CN201885976U - 一种快速检测鲜奶中含硫化物的试纸 - Google Patents

一种快速检测鲜奶中含硫化物的试纸 Download PDF

Info

Publication number
CN201885976U
CN201885976U CN2010206213738U CN201020621373U CN201885976U CN 201885976 U CN201885976 U CN 201885976U CN 2010206213738 U CN2010206213738 U CN 2010206213738U CN 201020621373 U CN201020621373 U CN 201020621373U CN 201885976 U CN201885976 U CN 201885976U
Authority
CN
China
Prior art keywords
test paper
fresh milk
bracket plate
handle
sulfur compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2010206213738U
Other languages
English (en)
Inventor
姚新奎
李海英
闫斌斌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xinjiang Agricultural University
Original Assignee
Xinjiang Agricultural University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xinjiang Agricultural University filed Critical Xinjiang Agricultural University
Priority to CN2010206213738U priority Critical patent/CN201885976U/zh
Application granted granted Critical
Publication of CN201885976U publication Critical patent/CN201885976U/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

本实用新型提供的一种快速检测鲜奶中含有硫化物的试纸,在圆形托板上安装手柄;托板上附着着试纸;组装时将托板的一端插入手柄的夹层中固定,使用时在托板的两面粘贴试纸直接插入牛奶中,润湿后取出,刮掉试纸上粘的鲜奶,观察颜色,呈灰色或黑色为阳性反应,即判定样品中含硫化物。该试纸重复测定8-10次即更换新的,有效保藏期为80-90天。该产品的手柄2与托板1可一次性加工成型,制作材料由木制、塑料及其他硬质材料构成。

Description

一种快速检测鲜奶中含硫化物的试纸
技术领域
本实用新型涉及畜产品质量安全检测,特别针对牛奶掺假的检测,在无检测设备条件下,采用该试纸能检测出鲜奶中硫化物的存在,具有重要的实用价值。
背景技术
牛乳营养丰富,富含多种人体所需的氨基酸及丰富的矿物质、蛋白质、脂肪、维生素等营养素,且易被消化吸收、物美价廉、食用方便,是生命最好的营养源,是自然界赐予我们的最理想天然食品之一。随着消费者对乳及乳制品需求量的逐年上升,为了牟取暴利,一些不法商贩,向牛乳中掺杂使假,这种行为不仅严重影响了鲜奶的品质,也极大地损害了广大消费者的切身利益和身体健康,同时也严重影响了乳品企业的经济效益。
奶农和养殖场为了防止鲜奶中加水以后比重下降而达不到收购标准,因此,常加入一些盐类物质增加比重,以便达到收购标准增加收入、谋取暴利,硫化物就是其中的一种。本实用新型为了保障消费者的身体健康,必须对乳中的硫化物掺入进行严格的检测,开发的试纸研制,受到消费者的青睐,同时也为牛乳收购单位以质论价提供客观依据等。
发明内容
本实用新型目的在于:所提供的快速检测鲜奶质量的试纸,易于生产,结构简单,携带方便;检测掺有硫化物的鲜奶灵敏度极高,既安全又环保。
本实用新型的目的是这样实现的:一种快速检测鲜奶中含有硫化物的试纸盒,在圆形托板1上安装手柄2;托板1上附着着试纸3。
本实用新型的产品,反应原理是硫离子与铅离子反应:S2-+Pb2+→PbS↓生成灰黑色的硫化铅沉淀,故得知鲜奶中的硫化物的存在,操作简单,十分灵敏,由于检测的下限为6μg/ml,故成本低廉,试纸不仅适用于奶站,也适用于家庭的检测,具有较高的实用价值,彰显技术进步。
附图说明
下面将结合附图对本实用新型作进一步说明。
图1为本实用新型的俯视结构示意图;
图2为本实用新型的主视结构示意图;
如图1、图2所示,试纸-3、手柄-2、托板-1;组装时将托板1的一端插入手柄2的夹层内固定;使用时将试纸3附着于托板1的面上即可。
具体实施方式
实施例
该产品的圆形托板1上安装手柄2;托板1上附着着试纸3;组装时将托板1的一端插入手柄2的夹层中固定;使用时在托板1的一面或两面粘贴试纸3,直接插入牛奶中,润湿后取出,刮掉试纸上粘的鲜奶,观察颜色,呈灰色或黑色为阳性反应,即可判定样品中含硫化物质。
该产品的手柄2与托板1可一次性加工成型,制作材料由木制、塑料及其他硬质材料构成。
试纸的制备及结果分析:
1、乙酸铅用量的确定
每个烧杯中加入不同量的乙酸铅试剂,再加入10ml95%乙醇、90ml去离子水,混匀,过滤,滤液中浸泡试纸(直径4cm),取出在暗处干燥,并按照上述试验方法进行检测。实验结果列于表1。
Figure 2010206213738100002DEST_PATH_IMAGE002
2、乙酸铅试纸浸泡时间确定
每个烧杯中加入10g乙酸铅试剂,再加入10ml95%乙醇、90ml蒸馏水,混匀,过滤,滤液中浸泡试纸(直径4cm),浸泡不同时间,取出在暗处干燥,并按照上述试验方法进行检测。实验结果列于表2。
Figure 2010206213738100002DEST_PATH_IMAGE004
3、硫化物检测下限的确定
按照上述确定的乙酸铅试纸做法,只改变硫化物在奶样中的浓度,试验结果列于表3。
Figure 2010206213738100002DEST_PATH_IMAGE006
4、试剂保存时间的确定
用当天制作的乙酸铅试纸,以及保存1个月、2个月、3个月的乙酸铅试纸,按照上述方法进行显色操作,重复测定10次,结果见表4。
Figure 2010206213738100002DEST_PATH_IMAGE008
综上所述,该试纸重复测定8-10次更换新的为宜。

