CN204699583U - A pickling tower inlet distribution device - Google Patents
A pickling tower inlet distribution device Download PDFInfo
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- CN204699583U CN204699583U CN201520393276.0U CN201520393276U CN204699583U CN 204699583 U CN204699583 U CN 204699583U CN 201520393276 U CN201520393276 U CN 201520393276U CN 204699583 U CN204699583 U CN 204699583U
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- 238000005554 pickling Methods 0.000 title claims abstract description 74
- 238000009826 distribution Methods 0.000 title claims abstract description 19
- 239000007788 liquid Substances 0.000 claims description 15
- 238000002425 crystallisation Methods 0.000 abstract description 8
- 230000008025 crystallization Effects 0.000 abstract description 8
- 230000007797 corrosion Effects 0.000 abstract description 7
- 238000005260 corrosion Methods 0.000 abstract description 7
- 235000021110 pickles Nutrition 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 10
- 238000000034 method Methods 0.000 description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- 239000002253 acid Substances 0.000 description 6
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 6
- 239000012452 mother liquor Substances 0.000 description 6
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 5
- 235000011130 ammonium sulphate Nutrition 0.000 description 5
- 238000009827 uniform distribution Methods 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 3
- 238000004939 coking Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 230000002787 reinforcement Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 230000000087 stabilizing effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910000851 Alloy steel Inorganic materials 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Landscapes
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
Abstract
Description
技术领域technical field
本实用新型涉及焦化设备技术领域,尤其涉及一种酸洗塔进气分布装置。The utility model relates to the technical field of coking equipment, in particular to an air inlet distribution device for a pickling tower.
背景技术Background technique
在焦化及煤化工方面,酸洗塔是煤气处理工艺中常用的化工设备。在酸洗法生产硫铵工艺中,主要采用硫酸母液吸收煤气中的氨,再经过蒸发结晶和分离干燥,生产出合格的硫铵。氨的吸收过程主要在酸洗塔中进行。酸洗塔为多段空喷塔,经过喷头均匀喷洒的硫酸母液和含氨煤气逆流接触吸收,在酸洗塔内形成不饱和硫铵母液,用于后续的蒸发、结晶工序。In terms of coking and coal chemical industry, the pickling tower is a commonly used chemical equipment in the gas treatment process. In the process of producing ammonium sulfate by pickling method, the sulfuric acid mother liquor is mainly used to absorb the ammonia in the gas, and then undergoes evaporation, crystallization, separation and drying to produce qualified ammonium sulfate. The absorption process of ammonia is mainly carried out in the pickling tower. The pickling tower is a multi-stage empty spraying tower. The sulfuric acid mother liquor evenly sprayed by the nozzle and the ammonia-containing gas are countercurrently contacted and absorbed, and an unsaturated ammonium sulfate mother liquor is formed in the pickling tower for subsequent evaporation and crystallization processes.
目前,焦化工业中使用的酸洗塔为价格较高的抗酸腐蚀材料,设备投资较高。At present, the pickling tower used in the coking industry is a relatively expensive acid corrosion-resistant material, and the investment in equipment is relatively high.
另外,为了防止结晶后的堵塞现象的发生,现有技术中的酸洗塔煤气进口段处、煤气与硫酸母液接触区域不设有其他装置。酸性气体会扩散混入进气管道口,造成输气管道腐蚀和破坏。In addition, in order to prevent the occurrence of clogging after crystallization, no other devices are installed at the gas inlet section of the pickling tower and the contact area between gas and sulfuric acid mother liquor in the prior art. Acid gas will diffuse and mix into the intake pipe opening, causing corrosion and damage to the gas pipeline.
同时,在硫铵形成的过程中完全靠塔内的气体与硫酸母液自然接触。而由于塔内气体分布不均匀,气体与酸液不能充分接触,因此反应也不充分。为了解决这一问题,往往需要加高酸洗塔的高度来延长气体与酸液的接触时间,达到反应充分的目的。这样就在很大程度上增加了设备的制作成本。At the same time, during the formation of ammonium sulfate, the gas in the tower is completely in contact with the sulfuric acid mother liquor. However, due to the uneven distribution of gas in the tower, the gas and acid liquid cannot fully contact, so the reaction is not sufficient. In order to solve this problem, it is often necessary to increase the height of the pickling tower to prolong the contact time between the gas and the acid liquid to achieve the purpose of sufficient reaction. This increases the manufacturing cost of the equipment to a large extent.
