CN203196348U - Vacuum decompression concentrator based on traditional Chinese medicine preparation extraction - Google Patents
Vacuum decompression concentrator based on traditional Chinese medicine preparation extraction Download PDFInfo
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- CN203196348U CN203196348U CN 201320226308 CN201320226308U CN203196348U CN 203196348 U CN203196348 U CN 203196348U CN 201320226308 CN201320226308 CN 201320226308 CN 201320226308 U CN201320226308 U CN 201320226308U CN 203196348 U CN203196348 U CN 203196348U
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Abstract
The utility model discloses a vacuum decompression concentrator based on traditional Chinese medicine preparation extraction. The vacuum decompression concentrator based on the traditional Chinese medicine preparation extraction is mainly composed of a vacuum concentration tank provided with a material liquid inlet (1), a cooling device and a liquid receiving barrel (2), wherein the cooling device and the liquid receiving barrel (2) are sequentially connected with the vacuum concentration tank, the vacuum concentration tank comprises a clamping sleeve (5) provided with a steam inlet (3) and a condensate water outlet (4), and a liner (6) assembled in the clamping sleeve (5), and the material liquid inlet (1) is formed in the liner (6). The vacuum decompression concentrator based on the traditional Chinese medicine preparation extraction can achieve decompression concentration of material liquid in a vacuum cavity, not only can evaporation of the material liquid be accelerated, but also the evaporation temperature can be lowered, and the vacuum decompression concentrator based on the traditional Chinese medicine preparation extraction is particularly applicable to concentration of thermo-sensitive substance solution poor in stability, and has the advantages of being high in concentration efficiency, easy to operate and the like.
Description
Technical field
The utility model relates to the traditional Chinese medicine extraction field, specifically, is based on the vacuum-concentrcted equipment that Chinese medicine preparation extracts.
Background technology
Chinese medicine extractor is a kind of process equipment that utilizes extraction element that the elite composition in the Chinese medicine is extract, at present, use comparatively general Chinese medicine extractor to include haplo-effect concentrator, the various structures such as dual-effect concentrator and Three-effect concentration device, applicable to pharmacy, food, the industrial departments such as chemical industry are concentrated to feed liquid, in the prior art, because there is great energy resource consumption in haplo-effect concentrator, therefore, gradually by dual-effect concentrator and Three-effect concentration device and substitute, but in the leaching process of Chinese medicine preparation, also there is following defective in the equipment such as dual-effect concentrator and Three-effect concentration device: (1) dual-effect concentrator and Three-effect concentration device all are to utilize the continuous circulating and evaporating of feed liquid and the unit equipment of realizing concentrating out cream, when actual production, living steam about all having adopted temperature up to 300 degrees centigrade is as heating energy source, when if feed liquid to be concentrated is the thermal sensitivity feed liquid, so for preventing that this thermal sensitivity feed liquid is subjected to the impact of temperature and heat time heating time the situations such as stable difference to occur, when operation, also need the heat time heating time of strict control feed liquid, prevent the generation of above-mentioned situation, operation easier is large.(2) because the Chinese medicine production environment is relative and production environment microbial reproduction preferably and the growth of chemicals, particularly extract concentrator and pipeline, if place, equipment dead angle cleaning is not thorough, residual liquid not only can pollute lower batch product, but also be very easy to grow mould, the microorganisms such as bacterium, thereby pollution medicine, therefore, in the production process of Chinese medicine extraction and preparation, production equipment to direct contact medicine, container, pipeline, after production is finished, also to clean it, in case active constituents of medicine residue and microorganism be to the pollution of next production batch feed liquid, but when dual-effect concentrator and the actual use of Three-effect concentration device, because the heater that the said equipment uses, the containers such as evaporimeter are more, pipeline configuration is relative complex also, therefore, not only can consume a large amount of manpower and materials when cleaning, more can delay producing of second batch of liquid, thereby reduce the production efficiency of equipment.
The utility model content
The purpose of this utility model is to provide the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation, can realize the reduced pressure concentration of feed liquid in the vacuum chamber by the setting of vacuum concentration pot, can not only accelerate the evaporation rate of feed liquid, can also reduce evaporating temperature, heat-sensitive substance solution concentrated, applied widely that is particularly useful for less stable.
