CN201416028Y - Metal titanium extracting device - Google Patents
Metal titanium extracting device Download PDFInfo
- Publication number
- CN201416028Y CN201416028Y CN2009201550516U CN200920155051U CN201416028Y CN 201416028 Y CN201416028 Y CN 201416028Y CN 2009201550516 U CN2009201550516 U CN 2009201550516U CN 200920155051 U CN200920155051 U CN 200920155051U CN 201416028 Y CN201416028 Y CN 201416028Y
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- main body
- metal titanium
- cover plate
- extraction plant
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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Abstract
The utility model discloses a metal titanium extracting device, including a main body the upper part of which forms an opening and the internal part of which is hollow; a cover plate for covering theopening and sealing the main body; a cooling unit arranged on the cover plate and extended to the inner part of the main body; a porous container arranged between the bottom of the main body and the cooling unit; and a gas draft tube communicated with the inner space of the main body. The metal titanium extracting device of the utility model has simple structure, convenient assembly and disassembly, and low equipment cost; is able to effectively utilize the extraction agent so as to have high extraction efficiency. It is unnecessary to separate the new and old titanium alloys.
Description
Technical field
The utility model relates to a kind of metal titanium extraction plant, relates in particular to a kind of extraction plant that extracts metal titanium from titanium alloy (for example titanium alloy waste material).
Background technology
Titanium and alloy thereof are because its fusing point height, light specific gravity, characteristics such as intensity is big, erosion resistance is strong have vast application at aspects such as modern aviation, rocket-powered missile industry, spationautics, firearms naval vessels, bio-medical material and chemical industry equipments.
Traditional system titanium method is the Kroll method, just adopts the reactive mode of MAGNESIUM METAL reducing metal titanium from titanium tetrachloride, and reaction unit is a sponge titanium reaction furnace.Therefore traditional sponge titanium reaction furnace efficient is low, and energy consumption is big, needs a kind of efficient height, simple in structure and reaction unit that cost is low.
The utility model content
The purpose of this utility model is to provide a kind of separation that can effectively improve extraction efficiency, be convenient to new and old titanium alloy, simple in structure, the installation and removal and the low metal titanium extraction plant of cost that are easy to equipment.
To achieve these goals, comprise according to metal titanium extraction plant of the present utility model: opening is formed at top, inside is the main body of hollow; Hide described opening and seal the cover plate of described main body; Be arranged at described cover plate and extend to the cooling unit of the inside of described main body; Be arranged at the bottom of described main body and the porous container between the described cooling unit; The gas diversion tube that is connected with the internal space of described main body.
At this, described cooling unit comprises: protrude and the cooling end that is used to hold refrigerant of formation to the inside of described main body from described cover plate; Connect described cover plate and extend to the refrigerant ingress pipe that described cooling end is used to supply with refrigerant; Connect described cover plate and extend to the refrigerant delivery line that described cooling end is used to discharge refrigerant.Described cooling end can form more than two, and described refrigerant can be water or other liquid or gas.
In addition, described gas diversion tube can connect described cover plate and be provided with, and also can connect the sidewall of described main body and is provided with.
In addition, inside in described main body also is provided with the support component that is used to support described porous container, and this support component can be formed as one the brace table at the inwall of described main body, also can be for be arranged on the support of the bottom of described main body with independent component form.
And the utility model is formed with a plurality of holes on described porous container, and the preferred diameter in this hole is 30%～90% of a titanium alloy size to be extracted.
And the utility model can also comprise the crucible of the bottom that is arranged at described main body as required.
In addition, the utility model also can comprise vapor pipe as required, and this vapor pipe can connect described cover plate and be provided with, and also can connect the sidewall of described main body and is provided with.
The utility model is as a kind of extraction plant that extracts metal titanium from titanium alloy, and it is simple in structure, and installation and removal are convenient, and equipment cost is low, and can effectively utilize extraction agent, and the extraction efficiency height need not to separate to new and old alloy.
Description of drawings
Fig. 1 is the structural representation according to the metal titanium extraction plant of the utility model first embodiment;
Fig. 2 is the structural representation according to the metal titanium extraction plant of the utility model second embodiment.
[nomenclature]
10: main body 11: cover plate 20: cooling unit
21: refrigerant 22: cooling end 23: the refrigerant ingress pipe
24: refrigerant delivery line 30: crucible 31: extraction agent
32: porous container 33: titanium alloy 40 to be extracted: brace table
41: support 50: gas diversion tube 51: vapor pipe
Embodiment
Below, describe embodiment of the present utility model in detail with reference to accompanying drawing.Following embodiment provides in order to make those skilled in the art fully understand content of the present utility model, and it can have various other distortion examples, and protection domain of the present utility model is not to be confined to the following embodiment that will illustrate.
Fig. 1 is the structural representation according to the metal titanium extraction plant of the utility model first embodiment.As shown in Figure 1, the extraction plant of present embodiment comprises: main body 10, cover plate 11, cooling unit 20, porous container 32 and gas diversion tube 50.
Wherein, described main body 10 is the top opening substantially as the container that extracts and inside is the cylindrical shape of hollow, generally adopts stainless steel to make, and will hold extraction agent 31 in its bottom.Described extraction agent 31 generally can use Metal Zn or metal Pb.In addition, described main body 10 can also be other shapes such as polygon prism, so long as the container of hollow, its shape there is no special qualification.
Described cover plate 11 constitutes with the shape corresponding to the opening of described main body 10, thereby with the opening covering of described cover plate 11 with described main body 10, to seal the internal space of described main body 10.
Described cooling unit 20 is arranged on described cover plate 11 and extends in the internal space of described main body 10.At this, described cooling unit 20 comprises: cooling end 22, and it protrudes and the formation certain inside space to the inside of described main body 10 from described cover plate 11, is contained with refrigerant 21 in this internal space; Refrigerant ingress pipe 23, the internal space that it connects described cover plate 11 and extends to described cooling end 22 is to be used for to the internal space of described cooling end 22 supply coolant 21; Refrigerant delivery line 24, discharge by the refrigerant 21 of heat exchange from the internal space of described cooling end 22 to the outside being used for the internal space that it connects described cover plate 11 and extends to described cooling end 22.Described refrigerant 21 can all can be used for the refrigerative fluidity substance for water or cryogenic gas etc.Wherein, cooling end 22 its surfaces of protruding to the internal space of described main body 10 have certain radian.Though 22 of the cooling ends among Fig. 1 form one, can also form more than two as required.When being two, cooling end 22 preferably is interconnected between the internal space of each cooling end when above, so that import and derive refrigerant smoothly to the inside of each cooling end.
Described porous container 32 is arranged on the inside of described main body 10, and is positioned at the below of the cooling end 22 of described cooling unit 20, and the bottom certain height of the described main body 10 of distance.Specifically, described porous container 32 is arranged in the position between the bottom of the cooling end 22 of described cooling unit 20 and described main body 10, and is positioned at the top of the extraction agent 31 that is contained in described main body 10 bottoms.Described porous container 32 is formed with a plurality of holes, and titanium alloy 33 to be extracted is contained in 32 li of this porous containers.At this, the diameter in hole that is formed at described porous container 32 is less than the size of titanium alloy to be extracted, and the preferred diameter in described hole is 30%～90% of a titanium alloy size to be extracted.
Described gas diversion tube 50 connects described cover plate 11 and is connected with the internal space of main body 10.Certainly, described gas diversion tube 50 can also connect the sidewall of described main body 10 and be connected with the internal space of main body 10.Described gas diversion tube 50 is used for internal space to described main body 10 and vacuumizes and/or import rare gas elementes such as argon gas to the inside of described main body 10.
According to the extraction plant of first embodiment, also can comprise vapor pipe 51, this vapor pipe 51 connects described cover plate 11 and is connected with the internal space of main body 10.At this, described vapor pipe 51 can also connect the sidewall of described main body 10 and be connected with the internal space of main body 10.Described vapor pipe 51 is used for the internal space of described main body 10 is vacuumized or discharges the air of main body 10 inside.
In addition, according to the extraction plant of first embodiment, also be formed with brace table 40 at the inwall of main body 10, to be used for described porous container 32 support arrangement in the inside of described main body 10.
Fig. 2 is the structural representation according to the metal titanium extraction plant of the utility model second embodiment.Compare with first embodiment, the structure of extraction plant and first embodiment are basic identical among second embodiment, give same symbol for identical parts, and detailed.
At this as shown in Figure 2, the difference of second embodiment and first embodiment is, also be provided with crucible 30 in the bottom of main body 10, and extraction agent 31 is contained in the inside of this crucible 30.Described crucible 30 generally is made of stainless steel or aluminum oxide material, and its shape can be the various shapes of being convenient to hold extraction agent 31 such as cylinder or polygon prism.
In addition, extraction plant according to second embodiment does not have the brace table 40 that adopts as first embodiment, but be provided with bracing frame 41 in the bottom of main body 10 with the form of separate part, to be used for described porous container 32 support arrangement in the inside of described main body 10.As long as can support described porous container 32, support frame as described above 40 can adopt arbitrary form.
Below, the embodiment shown in seeing figures.1.and.2 describes the working process of utilizing extraction plant of the present utility model to carry out the metal titanium extraction.
At first, extraction agent 31 is put into the bottom (as shown in Figure 1) of main body 10 or put into the inside (as shown in Figure 2) of the crucible 30 that is positioned at main body 10 bottoms.Then, the porous container 32 that titanium alloy to be extracted 33 is housed is fixed on the support component of main body 10 inside.At this, described support component can be brace table 40 or bracing frame as shown in Figure 2 41 as shown in Figure 1.Then, cover the upper opening of main body 10, thereby seal the internal space of described main body 10 with cover plate 11.Then, the internal space of main body 10 is vacuumized, and make refrigerant 21 flow into and flow out the internal space of cooling end 22 by refrigerant ingress pipe 23 and refrigerant delivery line 24.At this, need to prove when extraction plant does not have vapor pipe 51, vacuumize by 50 pairs of main bodys 10 of gas diversion tube, and when extraction plant also is provided with vapor pipe 51, can vacuumize by 51 pairs of main bodys 10 of this vapor pipe.Then, main body 10 heated make it to heat up, after temperature reached the fusing point of extraction agent 31, the steam of extraction agent 31 can rise rapidly, runs into cooling end 22, and the steam of extraction agent 31 will be condensate in the surface of cooling end 22.At this moment, the main body 10 inner argon gas that feed to vacuum, the extraction agent 31 that is condensate in cooling end 22 surfaces will drop onto on the porous container 32, titanium alloy to be extracted 33 reactions with the inside, titanium is wherein extracted, form liquid state, and fall into the bottom (as shown in Figure 1) of main body 10 or the inside (as shown in Figure 2) of crucible 30 by formed hole on the porous container 32.At this, need to prove no matter whether extraction plant have vapor pipe 51, all pass through main body 10 inner the feed argon gas of this gas diversion tube 50 to vacuum.After extraction finishes, cooling, the titanium alloy of this stylish formation is in the bottom (as shown in Figure 1) of main body 10 or the inside (as shown in Figure 2) of crucible 30, and original alloy is positioned at 32 li of porous containers.
In above-mentioned process, vacuumizing not is to be necessary step.It is in order to make extraction agent 31 easier evaporations when the heating that the inside of main body 10 is vacuumized, and be the better argon atmosphere of extraction construction of metal titanium.When extraction plant also is provided with vapor pipe 51, can vacuumize the internal space of main body 10.At this moment, import the argon gas of certain hour to the internal space of main body 10 by gas diversion tube 50, because the density of argon gas is greater than air, so importing along with argon gas, begin argon gas from the bottom of main body 10 inside and can replace air gradually, in this process, air can discharge by vapor pipe 51.
Below, explanation utilizes extraction plant shown in Figure 1 with reference to above-mentioned extraction process, the experimental example 1 that the Si-Fe-Ti alloy is extracted by the metal Pb extraction agent.
Get the Si-Fe-Ti alloy that 120g prepares, be placed in the porous container 32, the 250 gram metal Pb of weighing simultaneously join the bottom of main body 10.Under vacuum condition, heat up, when reaching the temperature of reaction (800 ℃), in main body, feed argon gas, made in the argon atmosphere that is reflected under the normal pressure reaction 2 hours, cool, thereby obtain the Pb-Ti alloy.Chemical analysis is carried out in sampling, and this alloy shows that through chemical analysis containing Ti is 11.98%, and Pb is 87.89%.Calculate according to chemical analysis results, this reaction, extraction efficient is 83%.
Below, explanation utilizes extraction plant shown in Figure 2 with reference to above-mentioned extraction process, the experimental example 2 that the Sn-Ti alloy is extracted by the Metal Zn extraction agent.
Get 130 and restrain the Sn-Ti alloy of getting ready, be placed in the porous container 32, the 250 gram Metal Zn of weighing simultaneously join in the crucible 30.Under vacuum condition, heat up, when reaching the temperature of reaction (800 ℃), in main body, feed argon gas, made in the argon atmosphere that is reflected under the normal pressure reaction 2 hours, cool, thereby obtain the Zn-Ti alloy.Chemical analysis is carried out in sampling, and this alloy shows that through chemical analysis containing Ti is 13.67%, and Zn is 86.04%.Calculate according to chemical analysis results, this reaction, extraction efficient is 86%.
Because the fusing point of Pb and Zn is low and volatile, so the product P b-Ti alloy or the Zn-Ti alloy that above-mentioned experimental example can be obtained distill according to 800 ℃ to 1200 ℃ temperature under vacuum condition, metal titanium extracts the most at last.
Can learn in view of the above, need not the new and old titanium alloy in the main body is separated by extraction plant of the present utility model, and can obtain quite high extraction efficiency.
Although illustrated and described embodiment more of the present utility model, but those skilled in the art will be appreciated that: under the situation that does not break away from principle of the present utility model and spirit, can change these embodiments, wherein, scope of the present utility model limits in claim and equivalent thereof.
Claims (10)
1, a kind of metal titanium extraction plant is characterized in that comprising:
Opening is formed at top, inside is the main body of hollow;
Hide described opening and seal the cover plate of described main body;
Be arranged at described cover plate and extend to the cooling unit of the inside of described main body;
Be arranged at the bottom of described main body and the porous container between the described cooling unit;
The gas diversion tube that is connected with the internal space of described main body.
2, metal titanium extraction plant according to claim 1 is characterized in that described cooling unit comprises: protrude and the cooling end that is used to hold refrigerant of formation to the inside of described main body from described cover plate; Connect described cover plate and extend to the refrigerant ingress pipe that described cooling end is used to supply with refrigerant; Connect described cover plate and extend to the refrigerant delivery line that described cooling end is used for discharging refrigerant.
3, metal titanium extraction plant according to claim 2 is characterized in that described cooling end forms more than two.
4, metal titanium extraction plant according to claim 2 is characterized in that described refrigerant is liquid or gas.
5, metal titanium extraction plant according to claim 1 is characterized in that described gas diversion tube connects the sidewall of described cover plate or described main body.
6, metal titanium extraction plant according to claim 1 is characterized in that also being provided with support component in the inside of described main body, to be used to support described porous container.
7, metal titanium extraction plant according to claim 6 is characterized in that described support component is formed as one at the brace table of the inwall of described main body or is arranged on the support of the bottom of described main body with independent parts.
8, metal titanium extraction plant according to claim 1, the aperture that it is characterized in that being formed on described porous container are 30%～90% of titanium alloy size to be extracted.
9, metal titanium extraction plant according to claim 1 is characterized in that also comprising the crucible of the bottom that is arranged at described main body.
10, according to any described metal titanium extraction plant in the claim 1 to 9, it is characterized in that also comprising vapor pipe, this vapor pipe connects the sidewall of described cover plate or described main body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009201550516U CN201416028Y (en) | 2009-06-10 | 2009-06-10 | Metal titanium extracting device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009201550516U CN201416028Y (en) | 2009-06-10 | 2009-06-10 | Metal titanium extracting device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201416028Y true CN201416028Y (en) | 2010-03-03 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2009201550516U Expired - Fee Related CN201416028Y (en) | 2009-06-10 | 2009-06-10 | Metal titanium extracting device |
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| CN (1) | CN201416028Y (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107567505A (en) * | 2015-02-12 | 2018-01-09 | 伊克有限责任公司 | For separating and reclaiming the device and method of alloy, the particularly component of precious metal alloys |
-
2009
- 2009-06-10 CN CN2009201550516U patent/CN201416028Y/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107567505A (en) * | 2015-02-12 | 2018-01-09 | 伊克有限责任公司 | For separating and reclaiming the device and method of alloy, the particularly component of precious metal alloys |
| US10550449B2 (en) | 2015-02-12 | 2020-02-04 | Ikoi S.P.A. | Apparatus and process for separating and recovering the components of an alloy, particularly a noble alloy |
| US11427885B2 (en) | 2015-02-12 | 2022-08-30 | Ikoi S.P.A. | Apparatus and process for separating and recovering the components of an alloy, particularly a noble alloy |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: PANZHIHUA IRON AND STEEL GROUP CO., LTD. PANZHIHUA Free format text: FORMER OWNER: PANZHIHUA IRON AND STEEL GROUP CO., LTD. PANZHIHUA IRON + STEEL INSTITUTE OF PANZHIHUA IRON + STEEL GROUP CO., LTD. |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20100416 Address after: 611731, Tianlong Road, Chengdu hi tech Zone (West Zone, Sichuan) 1 Patentee after: Pangang Group Institute Co., Ltd. Patentee after: Pangang Group Co., Ltd. Patentee after: Pangang Group Panzhihua Iron & Steel Research Institute Co., Ltd. Patentee after: Panzhihua New Steel & Vanadium Co., Ltd. Address before: 611731, Tianlong Road, Chengdu hi tech Zone (West Zone, Sichuan) 1 Patentee before: Pangang Group Institute Co., Ltd. Patentee before: Panzhihua Iron and Steel (Group) Co., Ltd. Patentee before: Pangang Group Panzhihua Iron & Steel Research Institute Co., Ltd. |
|
| C56 | Change in the name or address of the patentee | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 611731, Tianlong Road, Chengdu hi tech Zone (West Zone, Sichuan) 1 Co-patentee after: Pangang Group Co., Ltd. Patentee after: Pangang Group Institute Co., Ltd. Co-patentee after: Pangang Group Panzhihua Iron & Steel Research Institute Co., Ltd. Co-patentee after: Pangang Group Steel Vanadium & Titanium Co., Ltd. Address before: 611731, Tianlong Road, Chengdu hi tech Zone (West Zone, Sichuan) 1 Co-patentee before: Pangang Group Co., Ltd. Patentee before: Pangang Group Institute Co., Ltd. Co-patentee before: Pangang Group Panzhihua Iron & Steel Research Institute Co., Ltd. Co-patentee before: Panzhihua New Steel & Vanadium Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100303 Termination date: 20160610 |