A kind of online deuterium/nitrogen blending device of recyclable deuterium gas
Technical field
The utility model relates in a kind of optic fibre manufacture process process the recyclable deuterium/nitrogen scene that the utilizes deuterium gas again equipment that is mixed.
Background technology
In the optical fiber manufacture process, need reduce the operation of optical fiber hydrogen-sensitivity together, this operation by with pending optical fiber seal in a tank body and the deuterium nitrogen mixed gas that feeds debita spissitudo finish.The mixing of deuterium nitrogen realizes by online deuterium nitrogen blending device, has simplified the complicated process that is mixed into deuterium/nitrogen mixture gas thus, has reduced deuterium gas disposal cost.
Usually the deuterium gas that contains 1-10% in deuterium/nitrogen mixed gas, the concentration of deuterium is extremely important for diffusion process, and glass absorbs deuterium by diffusion, but it is considerably less to enter the deuterium of glass in the gaseous mixture, but the gaseous mixture that is used for after the optical fiber processing all will be taken out and be drained, and has caused very big waste.Because deuterium gas price lattice are very expensive, this means that deuterium gas accounts for very big cost in optical fiber production again.Therefore, need to improve online deuterium/nitrogen blending device, with reclaim, cycling and reutilization deuterium gas, further reduce deuterium gas disposal cost, the application just is being based on above-mentioned purpose and the improvement carried out.
The utility model content
What the utility model purpose provided a kind of recyclable, cycling and reutilization deuterium gas carries out the device that deuterium nitrogen is mixed at the factory scene.
In order to reach the foregoing invention purpose, the technical solution of the utility model is: a kind of online deuterium/nitrogen blending device of recyclable deuterium gas, it comprises liquid nitrogen storage tank, the deuterium air-capacitor is received bottle, receive the gas mixing device that pipeline bottle mutually is connected with liquid nitrogen storage tank and deuterium air-capacitor, be installed in the control valve and the flowmeter that are used to control deuterium nitrogen mixing ratio example on the gas mixing device, with the gas mixing device surge tank that connects of pipeline mutually, be used to measure the deuterium gas concentration analyzer of deuterium gas concentration in the surge tank, the optical fiber processing jar that is connected by pipeline respectively with surge tank and liquid nitrogen storage tank, between described optical fiber processing jar and surge tank, a recovery approach is set also, deuterium nitrogen mixed gas in the described optical fiber processing jar enters surge tank by described recovery approach after use, deuterium content according to deuterium gas concentration analyzer feedback, the deuterium nitrogen mixed gas of regulating the new concentration ratio of blender output is to surge tank, make that the deuterium concentration in the gaseous mixture reaches the setting working concentration in the surge tank, and input in the optical fiber processing jar and utilize once more.
Further, it also comprises and the surge tank outlet purifier that is used to collect pure deuterium gas of pipeline setting mutually.
Described liquid nitrogen storage tank and the pipeline connection mutually of optical fiber processing jar, the mist in the described optical fiber processing jar is blown into down at liquid nitrogen and enters surge tank through recovery approach.
Described optical fiber processing jar is provided with vavuum pump, after being blown into nitrogen, by vavuum pump the optical fiber processing jar is vacuumized.
Adopt such scheme, the utility model compared with prior art has following advantage: the utility model has increased by a recovery approach between optical fiber processing jar and surge tank on the basis of original deuterium nitrogen blending device, deuterium nitrogen mixed gas after once using enters surge tank through recovery approach, and by the new concentration gaseous mixture of adjustments of gas blender output, make that deuterium concentration reaches setting concentration once more in the gaseous mixture in the surge tank, utilize once more to be delivered in the optical fiber processing jar.This device not only greatly reduces deuterium gas disposal cost, and recyclable again, cycling and reutilization deuterium gas has further reached the purpose that reduces production costs.
Description of drawings
Accompanying drawing 1 is the principle schematic of the recyclable deuterium nitrogen of the utility model blending device;
Wherein: 1, liquid nitrogen storage tank; 2, the deuterium air-capacitor is received bottle; 3, gas mixing device; 4, surge tank; 5, optical fiber processing jar; 6, deuterium gas concentration analyzer; 7, recovery approach; 8, purifier.
The specific embodiment
Below in conjunction with accompanying drawing the utility model preferred embodiment is elaborated:
Deuterium nitrogen blending device as shown in Figure 1, it is suitable for scene that optical fiber makes and uses, and comprises optical fiber processing jar 5, the surge tank 4, the gas mixing device 3 that is connected with surge tank 4 phase pipelines and the liquid nitrogen storage tank 1 that is connected with gas mixing device 3 phase pipelines that connect of pipeline and deuterium air-capacitor receive bottles 2 mutually with optical fiber processing jar 5.Particularly, liquid nitrogen storage tank 1 is connected with gas mixing device 3 by pipeline 11, the deuterium air-capacitor is received bottle 2 and is connected with gas mixing device 3 by pipeline 21, on the gas mixing device 3 with pipeline 11 junctions with and be provided with control valve and flowmeter (not shown) with pipeline 21 junctions, to be used for controlling respectively the nitrogen that inputs to the gas mixing device and the amount of deuterium gas, make deuterium nitrogen mixed gas in the gas mixing device 3 reach the concentration of setting.
Gas mixing device 3 is connected with surge tank 4 by pipeline 31, the gaseous mixture of surge tank 4 storage setting pressures.Surge tank 4 is provided with deuterium gas concentration analyzer 6, by this analyzer 6, can measure the concentration of deuterium gas in the surge tank 4.
Optical fiber processing jar 5 has three pipeline connection ports, and first pipeline connection port is connected with liquid nitrogen storage tank 1 by pipeline 51, forms nitrogen and is blown into passage; Second pipeline connection port is connected with surge tank 4 by pipeline 52, forms gaseous mixture and is blown into passage; The 3rd pipeline connection port still is connected with surge tank 4 by pipeline 53, forms gaseous mixture recovery approach 7.Also be provided with vavuum pump and vacuum display list (not shown) in the optical fiber processing jar 5, before carrying out optical fiber processing, need optical fiber processing jar 5 is vacuumized.
The recyclable deuterium nitrogen of present embodiment blending device is mainly used in optical fiber and makes the scene, will describe gas mixing and recycling process below:
The optical fiber that at first will draw moulding is positioned over sealing locking in the optical fiber processing jar 5, the vavuum pump that starts optical fiber processing jar 5 earlier vacuumizes tank body, after the reading of vacuum display list reaches technological requirement, charge into nitrogen by pipeline 51 to the pure nitrogen gas of optical fiber processing jar 5 inlet and purge, so circulate and take out vacuum again one time after three times;
Then, open by-pass valve control and flowmeter that nitrogen and deuterium gas are supplied with simultaneously, nitrogen is transferred to variable proportioning gas mixer 3 from liquid storage tank 1 through pipeline 11; Deuterium gas is received bottle 2 through the variable proportioning gas mixer 3 of pipeline 21 feedings by the deuterium air-capacitor, directly carries out the deuterium nitrogen by adjusting control valve and flowmeter and is mixed, and arrives the pressure of setting, and stops inflation;
The deuterium nitrogen mixture gas that is mixed is entered surge tank 4 by pipeline 31, after deuterium gas and nitrogen are mixed certain hour, thereby utilize deuterium gas concentration analyzer 6 to detect gas concentrations and adjust deuterium gas and nitrogen amount is finely tuned mist by the accurate adjusting knob in the blender 3.
When the deuterium nitrogen mixed gas in the surge tank 4 need use, mist is filled into optical fiber processing jar 5 by pipeline 52.Keep optical fiber processing jar 5 environmental sealings, after keeping official hour under certain pressure, optical fiber processing finishes.Then, purge nitrogen to process tank 5, the deuterium/nitrogen mixed gas behind the processing optical fiber is recycled to surge tank 4 through pipeline 53 by pipeline 51.After the deuterium/nitrogen mixed gas that reclaims enters surge tank 4, thereby in processing range, will not charge into fresh deuterium/nitrogen mixed gas deuterium content is adjusted to suitable processing range by blender 3 if deuterium gas concentration analyzer 6 detects deuterium gas concentration, after treating that optical fiber processing jar 5 vacuumizes, gas in the surge tank after being mixed once more can be blown into utilization in the optical fiber processing jar 5, thereby realize the purpose of cycling and reutilization.
Because comprise hydrocarbon and other impurity in the deuterium/nitrogen that reclaims, thus the deuterium/nitrogen mixed gas that reclaims recycling can be discharged into after repeatedly outdoor.In the present embodiment, the purifier 8 that links to each other with surge tank 5, the deuterium/nitrogen mixed gas after repeatedly reclaiming is removed all gas beyond the deuterium gas by purifier 8, makes deuterium gas be collected, and has further reduced the optical fiber manufacturing cost.
The foregoing description only is explanation technical conceive of the present utility model and characteristics; its purpose is to allow the personage who is familiar with this technology can understand content of the present utility model and enforcement according to this; can not limit protection domain of the present utility model with this; all equivalences of doing according to the utility model spirit essence change or modify, and all should be encompassed within the protection domain of the present utility model.