CN204625204U - A kind of device preparing micron silver suboxide - Google Patents

A kind of device preparing micron silver suboxide Download PDF

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Publication number
CN204625204U
CN204625204U CN201520223080.7U CN201520223080U CN204625204U CN 204625204 U CN204625204 U CN 204625204U CN 201520223080 U CN201520223080 U CN 201520223080U CN 204625204 U CN204625204 U CN 204625204U
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CN
China
Prior art keywords
storage pipe
liquid storage
described liquid
storing cup
silver suboxide
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Expired - Fee Related
Application number
CN201520223080.7U
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Chinese (zh)
Inventor
陈庆春
邓慧宇
刘晓东
辛育东
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East China Institute of Technology
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East China Institute of Technology
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Priority to CN201520223080.7U priority Critical patent/CN204625204U/en
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Publication of CN204625204U publication Critical patent/CN204625204U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model relates to a kind of device preparing new function material, especially a kind of simple and convenient device for the preparation of micron silver suboxide, comprise liquid storage pipe, liquid storing cup, retaining collar, microfiltration membrane, stationary installation, described microfiltration membrane is sealed on described liquid storing cup rim of a cup place by described retaining collar, described retaining collar and described liquid storage pipe removably connect, described liquid storage pipe is located in described liquid storing cup by described stationary installation, and described stationary installation removably connects with described liquid storing cup and liquid storage pipe.The device of micron silver suboxide of the present utility model, structure is simple, easy assembly and disassembly, a micron silver suboxide cubic block can be prepared, preparation process does not use any organic additive and tensio-active agent, does not use High Temperature High Pressure, and gained silver suboxide cubic block size controls by regulator solution concentration.

Description

A kind of device preparing micron silver suboxide
Technical field
The utility model relates to a kind of device preparing new function material, especially a kind of simple and convenient device for the preparation of micron silver suboxide.
Background technology
Along with the development of science and technology, micro Nano material is more and more subject to people's attention, and nano material is a kind of brand-new material, generally refers to that particle diameter is less than the ultrafine particle of 100nm.It is large that this ultrafine particle has surface-area, and surfactivity is high, good catalysis characteristics, and it not only has metal but also have nonmetallic specific performance.Due to the property of nano material, make its potential application in all fields very extensive.Nano material has important using value in technical fields such as national defence, electronics, nuclear technique, metallurgy, aviation, light industry, medicine, thus has started the peak of nano material preparation and research.
Because micro Nano material shows character distinct with macroscopical block materials.In a lot of situation, the character of micro Nano material depends on its pattern showed.Silver suboxide is the oxide compound of a class silver, in a lot of, have application, and as being used as chemosynthesis catalyzer, zinc-silver oxide battery is medium.In prior art, work out multiple method and prepared the different silver suboxide micro Nano material of pattern.But most preparation process all needs organic additive or tensio-active agent to regulate and control the pattern of silver suboxide, too much introducing organism is not a green syt process.Micron silver suboxide cubic block has unique character, and how to utilize some simple and convenient devices to prepare a micron silver suboxide cubic block to become those skilled in the art's technical problem urgently to be resolved hurrily.
Utility model content
The utility model, in order to solve the problems of the technologies described above, provides a kind of device preparing micron silver suboxide, and this device has simple and fast and prepares micron silver suboxide cube block structured advantage.
In order to reach above-mentioned technique effect, the technical solution of the utility model comprises:
A kind of device preparing micron silver suboxide, comprise liquid storage pipe, liquid storing cup, retaining collar, microfiltration membrane, stationary installation, described microfiltration membrane is sealed on described liquid storage pipe mouth of pipe place by described retaining collar, described retaining collar and described liquid storage pipe removably connect, described liquid storage pipe is located in described liquid storing cup by described stationary installation, and described stationary installation removably connects with described liquid storing cup and liquid storage pipe.
Described stationary installation comprises liquid storage pipe clamp, link span, liquid storing cup folder, and described liquid storage pipe clamp is clipped in described liquid storage pipe body, and described liquid storing cup is clipped in described liquid storing cup cup, and described link span connects described liquid storage pipe clamp and described liquid storing cup folder.
The volume ratio of described liquid storing cup and described liquid storage pipe is 5 ~ 10:1.
The filter opening mean pore size of described microfiltration membrane is 0.2 micron.
The beneficial effects of the utility model comprise: the device of micron silver suboxide of the present utility model, structure is simple, easy assembly and disassembly, a micron silver suboxide cubic block can be prepared, preparation process does not use any organic additive and tensio-active agent, do not use High Temperature High Pressure, gained silver suboxide cubic block size controls by regulator solution concentration.
Accompanying drawing explanation
Figure 1 shows that a kind of device schematic diagram preparing micron silver suboxide of the utility model.
Figure 2 shows that a kind of bottom of device schematic diagram preparing micron silver suboxide of the utility model.
Diagram: 1-liquid storage pipe, 2-liquid storing cup, 3-microfiltration membrane, 4-retaining collar, 5-stationary installation, 51-liquid storage pipe clamp, 52, link span, 53-liquid storing cup folder.
Embodiment
Hereafter will describe the utility model specific embodiment in detail in conjunction with concrete accompanying drawing.It should be noted that the combination of technical characteristic or the technical characteristic described in following embodiment should not be considered to isolated, they can mutually be combined thus be reached better technique effect.In the accompanying drawing of following embodiment, the identical label that each accompanying drawing occurs represents identical feature or parts, can be applicable in different embodiment.
A kind of device preparing micron silver suboxide, Figure 1 shows that the utility model is a kind of prepare the device schematic diagram of micron silver suboxide and Figure 2 shows that a kind of bottom of device schematic diagram preparing micron silver suboxide of the utility model, the device of micron silver suboxide of the present utility model comprises liquid storage pipe 1, liquid storing cup 2, retaining collar 4, microfiltration membrane 3, stationary installation 5, described microfiltration membrane 3 is sealed on described liquid storage pipe 1 mouth of pipe place by described retaining collar 4, described retaining collar 4 removably connects with described liquid storage pipe 1, described liquid storage pipe 1 is located in described liquid storing cup 2 by described stationary installation 5, described stationary installation 5 removably connects with described liquid storing cup 2 and liquid storage pipe 1.
Described stationary installation 5 comprises liquid storage pipe clamp 51, link span 52, liquid storing cup folder 53, described liquid storage pipe clamp 51 is clipped in described liquid storage pipe 1 body, described liquid storing cup folder 53 is clipped on described liquid storing cup 2 cup, and described link span 52 connects described liquid storage pipe clamp 53 and described liquid storing cup folder 51.
Described liquid storing cup 2 is 5 ~ 10:1 with the volume ratio of described liquid storage pipe 1.
The filter opening mean pore size of described microfiltration membrane 3 is 0.2 micron.
Utilize the device of preparation micron silver suboxide described in the utility model, can be used for preparing micron silver suboxide cubic block, comprise the following steps: sodium hydroxide solution is loaded in liquid storage pipe 1, microfiltration membrane 3 is placed in described retaining collar 4 ring, described liquid storage pipe 1 mouth of pipe place is provided with draw-in groove, the retaining collar 4 that microfiltration membrane 3 is housed is snapped onto on described liquid storage pipe 1, splendid attire silver nitrate solution in liquid storing cup 2, liquid storage pipe 1 is stood upside down, be fixed in liquid storing cup by described stationary installation 5, the liquid storing cup folder 53 of stationary installation 5 is clipped on described liquid storing cup 2 cup, liquid storage pipe clamp 51 is clipped in described liquid storage pipe 1 body, realize being fixedly connected with of liquid storing cup 2 and liquid storage pipe 1.Described microfiltration membrane 3 is immersed in below described silver nitrate solution liquid level, after static 0.5 ~ 12 hour, in separating, washing beaker product can obtain a micron silver suboxide cubic block can.Concentration of sodium hydroxide solution is 0.04-0.2 mol/L, silver nitrate solution concentration is 0.05 mol/L, two kinds of liquor capacity ratios are 4 ~ 20:1, illustrate that device described in the utility model can realize a micron preparation for silver suboxide cubic block, and possess the advantage of assembling simple and easy to operate.
Above-mentioned detailed description is the illustrating of possible embodiments for utility model, this embodiment is also not used to limit the scope of the claims of the present utility model, all do not depart from of the present utility model equivalence implement or change, all should be contained in the scope of the claims of the present utility model.
In addition, those skilled in the art also can make various amendments in other form and details, interpolation and replacement in the utility model claim scope of disclosure and spirit.Certainly, the changes such as these various amendments made according to the utility model spirit, interpolation and replacement, all should be included within the utility model scope required for protection.

