CN1334329A - Shatian Pomelo wine and its preparing process - Google Patents
Shatian Pomelo wine and its preparing process Download PDFInfo
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Abstract
本发明属于果酒加工技术领域,具体涉及以沙田柚为原料生产沙田柚酒及其加工工艺的发明。其特点是,以食用酒精浸泡柚皮制备浸泡液,以蒸馏法制备柚皮蒸馏液,混合前述两液制备调香酒。柚汁接种酵母菌发酵,经勾兑、陈酿和过滤等工序,制成风味独特的沙田柚酒。与已有技术相比,本发明工艺简洁,系统配套,果实综合利用效率较高。The invention belongs to the technical field of fruit wine processing, and in particular relates to the invention of producing Shatian pomelo wine by using Shatian pomelo as a raw material and its processing technology. It is characterized in that the pomelo peel is soaked in edible alcohol to prepare soaking liquid, the pomelo peel distillate is prepared by distillation, and the two liquids are mixed to prepare flavored wine. The pomelo juice was inoculated with yeast and fermented, and then blended, aged and filtered to make Shatian pomelo wine with unique flavor. Compared with the prior art, the invention has simple process, complete system and high efficiency of fruit comprehensive utilization.
Description
本发明属于果酒加工技术领域,特别是关于应用发酵法结合浸泡和蒸馏法生产沙田柚酒系列及其加工工艺的发明。The invention belongs to the technical field of fruit wine processing, and in particular relates to the production of Shatian pomelo wine series and its processing technology by applying a fermentation method combined with soaking and distillation methods.
柚子属芸香科,柑桔亚科,是我国南方各省栽培较为广泛的常绿果树。柚子品种繁多,如沙田柚、官溪蜜柚、金香柚、四川梁山柚和浙江平阳四季抛等品种,其中最著名的品种为沙田柚,该品种在我国栽培面积大,品质佳,但不耐贮藏,贮藏不当,易引起汁囊沙化、严重影响其商品价值。Pomelo belongs to Rutaceae, Citrus subfamily, and is an evergreen fruit tree widely cultivated in southern provinces of my country. There are many varieties of pomelo, such as Shatian pomelo, Guanxi honey pomelo, Jinxiang pomelo, Sichuan Liangshan pomelo, and Zhejiang Pingyang Sijipo pomelo. The most famous variety is Shatian pomelo. This variety has a large cultivation area in my country and has good quality, but it is not resistant to storage. , Improper storage can easily cause desertification of the juice sac and seriously affect its commodity value.
沙田柚果实中含糖15g/100ml果汁、柠檬酸0.3-1.5g/100ml、维生素C35-200ml/100ml,此外,还含有丰富的维生素B1、维生素B2、维生素P、胡萝卜素、钙、铁、镁、钾、钠、高级醇、醛、酮挥发性有机酸与萜烯类,柚皮含枸橼醛、黄酮甙、柚甙、新橙皮甙、枸橘甙等。具有燥湿祛痰、止咳定喘、理气健胃消食、强化毛细管、防止血管脆化或破裂的功能。Shatian pomelo fruit contains sugar 15g/100ml juice, citric acid 0.3-1.5g/100ml, vitamin C 35-200ml/100ml, in addition, it is also rich in vitamin B1, vitamin B2, vitamin P, carotene, calcium, iron, magnesium Potassium, sodium, higher alcohols, aldehydes, ketones, volatile organic acids and terpenes, pomelo peel contains citral, flavonoid glycosides, naringin, neohesperidin, citrusin, etc. It has the functions of drying dampness and eliminating phlegm, relieving cough and relieving asthma, regulating qi, invigorating stomach and eliminating food, strengthening capillaries, and preventing vascular embrittlement or rupture.
目前国内外柚子的消费基本以鲜食为主,有些国家利用柚子中一个品种如葡萄柚加工制汁,或从柚子果皮中提香精油、果胶、色素、柚苷(新柚皮甙二氢查尔酮),有些则将柚子的皮渣制作饲料粉或饲料颗粒等产品(见《果树栽培学》南方本,中国农业出版社,修订本,1990)。At present, the consumption of pomelo at home and abroad is mainly fresh food. Some countries use a variety of pomelo such as grapefruit to process juice, or extract essential oil, pectin, pigment, naringin (neonaringin dihydro chalcone), and some make products such as feed powder or feed granules from pomelo skin dregs (see "Promaculture" Southern Edition, China Agricultural Press, revised edition, 1990).
在本发明做出以前,果酒的生产基本上沿用传统的果实榨汁,自然发酵加食用酒精补充酒精度,调糖、调酸和调香等工艺,经陈酿后进行人工勾兑作为食用果酒(亦称露酒、配制酒)出售,因而果实的利用率不高,果香及风味不突出,有些果酒还带有其特有的苦、涩味(如柚子)。Before the present invention is made, the production of fruit wine basically continues to use traditional fruit juice, natural fermentation adds edible alcohol to supplement alcohol, processes such as sugar adjustment, acid adjustment and flavoring, artificial blending is carried out as edible fruit wine (also known as edible fruit wine) after aging. Therefore, the utilization rate of the fruit is not high, and the fruit aroma and local flavor are not prominent, and some fruit wines also have their unique bitterness and astringency (such as grapefruit).
本发明的目的在于利用复合微生物多级发酵工艺方法酿造柚子酒,以提高果酒的风味和综合利用的效果The purpose of the present invention is to utilize the compound microbial multi-stage fermentation process method to brew pomelo wine, to improve the local flavor of fruit wine and the effect of comprehensive utilization
本发明通过以下技术方案实现:The present invention is realized through the following technical solutions:
一种以沙田柚为原料的酒,是由用食用酒精浸泡柚皮制备的浸泡液,以蒸馏法制备的柚皮蒸馏液,以上述浸泡液和蒸馏液混合制备的调香酒,以柚皮肉榨汁发酵的调味酒,经勾兑,陈酿,过滤工艺加工而成的沙田柚酒,该酒按以下配方制作:A kind of wine with Shatian pomelo as raw material, which is prepared by soaking pomelo peel with edible alcohol, distilled pomelo peel distillate prepared by distillation, flavored wine prepared by mixing the above soaking liquid and distillate, and pomelo peel meat The seasoning wine fermented by squeezing the juice is processed into Shatian pomelo wine through blending, aging and filtration. The wine is made according to the following formula:
按重量计:调香酒5L,调味酒1.5L,β-环糊精50-100克,浆水3.5L,余量是基酒。By weight: 5L of flavored wine, 1.5L of flavored wine, 50-100 grams of β-cyclodextrin, 3.5L of syrup, and the rest is base wine.
本发明以沙田柚(其它品种柚亦可)为原料经发酵、浸泡和蒸馏生产不同酒精度的沙田柚酒。In the invention, Shatian pomelo wines with different alcohols are produced by fermenting, immersing and distilling the Shatian pomelo (other types of pomelo are also acceptable).
一种沙田柚酒的加工工艺,其步骤包括:A processing technology of Shatian pomelo wine, the steps comprising:
1)选择完整、未发霉变质、保鲜较好的沙田柚,将皮、肉分开存放;1) Choose Shatian pomelo that is complete, not moldy and spoiled, and has a good freshness, and store the skin and meat separately;
2)柚皮的加工:首先将柚皮肉(果胶部分)用水果刀去除,用自来水冲洗干净,凉干备用;2) Processing of pomelo peel: first remove the pomelo peel (pectin part) with a fruit knife, rinse it with tap water, and dry it for later use;
3)柚肉的加工:将柚肉置于压榨机内榨汁取第一次汁液,然后将榨汁过的柚肉渣用含有5%的乙醇溶液按柚肉∶乙醇1∶1浸泡数小时(夏秋季为2-3小时、春冬季为8-12小时),榨汁得第二次汁。将第一、二次汁液混合供发酵用。3) Processing of pomelo meat: put the pomelo meat in a press to squeeze the juice for the first time, then soak the pomelo meat dregs with 5% ethanol solution according to pomelo meat: ethanol 1:1 for several hours (2-3 hours in summer and autumn, 8-12 hours in spring and winter), squeeze the juice to get the second juice. The first and second juices are mixed for fermentation.
4)按重量百分比浓度以0.1-0.3%的量加入粉末活性炭,并按百万分之一的量加入高锰酸钾对食用酒精进行处理。首先将高锰酸钾用水溶化,然后边加入边搅拌。24小时后加入粉末活性炭,边加入边搅拌。每隔4-6小时搅拌一次,搅拌4次后,静置72小时过滤备用。4) adding powdered activated carbon in an amount of 0.1-0.3% by weight percentage, and adding potassium permanganate in an amount of one millionth to treat the edible alcohol. First, dissolve potassium permanganate in water, and then stir while adding. After 24 hours, powdered activated carbon was added and stirred while adding. Stir once every 4-6 hours, after stirring 4 times, let stand for 72 hours and filter for later use.
5)柚皮的泡制:取处理好的酒精用蒸馏水或纯净水稀释至9-12度的酒精,按柚皮重量的6%加入浸泡20-24小时后立即将浸泡液过滤备用。然后再用同体积的9-12度的酒精再浸泡20-24小时,立即将浸泡液过滤,并与第一次浸泡液混合均匀备用。柚皮集中在一起蒸馏回收酒精(50度)。回收的酒精置于过滤好的浸泡液中混合后即得调香酒备用。5) Soaking of pomelo peel: take the processed alcohol and dilute it to 9-12 degrees with distilled water or pure water, add 6% of the weight of pomelo peel and soak for 20-24 hours, then immediately filter the soaking solution for later use. Then soak with the same volume of 9-12 degree alcohol for another 20-24 hours, filter the soaking solution immediately, and mix it with the first soaking solution evenly for later use. The pomelo peels are concentrated and distilled to recover alcohol (50 degrees). The recovered alcohol is placed in the filtered soaking liquid and mixed to obtain the flavored wine for later use.
6)柚肉汁的发酵:将榨汁好的柚肉汁立即放入发酵罐中,按发酵度重量的16%加入蔗糖糖浆,其然后按发酵液总重量的0.1-0.3%称取葡萄酒活性干酵母(该活性干酵母可以从市场上购得),先用2-2.5%的糖液,在35-37℃活化30分钟,然后将干酵母液倒入发酵罐中边搅拌边加入,发酵7天,待发酵完全终止后,检查酒精度、残糖量、酸度,并做好原始记录。过滤转入陈酿罐中后酵(夏秋季7天、春冬季10-15天),即得调味酒备用。6) Fermentation of pomelo gravy: put the pomelo gravy that has been squeezed into a fermenter immediately, add sucrose syrup according to 16% of the fermentation degree weight, and then weigh wine active dry yeast according to 0.1-0.3% of the total weight of the fermentation liquid (The active dry yeast can be purchased from the market), first use 2-2.5% sugar solution, activate it at 35-37°C for 30 minutes, then pour the dry yeast solution into the fermenter and add it while stirring, and ferment for 7 days After the fermentation is completely terminated, check the alcohol content, residual sugar content, acidity, and make original records. Filter and transfer to the aging tank for post-fermentation (7 days in summer and autumn, 10-15 days in spring and winter), and then get seasoning wine for later use.
7)勾兑:按重量百分比加入调香酒50%,调味酒15%,除苦剂(β-环糊精)0.5-1.0%(50-100克)进行勾兑。然后将勾兑好的酒过滤置陈酿罐中陈酿60-90天。7) Blending: Add 50% of flavored wine, 15% of flavored wine, and 0.5-1.0% (50-100 grams) of bittering agent (β-cyclodextrin) by weight percentage for blending. Then the blended wine is filtered and aged in aging tanks for 60-90 days.
8)过滤:发酵酒过滤、调味酒过滤为粗滤,半成品酒过滤为精滤。8) Filtration: Filtration of fermented wine and seasoning wine is coarse filtration, and filtration of semi-finished wine is fine filtration.
9)粗滤硅藻土的配比:发酵酒粗土∶细土=2∶1,调香酒粗土∶细土=1∶1,总用土量卧式过滤机为1.5kg左右。9) The ratio of diatomite for coarse filtration: coarse soil for fermented wine: fine soil = 2:1, coarse soil for flavored wine: fine soil = 1:1, and the total amount of soil used for the horizontal filter is about 1.5kg.
