CN200970526Y - Small self sucking pressure reducing distilling extractor - Google Patents
Small self sucking pressure reducing distilling extractor Download PDFInfo
- Publication number
- CN200970526Y CN200970526Y CN 200620011287 CN200620011287U CN200970526Y CN 200970526 Y CN200970526 Y CN 200970526Y CN 200620011287 CN200620011287 CN 200620011287 CN 200620011287 U CN200620011287 U CN 200620011287U CN 200970526 Y CN200970526 Y CN 200970526Y
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- Prior art keywords
- receiving flask
- pipe
- cold water
- water chamber
- vertical fluid
- Prior art date
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 238000004821 distillation Methods 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 8
- 238000007789 sealing Methods 0.000 claims abstract description 7
- 239000012530 fluid Substances 0.000 claims description 22
- 230000006837 decompression Effects 0.000 claims description 13
- 239000000498 cooling water Substances 0.000 claims description 9
- 238000005452 bending Methods 0.000 claims description 3
- 238000003780 insertion Methods 0.000 claims description 2
- 230000037431 insertion Effects 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 238000001816 cooling Methods 0.000 abstract description 4
- 238000010521 absorption reaction Methods 0.000 abstract 2
- 238000005292 vacuum distillation Methods 0.000 abstract 2
- 238000005265 energy consumption Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 description 5
- 239000003814 drug Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000973497 Siphonognathus argyrophanes Species 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
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- Extraction Or Liquid Replacement (AREA)
Abstract
The utility model discloses a minitype self-absorption vacuum distillation extractor, and composes a distillation flask (1), a heating boiler (2), a cooling tube (3), a cold water chamber (4), a receiving flask (5) and a bracket (6). A capillary (8), a thermometer (9) and a canal (10) are inserted onto a sealing rubber plug (7) on the opening of the distillation flask (1). The external end of the canal (10) is flexed downwards to connect the upper cooling tube (3). The utility model is characterized in that the cold water outlet of the cold water chamber (4) is connected with an upper vertical jet pipe (13). An upwards inclined side pipe (14) is positioned on the lower end of the vertical jet pipe (13). The upper end of the upwards inclined side pipe (14) threads the rubber plug on the opening of the receiving flask (5) and insert into the upper part of the receiving flask (5) after being bended. Not only the pressure can be reduced in the receiving flask, but also the receiving flask can be prevented from blast by using this minitype self-absorption vacuum distillation extractor. And with simple structure and easy operation, the utility model needs no evacuating equipment, so the energy consumption is saved and the manufacturing cost is reduced.
Description
Technical field
The utility model relates to the improvement that is usually used in the small-sized distillation extraction element that separates, extract volatile organic matter and produce distilled water in a kind of drug inspection and the fields such as pharmaceutical manufacturing, a kind of specifically small-sized self-priming decompression distillation extractor.
Background technology
In drug inspection and pharmaceutical manufacturing, small-sized distillation extraction element can be used for extraction of substance and separating volatile organic substance, also can be used to produce necessary distilled water.Present employed small-sized distilling apparatus, comprise that parts such as cucurbit, heating kettle, condenser pipe, cold water chamber, receiving flask and support constitute, oral area at cucurbit is established sealing rubber plug, and insertion capillary, thermometer and conduit, the liquid or the volatile materials of in cucurbit, packing into and being distilled, heating back forms steam or escaping gas, entering receiving flask after being cooled to liquid through condenser pipe, and condenser pipe generally is to pass the cooling of lowering the temperature of mobile cold water chamber.This small-sized distillation extraction element, steam is all insufficient through general cooling behind the condenser pipe, the fluid temperature that enters in the receiving flask is higher, and there is the steam that part is not condensed to enter in the receiving flask, breather pipe in the receiving flask can not in time be discharged gas, cause the increased pressure in the receiving flask, cause the receiving flask blast, produce unsafe factor.A kind of small-sized decompression distillation device is also arranged, its decompressor is the aspiration pump that adopts, reduce pressure though can make in the receiving flask by bleeding, prevent to explode because of increased pressure, but increased energy resource consumption, improved production cost, and complex structure, not easy to operate, the decompression pressure wayward, the excessive reduction that also causes condensation effect of reducing pressure.
