CN1615989A - Antiseptic and pest killing skin cleaning agent and preparing method - Google Patents

Antiseptic and pest killing skin cleaning agent and preparing method Download PDF

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CN1615989A
CN1615989A CN 200410060830 CN200410060830A CN1615989A CN 1615989 A CN1615989 A CN 1615989A CN 200410060830 CN200410060830 CN 200410060830 CN 200410060830 A CN200410060830 A CN 200410060830A CN 1615989 A CN1615989 A CN 1615989A
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oil
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insecticidal
benzophenone
antibacterial
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CN1279940C (en
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袁晓
袁萍
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Wuhan Botanical Garden
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Wuhan Botanical Garden
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Abstract

本发明公开了一种抗菌杀虫洁肤剂及制备方法,它由十六烷基三甲基氯化铵、苦参、黄芩、玫瑰花、樟脑、冰片、桉叶油、山苍子油、二苯酮-4和乙二胺四乙酸二钠按比例组成,首先是将苦参、黄芪、玫瑰花按95%乙醇超声提取、浓缩;其次是用纯净水溶解十六烷基三甲基氯化铵后加入苦参、黄芪、玫瑰花提取液,搅拌;第三是用纯净水溶解乙二胺四乙酸二钠、二苯酮-4,搅拌;第四是加入樟脑、冰片搅拌均匀;第五是加入桉叶油、山苍子油和氢化蓖麻油到烧杯中充分乳化;第六是加纯净水搅拌均匀即得。本发明清热解毒,消炎止痒,祛风杀虫,适用于人体体表,用于预防杀灭由于螨虫、真菌、霉菌引起的脚气、阴道炎、皮肤炎症、痤疮。The invention discloses an antibacterial and insecticidal skin cleanser and a preparation method thereof. Benzophenone-4 and disodium edetate are composed in proportion. Firstly, flavescens, astragalus, and rose are ultrasonically extracted and concentrated with 95% ethanol; secondly, hexadecyl trimethyl chloride is dissolved in pure water. Add flavescens, astragalus, and rose extracts after ammonium, and stir; the third is to dissolve disodium edetate and benzophenone-4 in pure water, and stir; the fourth is to add camphor and borneol and stir evenly; The fifth is to add eucalyptus oil, litsea cubeba oil and hydrogenated castor oil to the beaker to fully emulsify; the sixth is to add pure water and stir evenly. The invention clears heat and detoxifies, reduces inflammation and itching, dispels wind and kills insects, is suitable for human body surface, and is used for preventing and killing beriberi, vaginitis, skin inflammation and acne caused by mites, fungi and molds.

Description

抗菌杀虫洁肤剂及制备方法Antibacterial and insecticidal skin cleanser and preparation method

                          技术领域Technical field

本发明涉及一种含有多种天然活性植物的多功能抗菌杀虫洁肤剂,同时还涉及该抗菌杀虫洁肤剂的制备方法,该抗菌杀虫洁肤剂适用于人体体表,用于预防和治疗因螨虫、真菌或细菌引起的脚气、阴道炎、皮肤炎症、痤疮等。The invention relates to a multifunctional antibacterial and insecticidal skin cleanser containing various natural active plants, and also relates to a preparation method of the antibacterial and insecticidal skin cleanser. The antibacterial and insecticidal skin cleanser is suitable for human body surface and used for Prevent and treat athlete's foot, vaginitis, skin inflammation, acne, etc. caused by mites, fungi or bacteria.

