CN120094534B - A temperature-controlled vitamin H bromination reactor - Google Patents
A temperature-controlled vitamin H bromination reactorInfo
- Publication number
- CN120094534B CN120094534B CN202510261982.8A CN202510261982A CN120094534B CN 120094534 B CN120094534 B CN 120094534B CN 202510261982 A CN202510261982 A CN 202510261982A CN 120094534 B CN120094534 B CN 120094534B
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- China
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- wall
- fixedly connected
- reaction kettle
- outer side
- side wall
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention relates to the technical field of reaction kettles, in particular to a temperature control type vitamin H bromination reaction kettle which comprises a base, wherein the top end of the outer wall of the base is fixedly connected with a cylinder, the top end of the outer wall of the cylinder is rotationally connected with a reaction kettle body, the bottom end of the inner wall of the reaction kettle body is fixedly connected with a heating device, the bottom end of the outer wall of the reaction kettle body is provided with a discharging pipe, an electric control valve is arranged in the discharging pipe, and the top end of the outer wall of the reaction kettle body is provided with a feed inlet.
Description
Technical Field
The invention relates to the technical field of reaction kettles, in particular to a temperature control type vitamin H bromination treatment reaction kettle.
Background
Vitamin H, also known as biotin, is an important water-soluble vitamin which has wide application in the fields of pharmacy, health care products and the like after bromination, and because a reaction kettle is needed for bromination, the reaction kettle for bromination of vitamin H becomes one of the necessary equipment for bromination of vitamin H.
In the prior art, when the vitamin H is subjected to bromination treatment, the vitamin H is placed in a reaction kettle to be stirred and mixed with other medicaments, and then the reaction kettle is heated to a certain temperature to react, so that the existing vitamin H bromination treatment reaction kettle is used for simply stirring raw materials, so that the raw materials are easy to rotate simultaneously along with a stirring mechanism in the stirring and mixing process of the stirring mechanism, each raw material and the stirring mechanism are kept in a relatively static state, uneven raw material mixing is easy to cause, the efficiency of the vitamin H bromination mixing reaction is reduced, the energy consumption is increased, the cost of the vitamin H bromination reaction is increased, and the market competitiveness is reduced.
Disclosure of Invention
The invention aims to solve the problems that when vitamin H is subjected to bromination treatment, the vitamin H is placed in a reaction kettle to be stirred and mixed with other medicaments, and then heated to a certain temperature to react, and the conventional vitamin H bromination treatment reaction kettle is used for simply stirring raw materials, so that the raw materials are easy to rotate along with a stirring mechanism in the stirring and mixing process of the stirring mechanism, so that the raw materials and the stirring mechanism are kept in a relatively static state, uneven mixing of the raw materials is easy to cause, the efficiency of the vitamin H bromination mixing reaction is reduced, the energy consumption is increased, the cost of the vitamin H bromination reaction is increased, and the market competitiveness is reduced.
The aim of the invention can be achieved by the following technical scheme:
A temperature control type vitamin H bromination reaction kettle comprises a base; the top end of the outer wall of the base is fixedly connected with a cylinder, the top end of the outer wall of the cylinder is rotationally connected with a reaction kettle body, the bottom end of the inner wall of the reaction kettle body is fixedly connected with a heating device, the bottom end of the outer wall of the reaction kettle body is provided with a discharge pipe, an electric control valve is arranged in the discharge pipe, the top end of the outer wall of the reaction kettle body is provided with a feed inlet, the top end of the outer wall of the reaction kettle body is hinged with a sealing plate, the top end of the outer wall of the base is fixedly connected with a support column which is U-shaped, the top end of the inner wall of the support column is fixedly connected with a motor, the output end of the motor is provided with a rotating shaft, the bottom end of the outer wall of the rotating shaft extends into the reaction kettle body, one end outer side wall of the rotating shaft is provided with an annular column, the outer side wall of the rotating shaft is provided with a group of stirring plates, the outer side wall of the reaction kettle body is fixedly connected with an annular rack I, the inner wall top end of the support column is rotationally connected with a rotating rod, the bottom end of the outer wall of the rotating rod is fixedly connected with a first gear, the first gear is meshed with the annular rack I, the rotating rod and the outer side wall of the rotating rod is fixedly connected with a first sprocket I is connected with the first I through a chain I.
