CN203710745U - Vertical flow settlement device for refining yellow phosphorus - Google Patents
Vertical flow settlement device for refining yellow phosphorus Download PDFInfo
- Publication number
- CN203710745U CN203710745U CN201320780425.XU CN201320780425U CN203710745U CN 203710745 U CN203710745 U CN 203710745U CN 201320780425 U CN201320780425 U CN 201320780425U CN 203710745 U CN203710745 U CN 203710745U
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- CN
- China
- Prior art keywords
- pipe
- pot
- phosphorus
- sewage
- siphon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000007670 refining Methods 0.000 title abstract description 7
- OBSZRRSYVTXPNB-UHFFFAOYSA-N tetraphosphorus Chemical compound P12P3P1P32 OBSZRRSYVTXPNB-UHFFFAOYSA-N 0.000 title abstract description 7
- 239000010865 sewage Substances 0.000 claims abstract description 33
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 238000004062 sedimentation Methods 0.000 claims description 42
- 238000009826 distribution Methods 0.000 claims description 10
- 238000001556 precipitation Methods 0.000 claims description 10
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 52
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 52
- 239000011574 phosphorus Substances 0.000 abstract description 52
- 239000007788 liquid Substances 0.000 abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 9
- 238000007599 discharging Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000010802 sludge Substances 0.000 abstract 1
- 101100298222 Caenorhabditis elegans pot-1 gene Proteins 0.000 description 11
- 230000005484 gravity Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Removal Of Specific Substances (AREA)
Abstract
The utility model relates to a settlement device for the production process of yellow phosphorus, in particular to a vertical flow settlement device for refining yellow phosphorus. The vertical flow settlement device for refining the yellow phosphorus comprises a settlement pot (1), a sewage input pipe (2), a siphon pipe (3), a siphon pump (4), a sewage discharging pipe (5) and a sewage discharging valve (6); a pot body of the settlement pot (1) is provided with an observation port (7), a heating sleeve (8) is arranged outside the pot body, the upper part is provided with an overflow pipe (9), the bottom is provided with the sewage discharging pipe (5), and the sewage discharging pipe (5) is provided with the sewage discharging valve (6); the sewage input pipe (2) vertically stretches into the middle part of the settlement pot (1), and a water outlet of the sewage input pipe (2) is provided with a guide hood (10) and a distributing plate (11); one end of the siphon pipe (3) stretches into the settlement pot (1), and the other end is connected with the siphon pump (4). The vertical flow settlement device is simple in structure and the space is saved; the sewage can be continuously treated; liquid phosphorus can be completely separated from the phosphorus sludge, the resource is saved, and the environment is protected.
Description
Technical field
The utility model relates to the precipitation apparatus in a kind of phosphorus production process, especially relates to the perpendicular stream precipitation apparatus for yellow phosphorus-refined operation.
Background technology
In producing yellow Phosphorus by electric oven production process, from being subject to the thick phosphorus that the condensation of phosphorus groove is got off to obtain a part of product by rinsing refining kettle, stratification; A large amount of mud phosphorus and washings also must, by postorder processing, further reclaim the yellow phosphorus in mud phosphorus, to improve the productive rate of yellow phosphorus, alleviate its pollution to environment.Mud phosphorus is the accessory substance that a kind of phosphorus of forming in phosphorus production process and impurity mix, and main component comprises the phosphorus of 9%-50%, the solid impurity of 1%-5%, the water of 45%-90%.
Refining sedimentation device is originally square groove, and water inlet and delivery port are all above the sidewall of groove, contain the sewage of liquid phosphorus and mud phosphorus in the process from water inlet to delivery port, liquid phosphorus and mud phosphorus, by Action of Gravity Field natural subsidence, will be discharged the mud phosphorus of middle liquid phosphorus and bottom when depositing to certain thickness.In the time that natural sedimentation or mud phosphorus are pulled out, easily make current form disturbance, thereby make liquid phosphorus and mud phosphorus completely precipitation just discharge refining sedimentation device, cause the wasting of resources and contaminated environment.
Summary of the invention
The utility model, for the deficiencies in the prior art, provides a kind of perpendicular stream precipitation apparatus for yellow phosphorus-refined operation, has effectively solved the problem of the sewage sedimentation separation containing liquid phosphorus and mud phosphorus that in phosphorus production, refining phosphorus operation produces.