发明内容Contents of the invention
本实用新型的目的是提供一种酸洗塔进气分布装置,利用向下倾斜气体入口、导流筒、导流板和斜盖板实现气体均匀分配,防止输气管道腐蚀,不会造成硫铵结晶后堵塞现象,在技术上能够实现降低酸洗塔高度、减少设备投资;实现塔内气体均匀分布、无硫铵结晶堵塞现象和防止酸性气体腐蚀管道等性能。The purpose of this utility model is to provide an air intake distribution device for pickling towers, which uses downwardly inclined gas inlets, guide cylinders, guide plates and inclined cover plates to achieve uniform distribution of gas, prevents corrosion of gas pipelines, and does not cause sulfur The clogging phenomenon after ammonium crystallization can technically reduce the height of the pickling tower and reduce equipment investment; realize the uniform distribution of gas in the tower, no clogging phenomenon of ammonium sulfate crystallization, and prevent acid gas from corroding pipelines.
为实现上述目的,本实用新型采用以下技术方案实现:In order to achieve the above object, the utility model adopts the following technical solutions:
一种酸洗塔进气分布装置,包括酸洗塔进气口管道、斜盖板、导流筒、支撑板,所述酸洗塔进气管道与酸洗塔相贯连接,酸洗塔进气管道成向下倾斜设置,斜盖板位于酸洗塔的内部、酸洗塔进气管道的上方,斜盖板的上端与酸洗塔内壁固定密闭连接,斜盖板的下端与导流筒的上端固定密闭连接,导流筒的下端通过支撑板与酸洗塔内壁固定连接。A pickling tower inlet distribution device, comprising a pickling tower inlet pipe, an inclined cover plate, a guide cylinder, and a support plate, the pickling tower inlet pipe is connected to the pickling tower, and the pickling tower inlet The gas pipeline is set in a downward slope. The inclined cover is located inside the pickling tower and above the intake pipe of the pickling tower. The upper end of the inclined cover is fixed and airtightly connected with the inner wall of the pickling tower. The upper end of the guide tube is fixed and airtightly connected, and the lower end of the guide tube is fixedly connected with the inner wall of the pickling tower through a support plate.
所述酸洗塔进气口管道的下倾角度θ为10°~60°。The downward inclination angle θ of the inlet pipe of the pickling tower is 10°-60°.
所述斜盖板为向下倾斜的环板,向下倾斜的角度α为10°~60°。The inclined cover plate is a downwardly inclined ring plate, and the downwardly inclined angle α is 10°-60°.
在所述导流筒的底部朝向酸洗塔进气管道的一侧固定气体导向板,气体导向板与导流筒密闭连接,在所述导流筒底部的另一侧均匀排布矩形排液齿,排液齿中心角范围为30°~270°。A gas guide plate is fixed on the side of the bottom of the guide tube facing the intake pipe of the pickling tower, the gas guide plate is airtightly connected with the guide tube, and a rectangular discharge is evenly arranged on the other side of the bottom of the guide tube Teeth, the central angle of the liquid discharge teeth ranges from 30° to 270°.
所述气体导向板为弧形环板,气体导向板的中心角范围为30°~180°。The gas guide plate is an arc-shaped ring plate, and the central angle of the gas guide plate ranges from 30° to 180°.
与现有的技术相比,本实用新型的有益效果是:Compared with the prior art, the beneficial effects of the utility model are:
一种酸洗塔进气分布装置,向下倾斜的进气口能够有效地防止硫酸母液进入进气管道腐蚀管道,导流筒的设计使流入的气体均匀分布在塔体内部,排液齿有效地平衡气体压力和酸洗塔底部液位差,气体导向板能够很好地调节进入气体流入导流筒的方向和比例。本设备具有操作稳定、分布均匀、投资成本低,无结晶后堵塞现象等优点,同时维护方便,保证生产过程的安全稳定运行。A pickling tower air inlet distribution device, the downwardly inclined air inlet can effectively prevent the sulfuric acid mother liquor from entering the inlet pipe to corrode the pipe, the design of the guide tube makes the inflowing gas evenly distributed inside the tower body, and the liquid discharge teeth are effective To balance the gas pressure and the liquid level difference at the bottom of the pickling tower, the gas guide plate can well adjust the direction and proportion of the incoming gas flowing into the draft tube. This equipment has the advantages of stable operation, uniform distribution, low investment cost, no clogging after crystallization, etc., and convenient maintenance to ensure safe and stable operation of the production process.
附图说明Description of drawings
图1是本实用新型一种酸洗塔进气分布装置的结构示意图;Fig. 1 is the structural representation of a kind of pickling tower gas distribution device of the utility model;
图中:1.加强板 2.酸洗塔进气管道 3.气体导向板 4.酸洗塔塔体 5.斜盖板 6.导流筒 7.支撑板 8.排液齿In the figure: 1. Reinforcement plate 2. Pickling tower intake pipe 3. Gas guide plate 4. Pickling tower body 5. Inclined cover plate 6. Guide tube 7. Support plate 8. Liquid discharge teeth
具体实施方式Detailed ways
下面结合说明书附图对本实用新型进行详细地描述,但是应该指出本实用新型的实施不限于以下的实施方式。The utility model is described in detail below in conjunction with the accompanying drawings, but it should be pointed out that the implementation of the utility model is not limited to the following embodiments.
如图1所示,一种酸洗塔进气分布装置,包括酸洗塔进气口管道2、斜盖板5、导流筒6、支撑板7,所述酸洗塔进气管道2与酸洗塔4相贯连接,斜盖板5位于酸洗塔4的内部、酸洗塔进气管道2的上方,斜盖板5的上端与酸洗塔4内壁固定密闭连接,斜盖板5的下端与导流筒6的上端固定密闭连接,导流筒6的下端通过支撑板7与酸洗塔4内壁固定连接。As shown in Figure 1, a kind of pickling tower air inlet distribution device comprises pickling tower air inlet pipe 2, inclined cover plate 5, guide tube 6, support plate 7, described pickling tower air inlet pipe 2 and The pickling towers 4 are interlinked and connected, and the inclined cover plate 5 is located inside the pickling tower 4 and above the pickling tower inlet pipe 2. The upper end of the inclined cover plate 5 is fixed and airtightly connected with the inner wall of the pickling tower 4. The lower end of the guide tube 6 is fixedly and airtightly connected with the upper end of the guide tube 6, and the lower end of the guide tube 6 is fixedly connected with the inner wall of the pickling tower 4 through the support plate 7.
本实用新型中的导流筒起到稳定压力和导流的作用。The guide cylinder in the utility model plays the role of stabilizing pressure and guiding flow.
所述酸洗塔进气口管道2成倾斜向下设置,其向下倾角度θ为10°~60°。The inlet pipe 2 of the pickling tower is arranged obliquely downward, and its downward inclination angle θ is 10°-60°.
所述斜盖板5为向下倾斜的环板,向下倾斜的角度α为10°~60°。The inclined cover plate 5 is a downwardly inclined ring plate, and the downwardly inclined angle α is 10°-60°.
斜盖板与酸洗塔的内壁焊接连接,在斜盖板上部与酸洗塔的连接焊缝处均匀布置加强板,用以增强斜盖板与酸洗塔的焊接强度。The slanting cover plate is welded to the inner wall of the pickling tower, and reinforcement plates are evenly arranged at the joint weld between the upper part of the sloping cover plate and the pickling tower to enhance the welding strength between the sloping cover plate and the pickling tower.
在所述导流筒6的底部朝向酸洗塔进气管道2的一侧固定气体导向板3,气体导向板3与导流筒6密闭连接,在所述导流筒6底部的另一侧均匀排布矩形排液齿8,排液齿8中心角范围为30°~270°。On the side of the bottom of the guide tube 6 facing the pickling tower intake pipe 2, a gas guide plate 3 is fixed, and the gas guide plate 3 is airtightly connected with the guide tube 6, and on the other side of the bottom of the guide tube 6 The rectangular liquid discharge teeth 8 are evenly arranged, and the central angle of the liquid discharge teeth 8 ranges from 30° to 270°.
所述气体导向板3为弧形环板,气体导向板3的中心角范围为30°~180°。The gas guide plate 3 is an arc-shaped ring plate, and the central angle of the gas guide plate 3 ranges from 30° to 180°.
酸洗塔进气分布装置的材质为不锈钢、合金钢、陶瓷或塑料等抗酸液腐蚀的材料。The material of the air inlet distribution device of the pickling tower is stainless steel, alloy steel, ceramics or plastics and other materials resistant to acid corrosion.
使用时,气体通过酸洗塔进气管道2进入酸洗塔塔体内部,倾斜的进气管道入口内无腐蚀性液体滞留现象,具有防止腐蚀作用,气体进入酸洗塔塔体内部后,绕导流筒6流动,少量的雾化液体在离心力的作用下附着在酸洗塔塔壁上向下流淌,在导流筒6的导流作用下,气体流向改变,进行气体均匀分布,绕导流筒6流动的气体缓慢向下流动,到达导流筒6的底部时,均匀流入导流筒6内部,气体导向板3位于导流筒6下部,调节入口气量分配,导流筒6的底部的排液齿8实现气液压力平衡调节,支撑板7起连接和稳固导流筒6结构形状作用,最终,导流筒6内部气体均匀向上流动,完成气体在酸洗塔内均匀分布。When in use, the gas enters the pickling tower body through the pickling tower inlet pipe 2, and there is no corrosive liquid retention phenomenon in the inclined inlet pipe inlet, which has the effect of preventing corrosion. After the gas enters the pickling tower body, it goes around The diversion cylinder 6 flows, and a small amount of atomized liquid adheres to the wall of the pickling tower and flows downward under the action of centrifugal force. The gas flowing in the flow tube 6 flows down slowly, and when it reaches the bottom of the flow guide tube 6, it flows into the inside of the flow guide tube 6 evenly. The liquid discharge teeth 8 realize the balance adjustment of the gas-liquid pressure, and the support plate 7 plays the role of connecting and stabilizing the structural shape of the guide cylinder 6. Finally, the gas inside the guide cylinder 6 flows upward evenly, and the gas is evenly distributed in the pickling tower.
本实用新型利用气体分布、气液分离和压力平衡等原理实现酸洗塔进气均匀分布,在气体分布和硫铵形成过程中,无进气管道腐蚀、结晶后无堵塞现象、气体分布均匀;本设备降低投资成本,维护方便,保证生产过程的安全稳定运行。The utility model utilizes the principles of gas distribution, gas-liquid separation and pressure balance to realize the uniform distribution of the intake air of the pickling tower. In the process of gas distribution and ammonium sulfate formation, there is no corrosion of the intake pipe, no blockage after crystallization, and the gas distribution is uniform; This equipment reduces investment costs, is easy to maintain, and ensures safe and stable operation of the production process.
上面所述仅是本实用新型的基本原理,并非对本实用新型作任何限制,凡是依据本实用新型对其进行等同变化和修饰,均在本专利技术保护方案的范畴之内。The above is only the basic principle of the utility model, and does not limit the utility model in any way. All equivalent changes and modifications according to the utility model are within the scope of the technical protection scheme of this patent.
Claims (5)
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| Application Number | Priority Date | Filing Date | Title |
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| CN201520393276.0U CN204699583U (en) | 2015-06-08 | 2015-06-08 | A pickling tower inlet distribution device |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201520393276.0U CN204699583U (en) | 2015-06-08 | 2015-06-08 | A pickling tower inlet distribution device |
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| CN204699583U true CN204699583U (en) | 2015-10-14 |
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| CN201520393276.0U Withdrawn - After Issue CN204699583U (en) | 2015-06-08 | 2015-06-08 | A pickling tower inlet distribution device |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104941426A (en) * | 2015-06-08 | 2015-09-30 | 中冶焦耐工程技术有限公司 | A pickling tower gas distribution device and method |
| CN115199933A (en) * | 2022-07-07 | 2022-10-18 | 西安热工研究院有限公司 | Air storage chamber and gravity compressed air energy storage system based on flexible air guide |
-
2015
- 2015-06-08 CN CN201520393276.0U patent/CN204699583U/en not_active Withdrawn - After Issue
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104941426A (en) * | 2015-06-08 | 2015-09-30 | 中冶焦耐工程技术有限公司 | A pickling tower gas distribution device and method |
| CN115199933A (en) * | 2022-07-07 | 2022-10-18 | 西安热工研究院有限公司 | Air storage chamber and gravity compressed air energy storage system based on flexible air guide |
| CN115199933B (en) * | 2022-07-07 | 2024-04-02 | 西安热工研究院有限公司 | An air storage chamber and gravity compressed air energy storage system based on flexible air guidance |
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