CN204638187U - A kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus - Google Patents
A kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus Download PDFInfo
- Publication number
- CN204638187U CN204638187U CN201520061731.7U CN201520061731U CN204638187U CN 204638187 U CN204638187 U CN 204638187U CN 201520061731 U CN201520061731 U CN 201520061731U CN 204638187 U CN204638187 U CN 204638187U
- Authority
- CN
- China
- Prior art keywords
- kettle
- heat exchanger
- agitating device
- waste gas
- integrated apparatus
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Abstract
The utility model discloses a kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus, comprise kettle, agitating device, heat exchanger and waste gas purification and recovery integrated apparatus, described agitating device comprises main agitating device and secondary agitating device, the side, outside of described kettle is provided with the cooling water pipe and steam pipe that are connected with heat exchanger, opposite side is provided with the heat exchanger exit pipe be connected with heat exchanger, described kettle upper end is provided with gas outlet, described waste gas purification and recovery integrated apparatus comprise adsorption/desorption device and condensation recovering device, described condensation recovering device is arranged on the below of adsorption/desorption device, the secondary agitating device that the utility model is arranged can by the stirring of main agitating device, reduce energy consumption, the Steam Heating arranged makes kettle heat up rapidly, evaporated condensation water, also can fast cooling, the waste gas purification arranged and reclaim the integration that integrated apparatus achieves waste gas absorption, adsorbent desorption and solvent recovery, good purification, solvent recovering rate is high, and space hold is little.
Description
Technical field
The utility model relates to a kind of chemical industry equipment, specifically a kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus.
Background technology
Industrial chemicals can use reactor in process, and reactor is a kind of important chemical industry equipment, and its Main Function stores or supplies corresponding chemical substance reaction.The stirring intensity of reactor directly has influence on the reaction result of material, plays vital effect to the quality of final products.Existing reactor is generally a blade-carrying axle and rotates in tank body, plurality of raw materials is uniformly mixed, the liquid that existing agitating mode the produces inner wall of kettle that fails to be convened for lack of a quorum flows with layer flow mode, without shear action, mixed effect is bad, need the mixed uniformly effect that higher rotating speed and longer time just can reach required, reduce production efficiency; The heater arranged in General reactions still, bottom reactor, is difficult to the homogeneous heating being applicable to high request, and cannot realizes fast cooling; Some chemical raw materials easily cause local concentration too high when entering reactor; The gas discharging that reactor operationally produces the in the work environment easy health to operating personnel produces harm, directly be discharged in air easily to produce air and pollute, also result in the waste of resource, existing exhaust-gas treatment retracting device integration of equipments degree is low, bulky, floor space is large.
Utility model content
The purpose of this utility model is to provide a kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the utility model provides following technical scheme:
A kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus, comprise kettle, agitating device, heat exchanger and waste gas purification and recovery integrated apparatus, side, described kettle upper end is provided with charging aperture, lower end opposite side is provided with discharging opening, described agitating device comprises main agitating device and secondary agitating device, described main agitating device is arranged on the top of kettle inner chamber, described main agitating device comprises shaft and is arranged on the helical mixing blade on shaft, described shaft connects the motor that kettle is arranged outward, described shaft is positioned at above helical mixing blade and is provided with receiver, described secondary agitating device is arranged on autoclave body bottom, described secondary agitating device comprises blade, paddle, dwang and rotating shaft, described rotating shaft arrange kettle bottom and with shaft on the same axis, described dwang is connected with axis of rotation, the top of described dwang arranges blade, described paddle to be arranged on dwang and to be positioned under blade, described heat exchanger is arranged on the inside of kettle, the side, outside of described kettle is provided with the cooling water pipe and steam pipe that are connected with heat exchanger, opposite side is provided with the heat exchanger exit pipe be connected with heat exchanger, described kettle upper end is provided with gas outlet, described waste gas purification and recovery integrated apparatus comprise adsorption/desorption device and condensation recovering device, described condensation recovering device is arranged on the below of adsorption/desorption device, described adsorption/desorption device comprises housing, adsorption tube, adsorption tube shell side, be arranged on the clean gas outlet of housing tip, be arranged on the heat transferring medium import of side, adsorption tube shell side upper end and be arranged on adsorption tube shell side lower end opposite side heat transferring medium outlet, described condensation recovering device comprises heat exchanger fin, exhaust gas entrance, cooling medium inlet, cooling medium outlet and solvent collection mouth, described heat exchanger fin is connected with solvent collection mouth, described exhaust gas entrance is connected with the gas outlet on kettle by pipeline.
