CN1615761A - Preparation of instant cigarette tip additive solution and using method - Google Patents

Preparation of instant cigarette tip additive solution and using method Download PDF

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Publication number
CN1615761A
CN1615761A CN 200310111373 CN200310111373A CN1615761A CN 1615761 A CN1615761 A CN 1615761A CN 200310111373 CN200310111373 CN 200310111373 CN 200310111373 A CN200310111373 A CN 200310111373A CN 1615761 A CN1615761 A CN 1615761A
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China
Prior art keywords
solution
cigarette
cigarette smoking
instant
tip rod
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Pending
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CN 200310111373
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Chinese (zh)
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喻昕
裘锡贤
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喻昕
裘锡贤
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Priority to CN 200310111373 priority Critical patent/CN1615761A/en
Publication of CN1615761A publication Critical patent/CN1615761A/en
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Abstract

The instant cigarette tip additive solution is water solution or non-water solution of vitamins and naturally extracted antioxidant. It is added to cigarette just before the cigarette is ignited, with the added amount being 10-400 microliters. It is used to lower tar content, reduce harm of smoking and lower the humidity of smoke into respiratory tract. Into the instant cigarette tip additive solution, essence and perfume matter may be added to raise the cigarette grade.

Description

Preparation of cigarette smoking instant tip rod appended solution and using method
Technical field
The present invention relates to the preparation and the using method of cigarette smoking instant tip rod appended solution.
Background technology
Cigarette can be because the effect of thermal cracking, destructive distillation, imperfect combustion and evaporation produces harmful gaseous material down in combustion process, and wherein tar is that imperfect combustion and destructive distillation effect owing to the organic principles such as cellulose in the tobacco forms.Up to now, there has been a large amount of compositions to be harmful in the flue gas by evaluation, some are to distinctive nitrosamine, N-nitroso pyridine, benzo [α] pyrene, N-nitrosodiethanolamine and cadmium in the carcinogenic material that maybe may cause cancer of people such as benzene, 2-naphthylamines, 4-aminobphenyl, radioactive element polonium-210, aldehyde, hydrazine, volatile nitrosamine, the tobacco, known possible procarcinogen such as benzo [α] anthracene, butyrolactone, N-nitroso nornicotine etc. to animal, above material all has direct toxicity to body cell.
The reducing tar and reducing harm technology that generally adopts in the current tobacco business mainly contains:
(1) reform tobacco formulation structure is produced blended type cigarette; (2) by in the cigarette process, pipe tobacco, reconstituted tobacoo etc. being carried out the combustion position of the corresponding cigarette that improves.As in pipe tobacco, adding combustion adjuvant (as K etc.), additive in the cigarette bobbin paper is improved (as with potassium citrate, calcium carbonate and wood pulp cellulose mix preparation-obtained obbbin and have higher air permeability and high quiet combustion speed), adopt expanded cut tobacco, methods such as expanded cut stem, so, then can significantly reduce because of the tar content that imperfect combustion produced, in addition the reconstituted tobacoo of mixing is improved, also can reduce tar content, reach methods such as before the reconstituted tobacoo drying, adding the 10-18% sepiolite powder as adding zeolite, obtained application effectively with the method that reduces cigarette harm by in pipe tobacco or reconstituted tobacoo, adding material with selectivity catalysis and absorption; (3) development flavoring and casing technology, Application and Development novel fragrance reduce the needs of tar to cooperate cigarette; (4) the extraordinary cigarette (5) of researching and developing the pipe tobacco that do not burn is used cigarette filter, adopt different filter tip (filter tip and composite filter tip that common filter tip, extraordinary filter material are made) to be hinged with on the cigarette, can reduce tar content in cigarette 20%~50%, this also is the most widely used in the world at present burnt means of falling simultaneously.
The filter tip material that is prepared from by acetate fiber, artificial silk, cotton and paper etc. mainly is the effect that reaches granule phase substance in the reduction flue gas by the effect of machinery, simultaneously the gas phase in the flue gas is also had certain effect.Form by single vinegar fibre by about 90% filter tip now, but this class filter stick is when removing a large amount of harmful components, allow quite a few harmful components enter human body again inevitably, improvement to this class filter tip, as the increase of fiber surface crispation number, the increase of specific surface and the use of some additives all are the effective ways that further reduce harmful components in the flue gas.A very big class additive is some porous in the additives of filter tip adsorbent such as active carbon, sepiolite, montmorillonite, medical stone, silica gel, hydroxyapatite, organosilicon, synthetic mica, ferroheme, shitosan, anion and cationic ion-exchange resin etc., they often are used to the additive in the composite filter tip, and tealeaves, coffee, lichens, porphyrin and similar complex compound etc. also are used as additive in addition.Nowadays filter tip has obtained very big development, from common cellulose acetate filter to biodegradable environmental protection filter tip and the polynary composite filter tip etc. that can add different additive, wait and all develop to some extent from filter tip to the special-shaped filter tip (as hollow composite filter tip, the heart-shaped filter tip of band) of common shape and function.These filter tips are basically at the reduction or the removal of following harmful components: HCN, polycyclic aromatic hydrocarbon, free radical, nucleophilicity toxin, tar, nicotine and TPM etc. in the flue gas, resemble the punching filter tip and not only can play the effect of diluting flue gas, can effectively reduce the content of carbon monoxide in the master stream flue gas simultaneously.
Find in my the reducing cigarette tar and reducing harm reduction research process, though above measure can reduce the tar in the cigarette mainstream flue gas relatively effectively and poison composition, but their efficient is not high usually, additive is verified in the composite filter tip can not remain in the process of suction effectively, obviously this physicochemical characteristic with additive or additive is relevant, though the specific surface of some additive is very big, but its practical efficiency is not high, some highly active material such as free radical enter in people's the respiratory tract by filter tip rapidly under the high linear flow speed of main flume in the main flume, and be same because the specific surface of common vinegar fibre also just has only 4.5m 2About/g, therefore also be difficult to by a large amount of harmful substance of its surface absorption.
The first of the present invention is embodied on its design concept, promptly adds solution by the instant filter tip of clear and definite prepared cigarette smoking and adds separately in addition in preceding 1 minute at cigarette smoking, belongs to different parts with cigarette; It two is to add an amount of this solution on the cigarette filter tow, the tow surface is able to suitable wetting, by cooling effect, can effectively reduce the temperature that main flume enters respiratory tract, reduce the infringement of high temperature to respiratory mucosa, but and some high boiling trace harmful components such as polynuclear aromatic hydrocarbons etc. in the rapid condensation main flume; The reduction of temperature can also reduce the diffusion of harmful components in the main flume, thereby further reduces the infringement to mucous membrane; Because the cigarette smoking instant tip rod appended solution contains antioxidant content, therefore can effectively catch free radical and other strong active component of oxidisability in the main flume, remove the nucleophilicity toxin in the main flume simultaneously, when containing vitamin E in the solution, add the selenium element and can also strengthen this effect; The film that the aqueous solution forms can effectively dissolve water-soluble cilium toxin such as HCN in the main flume, methacrylaldehyde.The cigarette smoking instant tip rod appended solution can also be designed to fragrance interpolation or transmission solution, improves the suction grade of cigarette.
The specific embodiment:
Embodiment 1: take by weighing in 2.0 liters of pure water of vitamin C 100.0~2000.0g dissolving, taking by weighing watermiscible vitamin E 100.0g~2000.0g, sodium selenite 5.0~100.0g then respectively adds in the above-mentioned solution and is stirred to dissolving, be settled to 10.0L, get the instant filter tip of cigarette smoking and add solution.Contain VC, VE and sodium selenite in the solution and be respectively 10.0mg~200.0mg/ml, 10.0mg~200.0mg/ml and 0.5mg~10.0mg/ml.Before smoking cigarette, on filter tip, add 10 μ l~400 μ l, improve flue gas suction grade, smoke panel test and think that its too big excitant of improving cigarette mainstream flue gas, smoke are softer along larynx.
Embodiment 2: take by weighing sodium selenite 50.0g~500.0g, take by weighing watermiscible vitamin E 100.0g~1000.0g, be dissolved in 5 liters of pure water, then add TBHQ (ditert-butylhydro quinone) 20.0g, be diluted to 10.0L, get the instant filter tip of cigarette smoking and add solution.Containing sodium selenite, vitamin E, TBHQ in the solution is respectively: 5mg/ml~50mg/ml, 10.0mg/ml~100.0mg/ml.Before smoking cigarette, on filter tip, add 10 μ l~400 these solution of μ l, smoke panel test and think that it has improved the excitant of cigarette mainstream flue gas greatly, smoke is softer along larynx.
Embodiment 3: take by weighing Tea Polyphenols 1000.0g~3000.0g, be dissolved in 5 liters of pure water, add watermiscible vitamin E 50.0g~500.0g again, get the instant filter tip of cigarette smoking and add solution.Containing Tea Polyphenols and VE in the solution respectively is 100.0mg/ml~300.0mg/ml, 5.0mg/ml~50.0mg/ml.Smoke panel test and think that it has improved the excitant of cigarette mainstream flue gas greatly, smoke is softer along larynx.
Embodiment 4: take by weighing each 100.0g~4000.0g of zinc sulfate and vitamin C and E, be dissolved in the pure water, and be settled to 10.0 liters, get the instant filter tip of cigarette smoking and add solution.The concentration that contains three kinds of materials in the solution is the same, is: between 10.0mg/ml~400.0mg.Before smoking cigarette, on filter tip, add 10 μ l~400 these solution of μ l, smoke panel test and think that it has improved the excitant of cigarette mainstream flue gas greatly, smoke is softer along larynx.
Embodiment five: take by weighing zinc sulfate 100.0g~4000.0g, sodium selenite 20.0g~200.0g, ditert-butylhydro quinone 20.0g~100.0g is dissolved in 5 liters of pure water, add PVP (polyvinylpyrrolidone) 10.0g again, be settled to 10.0 liters after the dissolving, get the instant filter tip of cigarette smoking and add solution.Smoke panel test and think that it has improved the excitant of cigarette mainstream flue gas greatly, smoke is softer along larynx.
Embodiment six: take by weighing OPC (95%) 100.0g~2000.0g, zinc sulfate 100.0~1000.0g, ditert-butylhydro quinone 20.0g~100.0g are dissolved in 5 liters of pure water, are settled to 10.0 liters after the dissolving, get the instant filter tip of cigarette smoking and add solution.Smoke panel test and think that it has improved the excitant of cigarette mainstream flue gas greatly, smoke is softer along larynx.
Embodiment seven: take by weighing zinc sulfate 100.0g~4000.0g, sodium selenite 20.0g~200.0g, ditert-butylhydro quinone 20.0g~100.0g is dissolved in 5 liters of pure water, after waiting to dissolve, add 1 liter of saturated menthol solutions again, be settled to 10.0 liters, get the instant filter tip of cigarette smoking and add solution.Smoke panel test and think that it has improved the excitant of cigarette mainstream flue gas greatly, smoke is softer along larynx, and have refrigerant tasty and refreshing sensation, under the situation that does not increase technical difficulty, solved the problem that peppermint is volatilized rapidly in the peppermint cigarette aspiration procedure.
Embodiment eight: the cigarette smoking that is obtained by said method is added solution immediately, and in preceding 1 minute of smoking cigarette, adding is no more than 400 these solution of μ l, (inhaled 2 seconds in taking out the enterprising column criterion aspiration procedure of smoking machine again, stopped for 60 seconds), collect the tar on the cambridge filter, analyze.The result shows, can reduce nicotine more than 40%, and methacrylaldehyde wherein, HCN etc. have all descended more than 95%, and benzo [a] pyrene has descended more than 80%, and is better in the effect to its improvement of cigarette of some composite filter tip type, wherein can't detect free radical.

Claims (9)

1. the instant tip rod appended solution when being used for cigarette smoking based on vitamins, Tea Polyphenols, natural extract class polyphenoils for the aqueous solution on basis or non-aqueous solution;
2. according to the described cigarette smoking instant tip rod appended solution of claim 1, it is characterized in that: contained material is vitamin C, vitamin E, natural extract (natural extract that contains the natural anti-oxidation functional mass as a big class such as grape seed extract, Pine Bark, tea extract) etc. in the solution.
3. according to the described cigarette smoking instant tip rod appended solution of claim 1, it is characterized in that: material contained in the solution is except that being the right 1 described material, and it can also additionally add trace element (as selenium, zinc, calcium, iron etc.).
4. according to the described cigarette smoking instant tip rod appended solution of claim 1, it is characterized in that: material contained in the solution can also be by extra interpolation fragrance component such as peppermint etc. except that being the right 1 described material.
5. the instant tip rod appended solution preparation method during the described cigarette smoking of claim 1, it is characterized in that: one or more mixing in claim 1,2, the 3 and 4 described materials are dissolved in pure water or the nonaqueous solvents instant tip rod appended solution in the time of can obtaining cigarette smoking.
6. aforementioned cigarette smoking instant tip rod appended solution, it is characterized in that its design concept, that is: add immediately during cigarette smoking, comprise the solution design is designed in cigarette package at any position of cigarette filter tip end or with such solution, comprise also that certainly the cigarette smoking instant tip rod appended solution is separately as a kind of product.
7. aforementioned cigarette smoking instant tip rod appended solution, it is characterized in that: before cigarette smoking, add in 0~1 minute, its addition is between 10 μ L~400 μ L, be used for reducing harmful composition of cigarette mainstream flue gas such as methacrylaldehyde, hydrogen cyanide, maple aldehyde, nicotine, nitrosamine, some polynuclear aromatic hydrocarbons (as benzo [a] pyrene) and free radical etc., can effectively reduce the temperature that main flume enters respiratory tract simultaneously.
8. aforementioned cigarette smoking instant tip rod appended solution and preparation method thereof is characterized in that: can be designed as the interpolation solution with fragrance and fragrance transmission performance, improve the suction grade.
9. aforementioned cigarette smoking instant tip rod appended solution is characterized in that: itself and cigarette do not belong to same series products, and it and cigarette are two parts, add in the filter tip in 0~1 minute before cigarette smoking.
CN 200310111373 2003-11-12 2003-11-12 Preparation of instant cigarette tip additive solution and using method Pending CN1615761A (en)

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CN 200310111373 CN1615761A (en) 2003-11-12 2003-11-12 Preparation of instant cigarette tip additive solution and using method

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Application Number Priority Date Filing Date Title
CN 200310111373 CN1615761A (en) 2003-11-12 2003-11-12 Preparation of instant cigarette tip additive solution and using method

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CN1615761A true CN1615761A (en) 2005-05-18

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006097010A1 (en) * 2005-03-14 2006-09-21 Xixian Qiu AN INSTANT ADDITIVE SOLUTION FOR THE FILTER OF CIGARETTl, ITS PRODUCTION METHOD AND USE
CN105146702A (en) * 2015-08-21 2015-12-16 华南农业大学 Antioxidant solution for curing tobaccos, preparation method thereof and application thereof
CN107890136A (en) * 2017-11-08 2018-04-10 江苏瑾辉生物科技有限公司 Application of the Tea Polyphenols in harmful substance volatilization in reducing smoke of tobacco
CN108576922A (en) * 2018-03-21 2018-09-28 云南中烟工业有限责任公司 The complex additive and its preparation method and application of phenol release amount in a kind of reduction flue gas

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006097010A1 (en) * 2005-03-14 2006-09-21 Xixian Qiu AN INSTANT ADDITIVE SOLUTION FOR THE FILTER OF CIGARETTl, ITS PRODUCTION METHOD AND USE
CN105146702A (en) * 2015-08-21 2015-12-16 华南农业大学 Antioxidant solution for curing tobaccos, preparation method thereof and application thereof
CN105146702B (en) * 2015-08-21 2017-03-01 华南农业大学 A kind of flue-cured tobacco antioxidant solution and preparation method and application
CN107890136A (en) * 2017-11-08 2018-04-10 江苏瑾辉生物科技有限公司 Application of the Tea Polyphenols in harmful substance volatilization in reducing smoke of tobacco
CN108576922A (en) * 2018-03-21 2018-09-28 云南中烟工业有限责任公司 The complex additive and its preparation method and application of phenol release amount in a kind of reduction flue gas

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