                          背景技术 Background technique

随着人们生活水平的提高,化妆品的大量、长时间的使用,现代社会生活节奏加快,人们精神紧张日益严重;加之环境污染、不合理饮食、各种电子产品的辐射等等,皮肤问题越来越突出,尤其各种面部皮肤病发病率不断增高,而且有越来越顽固的趋势。人体的皮肤易受螨虫的感染引起脂溢性皮炎,如:痤疮、酒渣鼻、眼睑炎、脱发。另外,还易受到真菌、细菌的感染,引起脚气、妇科炎症等,奇痒无比,痛苦难忍。With the improvement of people's living standards, a large number of long-term use of cosmetics, the pace of life in modern society is accelerating, and people's mental stress is becoming more and more serious; coupled with environmental pollution, unreasonable diet, radiation from various electronic products, etc., skin problems are becoming more and more serious. The more prominent, especially the increasing incidence of various facial skin diseases, and there is a trend of becoming more and more stubborn. The skin of the human body is susceptible to seborrheic dermatitis caused by mite infection, such as: acne, rosacea, blepharitis, and hair loss. In addition, it is also susceptible to fungal and bacterial infections, causing beriberi and gynecological inflammation, which are extremely itchy and painful.

目前市场上各种疗效型化妆品层出不穷,有些疗效型化妆品为追求速效,用重金属、激素等对人体有害的物质直接对抗并不肯定的病因或已经形成的病灶,或许可以取得暂时的效果,但很快的复发和对皮肤以至于全身健康的损害则在所难免。At present, various curative cosmetics emerge in endlessly on the market. Some curative cosmetics use heavy metals, hormones and other substances harmful to the human body to directly fight against uncertain causes or lesions that have formed in order to pursue quick results. Temporary effects may be obtained, but it is very difficult. Rapid recurrence and damage to the skin and even the health of the whole body are inevitable.

                          发明内容Contents of Invention

本发明的目的是提供一种抗菌杀虫洁肤剂,配方合理,清热解毒,消炎止痒,祛风杀虫。The object of the present invention is to provide an antibacterial and insecticidal skin cleanser with reasonable formula, heat-clearing and toxic substances removing, anti-inflammatory and antipruritic, expelling wind and killing insects.

本发明的另一个目的在于制备抗菌杀虫洁肤剂的方法,该方法工艺简便,成本低廉,操作方便。Another object of the present invention is the method for preparing the antibacterial and insecticidal skin cleanser, which has the advantages of simple process, low cost and convenient operation.

目前既能够保养皮肤,防治皮肤早衰,预防和治疗多种损容性皮肤疾病,而且无论短期使用还是长期使用,都没有副作用,能够满足这些条件,到目前为止,中药是一个较好的选择。我国植物资源丰富,植物种类的繁多,植物及其生理功效成份的多种多样,利用植物资源挖掘和开发新型产品服务于社会已日见成效。At present, it can maintain the skin, prevent premature skin aging, prevent and treat a variety of skin diseases that damage the appearance, and no matter whether it is used for a short time or for a long time, it has no side effects and can meet these conditions. So far, traditional Chinese medicine is a better choice. Our country is rich in plant resources, there are many kinds of plants, and there are many kinds of plants and their physiological functions. The use of plant resources to excavate and develop new products to serve the society has achieved increasing results.

根据中医传统理论,选用对皮肤有美化作用和某些常见皮肤不良、皮肤疾病有治疗作用的中药,同时选用对皮肤有保护作用的中药和添加剂,在治疗疾病的同时,不但不损害皮肤,而且根据现代人的皮肤特点及东方人的审美观点美。According to the traditional theory of traditional Chinese medicine, choose traditional Chinese medicine that can beautify the skin and treat some common skin problems and skin diseases, and at the same time choose traditional Chinese medicine and additives that can protect the skin. While treating diseases, not only does not damage the skin, but also According to the skin characteristics of modern people and the aesthetic point of view of oriental people.

所用中草药有抗菌消炎、杀虫和洁肤等功效,并有广泛的应用,本专利着重在除去病因的同时,还有利于皮肤的保健。The Chinese herbal medicine used has the effects of antibacterial and anti-inflammatory, insecticidal and skin cleansing, and has a wide range of applications. This patent focuses on eliminating the cause of the disease, and is also beneficial to skin health care.