Summary of the invention
The purpose of this utility model is to provide a kind of can make the pressure in the receiving flask reach decompression, need not again increases new power set, utilizes self intrasystem energy just can reach decompression in the receiving flask and simple in structure, easy operation, excessive decompression can not occur, influences the small-sized self-priming decompression distillation extractor of condensation effect.
For reaching above purpose, the technical scheme that the utility model adopted is: this small-sized self-priming decompression distillation extractor, by cucurbit, heating kettle, condenser pipe, cold water chamber, receiving flask reaches to prop up and is configured to, oral area at cucurbit is established sealing rubber plug, insert capillary beyond the Great Wall at caulking gum, thermometer and conduit, the curved connection gone up condenser pipe under the outer end of conduit, condenser pipe is a helix tube, the rubber stopper that the receiving flask oral area is passed in the lower end inserts in the receiving flask, the pigtail of condenser pipe is located in the cold water chamber, the cooling water inlet of cold water chamber can be connected with running water pipe, it is characterized in that connecting the vertical fluid pipe on the cooling water outlet of cold water chamber, on the sidewall of the lower end of vertical fluid pipe, establish tiltedly side pipe, upward pass the rubber stopper of receiving flask oral area after the upper end bending of oblique side pipe, insert the top in the receiving flask, the operation principle of its characteristic is: after cold water enters cold water chamber, carry out heat exchange with condenser pipe, enter in the receiving flask after making the interior steam of condenser pipe condense into liquid, become malleation in the receiving flask, cooling water flows out from the vertical fluid pipe, under the hydraulic pressure in running water pipe, and the vertical fluid pipe is a plumbness, the flowing water non-resistance, make the flow velocity of water very fast, on flowing through, tiltedly during the oral area of side pipe, make oblique side pipe oral area formation negative pressure, have swabbing action, thereby the barotropic gas in the receiving flask is derived easily, under continuous duty, can become negative pressure state in the receiving flask, produce the generation of explosion accident so can avoid the supercharging of receiving flask internal cause.The utility model is also implemented by following measure: the described oral area of oblique side pipe is flat mouthful, communicate with the inner chamber of vertical fluid pipe, the angle of going up oblique side pipe and vertical fluid pipe intersection is the 5-15 degree, establish the piece that is locked that bonds at last oblique side pipe and vertical fluid pipe intersection, it is fixed, and prevent to break; The cooling water outlet of cold water chamber is located at the top of cold water chamber, and vertical fluid water inlet tube mouth potential is improved, and can help improving the flow velocity of water; Described support is made of base, montant and horizontal fixed bar, horizontal fixedly supporting plate, and receiving flask places on the base by cushion block, and the vertical fluid pipe is fixed by horizontal fixed bar, and heating kettle places on the horizontal fixedly supporting plate of montant upper end.
The beneficial effects of the utility model are: with at present medicine detect and pharmaceutical production in employed small-sized distillation extraction element compare, can not only make and form decompression in the receiving flask, prevent the blast of receiving flask, and simple in structure, easy operation, need not to increase air extractor, so but energy efficient reduces production costs.
Description of drawings
Fig. 1 is the utility model structure office cross-sectional schematic.
Fig. 2 analyses and observe enlarged diagram for the utility model vertical fluid pipe and last oblique side pipe infall.
