CN1416860A - Prepn process of life prolonging tablet - Google Patents
Prepn process of life prolonging tablet Download PDFInfo
- Publication number
- CN1416860A CN1416860A CN 02146612 CN02146612A CN1416860A CN 1416860 A CN1416860 A CN 1416860A CN 02146612 CN02146612 CN 02146612 CN 02146612 A CN02146612 A CN 02146612A CN 1416860 A CN1416860 A CN 1416860A
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- filter
- tapping
- timing
- storage tank
- material quantity
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- 238000000034 method Methods 0.000 title description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 29
- 239000000463 material Substances 0.000 claims abstract description 20
- 239000000843 powder Substances 0.000 claims abstract description 9
- 229920002472 Starch Polymers 0.000 claims abstract description 7
- 235000019698 starch Nutrition 0.000 claims abstract description 7
- 239000008107 starch Substances 0.000 claims abstract description 7
- 235000018167 Reynoutria japonica Nutrition 0.000 claims abstract description 6
- 240000001341 Reynoutria japonica Species 0.000 claims abstract description 6
- 238000010438 heat treatment Methods 0.000 claims abstract description 4
- 238000010992 reflux Methods 0.000 claims abstract description 4
- 238000010079 rubber tapping Methods 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000009835 boiling Methods 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 7
- 210000000582 Semen Anatomy 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 4
- 229920001353 Dextrin Polymers 0.000 claims description 3
- 239000004375 Dextrin Substances 0.000 claims description 3
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 235000019425 dextrin Nutrition 0.000 claims description 3
- 239000007888 film coating Substances 0.000 claims description 3
- 238000009501 film coating Methods 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000004064 recycling Methods 0.000 claims description 3
- KEAYESYHFKHZAL-UHFFFAOYSA-N sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 238000009495 sugar coating Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 2
- 240000007371 Cuscuta campestris Species 0.000 abstract 1
- 241000208688 Eucommia Species 0.000 abstract 1
- 240000000249 Morus alba Species 0.000 abstract 1
- 235000008708 Morus alba Nutrition 0.000 abstract 1
- 241000405414 Rehmannia Species 0.000 abstract 1
- 241001278833 Rosa laevigata Species 0.000 abstract 1
- 235000000661 Rosa laevigata Nutrition 0.000 abstract 1
- 235000013399 edible fruits Nutrition 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000005453 pelletization Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 4
- 230000018109 developmental process Effects 0.000 description 3
- 210000003734 Kidney Anatomy 0.000 description 2
- 210000004185 Liver Anatomy 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 206010049865 Achromotrichia acquired Diseases 0.000 description 1
- 210000000988 Bone and Bones Anatomy 0.000 description 1
- 241000668709 Dipterocarpus costatus Species 0.000 description 1
- 210000003205 Muscles Anatomy 0.000 description 1
- 229940095674 Pellet Product Drugs 0.000 description 1
- 201000004384 alopecia Diseases 0.000 description 1
- 231100000360 alopecia Toxicity 0.000 description 1
- 230000003698 anagen phase Effects 0.000 description 1
- 230000003005 anti-senility Effects 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000003779 hair growth Effects 0.000 description 1
- 239000002547 new drug Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001737 promoting Effects 0.000 description 1
- 231100000486 side effect Toxicity 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
Abstract
The present invention includes grinding partial fleeceflower root into fine powder, thrice decocting partial fleeceflower root together with seven kinds of Chinese medicinal materials including Cherokee rose fruit, mulberry, rehmannia root, etc., merging decoction, filtering and decompression concentrating to obtain the first thick paste; thrice heating reflux extracting Herba Siegesbackiae, dodder seed, eucommia bark and other three kinds of Chinese medicinal materials with 70% concentration ethanol and other steps to obtain the second thick paste; mixing two kinds of thick paste, fleeceflower root powder, starch or other excipient; pelletizing; and tabletting to the plain or coated tablet.
Description
Technical field
The present invention is a kind of preparation method of anti-senility life-prolonging sheet, relates to the pharmaceutical technology field.