The utility model is achieved through the following technical solutions: based on the vacuum-concentrcted equipment of Chinese medicine preparation extraction, this concentrator is mainly by the vacuum concentration pot that is provided with liquor inlet and the cooling device that links to each other with vacuum concentration pot successively, formed by the liquid bucket, in the utility model, vacuum concentration pot can be realized the reduced pressure concentration of feed liquid, be jacket type structure, specifically can be summarized as follows: vacuum concentration pot comprises and is provided with the steam inlet, the chuck of condensation-water drain and be assemblied in inner bag in the chuck, liquor inlet then is located on the inner bag, when reality is used, can also utilize vacuum environment to effectively reduce the evaporating temperature of feed liquid, be particularly useful for the concentrated of heat-sensitive substance solution.
For better realizing the utility model, between described vacuum concentration pot and cooling device, also be provided with vapour liquid separator, be provided with the communicating pipe that is communicated with respectively inner bag and cooling device at vapour liquid separator, then be provided with the return duct that is back to inner bag for feed liquid in the bottom of vapour liquid separator, the unevaporated feed liquid of part can be sent back to and continue reduction vaporization in the vacuum concentration pot, improve thickening efficiency of the present utility model.
In the utility model, described cooling device comprises condenser, the cooler that is communicated with successively from top to bottom, and condenser is subjected to the liquid bucket then to be located at the bottom of cooler by being connected to communicating pipe on the vapour liquid separator, and structure is very simple.
For better realizing said structure, described condenser is shell and tube condenser; Described cooler is the coil pipe type cooler.
For better realizing the utility model, described vacuum concentration pot, vapour liquid separator, cooling device, be made by stainless steel by the liquid bucket, have good decay resistance, meet medicine and food hygiene requirement, and reach the good job specification of GMP() requirement.
The utility model exports in the described lime set that is subjected to also to be provided with on the liquid bucket for the condensate liquid discharge, when reality is used, can realize the recovery of condensate liquid (organic solvent etc.), operates also very simple.
Be the control of more convenient operator to concentration technology, the utility model at described inner bag, be subjected to the liquid bucket to be equipped with the visor of liquid level in the observation ward; On described inner bag, also be respectively equipped with vacuum meter and thermometer.
The utility model compared with prior art has the following advantages and beneficial effect:
(1) the utility model adopts the setting of vacuum concentration pot, can realize that low-temperature reduced-pressure is concentrated, is particularly useful for heat-sensitive substance solution concentrated of less stable, suitablely extensively promotes the use of.
(2) the utility model not only can be realized the recovery of organic solvent (i.e. concentrated lotion) and condensate liquid (being alcohol), can also carry out Effect of Alcohol Extracting Procedureto Total to unevaporated feed liquid, improves the thickening efficiency of equipment, increases Business Economic Benefit.
(3) the utility model also can be realized the continuous feed of feed liquid in concentration process, simultaneously inlet amount is controlled, and realizes the operating procedure of the charging while concentrating, and is higher than indirect type equipment thickening efficiency.
(4) structure of the present utility model and tube side connect all comparatively simple, the main container such as vacuum concentration pot, vapour liquid separator, cooling device all adopts stainless steel to be made, not only has good decay resistance, simultaneously, based on its simple tube side design, also have the advantages such as easy to clean, that cleaning labour intensity is low.
Description of drawings
Fig. 1 is structural representation of the present utility model.
1-liquor inlet wherein, 2-be subjected to liquid bucket, 3-steam inlet, 4-condensation-water drain, 5-chuck, 6-inner bag, 7-vapour liquid separator, 8-communicating pipe, 9-return duct, 10-condenser, 11-cooler, the outlet of 12-lime set, 13-visor, 14-vacuum meter, 15-thermometer.
The specific embodiment
Below in conjunction with embodiment the utility model is described in further detail, but embodiment of the present utility model is not limited to this.
Embodiment:
The utility model proposes the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation, this concentrator is applicable to pharmacy, food, the industrial departments such as chemical industry are concentrated to feed liquid, has thickening efficiency high, technique is simple, the advantages such as equipment cleaning is convenient, its structure as shown in Figure 1, mainly by the vacuum concentration pot that is provided with liquor inlet 1 and the cooling device that links to each other with vacuum concentration pot successively, formed by liquid bucket 2, in the utility model, vacuum concentration pot can be realized the reduced pressure concentration of feed liquid, be jacket type structure, and formed by chuck 5 and the inner bags 6 that are assemblied in the chuck 5, wherein, chuck 5 is for being provided with the firing equipment of steam inlet 3 and condensation-water drain 4, can be for the heating of inner bag 6,1 of liquor inlet is located on the inner bag 6.When practical operation, feed liquid is entered the inner bag 6 with vacuum environment by liquor inlet 1, heat by being set in inner bag 6 outer chucks 5, can realize the vacuum-concentrcted of feed liquid, vacuum environment based on inner bag 6, the utility model can also effectively reduce the evaporating temperature of feed liquid, is particularly useful for the concentrated of heat-sensitive substance solution, has market value.When actual production, be the Production requirement of applicable different scales pharmaceutical factory and experimental department, the Capacity design of vacuum concentration pot has 200L, 300L, 500L, 700L, 1000L or six kinds of specifications of 2000L, can select according to different demands, and is practical.
