Natural active ingredient extraction process and equipment
Technical Field
The application relates to the technical field of biotechnology, in particular to a natural active ingredient extraction process and equipment.
Background
In the field of extraction of natural active ingredients, with rapid development of medicine, health products, cosmetics and functional food industries, the purity, yield and environmental protection requirements of plant source active substances are increasingly improved. Although the traditional solid-liquid extraction, repeated reflux or ultrasonic auxiliary extraction and other processes can obtain target components to a certain extent, the problems of long extraction time, high energy consumption, residual risk of organic solvents, low pretreatment efficiency of raw materials and the like often exist. Especially for plant branches and leaves with high cellulose and lignin content, the conventional crushing means are difficult to fully open cell walls, so that the release of active ingredients is insufficient, the extraction depth and the selectivity are limited, and the requirements of large-scale, low-cost and high-quality production are difficult to meet.
In the prior art, most factories rely on single mechanical stirring or simple crushing in the pretreatment stage of raw materials, enzyme preparations are not synchronously introduced to assist in cell breakage, so that incomplete branch and leaf breakage and uneven material mixing are easily caused, the subsequent extraction efficiency is influenced, the screening or separating step usually adopts a traditional screen or static vibrating screen mode, the wall breaking efficiency is low, the materials are easy to block, the screening precision is limited, the energy consumption and the maintenance cost are higher, in the aspect of deep extraction, the solvent permeation can be enhanced by means of conventional reflux or ultrasonic vibration, but the selective extraction capability of targeted components is insufficient, the secondary extraction effect is poor, the equipment transformation space is small, the cost input of large-scale production is large, and the requirements of modern, intelligent and green extraction process are difficult to meet.
Disclosure of Invention
In order to solve the above-mentioned problems, the present application provides a process and apparatus for extracting natural active ingredients.
The application provides a natural active ingredient extraction process and equipment, which adopts the following technical scheme that the process comprises the following steps:
Optionally, S1, raw material pretreatment:
The stirring structure at the upper end of the tank body is used for starting a driver to drive the stirring rod I and the stirring rod to complete the preliminary breaking and uniform mixing of the plant branches and leaves;
s2, dynamic wall breaking treatment:
A second screening disc of a driver of the screening structure is started to act with the first rotating plate in a synergistic way, and cell wall crushing is realized through the screening groove;
s3, compound extraction:
The positioning rod of the rotating structure drives the second rotating plate, the sorting rod and the ejector rod to form an eddy effect, and the deep extraction is performed by combining the vibration effect of the screening structure;
s4, liquid-solid separation and transmission:
driving a pump to start a spiral groove conveying system, utilizing centrifugal force to realize primary solid-liquid separation, and enabling concentrated solution to enter the next working procedure through a conveying pipe;
S5, secondary fine extraction optimization:
and the stirring structure and the rotating structure are combined, and the stirring intensity is regulated through the rotating frame, so that the secondary extraction of the target components is performed.
Optionally, in step 1, in order to improve the stirring performance of the stirring structure, an enzyme preparation needs to be added into the plant branches and leaves in advance, and the enzyme preparation is fully mixed, so that the plant branches and leaves can be fully stirred, and the cell rupture is accelerated.
Optionally, the stirring in step 2 and step 1 are both eddy-vibration coupled stirring, which has the advantages of high stirring speed, high efficiency, low cost, and the like compared with the conventional stirring method.
The natural active ingredient extraction equipment comprises a stirring structure for mixing materials, a screening structure for breaking walls of the materials, a rotating structure for improving mixing capacity, a transmission structure for transmitting liquid, wherein the stirring structure is arranged at the upper end of a tank body, the screening structure is fixedly arranged at the inner bottom of the tank body, the rotating structure is fixedly connected with the bottom of the screening structure, the transmission structure is fixedly arranged at the bottom of the rotating structure, the stirring structure comprises a stirring tank, a first driver is fixedly connected with the top of the stirring tank, a circular ring is fixedly arranged at the bottom of the first driver, a first stirring rod is fixedly connected with the bottom of the circular ring, a driving rod is fixedly connected with the outer side of the middle part of the first stirring rod, and a stirring rod is movably connected with the outer side of the driving rod.