Background technology
Increasing in view of the aged on the current social, the defying age new drug that development has curative effect, imperative.Existing 00112868.X life prolonging health care medicine prescription patent is to be used for tonifying liver, the kidney invigorating, YIN nourishing and YANG strengthening, promote hair restoration, effects such as black hair are the granule dosage forms, 95110178.1 be that Shengfaling electuary for promoting hair growth prescription patent is to be used for the treatment of alopecia, poliosis, documents such as 1998 the 21st the 2nd phases of volume of Luzhou Medical College journal 1998 the 21st volume the 1st phase " ancient prescription life-prolonging pellet product development research situation " and Luzhou Medical College journal " ancient prescription lengthen the life DANJI sanction side effect and product development research situation " disclose liquor, sublimed preparation, granule, the prescription of tablet, still it is open to find no the method for preparing the sheet of lengthening the life, little in order to obtain dosage, the eutherapeutic tablet of lengthening the life, we mend the vegetarian medical book in clear generation and lengthen the life and change sanction on the folk prescription basis and form prescription and proportioning and preparation method thereof and be different from prior art, be used for liver and kidney tonifying, lengthen the life tablet recipe and proportioning and preparation method thereof of strong muscles and bones.
Summary of the invention
Lengthen the life sheet by Radix Polygoni Multiflori Limitation-or-qualification Herba Siegesbeckiae, field dobber, the Cortex Eucommiae, Fructus Ligustri Lucidi, Folium Mori, Caulis Lonicerae, Fructus Mori, Semen Sesami Nigrum, Radix Rehmanniae, Fructus Rosae Laevigatae, black Fructus seu radix camptothecae acuminatae (Fructus Camptothecae Acuminatae), Semen sojae atricolor, compositions such as Radix Achyranthis Bidentatae, its preparation method is to get 69.4% of fleece-flower root total inventory to be ground into fine powder, residue cataclasm one-tenth fritter of Radix Polygoni Multiflori and Fructus Rosae Laevigatae, Fructus Mori, Radix Rehmanniae, Caulis Lonicerae, Radix Achyranthis Bidentatae, Herba Ecliptae, Semen sojae atricolor decocts with water, divide and decoct for three times, (98 ℃～102 ℃ of temperature) decocts for the first time amount of water is 7 times of material quantity, the timing of boiling, 1.5 after hour, filter, tapping is to storage tank, decoct for the second time amount of water and be 5 times of material quantity, the timing of boiling, after 1 hour, filter, tapping is to storage tank, decoct amount of water for the third time and be 5 times of material quantity, the timing of boiling, after 1 hour, filter, tapping is to storage tank, merge three times decoction liquor, leave standstill, filter, filtrate decompression is condensed into thick paste (relative density 1.35～1.40) Limitation-or-qualification Herba Siegesbeckiae, field dobber, the Cortex Eucommiae, Fructus Ligustri Lucidi, Folium Mori, Semen Sesami Nigrum is extracted three times (78 ℃～82 ℃ of temperature) with 70% alcohol heating reflux, add for the first time ethanol and be 5 times of material quantity, after the timing 1.5 hours, filter, tapping is to storage tank, add for the second time ethanol and be 4 times of material quantity, after the timing 1 hour, filter, tapping is to storage tank, add ethanol for the third time and be 4 times of material quantity, after the timing 1 hour, filter, tapping merges three times extracting solution to storage tank, leaves standstill, filter, decompression recycling ethanol, extracting solution is condensed into thick paste (relative density 1.30～1.35) starch or the auxiliary type agent mix homogeneously such as dextrin or carboxymethyl starch sodium of two kinds of thick pastes and Radix Polygoni Multiflori fine powder and 1%～10% is granulated decompression, drying is made plain sheet or sugar coating or film coating by prior art again.
Description of drawings
The invention provides process chart (process chart is attached), describe in detail and see the explanation of the specific embodiment.
The specific embodiment
For further understanding content of the present invention, characteristics and effect, existing combined process flow chart exemplifies following examples, Radix Polygoni Multiflori (72g) is got 69.4% of fleece-flower root total inventory and is ground into fine powder, residue cataclasm one-tenth fritter of Radix Polygoni Multiflori and Fructus Rosae Laevigatae (16g), Fructus Mori (16g), Radix Rehmanniae (4g), Caulis Lonicerae (4g), Radix Achyranthis Bidentatae (8g), Herba Ecliptae (16g), Semen sojae atricolor (16g) decocts with water, divide and decoct for three times, (98 ℃～102 ℃ of temperature) decocts for the first time amount of water is 7 times of material quantity, the timing of boiling, 1.5 after hour, filter, tapping is to storage tank, decoct for the second time amount of water and be 5 times of material quantity, the timing of boiling, after 1 hour, filter, tapping is to storage tank, decoct amount of water for the third time and be 5 times of material quantity, the timing of boiling, after 1 hour, filter, tapping is to storage tank, merge three times decoction liquor, leave standstill, filter, filtrate decompression is condensed into thick paste (relative density 1.35～1.40) Limitation-or-qualification Herba Siegesbeckiae (16g), field dobber (16g), the Cortex Eucommiae (8g), Fructus Ligustri Lucidi (8g), Folium Mori (8g), Semen Sesami Nigrum (16g) is extracted three times (78 ℃～82 ℃ of temperature) with 70% alcohol heating reflux, add for the first time ethanol and be 5 times of material quantity, after the timing 1.5 hours, filter, tapping is to storage tank, add for the second time ethanol and be 4 times of material quantity, after the timing 1 hour, filter, tapping is to storage tank, add ethanol for the third time and be 4 times of material quantity, after the timing 1 hour, filter, tapping is to storage tank, merge three times extracting solution, leave standstill, filter, decompression recycling ethanol, extracting solution is condensed into thick paste (relative density 1.30～1.35), the starch or the auxiliary type agent mix homogeneously such as dextrin or carboxymethyl starch sodium of two kinds of thick pastes and Radix Polygoni Multiflori fine powder and 1%～10% are granulated, decompression, dry, make plain sheet or sugar coating or film coating by prior art again, good effect, dosage is little.
Claims (1)
1, the lengthen the life method of sheet of a kind of preparation, it is characterized in that getting 69.4% of fleece-flower root total inventory is ground into fine powder and is ground into fine powder, residue cataclasm one-tenth fritter of Radix Polygoni Multiflori and Fructus Rosae Laevigatae, Fructus Mori, Radix Rehmanniae, Caulis Lonicerae, Radix Achyranthis Bidentatae, Herba Ecliptae, Semen sojae atricolor decocts with water, divide and decoct for three times, (98 ℃～102 ℃ of temperature) decocts for the first time amount of water is 7 times of material quantity, the timing of boiling, 1.5 after hour, filter, tapping is to storage tank, decoct for the second time amount of water and be 5 times of material quantity, the timing of boiling, after 1 hour, filter, tapping is to storage tank, decoct amount of water for the third time and be 5 times of material quantity, the timing of boiling, after 1 hour, filter, tapping is to storage tank, merge three times decoction liquor, leave standstill, filter, filtrate decompression is condensed into thick paste (relative density 1.35～1.40) Limitation-or-qualification Herba Siegesbeckiae, field dobber, the Cortex Eucommiae, Fructus Ligustri Lucidi, Folium Mori, Semen Sesami Nigrum is extracted three times (78 ℃～82 ℃ of temperature) with 70% alcohol heating reflux, add for the first time ethanol and be 5 times of material quantity, after the timing 1.5 hours, filter, tapping is to storage tank, add for the second time ethanol and be 4 times of material quantity, after the timing 1 hour, filter, tapping is to storage tank, add ethanol for the third time and be 4 times of material quantity, after the timing 1 hour, filter, tapping merges three times extracting solution to storage tank, leave standstill, filter, decompression recycling ethanol, extracting solution are condensed into thick paste (relative density 1.30～1.35), and the starch or the auxiliary type agent mix homogeneously such as dextrin or carboxymethyl starch sodium of two kinds of thick pastes and Radix Polygoni Multiflori fine powder and 1%～10% are granulated, decompression, drying is made plain sheet or sugar coating or film coating by prior art again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02146612 CN1416860A (en) | 2002-10-28 | 2002-10-28 | Prepn process of life prolonging tablet |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02146612 CN1416860A (en) | 2002-10-28 | 2002-10-28 | Prepn process of life prolonging tablet |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1416860A true CN1416860A (en) | 2003-05-14 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 02146612 Pending CN1416860A (en) | 2002-10-28 | 2002-10-28 | Prepn process of life prolonging tablet |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1416860A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103705624A (en) * | 2013-12-22 | 2014-04-09 | 青岛琴诚医药技术有限公司 | Preparation method and application of life-prolonging tablet |
| CN104096074A (en) * | 2014-06-05 | 2014-10-15 | 张金城 | Chinese medicinal composition for treatment of endocrine dyscrasia |
-
2002
- 2002-10-28 CN CN 02146612 patent/CN1416860A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103705624A (en) * | 2013-12-22 | 2014-04-09 | 青岛琴诚医药技术有限公司 | Preparation method and application of life-prolonging tablet |
| CN104096074A (en) * | 2014-06-05 | 2014-10-15 | 张金城 | Chinese medicinal composition for treatment of endocrine dyscrasia |
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| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |