CN204251338U - A kind of carbon nanotube continuous production equipment - Google Patents

A kind of carbon nanotube continuous production equipment Download PDF

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Publication number
CN204251338U
CN204251338U CN201420731712.6U CN201420731712U CN204251338U CN 204251338 U CN204251338 U CN 204251338U CN 201420731712 U CN201420731712 U CN 201420731712U CN 204251338 U CN204251338 U CN 204251338U
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CN
China
Prior art keywords
communicated
carbon nanotube
sealing radiator
storage unit
production equipment
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420731712.6U
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Chinese (zh)
Inventor
戴煜
胡祥龙
羊建高
周强
邓军旺
王艳艳
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Advanced Corp For Materials & Equipments Co Ltd
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Advanced Corp For Materials & Equipments Co Ltd
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Priority to CN201420731712.6U priority Critical patent/CN204251338U/en
Application granted granted Critical
Publication of CN204251338U publication Critical patent/CN204251338U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of carbon nanotube continuous production equipment, comprising: continuous feeding device; The vertical heater body that can be communicated with continuous feeding device; Be connected to bottom vertical heater body, and the vertical cooling room be communicated with vertical heater body; Be connected to bottom vertical cooling room, and the horizontal rewinding room be communicated with vertical cooling room, horizontal rewinding room offers discharging hermatic door; By the cyclonic separator that the first exhaust pipe is communicated with horizontal rewinding room, the bottom of cyclonic separator has material collecting device; Sealing radiator, sealing radiator has gas barrier, and is provided with water storage unit in sealing radiator; Second exhaust pipe, the first end of the second exhaust pipe seals with cyclonic separator and is communicated with, and the second end submerges in the water of water storage unit.The continous way that equipment in the utility model achieves carbon nanotube is produced, thus achieves the mass production of carbon nanotube.