本发明的技术方案是:它由十六烷基三甲基氯化铵、苦参、黄芩、玫瑰花、樟脑、冰片、桉叶油、山苍子油、二苯酮-4、乙二胺四乙酸二钠组成。各原料的重量百分比(%)为:The technical scheme of the present invention is: it is made of cetyltrimethylammonium chloride, flavescens, baicalin, rose, camphor, borneol, eucalyptus oil, litsea cubeba oil, benzophenone-4, ethylenediamine Composition of disodium tetraacetate. The weight percent (%) of each raw material is:

十六烷基三甲基氯化铵  4.0~8.0%    二苯酮-4      0.1~0.3%Cetyltrimethylammonium chloride 4.0~8.0% Benzophenone-4 0.1~0.3%

乙二胺四乙酸二钠      0.1~0.3%    氢化蓖麻油    1.0~2.0%Disodium edetate 0.1~0.3% Hydrogenated castor oil 1.0~2.0%

苦参                  2.0~5.0%    黄芪          2.0~5.0%Sophora flavescens 2.0~5.0% Astragalus 2.0~5.0%

玫瑰花                1.0~2.5%    樟脑          0.3~0.5%Rose 1.0~2.5% Camphor 0.3~0.5%

桉叶油                0.3~0.5%    山苍子油      0.5~0.7%Eucalyptus oil 0.3~0.5% Litsea cubeba oil 0.5~0.7%

冰片                  0.3~0.5%    纯净水        74.2~88.4%Borneol 0.3~0.5% Purified water 74.2~88.4%

多功能抗菌杀虫洁肤剂的制备方法,其步骤为:The preparation method of multifunctional antibacterial and insecticidal skin cleanser, the steps are:

(1)、将粉碎后过20目筛的苦参、黄芪和玫瑰花重量比例(2∶2∶1)混合得混合物,混合物中加入混合物重量8-12倍的95%乙醇,超声提取25-35分钟,滤出提取液,重复上述提取步骤2-3次,合并提取液,浓缩成混合物重量1倍的提取浓液;(1), the sophora flavescens that crosses 20 mesh sieves after pulverizing, Radix Astragali and rose flower weight ratio (2:2:1) are mixed to obtain a mixture, add 95% ethanol of 8-12 times of mixture weight in the mixture, ultrasonic extraction 25- For 35 minutes, filter out the extract, repeat the above extraction steps 2-3 times, combine the extracts, and concentrate them into an extract concentrate that is 1 times the weight of the mixture;

(2)、用十六烷基三甲基氯化铵的重量5-8倍纯净水溶解十六烷基三甲基氯化铵,搅拌溶解后加入(1)步骤的提取浓液中,搅拌均匀得混合液;(2), dissolve cetyltrimethylammonium chloride with 5-8 times the weight of cetyltrimethylammonium chloride in pure water, stir and dissolve, add to the extraction concentrate of step (1), stir homogeneous mixture;

(3)、用乙二胺四乙酸二钠和二苯酮-4的总重量8-12倍纯净水溶解乙二胺四乙酸二钠和二苯酮-4,加入(2)步骤的混合液中并搅拌均匀,得混合液;(3) Dissolve disodium edetate and benzophenone-4 in pure water 8-12 times the total weight of disodium edetate and benzophenone-4, and add the mixed solution of step (2) and stir evenly to obtain a mixture;

(4)、加入樟脑和冰片到(3)步骤的混合液中,并搅拌均匀,得混合液;(4), add camphor and borneol to the mixed solution of (3) step, and stir evenly, obtain mixed solution;

(5)、加入桉叶油、山苍子油和氢化蓖麻油到容器中充分乳化后倒入(4)步骤的混合液中搅拌均匀,得混合液;(5), add eucalyptus oil, litsea cubeba oil and hydrogenated castor oil to fully emulsify in the container and pour into the mixed solution of (4) step and stir evenly to obtain the mixed solution;

(6)、加入剩余的纯净水到(5)步骤的混合液中并搅拌均匀,得到一种抗菌杀虫洁肤剂。(6) Add remaining purified water to the mixture in step (5) and stir evenly to obtain an antibacterial, insecticidal and skin cleanser.