For achieving the above object, the technical solution that the utility model adopts is:
For the perpendicular stream precipitation apparatus of yellow phosphorus-refined operation, comprise sedimentation pot, sewage input pipe, siphon pipe, siphon-pump, blow-off pipe and blowoff valve; Sedimentation pot top is that drum, bottom are back taper, on sedimentation pot pot body, has observation port, the external heating jacket that is provided with of sedimentation pot pot, and sedimentation pot top is provided with overflow pipe; The bottom of sedimentation pot is provided with blow-off pipe, and blow-off pipe is provided with blowoff valve; Sewage input pipe vertically stretches into the middle part of sedimentation pot along the axis of sedimentation pot, the delivery port of sewage input pipe is provided with kuppe and flow distribution plate; Sedimentation pot is vertically stretched in siphon pipe one end, and opening is in the back taper part of sedimentation pot, and the siphonal other end is connected with siphon-pump.
Described kuppe is tubaeform.
Described flow distribution plate is for taper shape and be fixed on kuppe below.
When work, heating jacket heats sedimentation pot, sewage containing liquid phosphorus and mud phosphorus enters sedimentation pot by sewage input pipe, under the kuppe and flow distribution plate effect of sewage input pipe water outlet, sewage is distributed to four sides instead of always downward, and rear current liquid phosphorus and mud phosphorus in upwards flowing lean on Action of Gravity Field natural subsidence, and taper seat is pooled to sedimentation pot bottom on the lower, after layering, mud phosphorus is at bottommost, and liquid phosphorus is at middle part, and the water of topmost is discharged from overflow pipe; When observe the liquid phosphorus of opening siphon-pump extraction middle part when liquid phosphorus arrives certain thickness from observation port; In the time that mud phosphorus arrives certain height, the blowoff valve of opening on blow-off pipe is discharged mud phosphorus.
the beneficial effects of the utility model:
1, the utility model is simple in structure, has saved working space.
2, the utility model is because have kuppe and flow distribution plate at the delivery port of sewage input pipe, sewage is distributed to four sides, can not form impact to the liquid phosphorus of layering after sedimentation and mud phosphorus, current liquid phosphorus and mud phosphorus in upwards flowing lean on Action of Gravity Field natural subsidence, when making to extract out liquid phosphorus and discharging mud phosphorus, also can enter sewage, realize continual sewage disposal.
3, the utility model makes liquid phosphorus separate completely with mud phosphorus, thereby has saved resource, protected environment.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model;
Fig. 2 is water (flow) direction schematic diagram of the present utility model.
1-sedimentation pot, 2-sewage input pipe, 3-siphon pipe, 4-siphon-pump, 5-blow-off pipe, 6-blowoff valve, 7-observation port, 8-heating jacket, 9-overflow pipe, 10-kuppe, 11-flow distribution plate.
Specific embodiment
embodiment 1
As shown in Figure 1 and Figure 2, for the perpendicular stream precipitation apparatus of yellow phosphorus-refined operation, comprise sedimentation pot 1, sewage input pipe 2, siphon pipe 3, siphon-pump 4, blow-off pipe 5 and blowoff valve 6; Sedimentation pot 1 top is that drum, bottom are back taper, on 1 pot of body of sedimentation pot, has observation port 7,1 pot of external heating jacket 8 that is provided with of sedimentation pot, and sedimentation pot 1 top is provided with overflow pipe 9; The bottom of sedimentation pot 1 is provided with blow-off pipe 5, and blow-off pipe 5 is provided with blowoff valve 6; Sewage input pipe 2 vertically stretches into the middle part of sedimentation pot 1 along the axis of sedimentation pot 1, the delivery port of sewage input pipe 2 is provided with kuppe 10 and flow distribution plate 11; Sedimentation pot 1 is vertically stretched in siphon pipe 3 one end, and opening is in the back taper part of sedimentation pot 1, and the other end of siphon pipe 3 is connected with siphon-pump 4.
Described kuppe 10 is tubaeform.
Described flow distribution plate 11 is for taper shape and be fixed on kuppe 10 belows.
