CN202717583U - Colorless concentrated nitric acid production system - Google Patents

Colorless concentrated nitric acid production system Download PDF

Info

Publication number
CN202717583U
CN202717583U CN 201220420292 CN201220420292U CN202717583U CN 202717583 U CN202717583 U CN 202717583U CN 201220420292 CN201220420292 CN 201220420292 CN 201220420292 U CN201220420292 U CN 201220420292U CN 202717583 U CN202717583 U CN 202717583U
Authority
CN
China
Prior art keywords
oxynitride
acid
nitric acid
concentrated nitric
pump
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 201220420292
Other languages
Chinese (zh)
Inventor
李庆青
李广乾
赵广义
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HEBEI JIHENG GROUP CO Ltd
Original Assignee
HEBEI JIHENG GROUP CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HEBEI JIHENG GROUP CO Ltd filed Critical HEBEI JIHENG GROUP CO Ltd
Priority to CN 201220420292 priority Critical patent/CN202717583U/en
Application granted granted Critical
Publication of CN202717583U publication Critical patent/CN202717583U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Abstract

The utility model discloses a colorless concentrated nitric acid production system which comprises a reaction port, a compressed air inlet pipe, a concentrated nitric acid input pipe, an acid adding pump, a nitric oxide outlet pipe, a circulation acid pump and a nitric oxide washing system, wherein the reaction pot is provided with a metering device, and an air-blowing coiler provided with an air hole. The concentrated nitric acid input pipe is used for enabling concentrated nitric acid of 98% concentration to be inputted into the reactor pot, the acid adding pump is used for enabling concentrated nitric acid of 60% concentration to be inputted into the reactor pot, and the nitric oxide outlet pipe is used for enabling the nitric oxide produced in the reaction pot to be extracted out. The circulation acid pump is used for enabling mixed acid inside the reaction pot to be circulated, an outlet pipeline is provided with an acid collection branch pipe provided with an acid collection valve, and the nitric oxide washing system is used for receiving the nitric oxide extracted out by the nitric oxide outlet pipe and conducting washing process. The colorless concentrated nitric acid production system is used for producing nitric acid of 70% concentration, is simple to operate and low in production cost, and can fully meet market requirements.

