CN1203794A - Freeze-dried sheep placenta extract powder and its production method - Google Patents
Freeze-dried sheep placenta extract powder and its production method Download PDFInfo
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- CN1203794A CN1203794A CN98115761A CN98115761A CN1203794A CN 1203794 A CN1203794 A CN 1203794A CN 98115761 A CN98115761 A CN 98115761A CN 98115761 A CN98115761 A CN 98115761A CN 1203794 A CN1203794 A CN 1203794A
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Abstract
The present invention discloses a freeze-dried sheep embryonin extract powder and its production process, belonging to the field of nutrient health-care product and biopharmaceutical technology. Said invention is a composite containing several bio-active substances, and possesses miraculous health-preserving and face-beautifying action. Its production process includes the following steps: cleaning sheep embro and quick-freezing to 27 deg.C below zero, then beating by using ultra-low temperature beater and reciprocal freezing,and dehydration-drying by using ultra-low temp. freeze-drying machine so as to obtain the invented product whose water content is 3% and sheep embryonin extract content is 90-95%. Besides, said product can be stored for a long period.
Description
The invention belongs to nutrient and healthcare products, field of biological pharmacy, particularly a kind of freeze-dried sheep placenta extract powder and production method thereof.
Sheep placental extract is rich in conceived 1-3 the female intravital embryo of month sheep, it is the complex of multiple bioactive substance, it comprises each seed amino acid, phospholipid, lipopolysaccharide, multivitamin, various trace elements, the panimmunity factor, multiple many property enzyme, body fluid regulatory factor, somatomedin and does not decode as yet at present, but the effectively mysterious material of exciting human vitality, i.e. vitamin X etc.Sheep placental extract has good adjusting physiological equilibrium's effect, and the defence disease is that a kind of energy promotion is healthy, blood-enriching qi-invigorating, and skin maintenance keeps vitality, improves the natural materials of body immunity and resistance against diseases.Therefore, sheep placental extract can be used as the raw material or the additive of medicine, food, health product, cosmetics.
In Ningxia, farming and pastoral areas, northwest such as Qinghai, Gansu, Inner Mongol, the annual autumn and winter are butchered season, have a large amount of conceived early stage ewes slaughtered, sheep embryo resource is very abundant.But because process technology falls behind, make this valuable natural resources not obtain due development and utilization at present.Chinese patent CN 1142949A disclosed " frozen dry powder of sheep placenta " is to be raw material with the Placenta caprae seu ovis, enters the cryotherapy environment again after clean the pulverizing, adopts freeze drying process to be prepared from.This invention is to be raw material with the puerperal Placenta Hominis of ewe, and this moment Placenta Hominis in most of nutrition absorbed by lamb, utilization rate decreases, it is the pre-treatment of raw material that this invention also has a deficiency, promptly cleaning Placenta caprae seu ovis pulverizes at normal temperatures, such technical process can cause many heat to imitate the destruction and the forfeiture of inhibition biological active composition, has reduced use value.
The objective of the invention is to make full use of this resource of ewe body early embryo, and entire production process is under the ultralow temperature state and freeze-dried sheep placenta extract powder and the production method thereof made.
The objective of the invention is to realize by following technical scheme:
A kind of freeze-dried sheep placenta extract powder is characterized in that moisture content is 3%, and fineness is the 80-100 order, sheep placental extract content 90-95%, and preserve sheep embryo original nutrient contents.