When work, heating jacket 8 heats sedimentation pot 1, sewage containing liquid phosphorus and mud phosphorus enters sedimentation pot 1 by sewage input pipe 2, under the kuppe 10 of sewage input pipe 2 water outlets and flow distribution plate 11 effects, sewage is distributed to four sides instead of always downward, and rear current liquid phosphorus and mud phosphorus in upwards flowing lean on Action of Gravity Field natural subsidence, and taper seat is pooled to sedimentation pot 1 bottom on the lower, after layering, mud phosphorus is at bottommost, and liquid phosphorus is at middle part, and the water of topmost is discharged from overflow pipe 9; When observe the liquid phosphorus of opening siphon-pump 4 extraction middle parts when liquid phosphorus arrives certain thickness from observation port 7; In the time that mud phosphorus arrives certain height, the blowoff valve 6 of opening on blow-off pipe 5 is discharged mud phosphorus.
Claims (3)
1. for the perpendicular stream precipitation apparatus of yellow phosphorus-refined operation, it is characterized in that, comprise sedimentation pot (1), sewage input pipe (2), siphon pipe (3), siphon-pump (4), blow-off pipe (5) and blowoff valve (6); Sedimentation pot (1) top is that drum, bottom are back taper, on sedimentation pot (1) pot body, has observation port (7), the external heating jacket (8) that is provided with of sedimentation pot (1) pot, and sedimentation pot (1) top is provided with overflow pipe (9); The bottom of sedimentation pot (1) is provided with blow-off pipe (5), and blow-off pipe (5) is provided with blowoff valve (6); Sewage input pipe (2) vertically stretches into the middle part of sedimentation pot (1) along the axis of sedimentation pot (1), the delivery port of sewage input pipe (2) is provided with kuppe (10) and flow distribution plate (11); Sedimentation pot (1) is vertically stretched in siphon pipe (3) one end, and opening is in the back taper part of sedimentation pot (1), and the other end of siphon pipe (3) is connected with siphon-pump (4).
2. the perpendicular stream precipitation apparatus for yellow phosphorus-refined operation according to claim 1, is characterized in that, described kuppe (10) is tubaeform.
3. the perpendicular stream precipitation apparatus for yellow phosphorus-refined operation according to claim 1 and 2, is characterized in that, described flow distribution plate (11) is for taper shape and be fixed on kuppe (10) below.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320780425.XU CN203710745U (en) | 2013-12-03 | 2013-12-03 | Vertical flow settlement device for refining yellow phosphorus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320780425.XU CN203710745U (en) | 2013-12-03 | 2013-12-03 | Vertical flow settlement device for refining yellow phosphorus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203710745U true CN203710745U (en) | 2014-07-16 |
Family
ID=51149948
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320780425.XU Expired - Fee Related CN203710745U (en) | 2013-12-03 | 2013-12-03 | Vertical flow settlement device for refining yellow phosphorus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203710745U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106422434A (en) * | 2016-09-26 | 2017-02-22 | 四川省民众日化有限公司 | Free combination and transportation type phosphorus sludge settlement treatment recycling device and recycling method thereof |
| CN113926220A (en) * | 2020-06-29 | 2022-01-14 | 红河锦东化工股份有限公司 | Humic acid liquid continuous high-efficiency dynamic settler |
| CN116392745A (en) * | 2023-05-23 | 2023-07-07 | 无锡润年自动化科技有限公司 | Automatic fire extinguishing device |
| CN119160864A (en) * | 2024-09-26 | 2024-12-20 | 攀枝花市众立诚实业有限公司 | A system and method for efficiently recovering phosphorus from sludge phosphorus |
-
2013
- 2013-12-03 CN CN201320780425.XU patent/CN203710745U/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106422434A (en) * | 2016-09-26 | 2017-02-22 | 四川省民众日化有限公司 | Free combination and transportation type phosphorus sludge settlement treatment recycling device and recycling method thereof |
| CN113926220A (en) * | 2020-06-29 | 2022-01-14 | 红河锦东化工股份有限公司 | Humic acid liquid continuous high-efficiency dynamic settler |
| CN116392745A (en) * | 2023-05-23 | 2023-07-07 | 无锡润年自动化科技有限公司 | Automatic fire extinguishing device |
| CN116392745B (en) * | 2023-05-23 | 2024-01-09 | 无锡润年自动化科技有限公司 | Automatic fire extinguishing device |
| CN119160864A (en) * | 2024-09-26 | 2024-12-20 | 攀枝花市众立诚实业有限公司 | A system and method for efficiently recovering phosphorus from sludge phosphorus |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140716 Termination date: 20211203 |