10)预涂:将待过滤酒液泵入上土容器中,上土容器的容量为硅藻土机150-200kg。先加入粗土,搅拌均匀,上机循环5分钟,然后加入细土于上土容器中,保持循环保持10分钟左右,确认滤液中无沉淀物、悬浮物、清亮透明即可进行原酒的过滤。10) Pre-coating: pump the wine liquid to be filtered into the soil container, and the capacity of the soil container is 150-200kg for a diatomaceous earth machine. First add coarse soil, stir evenly, and circulate the machine for 5 minutes, then add fine soil to the soil container, keep circulating for about 10 minutes, confirm that there is no sediment, suspended matter in the filtrate, and it is clear and transparent to filter the raw wine.
11)预涂和过滤过程中不得停机,否则须循环稳定5分钟以上,确认过滤机视窗中酒液恢复透明后方可进行过滤,预涂和过滤过程中的转换可以通过泵进口和过滤机出口的三通来完成。11) Do not stop the machine during the pre-coating and filtering process, otherwise the cycle must be stable for more than 5 minutes. After confirming that the wine in the filter window becomes transparent, the filter can be performed. The conversion during the pre-coating and filtering process can be done through the pump inlet and filter outlet. Tee to complete.
12)过滤后的酒液要求清亮透明,无沉淀物、悬浮物。12) The filtered liquor should be clear and transparent without sediment or suspended matter.
13)色度的调整,过滤的初期可以在调配罐中进行循环,同时在过滤机上取酒样和标准色进行比较,如果未达到标准需要进行调整至合格。13) Adjustment of chromaticity, in the initial stage of filtration, it can be circulated in the blending tank, and at the same time, take a wine sample on the filter and compare it with the standard color, if it does not meet the standard, it needs to be adjusted to pass.
14)过滤好的酒液泵入陈酿罐中进行陈酿,陈酿周期为60天,容器要求密封好。14) The filtered wine is pumped into the aging tank for aging. The aging period is 60 days, and the container is required to be well sealed.
15)澄清处理:在陈酿期的7-10天内必须进行澄清处理,具体的方法及要求如下:按每吨原料酒加入50个鸡蛋的比例将蛋清完全打成泡沫,在循环或搅拌陈酿酒的情况下加入酒中,使其与酒液充分混合均匀,自然沉降。处理后的酒液严禁再次搅拌。15) Clarification treatment: clarification treatment must be carried out within 7-10 days of the aging period. The specific method and requirements are as follows: add 50 eggs per ton of raw wine to completely beat the egg white into foam, and then circulate or stir the aged wine. In case of adding to the wine, make it fully mixed with the wine liquid, and settle naturally. It is strictly forbidden to stir the processed liquor again.
16)半成品预测在陈酿结束前的1-3天应对陈酿酒进行抽样检查,项目为酒精度及技术部门的品尝意见,鉴定合格后才能进入下一道工序。16) Prediction of semi-finished products. The aging wine should be sampled and inspected 1-3 days before the end of aging. The items are the alcohol content and the tasting opinions of the technical department. Only after passing the appraisal can the next process be entered.
17)精滤取陈酿罐分离层以上的澄清酒液泵入过滤机中进行过滤,切勿使分离层以下的沉淀酒液混入。精滤时硅藻土配比为:粗土∶细土=1∶1,总用土量卧式过滤机为2kg,上土要求同步骤⑩。精滤后的酒液要求清澈透明。17) Fine filtration The clarified liquor above the separation layer of the aging tank is pumped into the filter for filtration, and the precipitated liquor below the separation layer must not be mixed in. The ratio of diatomite during fine filtration is: coarse soil: fine soil = 1:1, the total amount of soil used for the horizontal filter is 2kg, and the requirements for adding soil are the same as step ⑩. The finely filtered wine should be clear and transparent.
本发明与已有技术相比的效果:Effect of the present invention compared with prior art:
1、本发明的柚子酒产品柚子风味突出,且无柚子固有的苦味和涩味,适口性好。1. The pomelo wine product of the present invention has outstanding pomelo flavor, no inherent bitterness and astringency of pomelo, and good palatability.
2、本发明的工艺将现代发酵工艺与中国传统果酒制作工艺中的浸泡工艺和蒸馏工艺相结合,经多级发酵陈酿和调香等工艺步骤,可以最大限度利用柚子的全部果实和保持柚香风味,其工艺简洁,步骤配套,工艺适应性强,好操作,易管理。2. The process of the present invention combines the modern fermentation process with the immersion process and distillation process in the traditional Chinese fruit wine production process. Through the process steps such as multi-stage fermentation aging and flavoring, it can maximize the use of all pomelo fruits and maintain pomelo fragrance. Flavor, the process is simple, the steps are matched, the process is adaptable, easy to operate, and easy to manage.