Description

A kind of carbon nanotube continuous production equipment
Technical field
The utility model relates to carbon nanotube production field, more particularly, relates to a kind of carbon nanotube continuous production equipment.
Background technology
Carbon nanotube is as monodimension nanometer material, lightweight, and hexagonal structure connects perfect, has many abnormal mechanics, electricity and chemical property.Be expected to play a significant role in the fields such as high-strength composite structured material, nanostructure electron device, thermoelectric material, battery electrode material, low-temperature high-sensitivity sensor, biomolecule carrier, support of the catalyst.
But in present stage, prepare the equipment of carbon nanotube still based on the special purpose device of certain particular carbon nanotube, its function singleness, the mode of production are intermittent type or semi continuous, therefore, cannot realize the mass production of carbon nanotube.
Therefore, how designing a kind of continuous production equipment of carbon nanotube, realize the mass production of carbon nanotube, is those skilled in the art's critical problems urgently to be resolved hurrily.
Utility model content
The purpose of this utility model is to provide a kind of continuous production equipment of carbon nanotube, thus realizes the mass production of carbon nanotube.
For achieving the above object, the utility model provides following technical scheme:
A kind of carbon nanotube continuous production equipment, comprising:
Continuous feeding device;
The vertical heater body that can be communicated with described continuous feeding device;
Be connected to bottom described vertical heater body, and the vertical cooling room be communicated with described vertical heater body;
Be connected to bottom described vertical cooling room, and the horizontal rewinding room be communicated with described vertical cooling room, described horizontal rewinding room offers discharging hermatic door;
By the cyclonic separator that the first exhaust pipe is communicated with described horizontal rewinding room, the bottom of described cyclonic separator has material collecting device;
Sealing radiator, described sealing radiator has gas barrier, and is provided with water storage unit in described sealing radiator;
Second exhaust pipe, the first end of described second exhaust pipe seals with described cyclonic separator and is communicated with, and the second end submerges in the water of described water storage unit.
Preferably, described continuous feeding device comprises:
Be arranged at the feed nozzle at described vertical heater body top;
Solution bottle;
Hydro-pump, the liquid feeding end of described hydro-pump is communicated with described solution bottle, and the outlet end of described hydro-pump is communicated with described feed nozzle.
Preferably, described gas barrier comprises:
Be opened in the venting port on described sealing radiator;
The ignition control device be communicated with described venting port.
Preferably, described sealing radiator is provided with the water inlet pipe be communicated with described water storage unit;
Also comprise the taper bucket be arranged in described sealing radiator, described water storage unit is fixed in described taper bucket, and described taper bucket is provided with water shoot.
Preferably, described sealing radiator has openable tank lid.
As can be seen from technique scheme, in the process of continuously feeding, it is indoor that the carbon nanotube generated constantly deposits to horizontal rewinding, and cyclonic separator is separated tail gas constantly, and isolated carbon nanotube gathers in the material collecting device bottom cyclonic separator.In sealing radiator, gas barrier and the water storage unit pressure maintained in whole equipment is in the operating pressure of setting all the time.Clearly, the continous way that the equipment in the utility model achieves carbon nanotube is produced, thus achieves the mass production of carbon nanotube.
Accompanying drawing explanation
In order to be illustrated more clearly in the utility model embodiment or technical scheme of the prior art, be briefly described to the accompanying drawing used required in embodiment or description of the prior art below, apparently, accompanying drawing in the following describes is only embodiment of the present utility model, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawing can also be obtained according to the accompanying drawing provided.
The carbon nanotube continuous production equipment structural representation that Fig. 1 provides for the utility model one specific embodiment.
Wherein, 11 be vertical heater body, 12 be vertical cooling room, 13 be sealing radiator for horizontal rewinding room, 2 is the first exhaust pipe, 3 for cyclonic separator, 4 is the second exhaust pipe, 5,51 be water storage unit, 52 be taper bucket, 6 be ignition control device, 7 be solution bottle, 8 be hydro-pump, 9 for feed nozzle.
Embodiment
The utility model provides a kind of carbon nanotube continuous production equipment, this device achieves that the continous way of carbon nanotube is produced, thus achieves the mass production of carbon nanotube.
Below in conjunction with the accompanying drawing in the utility model embodiment, be clearly and completely described the technical scheme in the utility model embodiment, obviously, described embodiment is only a part of embodiment of the present utility model, instead of whole embodiments.Based on embodiment of the present utility model, other embodiments all that those of ordinary skill in the art obtain under the prerequisite not making creative work, all belong to the scope of the utility model protection.
Please refer to Fig. 1, the carbon nanotube continuous production equipment structural representation that Fig. 1 provides for the utility model one specific embodiment.
In the utility model one specific embodiment, carbon nanotube continuous production equipment comprises: continuous feeding device, vertical heater body 11, vertical cooling room 12, horizontal rewinding room 13, sealing radiator 5 and the water storage unit 51 be arranged in sealing radiator 5.
Wherein, continuous feeding device can be communicated with vertical heater body 11, for continuously feeding in vertical heater body 11.Vertical cooling room 12 is connected to the bottom of vertical heater body 11, and is communicated with vertical heater body 11, and horizontal rewinding room 13 is connected to the bottom of vertical cooling room 12, and is communicated with vertical cooling room 12.Vertical cooling room 12 is the transition section of cooling carbon nanotube, and the carbon nanotube generated in vertical heater body 11, through the cooling of vertical cooling room 12, is finally deposited in rewinding room, bedroom 13.Cyclonic separator 3 is communicated with rewinding room, bedroom 13 by the first exhaust pipe 2, and namely one end of the first exhaust pipe 2 is communicated with cyclonic separator 3, and the other end is communicated with rewinding room, bedroom 13.Tail gas enters into cyclonic separator 3 along the first exhaust pipe 2, and under the influence of centrifugal force, the carbon nanotube in tail gas deposits in the material collecting device bottom cyclonic separator 3.Sealing radiator 5 is provided with gas barrier, water storage unit 51 is provided with in sealing radiator 5, the first end of the second exhaust pipe 4 is communicated with cyclonic separator 3, second end reaches in the water of water storage unit 51, when in stove, pressure is greater than set(ting)value, the water surface of the water column in the second exhaust pipe 4 second end can decline, and the water surface in water storage unit 51 can rise, gas unnecessary in stove is discharged by gas barrier after overflowing from water, after unnecessary gas is discharged, in the water surface in water storage unit 51 and the second exhaust pipe 4 second end, the water surface of water column returns to sustained height.
In the utility model, in the process of continuously feeding, the carbon nanotube generated constantly deposits in horizontal rewinding room 13, and cyclonic separator 3 is separated tail gas constantly, and isolated carbon nanotube gathers in the material collecting device bottom cyclonic separator 3.In sealing radiator 5, gas barrier and water storage unit 51 pressure maintained in whole equipment is in the operating pressure of setting all the time.Clearly, the continous way that the equipment in the utility model achieves carbon nanotube is produced, thus achieves the mass production of carbon nanotube.
The first end of the second exhaust pipe 4 in above-mentioned preferably extend into the bottom of cyclonic separator 3.Its object is to the tail gas containing carbon nanotube is separated fully, avoid tail gas directly to discharge from the first end of the second exhaust pipe 4.
In the utility model one specific embodiment, the continuous feeding device in above-mentioned comprises: feed nozzle 9, solution bottle 7 and hydro-pump 8.
Feed nozzle 9 is arranged at the top of vertical heater body 11, and raw material can spray in vertical heater body 11 by feed nozzle 9 equably.Solution bottle 7 is for holding raw material liq.Hydro-pump 8 is for being delivered to the raw material liq in solution bottle 7 in feed nozzle 9.When starting to produce, opening hydro-pump 8, opening feed nozzle 9, the continuously feeding of material can be realized.
In the utility model one specific embodiment, the gas barrier in above-mentioned comprises the venting port be opened on sealing radiator 5 and the ignition control device 6 be communicated with venting port.The tail gas overflowed from water, containing the obnoxious flavour such as carbon monoxide, hydrogen, so in order to protect production environment, tail gas before discharging, first through the burning of ignition control device 6.
In the utility model one specific embodiment, the sealing radiator 5 in above-mentioned is provided with water inlet pipe, and this water inlet pipe is communicated with water storage unit 51, for water filling in water storage unit 51.Also comprise the taper bucket be arranged in sealing radiator 5 in the present embodiment, water storage unit 51 is arranged in taper bucket, and taper bucket is provided with water shoot.Become sewage after water in water storage unit 51 repeatedly utilizes, after end to be produced, open water shoot, the sewage in water storage unit 51 is discharged, then in water storage unit 51, injects fresh water by water inlet pipe.
In the utility model one specific embodiment, the sealing radiator 5 in above-mentioned has tank lid, and this tank lid can be opened.Tail gas is when through water storage unit 51, and the gas fraction in tail gas overflows from water, drains, and the solid carbon nanotube in tail gas then swims on the water surface.After end to be produced, open the tank lid on sealing radiator 5, the carbon nanotube floated on the water surface is collected out, thus the secondary achieving carbon nanotube is collected, and improves the collection effciency of carbon nanotube, has saved resource.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the utility model.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein when not departing from spirit or scope of the present utility model, can realize in other embodiments.Therefore, the utility model can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.

Claims (5)

1. a carbon nanotube continuous production equipment, is characterized in that, comprising:
Continuous feeding device;
The vertical heater body (11) that can be communicated with described continuous feeding device;
Be connected to described vertical heater body (11) bottom, and the vertical cooling room (12) be communicated with described vertical heater body (11);
Be connected to described vertical cooling room (12) bottom, and the horizontal rewinding room (13) be communicated with described vertical cooling room (12), described horizontal rewinding room (13) offers discharging hermatic door;
By the cyclonic separator (3) that the first exhaust pipe (2) is communicated with described horizontal rewinding room (13), the bottom of described cyclonic separator (3) has material collecting device (31);
Sealing radiator (5), described sealing radiator (5) has gas barrier, and is provided with water storage unit (51) in described sealing radiator (5);
Second exhaust pipe (4), the first end of described second exhaust pipe (4) seals with described cyclonic separator (3) and is communicated with, and the second end submerges in the water of described water storage unit (51).
2. carbon nanotube continuous production equipment according to claim 1, is characterized in that, described continuous feeding device comprises:
Be arranged at the feed nozzle (9) at described vertical heater body (11) top;
Solution bottle (7);
Hydro-pump (8), the liquid feeding end of described hydro-pump (8) is communicated with described solution bottle (7), and the outlet end of described hydro-pump (8) is communicated with described feed nozzle (9).
3. carbon nanotube continuous production equipment according to claim 1, is characterized in that, described gas barrier comprises:
Be opened in the venting port on described sealing radiator (5);
The ignition control device (6) be communicated with described venting port.
4. carbon nanotube continuous production equipment according to claim 1, is characterized in that, described sealing radiator (5) is provided with the water inlet pipe be communicated with described water storage unit (51);
Also comprise the taper bucket (52) be arranged in described sealing radiator (5), described water storage unit (51) is fixed in described taper bucket (52), and described taper bucket (52) is provided with water shoot.
5. the carbon nanotube continuous production equipment according to claim 1-4 any one, is characterized in that, described sealing radiator (5) has openable tank lid.
CN201420731712.6U 2014-11-28 2014-11-28 A kind of carbon nanotube continuous production equipment Expired - Fee Related CN204251338U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420731712.6U CN204251338U (en) 2014-11-28 2014-11-28 A kind of carbon nanotube continuous production equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420731712.6U CN204251338U (en) 2014-11-28 2014-11-28 A kind of carbon nanotube continuous production equipment

Publications (1)

Publication Number Publication Date
CN204251338U true CN204251338U (en) 2015-04-08

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Application Number Title Priority Date Filing Date
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104401966A (en) * 2014-11-28 2015-03-11 湖南顶立科技有限公司 Continuous type production equipment and method of carbon nano tube
CN106145089A (en) * 2016-08-31 2016-11-23 无锡东恒新能源科技有限公司 The synthesizer of batch production CNT
CN106477556A (en) * 2016-09-06 2017-03-08 南昌大学 A kind of automatic carbon nano material continuous producing apparatus and production method

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104401966A (en) * 2014-11-28 2015-03-11 湖南顶立科技有限公司 Continuous type production equipment and method of carbon nano tube
CN104401966B (en) * 2014-11-28 2017-01-25 湖南顶立科技有限公司 Continuous type production equipment and method of carbon nano tube
CN106145089A (en) * 2016-08-31 2016-11-23 无锡东恒新能源科技有限公司 The synthesizer of batch production CNT
CN106477556A (en) * 2016-09-06 2017-03-08 南昌大学 A kind of automatic carbon nano material continuous producing apparatus and production method

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C14 Grant of patent or utility model
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150408

Termination date: 20161128

CF01 Termination of patent right due to non-payment of annual fee