Feed liquid is behind inner bag 6 interior ebuillition of heated, transpiring moisture, the indirect steam that forms cools off by cooling device again, condensation material (being organic solute) is then by being subjected to liquid bucket 2 to carry out splendid attire, for better realizing above-mentioned steps, the utility model also is provided with vapour liquid separator 7 between vacuum concentration pot and cooling device, can prevent from entering in the cooling device with indirect steam with the foam of active ingredient, and be condensed into and be subjected in the liquid bucket 2 and the race that causes is expected, as shown in Figure 1, the utility model is provided with the communicating pipe 8 that is communicated with respectively inner bag 6 and cooling device at vapour liquid separator 7, then be provided with the return duct 9 that is back to inner bag 6 for condensate liquid in the bottom of vapour liquid separator 7, part can be separated with the foam that indirect steam carries, and be back in the inner bag 6 by return duct 9, proceed reduction vaporization, structure is very simple, and can effectively improve thickening efficiency of the present utility model, have fabulous economic benefit.
As shown in Figure 1, cooling device comprises condenser 10, the cooler 11 that is communicated with successively from top to bottom, and condenser 10 is by be connected on the vapour liquid separator 7 communicating pipe 8, and structure is also very simple.Certainly, for better realizing said structure, condenser 10 can adopt shell and tube condenser; 11 in cooler can adopt the coil pipe type cooler.In the utility model, be subjected to liquid bucket 2 to be located at the bottom of cooler 11, can be used for the splendid attire of condensate liquid, on its structure, also be provided with the lime set outlet 12 of discharging for condensate liquid, in actual production process, can realize the recovery of condensation material (organic solvent etc.), reduce the production cost of equipment; Be the control of more convenient operator to concentration technology, the utility model at inner bag 6, be subjected to liquid bucket 2 to be equipped with the visor 13 of liquid level in the observation ward; On inner bag 6, also be respectively equipped with vacuum meter 14 and thermometer 15, control very simple.
By said structure as can be known, the utility model can be realized the reduced pressure concentration of inner bag 6 interior feed liquids, can not only accelerate the evaporation rate of feed liquid, can also reduce evaporating temperature, be particularly useful for heat-sensitive substance solution concentrated of less stable, have the advantages such as thickening efficiency is high, simple to operate.Be better to realize the utility model, vacuum concentration pot, vapour liquid separator 7, cooling device, be made by stainless steel by liquid bucket 2, have good decay resistance, meet medicine and food hygiene requirement, and reach the good job specification of GMP() requirement.Its operating procedure is as follows: (1) vacuum charging: open first the vacuum environment that vavuum pump guarantees inner bag 6, open again the inlet valve charging of liquor inlet 1, for guaranteeing certain evaporating space, can observe by the visor 13 on the inner bag 6, generally speaking, close being advisable of liquid level and visor 13 positions; (2) heating is concentrated: open the valve of steam inlet 3 when closing inlet valve, make feed liquid appropriateness boiling in the container, start vaporizer in order to accelerate evaporation rate, can adopt reduced pressure concentration, and the height of its vacuum is required by user's different process and sets.Aforesaid operations can be realized the continuous feed of equipment, when actual production, can configure flowmeter at feeding pipe, the control inlet amount, and LZB-10 or LZB-15 are adopted in the suggestion of flowmeter model, and its range of flow is decided according to the amount of capacity of vacuum concentration pot.
The above; it only is preferred embodiment of the present utility model; be not that the utility model is done any pro forma restriction, every foundation technical spirit of the present utility model all falls within the protection domain of the present utility model any simple modification, equivalent variations that above embodiment does.
Claims (8)
1. the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation, it is characterized in that: mainly by the vacuum concentration pot that is provided with liquor inlet (1) and the cooling device that links to each other with vacuum concentration pot successively, formed by liquid bucket (2), vacuum concentration pot comprises the chuck (5) that is provided with steam inlet (3), condensation-water drain (4) and is assemblied in inner bag (6) in the chuck (5), and liquor inlet (1) then is located on the inner bag (6).
2. the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation according to claim 1, it is characterized in that: between described vacuum concentration pot and cooling device, also be provided with vapour liquid separator (7), be provided with the communicating pipe (8) that is communicated with respectively inner bag (6) and cooling device at vapour liquid separator (7), then be provided with the return duct (9) that is back to inner bag (6) for feed liquid in the bottom of vapour liquid separator (7).
3. the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation according to claim 2, it is characterized in that: described cooling device comprises condenser (10), the cooler (11) that is communicated with successively from top to bottom, condenser (10) was connected on the vapour liquid separator (7) by communicating pipe (8), was subjected to liquid bucket (2) then to be located at the bottom of cooler (11).
4. the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation according to claim 3, it is characterized in that: described condenser (10) is shell and tube condenser; Described cooler (11) is the coil pipe type cooler.
5. the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation according to claim 4 is characterized in that: described vacuum concentration pot, vapour liquid separator (7), cooling device, be made by stainless steel by liquid bucket (2).
6. each described vacuum-concentrcted equipment that extracts based on Chinese medicine preparation is characterized in that: in the described lime set outlet (12) that is subjected to also to be provided with on the liquid bucket (2) for the condensate liquid discharge according to claim 1~5.
7. the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation according to claim 6 is characterized in that: at described inner bag (6), be subjected to liquid bucket (2) to be equipped with the visor (13) of liquid level in the observation ward.
8. the vacuum-concentrcted equipment that extracts based on Chinese medicine preparation according to claim 7 is characterized in that: also be respectively equipped with vacuum meter (14) and thermometer (15) on described inner bag (6).
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CN 201320226308 CN203196348U (en) | 2013-04-28 | 2013-04-28 | Vacuum decompression concentrator based on traditional Chinese medicine preparation extraction |
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CN 201320226308 CN203196348U (en) | 2013-04-28 | 2013-04-28 | Vacuum decompression concentrator based on traditional Chinese medicine preparation extraction |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104324509A (en) * | 2014-11-13 | 2015-02-04 | 大理药业股份有限公司 | Special liquid medicine water bath heating and concentrating device used in clean area |
CN105381618A (en) * | 2015-12-01 | 2016-03-09 | 浙江凯迪药化机械有限公司 | Low temperature separation and concentration device |
CN106693412A (en) * | 2017-02-27 | 2017-05-24 | 四川德成动物保健品有限公司 | Alcohol volatilization device for medicinal material effective ingredient extraction |
CN106823420A (en) * | 2017-02-27 | 2017-06-13 | 四川德成动物保健品有限公司 | Chinese medicine material effective ingredient extract solution transmission volatilization collection device |
CN110559673A (en) * | 2019-10-08 | 2019-12-13 | 上海万仕诚药业有限公司 | vacuum concentration tank, vacuum concentration system, liquid inlet method and cleaning method |
CN110731445A (en) * | 2019-11-23 | 2020-01-31 | 吉林省利生源生物制品有限公司 | method for preparing Ginseng radix Rubri paste and vacuum concentrating furnace |
CN115088795A (en) * | 2022-07-05 | 2022-09-23 | 梁和标 | Preparation method of herbal beverage |
-
2013
- 2013-04-28 CN CN 201320226308 patent/CN203196348U/en not_active Expired - Fee Related
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104324509A (en) * | 2014-11-13 | 2015-02-04 | 大理药业股份有限公司 | Special liquid medicine water bath heating and concentrating device used in clean area |
CN105381618A (en) * | 2015-12-01 | 2016-03-09 | 浙江凯迪药化机械有限公司 | Low temperature separation and concentration device |
CN106693412A (en) * | 2017-02-27 | 2017-05-24 | 四川德成动物保健品有限公司 | Alcohol volatilization device for medicinal material effective ingredient extraction |
CN106823420A (en) * | 2017-02-27 | 2017-06-13 | 四川德成动物保健品有限公司 | Chinese medicine material effective ingredient extract solution transmission volatilization collection device |
CN110559673A (en) * | 2019-10-08 | 2019-12-13 | 上海万仕诚药业有限公司 | vacuum concentration tank, vacuum concentration system, liquid inlet method and cleaning method |
CN110731445A (en) * | 2019-11-23 | 2020-01-31 | 吉林省利生源生物制品有限公司 | method for preparing Ginseng radix Rubri paste and vacuum concentrating furnace |
CN115088795A (en) * | 2022-07-05 | 2022-09-23 | 梁和标 | Preparation method of herbal beverage |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130918 Termination date: 20150428 |
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EXPY | Termination of patent right or utility model |