CN204637641U - A kind of labyrinth type hypergravity liquid-liquid extraction separator - Google Patents
A kind of labyrinth type hypergravity liquid-liquid extraction separator Download PDFInfo
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- CN204637641U CN204637641U CN201520216992.1U CN201520216992U CN204637641U CN 204637641 U CN204637641 U CN 204637641U CN 201520216992 U CN201520216992 U CN 201520216992U CN 204637641 U CN204637641 U CN 204637641U
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- 238000000622 liquid--liquid extraction Methods 0.000 title claims abstract description 15
- 238000000638 solvent extraction Methods 0.000 title claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 93
- 238000012856 packing Methods 0.000 claims abstract description 79
- 238000002156 mixing Methods 0.000 claims abstract description 26
- 238000000926 separation method Methods 0.000 claims abstract description 15
- 239000000945 filler Substances 0.000 claims abstract description 13
- 238000000227 grinding Methods 0.000 claims description 62
- 230000003068 static effect Effects 0.000 claims description 15
- 238000005191 phase separation Methods 0.000 claims description 11
- 229910001220 stainless steel Inorganic materials 0.000 claims description 5
- 239000010935 stainless steel Substances 0.000 claims description 5
- -1 polytetrafluoroethylene Polymers 0.000 claims description 4
- 238000009434 installation Methods 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 229920000915 polyvinyl chloride Polymers 0.000 claims description 3
- 239000004800 polyvinyl chloride Substances 0.000 claims description 3
- 239000004743 Polypropylene Substances 0.000 claims description 2
- 238000005260 corrosion Methods 0.000 claims description 2
- 230000007797 corrosion Effects 0.000 claims description 2
- 239000003822 epoxy resin Substances 0.000 claims description 2
- 239000004033 plastic Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 claims description 2
- 229920000647 polyepoxide Polymers 0.000 claims description 2
- 229920001155 polypropylene Polymers 0.000 claims description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 2
- 238000000605 extraction Methods 0.000 abstract description 9
- 230000035484 reaction time Effects 0.000 abstract description 4
- 238000011049 filling Methods 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract 2
- 230000010354 integration Effects 0.000 abstract 1
- 239000010410 layer Substances 0.000 description 44
- 239000012071 phase Substances 0.000 description 25
- 239000012530 fluid Substances 0.000 description 17
- 238000010586 diagram Methods 0.000 description 12
- 230000000694 effects Effects 0.000 description 5
- 239000007921 spray Substances 0.000 description 5
- 238000000889 atomisation Methods 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000007769 metal material Substances 0.000 description 2
- 230000002572 peristaltic effect Effects 0.000 description 2
- 239000002356 single layer Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
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Abstract
Description
技术领域 technical field
本实用新型涉及一种迷宫式超重力液-液萃取分离器,属于强化传质技术领域。 The utility model relates to a labyrinth type supergravity liquid-liquid extraction separator, which belongs to the technical field of mass transfer enhancement.
背景技术 Background technique
超重力液-液萃取分离技术,由于其具有较好的萃取效果,已经被广泛应用于生物化学和生物化工领域。但是目前的设备在萃取的过程中停留时间过短,而且其单层填料结构使得传质面积过小。此外,还存在设备制造成本高、体积庞大、萃取速率慢、萃取效率低很多不足处。目前,在冶金领域的人才和设备较少,且现有技术的超重力工程技术装置大部分为整个转子一起转动,且大多为单层填料结构,故混合和传质不彻底,在萃取的过程中停留时间较短。 High-gravity liquid-liquid extraction separation technology has been widely used in the fields of biochemistry and biochemical industry because of its good extraction effect. However, the residence time of the current equipment is too short during the extraction process, and its single-layer packing structure makes the mass transfer area too small. In addition, there are many shortcomings such as high equipment manufacturing cost, bulky volume, slow extraction rate and low extraction efficiency. At present, there are few talents and equipment in the field of metallurgy, and most of the existing high-gravity engineering technology devices rotate with the entire rotor, and most of them have a single-layer packing structure, so the mixing and mass transfer are not thorough. shorter residence time.
另外,中国专利申请CN101254355A和CN1116125A公开了一种转动分布形式的液体分布器,即转轴为空心结构并没有出液小孔,液体由两相进液管进入空心轴,转轴内的液体随转轴一起转动,在离心力的作用下,由转轴上的孔送入填料层。虽然这种液体分布器提高了操作弹性,但是由于转轴半径的限制,液体在空心轴内受到的离心力小,液体处理量小。 In addition, Chinese patent applications CN101254355A and CN1116125A disclose a liquid distributor in the form of rotating distribution, that is, the rotating shaft is a hollow structure and has no liquid outlet holes, and the liquid enters the hollow shaft through the two-phase liquid inlet pipe, and the liquid in the rotating shaft is together Rotating, under the action of centrifugal force, it is sent into the packing layer through the hole on the rotating shaft. Although this kind of liquid distributor improves the operating flexibility, due to the limitation of the radius of the rotating shaft, the centrifugal force on the liquid in the hollow shaft is small, and the liquid handling capacity is small.