According to the scheme, the stirring tank provides a container space for stirring operation, the driver drives other components, the circular ring is connected with the supporting component, the stirring rod is driven by the driver to rotate, the stirring rod is movably connected to the driving rod, the components are matched to perform preliminary crushing and uniform mixing on plant branches and leaves, the screening structure is arranged at the inner bottom of the tank body and is responsible for wall breaking treatment of materials, the rotating structure is connected to the bottom of the screening structure and combines vibration lifting mixing capacity of the screening structure, power-assisted deep extraction is performed, the transmission structure is arranged at the bottom of the rotating structure, the driving pump drives the components, the spiral groove performs preliminary separation on solid and liquid, and concentrated liquid is conveyed to the next working procedure.
Optionally, screening structure includes rotor plate one, rotor plate one's bottom is provided with driver two, driver two's outside is fixed to be provided with the screening board, driver two's bottom fixedly connected with screening dish, screening dish's bottom is fixed to be provided with the drive plate, the bottom fixedly connected with dead lever of drive plate, screening plate's outside is fixedly provided with dwang, the periphery fixedly connected with puddler two of dwang, the top fixedly connected with drive gear of dwang, the top fixedly connected with rotating turret of drive gear, the inside at the standing groove is installed to the rotating turret, rotor plate one's top is fixed to be provided with the branch sieve groove.
According to the scheme, the screening groove arranged at the top of the first rotating plate breaks cell walls, the second driver drives the first rotating plate, the other end of the second driver is connected with the screening disc, the screening disc is driven to strengthen the wall breaking effect, the screening plate is fixed on the outer side of the second driver, the screening disc is enabled to stably operate, the bottom of the screening disc is connected with other parts through the driving plate and the fixing rod, the self structure is stabilized, power transmission is assisted, one end of the rotating rod is connected with the screening plate, one end of the rotating rod extends to the top and is connected with the driving gear, the power of the second driver is transmitted to the upper part, mounting support is provided for the second stirring rod, the second stirring rod is fixed on the periphery of the rotating rod, materials can be stirred during rotation, mixing uniformity and wall breaking efficiency are improved, the top of the driving gear is connected with the rotating frame, and the rotating frame is mounted in the placing groove, so that the screening structure can flexibly adapt to different extraction requirements through rotating and adjusting the running state of the screening structure.
Optionally, the revolution mechanic includes the locating lever, the outside fixedly connected with rotor plate two of locating lever, rotor plate two's bottom fixedly connected with connecting rod, the bottom fixedly connected with of connecting rod selects separately the pole, one side of selecting separately the pole is provided with the ejector pin.
According to the scheme, the positioning rod can ensure stable operation of the rotating structure, the second rotating plate is fixed on the outer side of the positioning rod and rotates along with rotation of the positioning rod to provide an installation platform for a lower part component, the connecting rod is connected with the second rotating plate, the separation rod is connected with the lower part of the second rotating plate, the rotating force of the second rotating plate can be transmitted to the separation rod, the separation rod rotates under the drive of the connecting rod, the separation rod is fully contacted with materials in the rotating process, separation operation can be carried out on the materials, effective components are separated, and the ejector rod is arranged on one side of the separation rod and matched with the separation rod to enhance mixing and extraction effects on the materials.
Optionally, the transmission structure includes the bottom plate, inside one side fixedly connected with drive pump of bottom plate, one side fixedly connected with helicla flute of drive pump.
Through the scheme, the bottom plate provides a stable mounting platform for other components, so that the conveying operation can be performed in a stable environment, the driving pump is fixed on one side of the inside of the bottom plate, the spiral groove is connected with the driving pump, the spiral groove guides the concentrated solution to stably advance along a spiral track, the solid and the liquid are primarily separated, and the concentrated solution is conveyed from the current process to the next process.
Optionally, the outside fixedly connected with lifting rod of jar body, the top periphery of jar body is fixedly provided with the rack, the bottom fixedly connected with v type funnel ring of jar body, the top fixedly connected with conveyer pipe of v type funnel ring.
According to the technical scheme, the lifting rod is fixed on the outer side of the tank body, so that operators can conveniently carry and move the tank body, the installation and position adjustment requirements of equipment in different scenes are met, the placement frame is arranged on the periphery of the top of the tank body, a placement space can be provided for related auxiliary parts or tools, the v-shaped funnel ring is connected to the bottom of the tank body, concentrated liquid after primary solid-liquid separation can be converged and guided, the liquid can flow downwards more smoothly, and one end of the conveying pipe is fixed on the top of the v-shaped funnel ring, so that the converged concentrated liquid can be conveyed to a designated position accurately and efficiently.
Optionally, the bottom periphery fixedly connected with support post of the jar body, the top periphery of the jar body is provided with the drum post, the top of drum post is fixedly provided with the rack, one side of rack is fixedly provided with base piece, the top fixedly connected with screening structure of base piece, the bottom of base piece is fixedly provided with the axis of rotation.
Through the scheme, the support column is fixed on the periphery of the bottom of the tank body, the tank body is ensured to be kept stable in the operation process and cannot shake or incline, the cylindrical column is arranged on the periphery of the top of the tank body, the structural strength of the top of the tank body can be enhanced, the placement frame at the top of the cylindrical column is convenient and reasonable to place components, one side of the base block is connected with the placement frame, the screening structure can be stably fixed, and the angle adjustment is provided for the screening structure through the rotating shaft arranged at the bottom, so that the screening structure can break walls and sort materials better in the operation of equipment.
In summary, the application has the following beneficial technical effects:
According to the invention, the first driver, the first stirring rod, the stirring rod and other parts in the stirring structure are arranged, and the first driver can drive the first stirring rod and the stirring rod to primarily crush and uniformly mix plant branches and leaves through the power transmission and connection relation between the first driver and the first stirring rod and between the first driver and the stirring rod, and enzyme preparations are added into the plant branches and leaves in advance and fully mixed, so that cell rupture is further accelerated, the technical problems of insufficient cell rupture and uneven mixing of the plant branches and leaves in the extraction process can be solved through the full stirring of the stirring structure and the assistance of the enzyme preparations, the raw material pretreatment efficiency and quality can be improved, and high-quality raw materials are provided for the subsequent extraction process.
According to the invention, the components such as the second driver, the first screening disc, the rotating plate and the screening groove in the screening structure are arranged, the screening disc and the first rotating plate are mutually matched through the dynamic connection relation between the second driver and the first screening disc and between the second driver and the first rotating plate, the screening groove is utilized to realize cell wall crushing, and compared with the traditional stirring mode, the vortex-vibration coupling stirring mode is adopted, the stirring speed is high, the efficiency is high, the cost is low, the technical problems of low cell wall crushing efficiency and high cost in the traditional extraction process can be solved through the screening structure, the dynamic wall breaking treatment efficiency can be improved, the production cost is reduced, and the extraction economic benefit is improved.
According to the invention, through arranging the positioning rod, the second rotating plate, the sorting rod, the ejector rod and other parts in the rotating structure, the positioning rod drives the second rotating plate, the sorting rod and the ejector rod to form a vortex effect through the connection relation between the positioning rod and the second rotating plate, the connection relation between the positioning rod and the sorting rod, the ejector rod, and the vortex effect of the rotating plate, the vortex effect of the second rotating plate is combined with the vibration effect of the screening structure to perform deep extraction, and meanwhile, the rotating plate is used in combination with the stirring structure, the stirring intensity is adjusted through the rotating frame to perform secondary extraction of the targeted component, the technical problems of insufficient extraction depth and low extraction rate of the targeted component in the traditional extraction process can be solved through the vortex effect of the rotating structure and the mutual cooperation of the rotating frame and the stirring structure, and the extraction purity and efficiency can be improved.
Drawings
FIG. 1 is a schematic view of the overall structure of an embodiment of the present application;
FIG. 2 is a schematic view of a tank body according to an embodiment of the present application;
FIG. 3 is a schematic view of a cylindrical column according to an embodiment of the present application;
FIG. 4 is a schematic view of a rack according to an embodiment of the present application;
FIG. 5 is a schematic view of the structure of a tank according to an embodiment of the present application;
FIG. 6 is a schematic top view of a first actuator according to an embodiment of the present application;
FIG. 7 is a schematic view of the internal part of the tank according to the embodiment of the application;
fig. 8 is a schematic structural view of a screening structure in an embodiment of the present application.
The device comprises the following components of 1, a tank body, 2, a stirring structure, 21, a stirring tank, 22, a driving rod, 23, a stirring rod I, 24, a circular ring, 25, a driver I, 26, a stirring rod, 3, a lifting rod, 4, a placing frame, 5, a transmission structure, 51, a spiral groove, 52, a bottom plate, 53, a driving pump, 6, a conveying pipe, 7, a support column, 8, a screening structure, 81, a rotating plate I, 82, a driver II, 83, a screening plate, 84, a rotating frame, 85, a placing groove, 86, a driving gear, 87, a stirring rod II, 88, a screening disc, 89, a driving plate, 810, a fixing rod, 811, a rotating rod, 812, a screening groove, 9, a base block, 10, a cylinder column, 11, a v-shaped funnel ring, 12, a rotating shaft, 13, a rotating structure, 131, a positioning rod, 132, a screening rod, 133, a connecting rod, 134, a push rod, 135 and a rotating plate II.
Detailed Description
The application is described in further detail below with reference to fig. 1-8.
The embodiment of the application discloses a natural active ingredient extraction process and equipment.
Example 1:
s1, pretreatment of raw materials:
The stirring structure 2 at the upper end of the tank body 1 is used for starting the first driver 25 to drive the first stirring rod 23 and the stirring rod 26 to complete the preliminary crushing and uniform mixing of the plant branches and leaves;
s2, dynamic wall breaking treatment:
The second driver 82 of the screening structure 8 is started to act cooperatively with the first rotating plate 81, and cell wall disruption is realized through the screening groove 812;
s3, compound extraction:
the positioning rod 131 of the rotary structure 13 drives the second rotary plate 135, the sorting rod 132 and the ejector rod 134 to form an eddy effect, and the deep extraction is performed by combining the vibration effect of the screening structure 8;
s4, liquid-solid separation and transmission:
the driving pump 53 starts the spiral groove 51 conveying system, the solid-liquid preliminary separation is realized by utilizing centrifugal force, and the concentrated solution enters the next working procedure through the conveying pipe 6;
S5, secondary fine extraction optimization:
the stirring mechanism 2 and the rotating mechanism 13 are used in combination, and the stirring intensity is adjusted by the rotating frame 84 to perform secondary extraction of the targeted component.
In step1, in order to improve the stirring performance of the stirring structure, an enzyme preparation needs to be added into the plant branches and leaves in advance, and the enzyme preparation is fully mixed, so that the plant branches and leaves can be fully stirred, and the cell rupture is accelerated.
The stirring in the step 2 and the step 1 are both eddy-vibration coupled stirring modes, and compared with the traditional stirring modes, the stirring method has the advantages of high stirring speed, high efficiency, low cost and the like.
Example 2:
Referring to fig. 1 to 8, a natural active ingredient extracting apparatus includes a stirring structure 2 for mixing materials, a screening structure 8 for breaking walls of the materials, a rotating structure 13 for improving mixing capability, a transmission structure 5 for transmitting liquid, the stirring structure 2 mounted at the upper end of a tank 1, the screening structure 8 fixedly mounted at the inner bottom of the tank 1, the rotating structure 13 fixedly connected with the bottom of the screening structure 8, the transmission structure 5 fixedly disposed at the bottom of the rotating structure 13, the stirring structure 2 including a stirring tank 21, a first driver 25 fixedly connected with the top of the stirring tank 21, a circular ring 24 fixedly disposed at the bottom of the first driver 25, a first stirring rod 23 fixedly connected with a driving rod 22 outside the middle of the stirring rod 23, and a stirring rod 26 movably connected with the outer side of the driving rod 22.
It should be explained that, in the stirring structure 2, the stirring tank 21 is a space for stirring operation, the first driver 25 drives the ring 24 to rotate, so that the first stirring rod 23 rotates, the driving rod 22 in the middle of the first stirring rod 23 rotates, the stirring rod 26 movably connected to the outside of the stirring rod can stir materials, so that the branches and leaves of plants are fully crushed and uniformly mixed, the screening structure 8 is fixed at the inner bottom of the tank 1 and is responsible for breaking wall, active components can be effectively broken by breaking cell walls, the rotating structure 13 is connected at the bottom of the screening structure 8 and can be matched with the screening structure 8, the mixing effect is enhanced, the extraction depth is improved, the transmission structure 5 is positioned at the bottom of the rotating structure 13, the driving pump 53 provides power, the spiral groove 51 guides the flow of concentrated solution, and performs preliminary separation on solid and liquid concentrate to the next procedure.
Referring to fig. 1 to 8, the screening structure 8 includes a first rotating plate 81, a second driver 82 is disposed at the bottom of the first rotating plate 81, a screening plate 83 is fixedly disposed at the outer side of the second driver 82, a screening disc 88 is fixedly connected to the bottom of the second driver 82, a driving plate 89 is fixedly disposed at the bottom of the screening disc 88, a fixing rod 810 is fixedly connected to the bottom of the driving plate 89, a rotating rod 811 is fixedly disposed at the outer side of the screening plate 83, a stirring rod second 87 is fixedly connected to the periphery of the rotating rod 811, a driving gear 86 is fixedly connected to the top of the rotating rod 811, a rotating frame 84 is fixedly connected to the top of the driving gear 86, the rotating frame 84 is mounted in the placement groove 85, and a screening groove 812 is fixedly disposed at the top of the first rotating plate 81.
It should be explained that, the screening groove 812 arranged at the top of the first rotating plate 81 can directly extrude and rub materials to crush cell walls, the second driver 82 drives the first connecting screening disc 88 to rotate and support the first rotating plate 81 to break walls cooperatively up and down, the screening plate 83 is fixed on the outer side of the second driver 82, the smooth power transmission is ensured, the screening disc 88 is connected with lower parts through the driving plate 89 and the fixing rod 810, the structural stability of the screening plate is enhanced, one end of the rotating rod 811 is connected with the screening plate 83, one end of the rotating rod extends to the top and is connected with the driving gear 86, the second stirring rod 87 fixed on the periphery can stir the materials during rotation, the mixing uniformity and the wall breaking efficiency are improved, the driving gear 86 drives the rotating frame 84 to rotate in the placing groove 85, the stirring strength can be flexibly adjusted, and different extraction requirements are adapted.
Referring to fig. 1 to 8, the rotating structure 13 includes a positioning rod 131, a second rotating plate 135 is fixedly connected to the outer side of the positioning rod 131, a connecting rod 133 is fixedly connected to the bottom of the second rotating plate 135, a sorting rod 132 is fixedly connected to the bottom of the connecting rod 133, and a push rod 134 is disposed on one side of the sorting rod 132.
It should be noted that, the positioning rod 131 ensures that the subsequent components can accurately run, the second rotating plate 135 is fixedly sleeved on the outer side of the positioning rod 131, and synchronously rotates along with the rotation of the positioning rod 131, the power of the positioning rod 131 is stably transmitted to the lower components, one end of the connecting rod 133 is tightly connected with the second rotating plate 135, the other end of the connecting rod pulls the sorting rod 132, the rotating force of the second rotating plate 135 can accurately drive the sorting rod 132 to act, the sorting rod 132 rotates at a high speed under the driving of the connecting rod 133, and fully contacts and collides with materials during the rotation, so that the materials are sorted, active ingredients are separated from impurities, and the ejector rod 134 is arranged on one side of the sorting rod 132, so that the mixing and extraction effects on the materials can be enhanced, and active ingredients are more fully released.
Referring to fig. 1 to 8, the transmission structure 5 includes a bottom plate 52, a driving pump 53 is fixedly connected to one side of the inside of the bottom plate 52, and a spiral groove 51 is fixedly connected to one side of the driving pump 53.
It should be noted that, the bottom plate 52 provides a reliable supporting platform for the whole transmission component, the driving pump 53 is installed at one side of the inside of the bottom plate 52, the spiral groove 51 is closely connected with the driving pump 53, so that the concentrated solution can be guided to flow along a predetermined track, the solid and the liquid can be primarily separated in the flowing process, the impact force of the liquid can be effectively buffered, and the concentrated solution can be stably and efficiently conveyed to the next process.
Referring to fig. 1 to 8, a lifting rod 3 is fixedly connected to the outer side of a tank body 1, a placement frame 4 is fixedly arranged on the periphery of the top of the tank body 1, a v-shaped funnel ring 11 is fixedly connected to the bottom of the tank body 1, and a conveying pipe 6 is fixedly connected to the top of the v-shaped funnel ring 11.
It should be explained that, the lifting rod 3 on the outer side of the tank body 1 enables operators to carry and move the tank body easily by means of the lifting rod, so that equipment can be arranged flexibly between different production links or sites, the rack 4 on the periphery of the top of the tank body 1 can be used for placing auxiliary tools or small accessories, the V-shaped funnel ring 11 at the bottom of the tank body 1 can be used for rapidly converging concentrated liquid after solid-liquid separation to the center, liquid residues or flowing everywhere are avoided, and the conveying pipe 6 connected to the top of the V-shaped funnel ring is used for accurately and efficiently conveying the converged concentrated liquid to the next processing link.
Referring to fig. 1 to 8, a support column 7 is fixedly connected to the outer periphery of the bottom of the tank 1, a cylindrical column 10 is arranged on the outer periphery of the top of the tank 1, a placement frame 4 is fixedly arranged on the top of the cylindrical column 10, a base block 9 is fixedly arranged on one side of the placement frame 4, a screening structure 8 is fixedly connected to the top of the base block 9, and a rotating shaft 12 is fixedly arranged at the bottom of the base block 9.
It should be explained that, the support column 7 of the outer periphery of the bottom of the tank body 1 ensures that the equipment can not shake or deviate during operation, the cylindrical column 10 of the outer periphery of the top of the tank body 1 promotes the top strength of the tank body 1, the placement frame 4 at the top of the cylindrical column 10 can be used for classifying and placing auxiliary tools, the auxiliary tools are convenient for operators to take at any time, the base block 9 at one side of the placement frame 4 bears the screening structure 8, a stable installation platform is provided for the screening structure, meanwhile, the screening structure 8 can swing or rotate in a small amplitude by means of the connection of the bottom rotating shaft 12 with other parts of the equipment, and the rotating shaft 12 can flexibly adjust the angle.
The embodiment of the application relates to a natural active ingredient extraction process and an implementation principle of equipment, wherein the implementation principle is as follows:
Firstly, raw materials are pretreated through a stirring structure 2 at the top of a tank body 1, a first driver 25 drives a first stirring rod 23 and a movable stirring rod 26 to rotate so as to efficiently crush and uniformly mix plant branches and leaves, and meanwhile, a second driver 82 of a screening structure 8 drives a first rotating plate 81 to be matched with a screening disc 88, so that cell walls are further crushed through extrusion friction of a screening groove 812, and primary structural damage of the raw materials is completed.
Secondly, the locating rod 131 of the rotary structure 13 drives the second rotary plate 135 to rotate at a high speed with the sorting rod 132, the ejector rod 134 and the screening structure 8 are combined to carry out deep extraction, the compound stirring of the sorting rod 132 and the second stirring rod 87 improves the mixing uniformity, and the driving gear 86 dynamically adjusts the stirring intensity through the rotary frame 84 to adapt to the release requirements of the targeted components of different materials.
Finally, the driving pump 53 of the conveying structure 5 starts the conveying system of the spiral groove 51, and after concentrated solution is converged by the v-shaped funnel ring 11, the concentrated solution is subjected to preliminary separation of solid and liquid through the spiral groove 51, and enters the next working procedure along the conveying pipe 6. In order to improve the extraction efficiency, the device restarts the stirring structure 2 and the rotating structure 13, and the rotating frame 84 is utilized to accurately match the stirring intensity and the vortex intensity, so as to perform directional enrichment and purification on the targeted component, and finally complete the whole process extraction from raw material pretreatment to high-purity active component.
The above embodiments are not intended to limit the scope of the application, so that the equivalent changes of the structure, shape and principle of the application are covered by the scope of the application.