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Cited By (12)
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| CN100396765C (en) * | 2005-04-25 | 2008-06-25 | 陈长寿 | Technique for producing fruit wine by using shaddock as raw material |
| CN101085950B (en) * | 2007-06-11 | 2011-04-06 | 林伟锋 | Shaddock whole-fruit beer and its production process |
| CN103305378A (en) * | 2013-06-06 | 2013-09-18 | 厦门圣尼诺生物科技有限公司 | Shaddock wine and preparation method thereof |
| CN103642641A (en) * | 2013-12-20 | 2014-03-19 | 山东师范大学 | Lonicera japonica and grapefruit fruit wine |
| CN104450386A (en) * | 2014-11-28 | 2015-03-25 | 柳州贵族酒业有限公司 | Fruit wine and preparation method thereof |
| CN105441288A (en) * | 2016-01-29 | 2016-03-30 | 刘延波 | Hawthorn wine and making process thereof |
| CN105713757A (en) * | 2016-01-28 | 2016-06-29 | 佛山市聚成生化技术研发有限公司 | Grape wine for female and containing peach leaf naringenin |
| CN107365669A (en) * | 2017-09-21 | 2017-11-21 | 闽南师范大学 | A kind of radix glycyrrhizae shaddock wine and preparation method thereof |
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| CN108949415A (en) * | 2018-06-29 | 2018-12-07 | 广西秀美壮乡能源环保有限公司 | A kind of preparation process of shatian pomelo health liquor |
| CN109055133A (en) * | 2018-09-17 | 2018-12-21 | 米益汀 | A kind of fruit flavoured type spirit preparation method |
| CN109735405A (en) * | 2019-03-07 | 2019-05-10 | 梅州市珍宝金柚实业有限公司 | A kind of method that semi-solid ferment preparation essence makes golden-pomelo beer |
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- 2000-07-14 CN CNB001159011A patent/CN1176201C/en not_active Expired - Fee Related
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|---|---|---|---|---|
| CN100396765C (en) * | 2005-04-25 | 2008-06-25 | 陈长寿 | Technique for producing fruit wine by using shaddock as raw material |
| CN101085950B (en) * | 2007-06-11 | 2011-04-06 | 林伟锋 | Shaddock whole-fruit beer and its production process |
| CN103305378A (en) * | 2013-06-06 | 2013-09-18 | 厦门圣尼诺生物科技有限公司 | Shaddock wine and preparation method thereof |
| CN103642641A (en) * | 2013-12-20 | 2014-03-19 | 山东师范大学 | Lonicera japonica and grapefruit fruit wine |
| CN104450386A (en) * | 2014-11-28 | 2015-03-25 | 柳州贵族酒业有限公司 | Fruit wine and preparation method thereof |
| CN105713757A (en) * | 2016-01-28 | 2016-06-29 | 佛山市聚成生化技术研发有限公司 | Grape wine for female and containing peach leaf naringenin |
| CN105441288A (en) * | 2016-01-29 | 2016-03-30 | 刘延波 | Hawthorn wine and making process thereof |
| CN107365669A (en) * | 2017-09-21 | 2017-11-21 | 闽南师范大学 | A kind of radix glycyrrhizae shaddock wine and preparation method thereof |
| CN108949415A (en) * | 2018-06-29 | 2018-12-07 | 广西秀美壮乡能源环保有限公司 | A kind of preparation process of shatian pomelo health liquor |
| CN108841486A (en) * | 2018-07-13 | 2018-11-20 | 江苏洋河酒厂股份有限公司 | A kind of preparation method of grapefruit honey alcoholic drink mixed with fruit juice |
| CN109055133A (en) * | 2018-09-17 | 2018-12-21 | 米益汀 | A kind of fruit flavoured type spirit preparation method |
| CN109735405A (en) * | 2019-03-07 | 2019-05-10 | 梅州市珍宝金柚实业有限公司 | A kind of method that semi-solid ferment preparation essence makes golden-pomelo beer |
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| CN1176201C (en) | 2004-11-17 |
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