A kind of production method of freeze-dried sheep placenta extract powder, its feature is as follows:
(1) pretreatment of raw material: the sheep embryo quick-freezing that cleans up is to-27 ℃, standby;
(2) making beating: with above-mentioned material chopping, enter in the beater and pull an oar, the pasty material temperature is controlled at below 0 ℃, and fineness is controlled at the 80-100 order;
(3) quick-freezing: with above-mentioned pasty material sabot, material thickness is sent into quick freezing repository less than 2cm, and quick-freezing is reduced to about-35 ℃ temperature of charge;
(4) back and forth freeze: above-mentioned material is sent in the freezer dryer dryness storehouse be cooled to-50 ℃, control temperature then, it is gone up to-27 ℃, kept 30-60 minute, be cooled to-40 ℃ again, constant temperature 1-2 hour;
(5) evacuation: the coagulator temperature of freezer dryer is transferred to below-50 ℃, evacuation, vacuum reaches 27-40Pa and gets final product;
(6) material distillation: temperature of charge transfers to about-27 ℃, and the coagulator temperature transfers to-60 ℃, and the time was controlled at 10 hours;
(7) drying of material: be divided into the two-stage, the phase I temperature of freezer dryer dryness storehouse is controlled between-10 ℃～10 ℃, and the time is 4 hours, and second stage dryness storehouse temperature is controlled at about 30 ℃, and the time is 2 hours;
(8) material delivers from godown and beats powder: enter after material is sent from dryness storehouse in the low temperature powder beater and beat powder, the finished product temperature of making is controlled at about 0 ℃, and fineness is the 80-100 order;
(9) packaging sterilizing of finished product: after the specification packing, sterilize.
Because production process of the present invention is controlled at the ultralow temperature state all the time, thus from sheep embryo's making beating to drying, all help the survival of the bioactive substance in its product, product of the present invention in addition has the dissolubility height, it is instant to meet water; Moisture content is easy to long preservation about 3%; Form is full, and Stability Analysis of Structures is difficult for advantages such as oxidized.
Embodiment 1:
The temperature cleaned is comprised 10 kilograms of choppings such as Placenta Hominis, amniotic fluid-27 ℃ sheep embryo, putting into the ultralow temperature beater that is connected with liquid nitrogen pulls an oar, control material temperature is at 0 ℃, with fineness is 80 orders, water content in 95% slurry sabot, thickness is 1.5cm, send into quick-freezing in the quick freezing repository, making temperature of charge is-35 ℃.This moment, the dryness storehouse of cryogenic temperature freezing drying machine was chilled to-40 ℃ in advance, the material disc that quick-freezing is good is put into dryness storehouse, between-27 ℃～-50 ℃, back and forth freeze, promptly earlier material is cooled to-50 ℃ at a slow speed, kept 1 hour, and then temperature of charge was gone up, kept 1 hour to eutectic point-27 ℃, be cooled to-40 ℃ again, constant temperature 1 hour.The condenser temperature of cryogenic temperature freezing drying machine is controlled at-50 ℃, starts vacuum pump, evacuation makes the vacuum in the dryness storehouse reach 27Pa.This moment, temperature of charge transferred to-27 ℃, and the temperature of condenser transfers to-60 ℃, and after 10 hours, free water is sublimed into gas in the material, condenses into frost through condenser, again material is carried out drying.Drying is divided into two stages, and the temperature of phase I with the freezer dryer dryness storehouse is controlled at-10 ℃, and the time is 4 hours, and second stage is controlled at 30 ℃ with the dryness storehouse temperature, and the time is 2 hours.Dry run finishes when the finished product moisture content is 3%, delivers from godown, and then enters rapidly in the ultralow temperature powder beater and beats powder, and temperature of charge is controlled at 0 ℃, and the fineness of finished product is 80 orders, and penetrating rate reaches 95%, adopts the gamma-rays radiation sterilization by specification packing back.
Embodiment 2:
The temperature cleaned is comprised 100 kilograms of choppings such as Placenta Hominis, amniotic fluid-27 ℃ sheep embryo, putting into the ultralow temperature beater that is connected with liquid nitrogen pulls an oar, control material temperature is at 0 ℃, with fineness is 60 orders, water content in 75% slurry sabot, thickness is 1cm, send into quick-freezing in the quick freezing repository, making temperature of charge is-30 ℃.This moment, the dryness storehouse of cryogenic temperature freezing drying machine was chilled to-40 ℃ in advance, the good material disc of quick-freezing is put into dryness storehouse, between-27 ℃～-50 ℃, back and forth freeze, promptly earlier material is cooled to-50 ℃ at a slow speed, kept 1 hour, and then temperature of charge was gone up, kept 1 hour to eutectic point-27 ℃, be cooled to-40 ℃ again, constant temperature 1 hour.The condenser temperature of cryogenic temperature freezing drying machine is controlled at-50 ℃, starts vacuum pump, evacuation makes the vacuum in the dryness storehouse reach 27Pa.This moment, temperature of charge transferred to-27 ℃, and the temperature of condenser transfers to-60 ℃, and after 10 hours, free water is sublimed into gas in the material, condenses into frost through condenser, again material is carried out drying.Drying is divided into two stages, and the temperature of phase I with the freezer dryer dryness storehouse is controlled at 10 ℃, and the time is 4 hours, and second stage is controlled at 30 ℃ with the dryness storehouse temperature, and the time is 2 hours.When the finished product moisture content was 3%, dry run finished, and delivers from godown, and then enters rapidly in the ultralow temperature powder beater and beats powder, and temperature of charge is controlled at 0 ℃, and the fineness of finished product is 100 orders, and penetrating rate reaches 95%, adopted the gamma-rays radiation sterilization by specification packing back.
Claims (2)
1. a freeze-dried sheep placenta extract powder is characterized in that moisture content is 3%, and fineness is the 80-100 order, sheep placental extract content 90-95%, and preserve sheep embryo original nutrient contents.
2. the production method of a freeze-dried sheep placenta extract powder, its feature is as follows:
(1) pretreatment of raw material: the sheep embryo quick-freezing that cleans up is to-27 ℃, standby;
(2) making beating: with above-mentioned material chopping, enter in the beater and pull an oar, the pasty material temperature is controlled at below 0 ℃, and fineness is controlled at the 80-100 order;
(3) quick-freezing: with above-mentioned pasty material sabot, material thickness is sent into quick freezing repository less than 2cm, and quick-freezing is reduced to about-35 ℃ temperature of charge;
(4) back and forth freeze: above-mentioned material is sent in the freezer dryer dryness storehouse be cooled to-50 ℃, control temperature then, it is gone up to-27 ℃, kept 30-60 minute, be cooled to-40 ℃ again, constant temperature 1-2 hour;
(5) evacuation: the coagulator temperature of freezer dryer is transferred to below-50 ℃, evacuation, vacuum reaches 27-40Pa and gets final product;
(6) material distillation: temperature of charge transfers to about-27 ℃, and the coagulator temperature transfers to-60 ℃, and the time was controlled at 10 hours;
(7) drying of material: be divided into the two-stage, the phase I temperature of freezer dryer dryness storehouse is controlled between-10 ℃～10 ℃, and the time is 4 hours, and second stage dryness storehouse temperature is controlled at about 30 ℃, and the time is 2 hours;
(8) material delivers from godown and beats powder: enter after material is sent from dryness storehouse in the low temperature powder beater and beat powder, the finished product temperature of making is controlled at about 0 ℃, and fineness is the 80-100 order;
(9) packaging sterilizing of finished product: after the specification packing, sterilize.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98115761A CN1203794A (en) | 1998-07-10 | 1998-07-10 | Freeze-dried sheep placenta extract powder and its production method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98115761A CN1203794A (en) | 1998-07-10 | 1998-07-10 | Freeze-dried sheep placenta extract powder and its production method |
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| Publication Number | Publication Date |
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| CN1203794A true CN1203794A (en) | 1999-01-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN98115761A Pending CN1203794A (en) | 1998-07-10 | 1998-07-10 | Freeze-dried sheep placenta extract powder and its production method |
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| CN (1) | CN1203794A (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1329041C (en) * | 2005-04-08 | 2007-08-01 | 广州拜迪生物医药有限公司 | Production method of zhutaisu (pig's born vegetarian) |
| CN103181553A (en) * | 2011-12-30 | 2013-07-03 | 广州拜迪生物医药有限公司 | Pig placentin production method |
| US20140147511A1 (en) * | 2011-06-10 | 2014-05-29 | Tissue Tech, Inc. | Methods of processing fetal support tissues, fetal support tissue powder products, and uses thereof |
| CN105343128A (en) * | 2015-11-19 | 2016-02-24 | 界首市菁华科技信息咨询服务有限公司 | Processing method of sheep placenta instant powder |
| US9526770B2 (en) | 2011-04-28 | 2016-12-27 | Tissuetech, Inc. | Methods of modulating bone remodeling |
| US9724370B2 (en) | 2005-09-27 | 2017-08-08 | Tissuetech, Inc. | Amniotic membrane preparations and purified compositions and therapy for scar reversal and inhibition |
| US9750772B2 (en) | 2005-09-27 | 2017-09-05 | Tissuetech, Inc. | Amniotic membrane preparations and purified compositions and anti-angiogenesis treatment |
| US9808491B2 (en) | 2014-06-03 | 2017-11-07 | Tissuetech, Inc. | Compositions of morselized umbilical cord and/or amniotic membrane and methods of use thereof |
| CN109350627A (en) * | 2018-11-28 | 2019-02-19 | 广东冠龙生物科技有限公司 | A kind of freeze-dried sheep placenta extract powder and preparation method thereof |
-
1998
- 1998-07-10 CN CN98115761A patent/CN1203794A/en active Pending
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1329041C (en) * | 2005-04-08 | 2007-08-01 | 广州拜迪生物医药有限公司 | Production method of zhutaisu (pig's born vegetarian) |
| US9724370B2 (en) | 2005-09-27 | 2017-08-08 | Tissuetech, Inc. | Amniotic membrane preparations and purified compositions and therapy for scar reversal and inhibition |
| US10632155B2 (en) | 2005-09-27 | 2020-04-28 | Tissuetech, Inc. | Amniotic membrane preparations and purified compositions and therapy for scar reversal and inhibition |
| US10272119B2 (en) | 2005-09-27 | 2019-04-30 | Tissuetech, Inc. | Amniotic membrane preparations and purified compositions and therapy for scar reversal and inhibition |
| US9956252B2 (en) | 2005-09-27 | 2018-05-01 | Tissuetech, Inc. | Purified amniotic membrane compositions and methods of use |
| US9750772B2 (en) | 2005-09-27 | 2017-09-05 | Tissuetech, Inc. | Amniotic membrane preparations and purified compositions and anti-angiogenesis treatment |
| US9750771B2 (en) | 2005-09-27 | 2017-09-05 | Tissuetech, Inc. | Amniotic membrane preparations and purified compositions and anti-inflammation methods |
| US9526770B2 (en) | 2011-04-28 | 2016-12-27 | Tissuetech, Inc. | Methods of modulating bone remodeling |
| US9675733B2 (en) | 2011-04-28 | 2017-06-13 | Tissuetech, Inc. | Methods of modulating bone remodeling |
| US9682044B2 (en) * | 2011-06-10 | 2017-06-20 | Tissuetech, Inc. | Methods of processing fetal support tissues, fetal support tissue powder products, and uses thereof |
| US20140147511A1 (en) * | 2011-06-10 | 2014-05-29 | Tissue Tech, Inc. | Methods of processing fetal support tissues, fetal support tissue powder products, and uses thereof |
| US10426731B2 (en) | 2011-06-10 | 2019-10-01 | Tissuetech, Inc. | Methods of processing fetal support tissues, fetal support tissue powder products, and uses thereof |
| CN103181553A (en) * | 2011-12-30 | 2013-07-03 | 广州拜迪生物医药有限公司 | Pig placentin production method |
| US9808491B2 (en) | 2014-06-03 | 2017-11-07 | Tissuetech, Inc. | Compositions of morselized umbilical cord and/or amniotic membrane and methods of use thereof |
| US11116800B2 (en) | 2014-06-03 | 2021-09-14 | Tissuetech, Inc. | Compositions of morselized umbilical cord and/or amniotic membrane and methods of use thereof |
| CN105343128A (en) * | 2015-11-19 | 2016-02-24 | 界首市菁华科技信息咨询服务有限公司 | Processing method of sheep placenta instant powder |
| CN109350627A (en) * | 2018-11-28 | 2019-02-19 | 广东冠龙生物科技有限公司 | A kind of freeze-dried sheep placenta extract powder and preparation method thereof |
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