本发明以药用植物活性成分及芳香植物精油为主要清热解毒、消炎止痒,祛风杀虫,配以与其能很好相溶的乳化剂,配制成具有天然芳香味的杀虫杀菌洁肤剂。苦参、黄芪、玫瑰花具有杀菌消炎止痒的功效,十六烷基三甲基氯化铵为表面活性剂,能去污垢。樟脑、冰片具有杀虫功效。乙二胺四乙酸二钠用于熬合金属离子。二苯酮-4用于吸收紫外线。桉叶油、山苍子精油起杀螨杀菌、驱蚊作用。氢化蓖麻油用于乳化植物精油。The present invention uses medicinal plant active ingredients and aromatic plant essential oils as the main heat-clearing and detoxifying, anti-inflammatory, antipruritic, wind-dispelling and insect-killing agents, and is formulated with an emulsifier that is well compatible with them to prepare an insect-killing, sterilizing, skin-cleansing product with a natural aroma. agent. Sophora flavescens, astragalus, and roses have the effects of sterilizing, reducing inflammation, and relieving itching. Cetyltrimethylammonium chloride is a surfactant that can remove dirt. Camphor and borneol have insecticidal effects. Disodium edetate is used to boil metal ions. Benzophenone-4 is used to absorb UV rays. Eucalyptus oil and Litsea cubeba essential oil have the functions of killing mites and bacteria, and repelling mosquitoes. Hydrogenated castor oil is used to emulsify plant essential oils.

                     具体实施方式 Detailed ways

实施例1:Example 1:

各原料的重量百分比(%)为:The weight percent (%) of each raw material is:

十六烷基三甲基氯化铵  4.0%    二苯酮-4      0.1%Cetyltrimethylammonium Chloride 4.0% Benzophenone-4 0.1%

乙二胺四乙酸二钠      0.1%    氢化蓖麻油    1.0%Disodium EDTA 0.1% Hydrogenated Castor Oil 1.0%

苦参                  2.0%    黄芪          2.0%Sophora flavescens 2.0% Astragalus 2.0%

玫瑰花                1.0%    樟脑          0.3%Rose 1.0% Camphor 0.3%

桉叶油                0.3%    山苍子油      0.5%Eucalyptus oil 0.3% Litsea cubeba oil 0.5%

冰片                  0.3%    纯净水        88.4%Ice flakes 0.3% Purified water 88.4%

制备方法与实施步骤为:Preparation method and implementation steps are:

(1)、将粉碎后过20目筛的苦参、黄芪和玫瑰花按配方比例混合得混合物,混合物中加入混合物重量8倍的95%乙醇,超声提取30分钟,滤出提取液,重复上述提取步骤2次,合并提取液,浓缩成混合物重量1倍的提取浓液(1), mix the flavescens, astragalus and roses that have been crushed through a 20-mesh sieve according to the formula ratio to obtain a mixture, add 95% ethanol that is 8 times the weight of the mixture in the mixture, ultrasonically extract for 30 minutes, filter the extract, repeat the above Extraction step 2 times, combine the extracts, concentrate to 1 times the weight of the mixture

(2)、用纯净水溶解十六烷基三甲基氯化铵,搅拌溶解后加入苦参、黄芪和玫瑰花提取浓液,搅拌均匀得混合液;(2), dissolving cetyltrimethylammonium chloride with pure water, stirring and dissolving, adding sophora flavescens, astragalus and rose to extract the concentrated solution, and stirring evenly to obtain a mixed solution;