Claims (4)

1. prepare the device of micron silver suboxide for one kind, it is characterized in that, comprise liquid storage pipe, liquid storing cup, retaining collar, microfiltration membrane, stationary installation, described microfiltration membrane is sealed on described liquid storage pipe mouth of pipe place by described retaining collar, described retaining collar and described liquid storage pipe removably connect, described liquid storage pipe is located in described liquid storing cup by described stationary installation, and described stationary installation removably connects with described liquid storing cup and liquid storage pipe.
2. a kind of device preparing micron silver suboxide according to claim 1, it is characterized in that, described stationary installation comprises liquid storage pipe clamp, link span, liquid storing cup folder, described liquid storage pipe clamp is clipped in described liquid storage pipe body, described liquid storing cup is clipped in described liquid storing cup cup, and described link span connects described liquid storage pipe clamp and described liquid storing cup folder.
3. a kind of device preparing micron silver suboxide according to claim 1, is characterized in that, the volume ratio of described liquid storing cup and described liquid storage pipe is 5 ~ 10:1.
4. a kind of device preparing micron silver suboxide according to claim 1, is characterized in that, the filter opening mean pore size of described microfiltration membrane is 0.2 micron.
CN201520223080.7U 2015-04-14 2015-04-14 A kind of device preparing micron silver suboxide Expired - Fee Related CN204625204U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520223080.7U CN204625204U (en) 2015-04-14 2015-04-14 A kind of device preparing micron silver suboxide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520223080.7U CN204625204U (en) 2015-04-14 2015-04-14 A kind of device preparing micron silver suboxide

Publications (1)

Publication Number Publication Date
CN204625204U true CN204625204U (en) 2015-09-09

Family

ID=54044253

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201520223080.7U Expired - Fee Related CN204625204U (en) 2015-04-14 2015-04-14 A kind of device preparing micron silver suboxide

Country Status (1)

Country Link
CN (1) CN204625204U (en)

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150909

Termination date: 20160414

CF01 Termination of patent right due to non-payment of annual fee