Description

Colourless concentrated nitric acid production system
Technical field
The utility model relates to nitric acid production equipment, specifically a kind of colourless concentrated nitric acid production system.
Background technology
At present, nitric acid adopts double pressurized method production, and it is 65% nitric acid that maximum concentration can only produce concentration, and contains relatively large oxides of nitrogen gas in the acid, so that made nitric acid is yellow.At present concentration is that 98% concentrated nitric acid adopts indirect denitration method to produce, and after the magnesium nitrate dewatering agent dewaters, produces the concentrated nitric acid that meets national standard with rare nitric acid.But, in the actual production, produce the needed concentration of some Chemicals and be about 70% colourless nitric acid, at home also not preferably production unit and method.
The utility model content
The purpose of this utility model will provide a kind of colourless concentrated nitric acid production system exactly, to realize the purpose of the colourless concentrated nitric acid of direct production, meets the need of market preferably.
The utility model is achieved in that
Colourless concentrated nitric acid production system comprises:
One retort with measuring apparatus is provided with bulging air-coil in tank body, described bulging air-coil has pore;
One compressed air inlet pipe is used for sending into pressurized air in described bulging air-coil;
One concentrated nitric acid input tube is used in described retort tank body input concentration and is 98% concentrated nitric acid;
One acid adding pump is used in described retort tank body input concentration and is 60% nitric acid;
One oxynitride fairlead is used for the oxynitride that produces in the described retort tank body is drawn;
One cyclic acid pump, the input terminus of described cyclic acid pump joins by intake line and the outlet of described retort tank body lower part, described recycle acid delivery side of pump joins by delivery conduit and described retort tank body upper inlet, is used for making the mixing acid circulation in the described retort tank body; Be provided with at described delivery conduit and adopt sour arm, described adopt to be provided with on the sour arm adopt sour valve;
And an oxynitride washing system, be used for receiving the oxynitride that described oxynitride fairlead draws and carry out carrying out washing treatment.
Described oxynitride washing system comprises:
The oxynitride washing tower;
And the oxynitride cleaning circulation pump, be used for making the liquid circulation in the oxynitride washing tower; The input terminus of described cyclic acid pump joins by intake line and described oxynitride washing tower lower part outlet, described oxynitride cycles of washing delivery side of pump joins by delivery conduit and described oxynitride washing tower upper inlet, is used for making the liquid circulation in the oxynitride washing tower; Be provided with sour water extraction pipe at described delivery conduit, be provided with valve on the described sour water extraction pipe.
The utility model adopts this structure, will squeeze in the retort with measuring apparatus through the acid adding pump from 60% nitric acid of dilute nitric acid production device, gets to suitable scale value in the tank, termination of pumping.Compressed air inlet pipe is used for sending into the pressurized air that pressure is 0.3MPa in described bulging air-coil, and the pore of offering through described bulging air-coil outwards blows out.98% concentrated nitric acid from the production of concentrated nitric acid device is inputted in the described retort tank body by the concentrated nitric acid input tube.In the retort tank body, the oxynitride tobacco that overflows when two kinds of acid of 60% nitric acid and 98% concentrated nitric acid mix is introduced the processing of oxynitride washing system by the Air blowing that bloats in the coil pipe via the oxynitride fairlead.Mixing acid in the retort circulates through cyclic acid pump, until acid becomes colorless when transparent by yellow, is 70% nitric acid through adopting sour valve extraction concentration.
The utility model is 70% nitric acid for the production of concentration, and operation is succinct, production cost is low, good product quality, and fully satisfying the market is the user demand of 70% nitric acid to concentration.
Description of drawings
Fig. 1 is structural representation of the present utility model.
Embodiment
Below in conjunction with accompanying drawing embodiment of the present utility model is made and to be further specified
Shown in Figure 1, colourless concentrated nitric acid production system comprises retort 1, a compressed air inlet pipe 3, a concentrated nitric acid input tube 4, an acid adding pump, an oxynitride fairlead 5, a cyclic acid pump 7 and an oxynitride washing system with measuring apparatus.
Be provided with bulging air-coil 2 in the tank body of described retort 1 with measuring apparatus, described bulging air-coil has pore 21.Described compressed air inlet pipe 3 is used for sending into pressurized air in described bulging air-coil.Described concentrated nitric acid input tube 4 is 98% concentrated nitric acid for input concentration in described retort tank body.Described acid adding pump (not shown) is used in described retort tank body input concentration and is 60% nitric acid.Described oxynitride fairlead 5 for vertical body side of inserting in tank is equipped with the aluminum pipe of some apertures, is used for the oxynitride that produces in the described retort tank body is drawn.The input terminus of described cyclic acid pump 7 joins by intake line and the outlet of described retort 1 tank body lower part, at described input tube valve is installed; Described recycle acid delivery side of pump joins by delivery conduit and described retort 1 tank body upper inlet, is used for making the mixing acid circulation in the described retort tank body, and valve also is installed on described delivery conduit; Be provided with at described delivery conduit and adopt sour arm 6, described adopt to be provided with on the sour arm adopt sour valve.Described oxynitride washing system is used for receiving the oxynitride that described oxynitride fairlead 5 draws and carries out carrying out washing treatment.Described oxynitride washing system comprises: oxynitride washing tower 8 and oxynitride cleaning circulation pump 9.Described oxynitride cleaning circulation pump is used for making the liquid circulation in the oxynitride washing tower; The input terminus of described cyclic acid pump 9 joins by intake line and described oxynitride washing tower 8 lower part outlets, described oxynitride cycles of washing delivery side of pump joins by delivery conduit and described oxynitride washing tower upper inlet, is used for making the liquid circulation in the oxynitride washing tower.Be provided with sour water extraction pipe 10 at described delivery conduit, be provided with valve on the described sour water extraction pipe.

Claims (2)

1. colourless concentrated nitric acid production system is characterized in that comprising:
One retort with measuring apparatus is provided with bulging air-coil in tank body, described bulging air-coil has pore;
One compressed air inlet pipe is used for sending into pressurized air in described bulging air-coil;
One concentrated nitric acid input tube is used in described retort tank body input concentration and is 98% concentrated nitric acid;
One acid adding pump is used in described retort tank body input concentration and is 60% nitric acid;
One oxynitride fairlead is used for the oxynitride that produces in the described retort tank body is drawn;
One cyclic acid pump, the input terminus of described cyclic acid pump joins by intake line and the outlet of described retort tank body lower part, described recycle acid delivery side of pump joins by delivery conduit and described retort tank body upper inlet, is used for making the mixing acid circulation in the described retort tank body; Be provided with at described delivery conduit and adopt sour arm, described adopt to be provided with on the sour arm adopt sour valve;
One oxynitride washing system is used for receiving the oxynitride that described oxynitride fairlead draws and carries out carrying out washing treatment.
2. colourless concentrated nitric acid production system according to claim 1 is characterized in that described oxynitride washing system comprises:
The oxynitride washing tower;
The oxynitride cleaning circulation pump is used for making the liquid circulation in the oxynitride washing tower; The input terminus of described cyclic acid pump joins by intake line and described oxynitride washing tower lower part outlet, described oxynitride cycles of washing delivery side of pump joins by delivery conduit and described oxynitride washing tower upper inlet, is used for making the liquid circulation in the oxynitride washing tower; Be provided with sour water extraction pipe at described delivery conduit, be provided with valve on the described sour water extraction pipe.
CN 201220420292 2012-08-23 2012-08-23 Colorless concentrated nitric acid production system Expired - Fee Related CN202717583U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220420292 CN202717583U (en) 2012-08-23 2012-08-23 Colorless concentrated nitric acid production system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220420292 CN202717583U (en) 2012-08-23 2012-08-23 Colorless concentrated nitric acid production system

Publications (1)

Publication Number Publication Date
CN202717583U true CN202717583U (en) 2013-02-06

Family

ID=47619412

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201220420292 Expired - Fee Related CN202717583U (en) 2012-08-23 2012-08-23 Colorless concentrated nitric acid production system

Country Status (1)

Country Link
CN (1) CN202717583U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103569978A (en) * 2013-11-01 2014-02-12 安徽金禾实业股份有限公司 Nitric acid gas stripping and decolorizing method and device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103569978A (en) * 2013-11-01 2014-02-12 安徽金禾实业股份有限公司 Nitric acid gas stripping and decolorizing method and device
CN103569978B (en) * 2013-11-01 2015-11-18 安徽金禾实业股份有限公司 A kind of nitric acid air lift decoloring method and device

Similar Documents

Publication Publication Date Title
CN207811449U (en) A kind of oxygen-dissolving apparatus
CN106702184A (en) Clear water desorption process of alkalescence anion resin
CN201957717U (en) Novel carbonic water preparing equipment
CN202717583U (en) Colorless concentrated nitric acid production system
CN203845925U (en) Sludge treatment system
CN202778298U (en) Regenerative acid preparation device for deionizing cation bed
CN202729795U (en) Online acidifying device for carbon
CN204154538U (en) A kind of reactor plain type sampling apparatus
CN202179923U (en) Hydrogen bromide tail gas absorption device
CN105460901A (en) Dilute phosphoric acid solution distribution device for hydrogen peroxide production
CN102838103B (en) Synthesizer for lithium hexafluorophosphate
CN207667619U (en) A kind of phenols and isobutene reaction device
CN202566172U (en) Device used for increasing dissolved oxygen content in instant tea
CN206730840U (en) A kind of acid mist absorbing device
CN206666156U (en) A kind of full-automatic extraction equipment of high purity rare earth oxides
CN205076818U (en) Workshop section's regeneration gas preparation weak aqua ammonia device is washed to synthetic ammonia technology copper
CN205002622U (en) Vacuum pump system for chemical industry
CN204057962U (en) Dilute phosphoric acid solution dispenser in a kind of Hydrogen Peroxide Production
CN203474699U (en) Rectification type esterification reaction system for polycarboxylate water reducer
CN202785657U (en) Nitrogen dioxide recovery system
CN203715542U (en) Metering control device of recycling cyanuric acid from mother liquor
CN203484158U (en) Speed increasing device for hydrogenation reaction kettle
CN204017693U (en) Pump type wastewater treatment chemical-dosing mixer
CN103846081B (en) A kind of D382 type resin acidic resolves technique
CN204324875U (en) Chemical plant sulfurous gas extraction element

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130206

Termination date: 20180823