(3)、用纯净水溶解乙二胺四乙酸二钠和二苯酮-4得溶液,将溶液加入(2)步骤的混合液中并搅拌均匀;(3), dissolving disodium edetate and benzophenone-4 with purified water to obtain a solution, adding the solution to the mixed solution in step (2) and stirring evenly;

(4)、加入樟脑和冰片到(3)步骤的混合液中并搅拌均匀;(4), add camphor and borneol to the mixed solution of (3) step and stir;

(5)、加入桉叶油、山苍子油和氢化蓖麻油到容器中充分乳化后倒入(4)步骤的混合液并搅拌均匀;(5), add eucalyptus oil, litsea cubeba oil and hydrogenated castor oil to fully emulsify in the container and pour into the mixed solution of (4) step and stir evenly;

(6)、加入纯净水到(5)步骤的混合液中并搅拌均匀,得到一种抗菌杀虫洁肤剂。(6) Add pure water to the mixture in step (5) and stir evenly to obtain an antibacterial and insecticidal skin cleanser.

实施例2:各原料的重量百分比(%)为:Embodiment 2: the weight percent (%) of each raw material is:

十六烷基三甲基氯化铵  6.0%    二苯酮-4      0.2%Cetyltrimethylammonium Chloride 6.0% Benzophenone-4 0.2%

乙二胺四乙酸二钠      0.2%    氢化蓖麻油    1.5%Disodium EDTA 0.2% Hydrogenated Castor Oil 1.5%

苦参                  4.0%    黄芪          4.0%Sophora flavescens 4.0% Astragalus 4.0%

玫瑰花                2.0%    樟脑          0.4%Rose 2.0% Camphor 0.4%

桉叶油                0.4%    山苍子油      0.6%Eucalyptus oil 0.4% Litsea cubeba oil 0.6%

冰片                  0.4%    纯净水        80.3%Ice flakes 0.4% Purified water 80.3%

制备方法与实施例1相同。The preparation method is the same as in Example 1.

实施例3:各原料的重量百分比(%)为:Embodiment 3: the weight percent (%) of each raw material is:

十六烷基三甲基氯化铵  8.0%    二苯酮-4      0.3%Cetyltrimethylammonium Chloride 8.0% Benzophenone-4 0.3%

乙二胺四乙酸二钠      0.3%    氢化蓖麻油    2.0%Disodium EDTA 0.3% Hydrogenated Castor Oil 2.0%

苦参                  5.0%    黄芪          5.0%Sophora flavescens 5.0% Astragalus 5.0%

玫瑰花                2.5%    樟脑          0.5%Rose 2.5% Camphor 0.5%

桉叶油                0.5%    山苍子油      0.7%Eucalyptus oil 0.5% Litsea cubeba oil 0.7%

冰片                  0.5%    纯净水        74.7%Ice flakes 0.5% Purified water 74.7%

制备方法与实施例1相同。The preparation method is the same as in Example 1.

Claims (5)

1、一种抗菌杀虫洁肤剂,它由以下原料的重量百分比制成:1. An antibacterial and insecticidal skin cleanser, which is made of the following raw materials in weight percentage: 十六烷基三甲基氯化铵  4.0~8.0%      二苯酮-4       0.1~0.3%Cetyltrimethylammonium Chloride 4.0~8.0% Benzophenone-4 0.1~0.3% 乙二胺四乙酸二钠      0.1~0.3%      氢化蓖麻油     1.0~2.0%Disodium edetate 0.1~0.3% Hydrogenated castor oil 1.0~2.0% 苦参                  2.0~5.0%      黄芪           2.0~5.0%Sophora flavescens 2.0~5.0% Astragalus 2.0~5.0% 玫瑰花                1.0~2.5%      樟脑           0.3~0.5%Rose 1.0~2.5% Camphor 0.3~0.5% 桉叶油                0.3~0.5%      山苍子油       0.5~0.7%Eucalyptus oil 0.3~0.5% Litsea cubeba oil 0.5~0.7% 冰片                  0.3~0.5%      纯净水         74.7~88.4%Borneol 0.3~0.5% Purified water 74.7~88.4% 2、根据权利要求1所述的一种抗菌杀虫洁肤剂,其特征在于各原料的重量百分比为:2. An antibacterial and insecticidal skin cleanser according to claim 1, wherein the weight percentage of each raw material is: 十六烷基三甲基氯化铵  4.0%           二苯酮-4        0.1%Cetyltrimethylammonium Chloride 4.0% Benzophenone-4 0.1% 乙二胺四乙酸二钠      0.1%           氢化蓖麻油      1.0%Disodium EDTA 0.1% Hydrogenated castor oil 1.0% 苦参                  2.0%           黄芪            2.0%Sophora flavescens 2.0% Astragalus 2.0% 玫瑰花                1.0%           樟脑            0.3%Rose 1.0% Camphor 0.3% 桉叶油                0.3%           山苍子油        0.5%Eucalyptus oil 0.3% Litsea cubeba oil 0.5% 冰片                  0.3%           纯净水          88.4%Ice flakes 0.3% Purified water 88.4% 3、根据权利要求1所述的一种抗菌杀虫洁肤剂,其特征在于各原料的重量百分比为:3. An antibacterial and insecticidal skin cleanser according to claim 1, wherein the weight percentage of each raw material is: 十六烷基三甲基氯化铵  6.0%           二苯酮-4        0.2%Cetyltrimethylammonium Chloride 6.0% Benzophenone-4 0.2% 乙二胺四乙酸二钠      0.2%           氢化蓖麻油      1.5%Disodium EDTA 0.2% Hydrogenated Castor Oil 1.5% 苦参                  4.0%           黄芪            4.0%Sophora flavescens 4.0% Astragalus 4.0% 玫瑰花                2.0%           樟脑            0.4%Rose 2.0% Camphor 0.4% 桉叶油                0.4%           山苍子油        0.6%Eucalyptus oil 0.4% Litsea cubeba oil 0.6% 冰片                  0.4%           纯净水          80.3%Ice flakes 0.4% Purified water 80.3% 4、根据权利要求1所述的一种抗菌杀虫洁肤剂,其特征在于各原料的重量百分比为:4. An antibacterial and insecticidal skin cleanser according to claim 1, wherein the weight percentage of each raw material is: 十六烷基三甲基氯化铵  8.0%           二苯酮-4        0.3%Cetyltrimethylammonium Chloride 8.0% Benzophenone-4 0.3% 乙二胺四乙酸二钠      0.3%           氢化蓖麻油      2.0%Disodium EDTA 0.3% Hydrogenated Castor Oil 2.0% 苦参              5.0%         黄芪             5.0%Sophora flavescens 5.0% Astragalus 5.0% 玫瑰花            2.5%         樟脑             0.5%Rose 2.5% Camphor 0.5% 桉叶油            0.5%         山苍子油         0.7%Eucalyptus oil 0.5% Litsea cubeba oil 0.7% 冰片              0.5%         纯净水           74.7%Ice flakes 0.5% Purified water 74.7% 5、一种实现权利要求1所述的抗菌杀虫洁肤剂的制备方法,其步骤是:5. A preparation method for realizing the antibacterial and insecticidal skin cleanser according to claim 1, the steps of which are: A、将粉碎后的苦参、黄芪和玫瑰花比例2∶2∶1混合得混合物,混合物中加入95%乙醇,超声提取25-35分钟,滤出提取液,重复上述提取步骤2-3次,合并提取液,浓缩成混合物的提取浓液;A. Mix crushed sophora flavescens, astragalus and rose at a ratio of 2:2:1 to obtain a mixture, add 95% ethanol to the mixture, ultrasonically extract for 25-35 minutes, filter out the extract, and repeat the above extraction steps 2-3 times , combining the extracts and concentrating into the extract concentrate of the mixture; B、用纯净水溶解十六烷基三甲基氯化铵,搅拌溶解后加入A步骤的提取浓液,搅拌均匀得混合液;B. Dissolve cetyltrimethylammonium chloride with pure water, stir and dissolve, add the extraction dope of step A, and stir to obtain a mixed solution; C、用纯净水溶解乙二胺四乙酸二钠和二苯酮-4,加入B步骤的混合液并搅拌均匀,得混合液;C. Dissolve disodium edetate and benzophenone-4 in pure water, add the mixed solution in step B and stir evenly to obtain the mixed solution; D、加入樟脑和冰片到C步骤的混合液中并搅拌均匀混合液;D, add camphor and borneol to the mixed solution of step C and stir the mixed solution; E、加入桉叶油、山苍子油和氢化蓖麻油到容器中充分乳化后倒入D步骤的混合液中并搅拌均匀,得混合液;E, add eucalyptus oil, litsea cubeba oil and hydrogenated castor oil to fully emulsify in the container and then pour into the mixed solution in step D and stir evenly to obtain the mixed solution; F、加入纯净水到E步骤的混合液中并搅拌均匀,得到一种抗菌杀虫洁肤剂。F. Add purified water to the mixture in step E and stir evenly to obtain an antibacterial and insecticidal cleanser.
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102177924A (en) * 2011-05-13 2011-09-14 湖南红蔓草生物科技股份有限公司 Chinese herbal antibacterial crude cleaning liquid and preparation method thereof
CN102579930A (en) * 2012-03-16 2012-07-18 张玲 Medical antibacterial cleansing liquid
CN102600048A (en) * 2012-03-16 2012-07-25 张玲 Preparation method of medical antibiosis washing-protection liquid
CN102921051A (en) * 2012-09-04 2013-02-13 尹运贵 Formula and preparation of mite removing patch
CN103239676A (en) * 2013-04-22 2013-08-14 马南行 Topical pharmaceutical composition for preventing and treating bacterial vaginosis
CN106727003A (en) * 2016-12-30 2017-05-31 邵武市美菰林卫生用品有限公司 One kind dimension skin emulsion
CN110507696A (en) * 2019-08-22 2019-11-29 徐永福 It is a kind of to itch the antibacterial liquid and preparation method thereof of effect with foot smell prevention foot

