin conductive plate (2) connects the upper end of conductive pole I (3-1), and the upper end of conductive pole I (3-1) is connected with the positive pole of high-voltage DC power supply simultaneously;
Described bottom crown comprises insulation board II (6) and conductive pole II (3-2), at the upper fixing conductive plate (5) of insulation board II (6), the upper lower end connecting conductive pole II (3-2) of conductive plate (5), the upper end of conductive pole II (3-2) is connected with the ground wire of high-voltage DC power supply;
The lower end of described conductive pole I (3-1) is connected with insulation board II (6), and the upper end of described conductive pole II (3-2) is connected with insulation board I (1) simultaneously;
Described polarization clamp comprises conductive pole IV (4-1) and the bottom crown of suit in the through hole (4) of top crown;
The container that described integrated heating device comprises the adjustable integrated heating device pedestal (9) of temperature and is attached thereto, container content has silicone oil or transformer oil (7), insulation board II (6) and conductive plate (5) are dipped in silicone oil or transformer oil (7), polarized sample (8) is placed on conductive plate (5), is pressed into completely in silicone oil or transformer oil (7) by sample by the conductive pole IV (4-1) of suit in through hole (4).
2. the polarization device of a kind of temperature-controllable according to claim 1, is characterized in that: connect hours relay (10) between the upper end of described conductive pole I (3-1) and the positive pole of high-voltage DC power supply.
3. the polarization device of a kind of temperature-controllable according to claim 1, it is characterized in that: between described top crown and bottom crown, be also provided with the conductive pole III (3-3) for supporting top crown and bottom crown, described conductive pole III (3-3) is no less than 1, and the two ends of conductive pole III (3-3) are separately fixed on insulation board I (1) and insulation board II (6), and do not contact with thin conductive plate (2) and conductive plate (5).
4. the polarization device of a kind of temperature-controllable according to claim 1, is characterized in that: described through hole (4) is no less than 1, and the conductive pole IV (4-1) supporting with through hole (4) is quite a few in one.
5. the polarization device of a kind of temperature-controllable according to claim 1, is characterized in that: described thin conductive plate (2) is screwed in insulation board I (1), and described conductive plate (5) is screwed in insulation board II (6).
6. the polarization device of a kind of temperature-controllable according to claim 1, is characterized in that: described insulation board I (1) and insulation board II (6) are heat resistance insulating sheet.
7. the polarization device of a kind of temperature-controllable according to claim 1, is characterized in that: the material of described thin conductive plate (2), conductive plate (5), conductive pole I (3-1), conductive pole IV (4-1), conductive pole II (3-2) is copper.
8. the polarization device of a kind of temperature-controllable according to claim 3, is characterized in that: the material of described conductive pole III (3-3) is copper.
9. the polarization device of a kind of temperature-controllable according to claim 1, is characterized in that: described polarized sample (8) is leadless piezoelectric ceramics sheet, lead-free piezoelectric thin film or lead-free piezoelectric thick film.
CN201520487115.8U 2015-07-08 2015-07-08 A kind of polarization device of temperature-controllable Expired - Fee Related CN204946944U (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107026232A (en) * 2017-05-09 2017-08-08 湖南科技大学 A kind of piezoelectric fabric polar system and method
CN107240640A (en) * 2017-06-06 2017-10-10 西南科技大学 A kind of piezoelectric polarization device
CN107342358A (en) * 2017-07-26 2017-11-10 电子科技大学 A kind of organic ferroelectric thin film polarization device
CN108630803A (en) * 2018-06-27 2018-10-09 武汉工程大学 A kind of piezoelectric rubber polarization device for standing wave tube test

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107026232A (en) * 2017-05-09 2017-08-08 湖南科技大学 A kind of piezoelectric fabric polar system and method
CN107240640A (en) * 2017-06-06 2017-10-10 西南科技大学 A kind of piezoelectric polarization device
CN107342358A (en) * 2017-07-26 2017-11-10 电子科技大学 A kind of organic ferroelectric thin film polarization device
CN108630803A (en) * 2018-06-27 2018-10-09 武汉工程大学 A kind of piezoelectric rubber polarization device for standing wave tube test

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160106

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CF01 Termination of patent right due to non-payment of annual fee