The specific embodiment
Make the utility model with reference to accompanying drawing 1,2.This small-sized self-priming decompression distillation extractor, by cucurbit 1, heating kettle 2, condenser pipe 3, cold water chamber 4, receiving flask 5 and support 6 constitute, establish sealing rubber plug 7 at the oral area of cucurbit 1, on sealing rubber plug 7, insert capillary 8, thermometer 9 and conduit 10, curved down connection of the outer end of conduit 10 gone up condenser pipe 3, condenser pipe 3 is a helix tube, the rubber stopper that receiving flask 5 oral areas are passed in the lower end inserts in the receiving flask 5, the pigtail of condenser pipe 3 is located in the cold water chamber 4, the cooling water inlet 11 of cold water chamber 4 can be connected with running water pipe, on the cooling water outlet 12 of cold water chamber 4, connect vertical fluid pipe 13, on the sidewall of the lower end of vertical fluid pipe 13, establish tiltedly side pipe 14, upward pass the rubber stopper of receiving flask 5 oral areas after the upper end bending of oblique side pipe 14, the top of inserting receiving flask 5.The described oral area of oblique side pipe 14 is flat mouthful, and with the intracavity inter-connection of vertical fluid pipe 13, the angle of going up oblique side pipe 14 and vertical fluid pipe 13 intersections is the 5-15 degree, establishes the piece 15 that is locked that bonds at last oblique side pipe 14 with vertical fluid pipe 13 intersections; The cooling water outlet 12 of cold water chamber 4 is located at the top of cold water chamber 4; Described support 6 is made of base, montant and horizontal fixed bar, horizontal fixed head, and receiving flask 5 places on the base by cushion block, and vertical fluid pipe 13 is fixed by horizontal fixed bar, and heating kettle 2 places on the horizontal fixedly supporting plate of montant upper end.
Claims (2)
1, a kind of small-sized self-priming decompression distillation extractor, by cucurbit (1), heating kettle (2), condenser pipe (3), cold water chamber (4), receiving flask (5) and support (6) constitute, establish sealing rubber plug (7) at the oral area of cucurbit (1), go up insertion capillary (8) at sealing rubber plug (7), thermometer (9) and conduit (10), curved down connection of the outer end of conduit (10) gone up condenser pipe (3), condenser pipe (3) is a helix tube, the rubber stopper that receiving flask (5) oral area is passed in the lower end inserts in the receiving flask (5), the pigtail of condenser pipe (3) is located in the cold water chamber (4), it is characterized in that on the cooling water outlet (12) of cold water chamber (4), connecting vertical fluid pipe (13), on the lower end sidewall of vertical fluid pipe (13), establish oblique side pipe (14), upward pass the rubber stopper of receiving flask (5) oral area after the upper end bending of oblique side pipe (14), the top of inserting receiving flask (5).
2, small-sized self-priming decompression distillation extractor according to claim 1, it is characterized in that the described oral area of oblique side pipe (14) is flat mouthful, communicate with the inner chamber of vertical fluid pipe (13), the angle of going up oblique side pipe (14) and vertical fluid pipe (13) intersection is the 5-15 degree, establishes the piece (15) that is locked that bonds in last oblique side pipe (14) and vertical fluid pipe (13) intersection; The cooling water outlet (12) of cold water chamber (4) is located at the top of cold water chamber (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200620011287 CN200970526Y (en) | 2006-10-30 | 2006-10-30 | Small self sucking pressure reducing distilling extractor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200620011287 CN200970526Y (en) | 2006-10-30 | 2006-10-30 | Small self sucking pressure reducing distilling extractor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN200970526Y true CN200970526Y (en) | 2007-11-07 |
Family
ID=38881784
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200620011287 Expired - Fee Related CN200970526Y (en) | 2006-10-30 | 2006-10-30 | Small self sucking pressure reducing distilling extractor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN200970526Y (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101530821B (en) * | 2009-03-16 | 2011-03-16 | 段作敏 | Intelligent integrated distillation apparatus |
| CN102343290A (en) * | 2011-11-11 | 2012-02-08 | 河南科技大学 | Circulating water distiller for laboratory |
| CN103263783A (en) * | 2013-05-23 | 2013-08-28 | 湖北民族学院 | Self-suction extracting and recycling device |
| CN103484255A (en) * | 2013-09-24 | 2014-01-01 | 济南惠农玫瑰花精油有限公司 | Secondary condensation extraction process and condensation equipment for rose essential oil |
| CN103657459A (en) * | 2013-08-26 | 2014-03-26 | 上海维埃姆环保科技有限公司 | Ozone water production equipment |
| CN105013549A (en) * | 2015-07-09 | 2015-11-04 | 滁州市润达溶剂有限公司 | Decompression distillation flask |
| CN105597353A (en) * | 2015-12-18 | 2016-05-25 | 济南盛泰电子科技有限公司 | Liquid distillation condensing device |
| CN107715936A (en) * | 2017-11-02 | 2018-02-23 | 西安工程大学 | A kind of integral type distilling apparatus and distillating method |
| CN109100465A (en) * | 2017-06-21 | 2018-12-28 | 中国计量科学研究院 | A kind of azeotropic distillation sampling device and the line measuring system for moisture content comprising the sampling device |
| CN114642893A (en) * | 2022-03-25 | 2022-06-21 | 百色学院 | Energy-saving device and method for reduced pressure distillation of water-insoluble organic solvent |
| CN116355688A (en) * | 2023-04-04 | 2023-06-30 | 浙江工业大学 | Chimonanthus salicifolius volatile oil, and its preparation method and application by decompression extraction |
-
2006
- 2006-10-30 CN CN 200620011287 patent/CN200970526Y/en not_active Expired - Fee Related
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101530821B (en) * | 2009-03-16 | 2011-03-16 | 段作敏 | Intelligent integrated distillation apparatus |
| CN102343290A (en) * | 2011-11-11 | 2012-02-08 | 河南科技大学 | Circulating water distiller for laboratory |
| CN102343290B (en) * | 2011-11-11 | 2013-12-11 | 河南科技大学 | Circulating water distiller for laboratory |
| CN103263783A (en) * | 2013-05-23 | 2013-08-28 | 湖北民族学院 | Self-suction extracting and recycling device |
| CN103263783B (en) * | 2013-05-23 | 2015-03-25 | 湖北民族学院 | A self-priming extraction and recovery device |
| CN103657459B (en) * | 2013-08-26 | 2016-02-03 | 上海维埃姆环保科技有限公司 | A kind of ozone water production equipment |
| CN103657459A (en) * | 2013-08-26 | 2014-03-26 | 上海维埃姆环保科技有限公司 | Ozone water production equipment |
| CN103484255A (en) * | 2013-09-24 | 2014-01-01 | 济南惠农玫瑰花精油有限公司 | Secondary condensation extraction process and condensation equipment for rose essential oil |
| CN103484255B (en) * | 2013-09-24 | 2015-03-25 | 济南惠农玫瑰花精油有限公司 | Secondary condensation extraction process and condensation equipment for rose essential oil |
| CN105013549A (en) * | 2015-07-09 | 2015-11-04 | 滁州市润达溶剂有限公司 | Decompression distillation flask |
| CN105597353A (en) * | 2015-12-18 | 2016-05-25 | 济南盛泰电子科技有限公司 | Liquid distillation condensing device |
| CN109100465A (en) * | 2017-06-21 | 2018-12-28 | 中国计量科学研究院 | A kind of azeotropic distillation sampling device and the line measuring system for moisture content comprising the sampling device |
| CN109100465B (en) * | 2017-06-21 | 2024-04-12 | 中国计量科学研究院 | Azeotropic distillation sampling device and moisture measurement system comprising same |
| CN107715936A (en) * | 2017-11-02 | 2018-02-23 | 西安工程大学 | A kind of integral type distilling apparatus and distillating method |
| CN114642893A (en) * | 2022-03-25 | 2022-06-21 | 百色学院 | Energy-saving device and method for reduced pressure distillation of water-insoluble organic solvent |
| CN114642893B (en) * | 2022-03-25 | 2024-02-06 | 百色学院 | Energy-saving device and method for reduced pressure distillation of water-insoluble organic solvent |
| CN116355688A (en) * | 2023-04-04 | 2023-06-30 | 浙江工业大学 | Chimonanthus salicifolius volatile oil, and its preparation method and application by decompression extraction |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |