CN1769260A - Trimellitic tri(C8-9 ol)ester preparation method - Google Patents
Trimellitic tri(C8-9 ol)ester preparation method Download PDFInfo
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- CN1769260A CN1769260A CN 200510095365 CN200510095365A CN1769260A CN 1769260 A CN1769260 A CN 1769260A CN 200510095365 CN200510095365 CN 200510095365 CN 200510095365 A CN200510095365 A CN 200510095365A CN 1769260 A CN1769260 A CN 1769260A
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- alcohol
- esterification
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- anhydride
- ester
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Trimellitate | Phthalic ester | ||
TOTM | 9-11P | 11P | |
Anti-mist degree begins luminosity reflectivity % and reclaimed recovery in 16 hours in 1 hour | 36 88 | 27 71 | 34 100 |
The minimum weight deposition, mg | 4.8 | 4.6 | 9.8 |
Temperature limit of brittleness, ℃ | -19 | -28 | -34 |
85 ℃ after 100 hours; Elongation retention % | 99 | 94 | 87 |
85 ℃ after 100 hours; Stretching strength retentivity % | 104 | 69 | 91 |
Claims (3)
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CNB2005100953658A CN100363328C (en) | 2005-11-08 | 2005-11-08 | Trimellitic tri(C8-9 ol)ester preparation method |
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CNB2005100953658A CN100363328C (en) | 2005-11-08 | 2005-11-08 | Trimellitic tri(C8-9 ol)ester preparation method |
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CN1769260A true CN1769260A (en) | 2006-05-10 |
CN100363328C CN100363328C (en) | 2008-01-23 |
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CNB2005100953658A Expired - Fee Related CN100363328C (en) | 2005-11-08 | 2005-11-08 | Trimellitic tri(C8-9 ol)ester preparation method |
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101973884A (en) * | 2010-09-26 | 2011-02-16 | 昆山合峰化工有限公司 | Method for preparing triisononyl trimellitate (TINTM) |
CN101429126B (en) * | 2008-12-22 | 2011-09-21 | 无锡百川化工股份有限公司 | Method for producing trioctyl trimellitate with trimellitic acid |
CN102924280A (en) * | 2012-10-25 | 2013-02-13 | 浙江皇马科技股份有限公司 | Preparation method of trimellitate |
CN102924279A (en) * | 2012-10-16 | 2013-02-13 | 江苏正丹化学工业股份有限公司 | Catalytic synthesis method of tri-octyl tri-meta-benzoate |
CN103864620A (en) * | 2014-04-04 | 2014-06-18 | 百川化工(如皋)有限公司 | Production method of trioctyl trimellate |
JP2016141787A (en) * | 2015-02-05 | 2016-08-08 | 新日本理化株式会社 | Non-phthalic acid ester based plasticizer for vinyl chloride-based resin and vinyl chloride-based resin composition comprising the same |
CN107250098A (en) * | 2014-12-02 | 2017-10-13 | 埃默里油脂化学有限公司 | Ester plasticiser based on ethyl hexanol and propyl enanthol |
CN107698449A (en) * | 2017-09-28 | 2018-02-16 | 江苏正丹化学工业股份有限公司 | A kind of synthetic method of the positive nonyl ester plasticiser of tri trimellitate |
CN108892614A (en) * | 2018-08-30 | 2018-11-27 | 江苏正丹化学工业股份有限公司 | A kind of synthetic method of triisononyl trimellitate plasticizer |
CN112552170A (en) * | 2020-11-16 | 2021-03-26 | 南通百川新材料有限公司 | Preparation method of low-color tri (C8-10 alcohol) trimellitate |
CN112619689A (en) * | 2021-01-07 | 2021-04-09 | 江苏正丹化学工业股份有限公司 | Preparation and application method of catalyst for synthesizing triisononyl trimellitate |
Families Citing this family (1)
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---|---|---|---|---|
EP3464230A1 (en) | 2016-05-25 | 2019-04-10 | SABIC Global Technologies B.V. | Synthesis of alkyl tribenzanoate |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5532405A (en) * | 1994-04-29 | 1996-07-02 | Exxon Chemical Patents Inc. | Preparation of plasticizer or polyol esters by the staged addition of the lower boiling point reactant |
KR960000850A (en) * | 1994-06-06 | 1996-01-25 | 사토 아키오 | Continuous production method of methyl methacrylate |
CN100404496C (en) * | 2003-03-26 | 2008-07-23 | 蒋平平 | Production process of plasticizer with multiple variety and low consumption |
CN1268675C (en) * | 2004-03-18 | 2006-08-09 | 杨家勇 | Technique for preparing plasticizer of dioctyl terephthalate from terephthalic acid and capryl alcohol |
CN100491324C (en) * | 2004-09-27 | 2009-05-27 | 广西民族学院 | Method and apparatus for continuously preparing ethyl acetate by single tower |
-
2005
- 2005-11-08 CN CNB2005100953658A patent/CN100363328C/en not_active Expired - Fee Related
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101429126B (en) * | 2008-12-22 | 2011-09-21 | 无锡百川化工股份有限公司 | Method for producing trioctyl trimellitate with trimellitic acid |
CN101973884A (en) * | 2010-09-26 | 2011-02-16 | 昆山合峰化工有限公司 | Method for preparing triisononyl trimellitate (TINTM) |
CN102924279B (en) * | 2012-10-16 | 2015-09-16 | 江苏正丹化学工业股份有限公司 | A kind of process for catalytic synthesis of trioctyl trimellitate |
CN102924279A (en) * | 2012-10-16 | 2013-02-13 | 江苏正丹化学工业股份有限公司 | Catalytic synthesis method of tri-octyl tri-meta-benzoate |
CN102924280B (en) * | 2012-10-25 | 2015-08-19 | 浙江皇马科技股份有限公司 | A kind of preparation method of trimellitate |
CN102924280A (en) * | 2012-10-25 | 2013-02-13 | 浙江皇马科技股份有限公司 | Preparation method of trimellitate |
CN103864620A (en) * | 2014-04-04 | 2014-06-18 | 百川化工(如皋)有限公司 | Production method of trioctyl trimellate |
CN103864620B (en) * | 2014-04-04 | 2016-08-17 | 百川化工(如皋)有限公司 | A kind of production method of trioctyl trimellitate (TOTM) |
CN107250098A (en) * | 2014-12-02 | 2017-10-13 | 埃默里油脂化学有限公司 | Ester plasticiser based on ethyl hexanol and propyl enanthol |
JP2016141787A (en) * | 2015-02-05 | 2016-08-08 | 新日本理化株式会社 | Non-phthalic acid ester based plasticizer for vinyl chloride-based resin and vinyl chloride-based resin composition comprising the same |
CN107698449A (en) * | 2017-09-28 | 2018-02-16 | 江苏正丹化学工业股份有限公司 | A kind of synthetic method of the positive nonyl ester plasticiser of tri trimellitate |
CN108892614A (en) * | 2018-08-30 | 2018-11-27 | 江苏正丹化学工业股份有限公司 | A kind of synthetic method of triisononyl trimellitate plasticizer |
CN112552170A (en) * | 2020-11-16 | 2021-03-26 | 南通百川新材料有限公司 | Preparation method of low-color tri (C8-10 alcohol) trimellitate |
CN112619689A (en) * | 2021-01-07 | 2021-04-09 | 江苏正丹化学工业股份有限公司 | Preparation and application method of catalyst for synthesizing triisononyl trimellitate |
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Publication number | Publication date |
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CN100363328C (en) | 2008-01-23 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Yixing Yuxing Industrial And Trade Co., Ltd. Assignor: Jiangnan University Contract fulfillment period: 2008.9.21 to 2014.12.31 contract change Contract record no.: 2009320001208 Denomination of invention: Method for preparing amino acid three (C#-[8-10] alcohol) ester Granted publication date: 20080123 License type: Exclusive license Record date: 2009.7.23 |
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LIC | Patent licence contract for exploitation submitted for record |
Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2008.9.21 TO 2014.12.31; CHANGE OF CONTRACT Name of requester: YIXING CITY YUXING INDUSTRY AND TRADE CO., LTD. Effective date: 20090723 |
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Granted publication date: 20080123 Termination date: 20131108 |