Claims (2)

1.一种快速检测鲜奶中含有硫化物的试纸,其特征在于:在圆形托板(1)上安装手柄(2);托板(1)上附着着试纸(3)。
2.根据权利要求1所述的试纸,其特征在于:托板(1)和手柄(2)由木制、塑料及其他硬质材料构成。
CN2010206213738U 2010-11-24 2010-11-24 一种快速检测鲜奶中含硫化物的试纸 Expired - Fee Related CN201885976U (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2010206213738U CN201885976U (zh) 2010-11-24 2010-11-24 一种快速检测鲜奶中含硫化物的试纸

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2010206213738U CN201885976U (zh) 2010-11-24 2010-11-24 一种快速检测鲜奶中含硫化物的试纸

Publications (1)

Publication Number Publication Date
CN201885976U true CN201885976U (zh) 2011-06-29

Family

ID=44183521

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2010206213738U Expired - Fee Related CN201885976U (zh) 2010-11-24 2010-11-24 一种快速检测鲜奶中含硫化物的试纸

Country Status (1)

Country Link
CN (1) CN201885976U (zh)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102735797A (zh) * 2011-07-19 2012-10-17 成都中医药大学 一种中药材或中药饮片二氧化硫残留量限量的检测方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102735797A (zh) * 2011-07-19 2012-10-17 成都中医药大学 一种中药材或中药饮片二氧化硫残留量限量的检测方法
CN102735797B (zh) * 2011-07-19 2016-01-06 成都中医药大学 一种中药材或中药饮片二氧化硫残留量限量的检测方法

Similar Documents

Publication Publication Date Title
Boersma et al. Temperature driven changes in the diet preference of omnivorous copepods: no more meat when it's hot?
Pen et al. Effects of Yucca schidigera and Quillaja saponaria extracts on in vitro ruminal fermentation and methane emission
Trabue et al. Emissions of greenhouse gases, ammonia, and hydrogen sulfide from pigs fed standard diets and diets supplemented with dried distillers grains with solubles
Sun et al. Latitudinal distribution of zooplankton communities in the Western Pacific along 160 E during summer 2014
Molano et al. Fumaric acid supplements have no effect on methane emissions per unit of feed intake in wether lambs
Brulé et al. Modified batch anaerobic digestion assay for testing efficiencies of trace metal additives to enhance methane production of energy crops
Rosato Managing biogas plants: A practical guide
CN201885976U (zh) 一种快速检测鲜奶中含硫化物的试纸
Fang et al. Freshwater fish–consumption relations with total hair mercury and selenium among women in Eastern China
Ren et al. Effects of tributyrin supplementation on ruminal microbial protein yield, fermentation characteristics and nutrients degradability in adult Small Tail ewes
Wang et al. Tracing the organic matter source of cage culture sediments based on stable carbon and nitrogen isotopes in Poyang Lake, China
Bayne Carbon and nitrogen relationships in the feeding and growth of the Pacific oyster, Crassostrea gigas (Thunberg)
Koski et al. Seasonal changes in food quantity and quality of the common North Sea copepods Temora longicornis and Pseudocalanus elongatus: a bioassay approach
Barham et al. Risk of adulteration in milk consumed at Shaheed Benazirabad District of Sindh
Thanh et al. Effect of potassium nitrate or urea as NPN source and levels of Mangosteen peel on in vitro gas and methane production using molasses, Operculina turpethum and Brachiaria mutica as substrate
Min et al. Condensed and hydrolyzable tannins for reducing methane and nitrous oxide emissions in dairy manure—A laboratory incubation study
Koski et al. Post-bloom feeding of Calanus finmarchicus copepodites: selection for autotrophic versus heterotrophic prey
Galindo et al. Effect of Tithonia diversifolia (Hemsl.) Gray (Giant Mexican Sunflower) on the population of rumen protozoa and methanogens under in vitro conditions
Niu et al. Effects of Caragana korshinskii tannin on fermentation, methane emission, community of methanogens, and metabolome of rumen in sheep
Jin et al. Effects of winter and spring housing on growth performance and blood metabolites of Pengbo semi-wool sheep in Tibet
Gutseit et al. Food quality for Daphnia in humic and clear water lakes
Bulliyya et al. Determination of iodine nutrition and community knowledge regarding iodine deficiency disorders in selected tribal blocks of Orissa, India
Serra Estimation of carbon footprint in dairy cattle farms of Southern Italy
Lee et al. Stable carbon and nitrogen isotope composition of co-existing herbivorous zooplankton species in an oligo-dystrophic lake (Shirakoma-ike, Japan)
Kang et al. Improving ruminal fermentation and nutrient digestibility in dairy steers by banana flower powder-pellet supplementation

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110629

Termination date: 20151124