As further program of the utility model: described blade is provided with two, two described blades become V-shape, and the angle between two described blades is 90 °.
As the utility model further scheme: described cooling water pipe is provided with cooling water valve, described steam pipe is provided with steam valve, and described heat exchanger exit pipe is provided with heat exchanger exit valve.
As the utility model further scheme: be filled with adsorbent in described adsorption tube, adsorbent adopts granular activated carbon.
Compared with prior art, the beneficial effects of the utility model are: the receiver of setting makes the industrial chemicals put in reactor be uniformly dispersed, and prevents local concentration too high, improves product quality; The secondary agitating device arranged by the stirring of main agitating device, can need not consume the energy and carry out passive stirring, makes the solution in kettle corner produce axial flow, reduces energy consumption, makes mixing more even, accelerates reaction; The Steam Heating arranged is simple to operate, kettle is heated up rapidly, evaporated condensation water, also can fast cooling; The waste gas purification arranged and reclaim the integration that integrated apparatus achieves waste gas absorption, adsorbent desorption and solvent recovery, good purification, solvent recovering rate is high, and space hold is little.
Accompanying drawing explanation
Fig. 1 is with the structural representation of waste gas purification with the chemical reaction still of recovery integrated apparatus.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the utility model embodiment, be clearly and completely described the technical scheme in the utility model embodiment, obviously, described embodiment is only the utility model part embodiment, instead of whole embodiments.Based on the embodiment in the utility model, those of ordinary skill in the art are not making the every other embodiment obtained under creative work prerequisite, all belong to the scope of the utility model protection.
Refer to Fig. 1, in the utility model embodiment, a kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus, comprise kettle 1, agitating device, heat exchanger 11 and waste gas purification and recovery integrated apparatus, side, described kettle 1 upper end is provided with charging aperture 3, lower end opposite side is provided with discharging opening 16, described agitating device comprises main agitating device and secondary agitating device, described main agitating device is arranged on the top of kettle 1 inner chamber, the helical mixing blade 6 that described main agitating device comprises shaft 5 and is arranged on shaft 5, described shaft 5 connects the outer motor 2 arranged of kettle 1, described shaft 3 is positioned at above helical mixing blade 6 and is provided with receiver 4, described secondary agitating device is arranged on bottom kettle 1, described secondary agitating device comprises blade 12, paddle 13, dwang 14 and rotating shaft 15, described rotating shaft 15 arrange kettle 1 bottom and with shaft 5 on the same axis, described dwang 14 is rotationally connected with rotating shaft 15, the top of described dwang 14 arranges blade 12, described blade 12 is provided with two, two described 12 one-tenth, blade V-shapes, angle between two described blades 12 is 90 °, described paddle 13 to be arranged on dwang 14 and to be positioned under blade 12, described heat exchanger 11 is arranged on the inside of kettle 1, the side, outside of described kettle 1 is provided with the cooling water pipe 7 and steam pipe 10 that are connected with heat exchanger 11, opposite side is provided with the heat exchanger exit pipe 17 be connected with heat exchanger 11, described cooling water pipe 7 is provided with cooling water valve 8, described steam pipe 10 is provided with steam valve 9, described heat exchanger exit pipe 17 is provided with heat exchanger exit valve 18, described kettle 1 upper end is provided with gas outlet 19, described waste gas purification and recovery integrated apparatus comprise adsorption/desorption device and condensation recovering device, described condensation recovering device is arranged on the below of adsorption/desorption device, described adsorption/desorption device comprises housing 22, adsorption tube 25, adsorption tube shell side 24, be arranged on the clean gas outlet 21 on housing 22 top, be arranged on side, adsorption tube shell side 24 upper end heat transferring medium import 23 and the heat transferring medium outlet 26 being arranged on adsorption tube shell side 24 lower end opposite side, adsorbent is filled with in described adsorption tube 25, adsorbent adopts granular activated carbon, heat transferring medium is passed in described adsorption tube shell side 24, for absorption, desorption provides cold and heat, described condensation recovering device comprises heat exchanger fin 27, exhaust gas entrance 29, cooling medium inlet 28, cooling medium outlet 30 and solvent collection mouth 31, described heat exchanger fin 27 is connected with solvent collection mouth 31, for reclaiming the solvent of condensation, described exhaust gas entrance 29 is connected with the gas outlet 19 on kettle 1 by pipeline 20.
Operation principle of the present utility model is: in adsorption tube 25, load adsorbent in advance, when industrial chemicals to fall into the receiver 4 be arranged in reactor from charging aperture 3, receiver 4 rotates together along with shaft 5, the industrial chemicals put in reactor is uniformly dispersed, prevent local concentration too high, improve product quality, main agitating device rotarily drives the liquid in rotation flowing in reactor, the blade 12 of secondary agitating device carries out passive rotation under the drive of fluid vortex, and then drive the rotation of the paddle 13 be positioned at equally on dwang 14, the liquid in reactor corner is also flowed, be conducive to the abundant mixing of solution in whole reactor, both the reaction time of reactant had been shortened, reduce energy consumption, dissolution homogeneity is made again to mix further, open steam valve 9 and heat exchanger exit valve 18, steam is made to enter heat exchanger 11, the opening degree of adjustment steam valve 9 controls certain heating power, heat to industrial chemicals, industrial chemicals reacts the harmful exhaust that produces and enters condensation recovering device by the gas outlet 20 of reactor and pipeline 20 from exhaust gas entrance 29, enter in the adsorption tube 25 of adsorption/desorption device after cooling, discharged by clean gas outlet 21 after absorption, after adsorbent is saturated, carrier gas is passed into from clean gas outlet 21, pass into heat medium from heat transferring medium import 23 to adsorption tube shell side 24 to heat up to adsorbent in pipe and carrier gas, desorption gas enters after condensation recovering device carries out solvent recovery and discharges from exhaust gas entrance 29, condensation recovered solvent reclaims from solvent collection mouth 31, heat medium is discharged by heat transferring medium outlet 26, thus realize adsorbent desorption and solvent recovery, add cooling medium by heat transferring medium import 23 to adsorption tube shell side 24 after desorption completes to cool, and export 26 discharges by heat transferring medium, namely an adsorption cycle is completed after system cools.When needing cooling in reactor, opening cooling water valve 8, keeping heat exchanger exit valve 18 to open, lowering the temperature, after dropping to uniform temperature, close cooling water valve 8 and heat exchanger exit valve 18.
To those skilled in the art, obvious the utility model is not limited to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present utility model or essential characteristic, can realize the utility model in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present utility model is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the utility model.Any Reference numeral in claim should be considered as the claim involved by limiting.
In addition, be to be understood that, although this description is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of description is only for clarity sake, those skilled in the art should by description integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (4)
1. one kind with waste gas purification with reclaim the chemical reaction still of integrated apparatus, comprise kettle (1), agitating device, heat exchanger (11) and waste gas purification and reclaim integrated apparatus, it is characterized in that, described kettle (1) side, upper end is provided with charging aperture (3), lower end opposite side is provided with discharging opening (16), described agitating device comprises main agitating device and secondary agitating device, described main agitating device is arranged on the top of kettle (1) inner chamber, described main agitating device comprises shaft (5) and is arranged on the helical mixing blade (6) on shaft (5), described shaft (5) connects the motor (2) that kettle (1) is arranged outward, described shaft (3) is gone up and is positioned at helical mixing blade (6) top and is provided with receiver (4), described secondary agitating device is arranged on kettle (1) bottom, described secondary agitating device comprises blade (12), paddle (13), dwang (14) and rotating shaft (15), described rotating shaft (15) arrange kettle (1) bottom and with shaft (5) on the same axis, described dwang (14) and rotating shaft (15) are rotationally connected, the top of described dwang (14) arranges blade (12), described paddle (13) is arranged on dwang (14) and goes up and be positioned under blade (12), described heat exchanger (11) is arranged on the inside of kettle (1), the side, outside of described kettle (1) is provided with the cooling water pipe (7) and steam pipe (10) that are connected with heat exchanger (11), opposite side is provided with the heat exchanger exit pipe (17) be connected with heat exchanger (11), described kettle (1) upper end is provided with gas outlet (19), described waste gas purification and recovery integrated apparatus comprise adsorption/desorption device and condensation recovering device, described condensation recovering device is arranged on the below of adsorption/desorption device, described adsorption/desorption device comprises housing (22), adsorption tube (25), adsorption tube shell side (24), be arranged on the clean gas outlet (21) on housing (22) top, be arranged on adsorption tube shell side (24) side, upper end heat transferring medium import (23) and be arranged on adsorption tube shell side (24) lower end opposite side heat transferring medium outlet (26), described condensation recovering device comprises heat exchanger fin (27), exhaust gas entrance (29), cooling medium inlet (28), cooling medium outlet (30) and solvent collection mouth (31), described heat exchanger fin (27) is connected with solvent collection mouth (31), described exhaust gas entrance (29) is connected with the gas outlet (19) on kettle (1) by pipeline (20).
2. according to claim 1 with waste gas purification and the chemical reaction still reclaiming integrated apparatus, it is characterized in that, described blade (12) is provided with two, and two described blades (12) become V-shape, and the angle between two described blades (12) is 90 °.
3. according to claim 1 with waste gas purification and the chemical reaction still reclaiming integrated apparatus, it is characterized in that, described cooling water pipe (7) is provided with cooling water valve (8), described steam pipe (10) is provided with steam valve (9), and described heat exchanger exit pipe (17) is provided with heat exchanger exit valve (18).
4. according to claim 1 with waste gas purification and the chemical reaction still reclaiming integrated apparatus, it is characterized in that, described adsorption tube is filled with adsorbent in (25), and adsorbent adopts granular activated carbon.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520061731.7U CN204638187U (en) | 2015-01-23 | 2015-01-23 | A kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520061731.7U CN204638187U (en) | 2015-01-23 | 2015-01-23 | A kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204638187U true CN204638187U (en) | 2015-09-16 |
Family
ID=54090963
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520061731.7U Expired - Fee Related CN204638187U (en) | 2015-01-23 | 2015-01-23 | A kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204638187U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106390828A (en) * | 2016-10-17 | 2017-02-15 | 无锡市日升化工有限公司 | Stirrer realizing uniform stirring and heat dissipation and used for chemical equipment |
| CN111020236A (en) * | 2019-11-30 | 2020-04-17 | 沈阳环境科学研究院 | Method for recovering waste mercury iodide reagent |
-
2015
- 2015-01-23 CN CN201520061731.7U patent/CN204638187U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106390828A (en) * | 2016-10-17 | 2017-02-15 | 无锡市日升化工有限公司 | Stirrer realizing uniform stirring and heat dissipation and used for chemical equipment |
| CN111020236A (en) * | 2019-11-30 | 2020-04-17 | 沈阳环境科学研究院 | Method for recovering waste mercury iodide reagent |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN204074077U (en) | A kind of automatic charging reactor with gas recycling device | |
| CN202921320U (en) | Reaction kettle for experiment | |
| CN204638187U (en) | A kind of with waste gas purification and the chemical reaction still reclaiming integrated apparatus | |
| CN108249737A (en) | A kind of method of microwave reinforced catalytic wet oxidation processing sludge | |
| CN205443312U (en) | Hydrologic cycle oxygenation fermentation cylinder for bio -pharmaceuticals | |
| CN207076283U (en) | A kind of agitating device for chemical emission processing | |
| CN110029555B (en) | Asphalt environment-friendly stirring device for highway construction | |
| CN203976693U (en) | Regenerated rubber digester | |
| CN206474152U (en) | A kind of NBB reaction unit | |
| CN204509136U (en) | The small-sized simulated composting device of a kind of feces of livestock and poultry | |
| CN204208551U (en) | A kind of chemical industry liquid reactions still | |
| CN211492542U (en) | High-pressure foaming machine for processing heat-insulating pipe | |
| CN201813772U (en) | Powdered milk preparation drying system with surplus heat utilization and dust recovery | |
| CN204644042U (en) | A kind of liquid waste treating apparatus of ammonium nitrate production line | |
| CN112370947B (en) | Energy-concerving and environment-protective type nitrile rubber reforms transform waste gas waste heat recovery and utilizes device | |
| CN212119103U (en) | Ammonium perchlorate crystal prevents liquid processing apparatus | |
| CN208279620U (en) | A kind of fermentation optical wave heating film enrichment facility | |
| CN103768890B (en) | A kind of active carbon by chemical method produces the purification of tail gas and recovery system and absorber | |
| CN209451606U (en) | A kind of energy-saving gas drying tower | |
| CN206082528U (en) | High performance fluid mixing stirring reation kettle | |
| CN209597190U (en) | A kind of reaction kettle | |
| CN209069077U (en) | A kind of epoxy hardener cooling device | |
| CN203598823U (en) | Super-gravity reactor | |
| CN204417131U (en) | A kind of device for reclaiming phosphoric acid in activated carbon of phosphoric acid method tail gas | |
| CN204778906U (en) | Waste liquid enrichment facility |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150916 Termination date: 20180123 |