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102177924A (en) * 2011-05-13 2011-09-14 湖南红蔓草生物科技股份有限公司 Chinese herbal antibacterial crude cleaning liquid and preparation method thereof
CN102177924B (en) * 2011-05-13 2013-01-02 湖南红蔓草生物科技股份有限公司 Chinese herbal antibacterial crude cleaning liquid and preparation method thereof
CN102579930A (en) * 2012-03-16 2012-07-18 张玲 Medical antibacterial cleansing liquid
CN102600048A (en) * 2012-03-16 2012-07-25 张玲 Preparation method of medical antibiosis washing-protection liquid
CN102600048B (en) * 2012-03-16 2013-04-10 张玲 Preparation method of medical antibiosis washing-protection liquid
CN102921051A (en) * 2012-09-04 2013-02-13 尹运贵 Formula and preparation of mite removing patch
CN103239676A (en) * 2013-04-22 2013-08-14 马南行 Topical pharmaceutical composition for preventing and treating bacterial vaginosis
CN103239676B (en) * 2013-04-22 2015-06-24 马南行 Topical pharmaceutical composition for preventing and treating bacterial vaginosis
CN106727003A (en) * 2016-12-30 2017-05-31 邵武市美菰林卫生用品有限公司 One kind dimension skin emulsion
CN110507696A (en) * 2019-08-22 2019-11-29 徐永福 It is a kind of to itch the antibacterial liquid and preparation method thereof of effect with foot smell prevention foot

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