发明内容 Contents of the invention
本实用新型针对上述现有技术的缺点,提供了一种迷宫式超重力液液萃取分离器,其包括外壳1、填料螺旋管2、混合传质机构、分离收集机构、顶盖板12、底座13、轴承座套18、轴24、电机33;顶盖板12通过螺钉连接固定在外壳1上端,底座13设置在外壳1腔体中且其下端与轴24固连,混合传质机构设置在底座13上,分离收集机构设置在底座13下端并与外壳1下端连接,填料螺旋管2固定在外壳1内侧,轴承座套18与旋转开关17为螺纹副动连接,轴承座套18套装在轴24上,轴承座套18通过螺钉连接固定在机架34上,电机33安装在机架34上并通过同步带26与轴24上的小带轮25连接,带动轴24转动; The utility model aims at the shortcomings of the above-mentioned prior art, and provides a labyrinth type supergravity liquid-liquid extraction separator, which includes a casing 1, a packing spiral tube 2, a mixing mass transfer mechanism, a separation and collection mechanism, a top cover plate 12, a base 13. Bearing sleeve 18, shaft 24, motor 33; top cover plate 12 is fixed on the upper end of shell 1 through screw connection, base 13 is set in the cavity of shell 1 and its lower end is fixedly connected with shaft 24, and the mixing mass transfer mechanism is set on On the base 13, the separation and collection mechanism is arranged at the lower end of the base 13 and connected with the lower end of the casing 1, the packing spiral tube 2 is fixed inside the casing 1, the bearing seat sleeve 18 and the rotary switch 17 are threaded secondary dynamic connections, and the bearing seat sleeve 18 is set on the shaft 24, the bearing seat cover 18 is fixed on the frame 34 by screw connection, the motor 33 is installed on the frame 34 and is connected with the small pulley 25 on the shaft 24 through the timing belt 26, and drives the shaft 24 to rotate;
其中混合传质机构包括进料行星叶轮混合装置、传质装置、锥形磨液轮,传质装置设在进料行星叶轮混合装置和锥形磨液轮之间,其中进料行星叶轮混合装置包括两相进液管11、至少3个小叶轮10、行星轮19、固定柱20、太阳轮21、行星架22,固定柱20下端与底座13固定连接,上端与行星架22固定连接,呈圆周对称分布;行星轮19套装在小叶轮10上并设置在行星架22上方,小叶轮10下端通过轴承与底座13相连;太阳轮21固定在行星架22上并与行星轮19相啮合;两相进液管11经过行星架22向下延伸至底座上方且不与底座接触;所述传质装置包括动盘外填料层5、静盘填料层6、大叶轮7、鼓形挡板8、动盘内填料层9,动盘内填料层9、鼓形挡板8、大叶轮7、动盘外填料层5依次由内到外固定在底座13上;动盘内填料层9设置在小叶轮10外侧,鼓形挡板8设置在动盘内填料层9与大叶轮7之间,静盘填料层6设置在大叶轮7与动盘外填料层5之间,静盘填料层6固定在顶盖板12上;所述锥形磨液轮包括锥形磨液内轮4和锥形磨液外轮3,锥形磨液外轮3套装在锥形磨液内轮4外并构成相对旋转配合关系,锥形磨液内轮4固定在顶盖板12上,锥形磨液外轮3固定在底座13上,锥形磨液外轮3上端的出液孔与填料螺旋管2入口相通; The mixing and mass transfer mechanism includes a feeding planetary impeller mixing device, a mass transfer device, and a conical grinding wheel. The mass transfer device is arranged between the feeding planetary impeller mixing device and the conical grinding wheel. The feeding planetary impeller mixing device It includes a two-phase liquid inlet pipe 11, at least three small impellers 10, a planetary wheel 19, a fixed column 20, a sun gear 21, and a planetary carrier 22. The lower end of the fixed column 20 is fixedly connected to the base 13, and the upper end is fixedly connected to the planetary carrier 22. Circumferentially symmetrical distribution; the planetary wheel 19 is set on the small impeller 10 and arranged above the planetary carrier 22, and the lower end of the small impeller 10 is connected to the base 13 through a bearing; the sun wheel 21 is fixed on the planetary carrier 22 and meshed with the planetary wheel 19; The phase inlet pipe 11 extends downwards to the top of the base through the planet carrier 22 and does not contact the base; the mass transfer device includes the outer packing layer 5 of the moving disk, the packing layer 6 of the static disk, the large impeller 7, the drum baffle 8, The inner packing layer 9 of the moving disk, the inner packing layer 9 of the moving disk, the drum baffle plate 8, the large impeller 7, and the outer packing layer 5 of the moving disk are fixed on the base 13 from the inside to the outside in sequence; the inner packing layer 9 of the moving disk is arranged on the small Outside the impeller 10, the drum-shaped baffle 8 is arranged between the inner packing layer 9 of the moving disk and the large impeller 7, the packing layer 6 of the static disk is arranged between the large impeller 7 and the outer packing layer 5 of the moving disk, and the packing layer 6 of the static disk is fixed On the top cover plate 12; the conical grinding fluid wheel includes a conical grinding fluid inner wheel 4 and a conical grinding fluid outer wheel 3, and the conical grinding fluid outer wheel 3 is set outside the conical grinding fluid inner wheel 4 and forms a relative rotation Cooperating relationship, the conical grinding liquid inner wheel 4 is fixed on the top cover plate 12, the conical grinding liquid outer wheel 3 is fixed on the base 13, and the liquid outlet hole at the upper end of the conical grinding liquid outer wheel 3 communicates with the inlet of the packing spiral tube 2;
所述分离收集机构包括分相槽14、弹性开关15、收集槽16;填料螺旋管2的出口与分相槽14相通,收集槽16设置在分相槽14下方,收集槽16由内外两个环形槽组成,内侧出料导管23-1和外侧出料导管23-2呈周向交叉均匀分布在分相槽14的内侧和外侧,内侧出料导管23-1与收集槽16的内槽35相连通,外侧出料导管23-2与收集槽16的外槽36相连通,弹性开关15穿过分相槽14底部的安装孔分别与内侧出料导管23-1、外侧出料导管23-2垂直相交,实现控制内侧出料导管23-1或外侧出料导管23-2开闭功能,旋转开关17设置在收集槽16内侧并与弹性开关15为点接触,内侧出料导管23-1、外侧出料导管23-2可以旋转角度。 Described separating and collecting mechanism comprises phase-splitting tank 14, elastic switch 15, collecting tank 16; The outlet of packing helical tube 2 communicates with phase-splitting tank 14, and collecting tank 16 is arranged below phase-splitting tank 14, and collecting tank 16 is made of two inside and outside. Composed of annular grooves, the inner discharge conduit 23-1 and the outer discharge conduit 23-2 are circumferentially intersected and evenly distributed on the inside and outside of the phase separation tank 14, the inner discharge conduit 23-1 and the inner groove 35 of the collection tank 16 The outer discharge conduit 23-2 is connected with the outer groove 36 of the collection tank 16, and the elastic switch 15 passes through the installation hole at the bottom of the phase separation tank 14 to connect with the inner discharge conduit 23-1 and the outer discharge conduit 23-2 respectively. Vertically intersect to realize the function of controlling the opening and closing of the inner discharge conduit 23-1 or the outer discharge conduit 23-2. The rotary switch 17 is arranged on the inside of the collection tank 16 and is in point contact with the elastic switch 15. The inner discharge conduit 23-1, Outer discharge conduit 23-2 can rotate angle.
所述小叶轮10由小叶轮轴27和固定在轴上的横截面呈三角形的叶片28构成。 The small impeller 10 is composed of a small impeller shaft 27 and a blade 28 fixed on the shaft with a triangular cross section.
所述大叶轮7为中空圆筒状,其上开有两层百叶窗叶片29,百叶窗叶片开启角度为3o~5o。 The big impeller 7 is hollow cylindrical, on which there are two layers of louver blades 29, and the opening angle of the louver blades is 3 ° ~5 ° .
所述鼓形挡板8为中空鼓型结构,其中间部分为多孔圆环结构。 The drum-shaped baffle 8 is a hollow drum-shaped structure, and its middle part is a porous ring structure.
所述锥形磨液外轮3为中空圆锥台形,轴向磨条Ⅰ31均匀分布在其内表面,锥形磨液外轮3顶端带有出液孔30且与填料螺旋管2相通。 The conical grinding liquid outer wheel 3 is hollow truncated cone, and the axial grinding bars I31 are evenly distributed on its inner surface.
所述锥形磨液内轮4为中空圆锥台形,轴向磨条轴向磨条Ⅱ32均匀分布在其外表面。 The conical grinding liquid inner wheel 4 is hollow truncated cone, and the axial grinding bars II 32 are evenly distributed on its outer surface.
所述动盘内填料层9、静盘填料层6、动盘外填料层5均由内外两块环形多孔板构成,且两块环形多孔板之间填塞有填料,多孔板为不锈钢、特种钢等金属材质,填充物为聚氯乙烯、聚四氟乙烯、环氧树脂、聚丙烯等非金属材质,填料具体材质根据具体操作温度和介质选择,填料的设置增加了传质接触面积。 The inner packing layer 9 of the moving disc, the packing layer 6 of the static disc, and the outer packing layer 5 of the moving disc are all composed of two annular porous plates inside and outside, and fillers are filled between the two annular porous plates. The porous plates are made of stainless steel or special steel. And other metal materials, the filler is polyvinyl chloride, polytetrafluoroethylene, epoxy resin, polypropylene and other non-metallic materials, the specific material of the filler is selected according to the specific operating temperature and medium, and the setting of the filler increases the mass transfer contact area.
所述填料螺旋管2为螺旋状不锈钢金属软管或耐腐蚀塑料软管。 The packing spiral pipe 2 is a spiral stainless steel metal hose or a corrosion-resistant plastic hose.
所述收集槽16由内外两个环形槽组成,外槽收集重相液体,内槽收集轻相液体。 The collection tank 16 is composed of two annular tanks, the outer tank collects the heavy phase liquid, and the inner tank collects the light phase liquid.
本实用新型装置使用时,开启电机33电源,调节转子转速,电机33带动轴24转动,同时带动底座13的旋转;通过蠕动泵调节两相液体的压力和流速后,将两相液体分别通入2个两相进液管11后实现逆流对撞,对撞流再经过小叶轮10的紊流阻挡改变运动轨迹后被甩到动盘内填料层9,在动盘内填料层9内扩大了传质面积;在离心力的作用下,混合液体喷向鼓形挡板8,液体收集到鼓形挡板8底部,并通过其中间喷孔向外喷射,形成二次雾化。混合液体甩到大叶轮7后,因为其百叶窗叶片29的偏角作用,产生负压,使液体产生向内的趋势,形成部分逆流对撞;混合液体再甩到静盘填料层6上,最后甩到动盘外填料层5上,反应后由于重力的作用液体下落。在离心力的作用下,混合液体喷向锥形磨液内轮4并汇聚于其底部,在锥形磨液内轮4和锥形磨液外轮3的配合作用下,混合液体被带到锥形磨液外轮3的上端,通过锥形磨液外轮3上端的出液孔30流到填料螺旋管2中。混合液体经过填料螺旋管2后流入分相槽14中,在分相槽14的内侧和外侧均匀分布有内侧出料导管23-1、外侧出料导管23-2,内侧出料导管23-1与收集槽16的内槽35相连通,外侧出料导管23-2与收集槽16的外槽36相连通,由于液体密度不同重相流体将流入收集槽16的外槽,轻相流体将流入收集槽16的内槽,在收集槽16的内槽和外槽分别收集了最终产物。 When the utility model device is in use, turn on the power supply of the motor 33, adjust the rotor speed, the motor 33 drives the shaft 24 to rotate, and simultaneously drives the rotation of the base 13; after adjusting the pressure and flow rate of the two-phase liquid through the peristaltic pump, the two-phase liquid is respectively passed into After the two two-phase liquid inlet pipes 11, countercurrent collision is realized, and the collision flow is thrown to the inner packing layer 9 of the moving disk after being blocked by the turbulent flow of the small impeller 10 to change the trajectory, and the inner packing layer 9 of the moving disk expands Mass transfer area; under the action of centrifugal force, the mixed liquid is sprayed to the drum baffle 8, the liquid is collected at the bottom of the drum baffle 8, and sprayed outward through the middle nozzle hole to form secondary atomization. After the mixed liquid is thrown to the large impeller 7, because of the deflection effect of the louver blades 29, a negative pressure is generated, which makes the liquid tend to inward, forming a partial countercurrent collision; the mixed liquid is then thrown to the static disk packing layer 6, and finally Throw it on the outer packing layer 5 of the moving disk, and after the reaction, the liquid will fall due to the effect of gravity. Under the action of centrifugal force, the mixed liquid sprays to the conical grinding liquid inner wheel 4 and gathers at its bottom. Under the cooperation of the conical grinding liquid inner wheel 4 and the conical grinding liquid outer wheel 3, the mixed liquid is brought to the cone The upper end of the grinding liquid outer wheel 3 flows into the filler spiral tube 2 through the liquid outlet hole 30 at the upper end of the conical grinding liquid outer wheel 3 . The mixed liquid flows into the phase-splitting tank 14 after passing through the packing spiral tube 2, and the inside and outside of the phase-splitting tank 14 are evenly distributed with an inner discharge conduit 23-1, an outer discharge conduit 23-2, and an inner discharge conduit 23-1. It communicates with the inner tank 35 of the collecting tank 16, and the outer discharge conduit 23-2 communicates with the outer tank 36 of the collecting tank 16. Due to the difference in liquid density, the heavy phase fluid will flow into the outer tank of the collecting tank 16, and the light phase fluid will flow into the outer tank of the collecting tank 16. In the inner tank of the collecting tank 16, the final product is collected in the inner tank and the outer tank of the collecting tank 16, respectively.
本实用新型中四个两相进液管11两两对喷;行星轮19带动小叶轮10即公转又自转; In the utility model, four two-phase liquid inlet pipes 11 spray in pairs; the planetary wheel 19 drives the small impeller 10 to revolve and rotate;
本实用新型有益的效果是:1、高效萃取的同时兼顾两相分离;2、传质装置中的多层填料结构增大了两相液体的传质面积,复杂的填料层结构使混合更加均匀,延长了反应时间,提高了萃取率;3、带多喷孔的鼓形挡板起到收集液体、集中喷洒的效果,实现了两相混合的二次雾化;4、大叶轮的百叶窗叶片在旋转条件下将产生负压,让液体向内喷射,实现二次逆流对撞;5、锥形磨液内轮通过与锥形磨液外轮的磨条配合,能使液体顺着锥面上升并从锥形磨液外轮上端的孔流入带填料螺旋管,延长反应时间。 The beneficial effects of the utility model are: 1. The separation of the two phases is taken into account while the extraction is efficient; 2. The multi-layer packing structure in the mass transfer device increases the mass transfer area of the two-phase liquid, and the complex packing layer structure makes the mixing more uniform , which prolongs the reaction time and improves the extraction rate; 3. The drum-shaped baffle with multi-spray holes plays the role of collecting liquid and spraying concentratedly, realizing the secondary atomization of two-phase mixing; 4. The louver blades of the large impeller Negative pressure will be generated under the condition of rotation, so that the liquid is sprayed inward to realize the second countercurrent collision; 5. The conical grinding liquid inner wheel can make the liquid rise along the cone surface by cooperating with the grinding rod of the conical grinding liquid outer wheel And flow into the spiral tube with packing from the hole at the upper end of the conical grinding liquid outer wheel to prolong the reaction time.
附图说明 Description of drawings
图1是本实用新型迷宫式超重力液液萃取分离器结构示意图; Fig. 1 is a schematic diagram of the structure of a labyrinth type supergravity liquid-liquid extraction separator of the present invention;
图2是本实用新型进料行星叶轮混合装置结构示意图; Fig. 2 is a schematic structural view of the feeding planetary impeller mixing device of the utility model;
图3是本实用新型传质装置及锥形磨液轮的结构示意图; Fig. 3 is a structural schematic diagram of the mass transfer device and the conical grinding wheel of the utility model;
图4是本实用新型传质装置及锥形磨液轮设置结构示意图; Fig. 4 is a schematic diagram of the arrangement structure of the mass transfer device and the conical grinding wheel of the present invention;
图5是本实用新型分离收集机构的剖面结构示意图; Fig. 5 is a schematic cross-sectional structure diagram of the separation and collection mechanism of the present utility model;
图6是本实用新型分离收集机构的结构示意图; Fig. 6 is a schematic structural view of the separation and collection mechanism of the utility model;
图7是本实用新型小叶轮结构示意图; Fig. 7 is a structural schematic diagram of the small impeller of the present invention;
图8是本实用新型大叶轮的结构示意图; Fig. 8 is a structural schematic diagram of the large impeller of the present invention;
图9是本实用新型大叶轮的俯视结构示意图; Fig. 9 is a top view structural schematic diagram of the large impeller of the present invention;
图10是本实用新型鼓形挡板结构示意图; Fig. 10 is a structural schematic diagram of a drum-shaped baffle of the present invention;
图11是本实用新型锥形磨液外轮结构示意图; Fig. 11 is a schematic diagram of the structure of the conical abrasive liquid outer wheel of the utility model;
图12是本实用新型锥形磨液内轮结构示意图; Fig. 12 is a schematic diagram of the structure of the conical grinding fluid inner wheel of the utility model;
图13是本实用新型填料螺旋管结构示意图; Fig. 13 is a structural schematic diagram of a packing spiral tube of the present invention;
图14是本实用新型收集槽结构示意图; Fig. 14 is a schematic diagram of the structure of the collection tank of the present invention;
图中:1-外壳,2-填料螺旋管,3-锥形磨液外轮,4-锥形磨液内轮,5-动盘外填料层,6-静盘填料层,7-大叶轮,8-鼓形挡板,9-动盘内填料层,10-小叶轮,11-两相进液管,12-顶盖板,13-底座,14-分相槽,15-弹性开关,16-收集槽,17-旋转开关,18-轴承座套,19-行星轮,20-固定柱,21-太阳轮,22-行星架,23-1-内侧出料导管,23-2-外侧出料导管,24-轴,25-小带轮,26-同步带,27-小叶轮轴,28-叶片,29-百叶窗叶片,30-出液孔,31-轴向磨条Ⅰ,32-轴向磨条Ⅱ,33-电机,34-机架,35-内槽,36-外槽。 In the figure: 1-housing, 2-filling spiral tube, 3-conical grinding liquid outer wheel, 4-conical grinding liquid inner wheel, 5-moving disc outer packing layer, 6-static disc packing layer, 7-big impeller, 8-Drum-shaped baffle, 9-Packing layer of moving disk, 10-Small impeller, 11-Two-phase liquid inlet pipe, 12-Top cover plate, 13-Base, 14-Phase separation tank, 15-Elastic switch, 16 -Collecting tank, 17-rotary switch, 18-bearing seat sleeve, 19-planetary wheel, 20-fixed column, 21-sun gear, 22-planetary frame, 23-1-inside discharge guide, 23-2-outside discharge Material conduit, 24-shaft, 25-small pulley, 26-synchronous belt, 27-small impeller shaft, 28-blade, 29-louver blade, 30-liquid outlet, 31-axial grinding bar Ⅰ, 32-axial Grinding bar II, 33-motor, 34-frame, 35-inner tank, 36-outer tank.
具体实施方法Specific implementation method
下面通过附图和实施例对本实用新型作进一步详细说明,但本实用新型的保护范围不局限于所述内容。 The utility model will be described in further detail below through the accompanying drawings and embodiments, but the protection scope of the utility model is not limited to the content described.
实施例1: 如图1~14所示,本迷宫式超重力液液萃取分离器包括外壳1、填料螺旋管2、混合传质机构、分离收集机构、顶盖板12、底座13、轴承座套18、轴24、电机33;顶盖板12通过螺钉连接固定在外壳1上端,底座13设置在外壳1腔体中且其下端与轴24固连,混合传质机构设置在底座13上,分离收集机构设置在底座13下端并与外壳1下端连接,填料螺旋管2固定在外壳1内侧,轴承座套18与旋转开关17为螺纹副动连接,轴承座套18套装在轴24上,轴承座套18通过螺钉连接固定在机架34上,电机33安装在机架34上并通过同步带26与轴24上的小带轮25连接,带动轴24转动; Embodiment 1: As shown in Figures 1 to 14, this labyrinth type supergravity liquid-liquid extraction separator includes a shell 1, a packing spiral tube 2, a mixing and mass transfer mechanism, a separation and collection mechanism, a top cover plate 12, a base 13, and a bearing seat Cover 18, shaft 24, motor 33; top cover plate 12 is fixed on the upper end of casing 1 by screw connection, base 13 is arranged in the cavity of casing 1 and its lower end is fixedly connected with shaft 24, and the mixing mass transfer mechanism is arranged on the base 13, The separation and collection mechanism is arranged at the lower end of the base 13 and connected with the lower end of the casing 1, the packing spiral tube 2 is fixed inside the casing 1, the bearing seat sleeve 18 and the rotary switch 17 are threaded auxiliary dynamic connections, the bearing seat sleeve 18 is set on the shaft 24, and the bearing The seat cover 18 is fixed on the frame 34 by screw connection, the motor 33 is installed on the frame 34 and is connected with the small pulley 25 on the shaft 24 through the timing belt 26, and drives the shaft 24 to rotate;
其中混合传质机构包括进料行星叶轮混合装置、传质装置、锥形磨液轮,传质装置设在进料行星叶轮混合装置和锥形磨液轮之间,其中进料行星叶轮混合装置包括4个两相进液管11、3个小叶轮10、行星轮19、固定柱20、太阳轮21、行星架22,固定柱20下端与底座13固定连接,上端与行星架22固定连接,呈圆周对称分布;行星轮19套装在小叶轮10上并设置在行星架22上方,小叶轮10下端通过轴承与底座13相连;太阳轮21固定在行星架22上并与行星轮19相啮合;两相进液管11经过行星架22向下延伸至底座上方且不与底座接触;所述传质装置包括动盘外填料层5、静盘填料层6、大叶轮7、鼓形挡板8、动盘内填料层9,动盘内填料层9、鼓形挡板8、大叶轮7、动盘外填料层5依次由内到外固定在底座13上;动盘内填料层9设置在小叶轮10外侧,鼓形挡板8设置在动盘内填料层9与大叶轮7之间,静盘填料层6设置在大叶轮7与动盘外填料层5之间,静盘填料层6固定在顶盖板12上;所述锥形磨液轮包括锥形磨液内轮4和锥形磨液外轮3,锥形磨液外轮3套装在锥形磨液内轮4外并构成相对旋转配合关系,锥形磨液内轮4固定在顶盖板12上,锥形磨液外轮3固定在底座13上,锥形磨液外轮3上端的出液孔与填料螺旋管2入口相通; The mixing and mass transfer mechanism includes a feeding planetary impeller mixing device, a mass transfer device, and a conical grinding wheel. The mass transfer device is arranged between the feeding planetary impeller mixing device and the conical grinding wheel. The feeding planetary impeller mixing device It includes four two-phase liquid inlet pipes 11, three small impellers 10, a planetary wheel 19, a fixed column 20, a sun gear 21, and a planetary carrier 22. The lower end of the fixed column 20 is fixedly connected to the base 13, and the upper end is fixedly connected to the planetary carrier 22. Circumferentially symmetrical distribution; the planetary wheel 19 is set on the small impeller 10 and arranged above the planetary carrier 22, the lower end of the small impeller 10 is connected to the base 13 through a bearing; the sun wheel 21 is fixed on the planetary carrier 22 and meshed with the planetary wheel 19; The two-phase liquid inlet pipe 11 extends downwards to the top of the base through the planet carrier 22 and does not contact the base; the mass transfer device includes the outer packing layer 5 of the moving disk, the packing layer 6 of the static disk, the large impeller 7, and the drum baffle 8 1. The inner packing layer 9 of the moving disk, the inner packing layer 9 of the moving disk, the drum baffle 8, the large impeller 7, and the outer packing layer 5 of the moving disk are fixed on the base 13 from the inside to the outside in sequence; the inner packing layer 9 of the moving disk is arranged on Outside the small impeller 10, the drum-shaped baffle 8 is arranged between the inner packing layer 9 of the moving disk and the big impeller 7, the packing layer 6 of the static disk is arranged between the big impeller 7 and the outer packing layer 5 of the moving disk, and the packing layer 6 of the static disk It is fixed on the top cover plate 12; the conical grinding fluid wheel includes a conical grinding fluid inner wheel 4 and a conical grinding fluid outer wheel 3, and the conical grinding fluid outer wheel 3 is set outside the conical grinding fluid inner wheel 4 and forms a relative Rotation fit relationship, the conical abrasive liquid inner wheel 4 is fixed on the top cover plate 12, the conical abrasive liquid outer wheel 3 is fixed on the base 13, and the liquid outlet hole at the upper end of the conical abrasive liquid outer wheel 3 communicates with the inlet of the packing spiral tube 2;
所述分离收集机构包括分相槽14、弹性开关15、收集槽16;填料螺旋管2的出口与分相槽14相通,收集槽16设置在分相槽14下方,收集槽16由内外两个环形槽组成,内侧出料导管23-1和外侧出料导管23-2呈周向交叉均匀分布在分相槽14的内侧和外侧,内侧出料导管23-1与收集槽16的内槽35相连通,外侧出料导管23-2与收集槽16的外槽36相连通,弹性开关15穿过分相槽14底部的安装孔分别与内侧出料导管23-1、外侧出料导管23-2垂直相交,实现控制内侧出料导管23-1或外侧出料导管23-2开闭功能,旋转开关17设置在收集槽16内侧并与弹性开关15为点接触,内侧出料导管23-1、外侧出料导管23-2可以旋转角度。 Described separating and collecting mechanism comprises phase-splitting tank 14, elastic switch 15, collecting tank 16; The outlet of packing helical tube 2 communicates with phase-splitting tank 14, and collecting tank 16 is arranged below phase-splitting tank 14, and collecting tank 16 is made of two inside and outside. Composed of annular grooves, the inner discharge conduit 23-1 and the outer discharge conduit 23-2 are circumferentially intersected and evenly distributed on the inside and outside of the phase separation tank 14, the inner discharge conduit 23-1 and the inner groove 35 of the collection tank 16 The outer discharge conduit 23-2 is connected with the outer groove 36 of the collection tank 16, and the elastic switch 15 passes through the installation hole at the bottom of the phase separation tank 14 to connect with the inner discharge conduit 23-1 and the outer discharge conduit 23-2 respectively. Vertically intersect to realize the function of controlling the opening and closing of the inner discharge conduit 23-1 or the outer discharge conduit 23-2. The rotary switch 17 is arranged on the inside of the collection tank 16 and is in point contact with the elastic switch 15. The inner discharge conduit 23-1, Outer discharge conduit 23-2 can rotate angle.
所述小叶轮10由小叶轮轴27和固定在轴上的横截面呈三角形的叶片28构成;大叶轮7为中空圆筒状,其上开有两层百叶窗叶片29,百叶窗叶片开启角度为3o~5o;鼓形挡板8为中空鼓型结构,其中间部分为多孔圆环结构;锥形磨液外轮3为中空圆锥台形,轴向磨条Ⅰ31均匀分布在其内表面,锥形磨液外轮3顶端带有出液孔30且与填料螺旋管2相通;锥形磨液内轮4为中空圆锥台形,轴向磨条轴向磨条Ⅱ32均匀分布在其外表面;动盘内填料层9、静盘填料层6、动盘外填料层5均由内外两块环形多孔板构成,且两块环形多孔板之间填塞有填料,多孔板为不锈钢,填充物为聚氯乙烯,填料的设置增加了传质接触面积;所述填料螺旋管2为螺旋状不锈钢金属软管;所述收集槽16由内外两个环形槽组成,外槽收集重相液体,内槽收集轻相液体。 The small impeller 10 is composed of a small impeller shaft 27 and a blade 28 with a triangular cross-section fixed on the shaft; the large impeller 7 is a hollow cylinder with two layers of louver blades 29 on it, and the opening angle of the louver blades is 3 ° ~5 o ; the drum-shaped baffle 8 is a hollow drum-shaped structure, and its middle part is a porous ring structure; the conical grinding fluid outer wheel 3 is hollow and frustum-shaped, and the axial grinding bars I31 are evenly distributed on its inner surface, and the conical grinding fluid The top of the liquid outer wheel 3 has a liquid outlet hole 30 and communicates with the packing spiral tube 2; the conical grinding liquid inner wheel 4 is a hollow truncated cone, and the axial grinding bars II 32 are evenly distributed on its outer surface; Layer 9, static disk packing layer 6, and moving disk outer packing layer 5 are all composed of two annular porous plates inside and outside, and fillers are filled between the two annular porous plates. The porous plate is made of stainless steel, and the filler is polyvinyl chloride. The setting of the mass transfer contact area increases; the packing spiral tube 2 is a spiral stainless steel metal hose; the collection tank 16 is composed of two inner and outer annular grooves, the outer groove collects the heavy phase liquid, and the inner groove collects the light phase liquid.
本实用新型装置使用时,开启电机33电源,调节转子转速,电机33带动轴24转动,同时带动底座13的旋转;通过蠕动泵调节两相液体的压力和流速后,将两相液体分别通入2个两相进液管11后实现逆流对撞,对撞流再经过3个小叶轮10的紊流阻挡改变运动轨迹后被甩到动盘内填料层9,在动盘内填料层9内扩大了传质面积;在离心力的作用下,混合液体喷向鼓形挡板8,液体收集到鼓形挡板8底部,并通过其中间喷孔向外喷射,形成二次雾化。混合液体甩到大叶轮7后,因为其百叶窗叶片29的偏角作用,产生负压,使液体产生向内的趋势,形成部分逆流对撞;混合液体再甩到静盘填料层6上,最后甩到动盘外填料层5上,反应后由于重力的作用液体下落。在离心力的作用下,混合液体喷向锥形磨液内轮4并汇聚于其底部,在锥形磨液内轮4和锥形磨液外轮3的配合作用下,混合液体被带到锥形磨液外轮3的上端,通过锥形磨液外轮3上端的出液孔30流到填料螺旋管2中。混合液体经过填料螺旋管2后流入分相槽14中,在分相槽14的内侧和外侧均匀分布有内侧出料导管23-1、外侧出料导管23-2,内侧出料导管23-1与收集槽16的内槽35相连通,外侧出料导管23-2与收集槽16的外槽36相连通,由于液体密度不同重相流体将流入收集槽16的外槽,轻相流体将流入收集槽16的内槽,在收集槽16的内槽和外槽分别收集了最终产物。 When the utility model device is in use, turn on the power supply of the motor 33, adjust the rotor speed, the motor 33 drives the shaft 24 to rotate, and simultaneously drives the rotation of the base 13; after adjusting the pressure and flow rate of the two-phase liquid through the peristaltic pump, the two-phase liquid is respectively passed into After the two two-phase liquid inlet pipes 11, the countercurrent collision is realized, and the collision flow is thrown to the inner packing layer 9 of the moving disk after passing through the turbulent flow of the three small impellers 10 to change the trajectory, and then the inner packing layer 9 of the moving disk The mass transfer area is enlarged; under the action of centrifugal force, the mixed liquid is sprayed to the drum-shaped baffle 8, and the liquid is collected at the bottom of the drum-shaped baffle 8, and sprayed outward through the middle spray hole to form secondary atomization. After the mixed liquid is thrown to the large impeller 7, because of the deflection effect of the louver blades 29, a negative pressure is generated, which makes the liquid tend to inward, forming a partial countercurrent collision; the mixed liquid is then thrown to the static disk packing layer 6, and finally Throw it on the outer packing layer 5 of the moving disk, and after the reaction, the liquid will fall due to the effect of gravity. Under the action of centrifugal force, the mixed liquid sprays to the conical grinding liquid inner wheel 4 and gathers at its bottom. Under the cooperation of the conical grinding liquid inner wheel 4 and the conical grinding liquid outer wheel 3, the mixed liquid is brought to the cone The upper end of the grinding liquid outer wheel 3 flows into the filler spiral tube 2 through the liquid outlet hole 30 at the upper end of the conical grinding liquid outer wheel 3 . The mixed liquid flows into the phase-separation tank 14 after passing through the packing spiral tube 2, and the inside and outside of the phase-separation tank 14 are evenly distributed with an inner discharge conduit 23-1, an outer discharge conduit 23-2, and an inner discharge conduit 23-1. It communicates with the inner tank 35 of the collecting tank 16, and the outer discharge conduit 23-2 communicates with the outer tank 36 of the collecting tank 16. Due to the difference in liquid density, the heavy phase fluid will flow into the outer tank of the collecting tank 16, and the light phase fluid will flow into the outer tank of the collecting tank 16. In the inner tank of the collecting tank 16, the final product is collected in the inner tank and the outer tank of the collecting tank 16, respectively.
由于液相在转子内经历了动盘—静盘—动盘的反复过程,不但增加了传质、传热及反应接触面积,而且适当延长了两相在转子内的反应时间。 Because the liquid phase has experienced the repeated process of moving disk-static disk-moving disk in the rotor, it not only increases the mass transfer, heat transfer and reaction contact area, but also prolongs the reaction time of the two phases in the rotor appropriately.
实施例2:本实施例装置结构同实施例1,不同在于增加两对小叶轮,增大填料螺旋管的外壳半径,其他条件保持不变。 Embodiment 2: The device structure of this embodiment is the same as that of Embodiment 1, the difference is that two pairs of small impellers are added, the shell radius of the packing spiral tube is increased, and other conditions remain unchanged.
实施例3:本实施例装置结构同实施例1,增加传质装置中的动盘填料层和静盘填料层的环数,增大填料螺旋管的外壳半径,其他条件保持不变。 Embodiment 3: The structure of the device in this embodiment is the same as that in Embodiment 1. The number of rings of the moving disk packing layer and the static disk packing layer in the mass transfer device is increased, the shell radius of the packing spiral tube is increased, and other conditions remain unchanged.
Claims (8)
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| CN201520216992.1U CN204637641U (en) | 2015-04-13 | 2015-04-13 | A kind of labyrinth type hypergravity liquid-liquid extraction separator |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104815459A (en) * | 2015-04-13 | 2015-08-05 | 昆明理工大学 | Labyrinth type hypergravity liquid-liquid extraction separator |
| CN107088737A (en) * | 2016-07-29 | 2017-08-25 | 中航湖南通用航空发动机有限公司 | A kind of manufacture method of the disc component of aircraft engine |
| CN111408160A (en) * | 2020-04-26 | 2020-07-14 | 安徽省金宜食品有限公司 | Hanging basket type tea extraction device |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104815459A (en) * | 2015-04-13 | 2015-08-05 | 昆明理工大学 | Labyrinth type hypergravity liquid-liquid extraction separator |
| CN104815459B (en) * | 2015-04-13 | 2016-06-22 | 昆明理工大学 | A kind of labyrinth type hypergravity liquid-liquid extraction separator |
| CN107088737A (en) * | 2016-07-29 | 2017-08-25 | 中航湖南通用航空发动机有限公司 | A kind of manufacture method of the disc component of aircraft engine |
| CN111408160A (en) * | 2020-04-26 | 2020-07-14 | 安徽省金宜食品有限公司 | Hanging basket type tea extraction device |
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