The reaction kettle body comprises a round shell and a cover plate, wherein the bottom end of the outer wall of the cover plate is connected to the top end of the outer wall of the round shell in a sealing and rotating mode, a connecting column is fixedly connected to the top end of the outer wall of the cover plate, the top end of the outer wall of the connecting column is fixedly connected to the top end of the inner wall of a supporting column, an annular rack II is fixedly connected to the bottom end of the outer wall of the cover plate, a pair of first reciprocating rotating rods are rotatably connected to the bottom end of the inner wall of the round shell, cleaning plates are arranged on the outer side walls of the first reciprocating rotating rods, the outer side walls of the cleaning plates are in contact with the inner side walls of the round shell, gears II are fixedly connected to the top ends of the outer walls of the first reciprocating rotating rods, and the gears II are meshed with the annular rack II.
As a preferable implementation mode, the outer side wall of the first reciprocating rotating rod is connected with a third gear in a sliding mode, the top end of the outer wall of the third gear is connected to the bottom end of the outer wall of the cleaning plate in a rotating mode, the bottom end of the outer wall of the cleaning plate is connected with an auxiliary plate in a ring-shaped mode, the inner side wall of the auxiliary plate is fixedly connected with a third annular rack, the third annular rack is meshed with the third gear, and a plurality of groups of bristles are arranged on the outer side wall of the auxiliary plate through a group of connecting rods.
As a preferable implementation mode of the invention, one end of the outer wall of the connecting rod is rotatably connected to the outer side wall of the auxiliary plate, a plurality of groups of bristles are fixedly connected to one end of the outer wall of one group of connecting rods respectively, an annular rack IV is fixedly connected to the bottom end of the outer wall of the cleaning plate, gears IV are fixedly connected to the outer side wall of the connecting rod, and the gears IV are meshed with the annular rack IV.
As a preferable implementation mode of the invention, the outer side wall of the auxiliary plate is rotationally connected with a group of reciprocating rotating rods II, cleaning blocks are respectively arranged on the outer side wall of the group of reciprocating rotating rods II and are respectively matched with a plurality of groups of bristles, a group of guide rods are fixedly connected with the outer side wall of the auxiliary plate and respectively penetrate through the group of cleaning blocks, the group of guide rods are respectively connected with the group of cleaning blocks in a sliding manner, gears five are respectively fixedly connected with the outer side wall of the group of reciprocating rotating rods II, and the gears five are mutually meshed with the annular racks.
As a preferable implementation mode of the invention, the top end of the outer wall of the cleaning plate is in threaded connection with a threaded rod, the bottom end of the outer wall of the threaded rod penetrates through the cleaning plate, the bottom end of the outer wall of the threaded rod is in rotary connection with a sealing shell, the outer side wall of the sealing shell is in contact with the inner side wall of the round shell, the sealing shell is matched with the auxiliary plate and bristles, and a sealing space is formed between the sealing shell and the auxiliary plate.
The invention is characterized in that the inner side wall of the annular column is in sliding connection with the outer side wall of the rotating shaft, the outer side wall of the rotating shaft is rotationally connected with a third reciprocating rotating rod through a first square plate, the bottom end of the outer wall of the third reciprocating rotating rod penetrates through the annular column and is matched with the annular column, a gear six is fixedly connected to the top end of the outer wall of the third reciprocating rotating rod, an annular rack six is fixedly connected to the bottom end of the outer wall of the cover plate, and the annular rack six is meshed with the gear six.
The stirring plate comprises a fixing seat and stirring blades, one end of the outer wall of the fixing seat is fixedly connected to the outer side wall of an annular column, the top end and the bottom end of the outer wall of the fixing seat are respectively provided with a placing groove, one side of the inner wall of each placing groove is provided with a threaded groove, the outer side walls of the stirring blades are respectively and slidably placed on the inner side walls of the placing grooves, one end of the outer wall of each stirring blade is connected with a bolt in a threaded manner, the bolts penetrate through the stirring blades, and the bolts are matched with the threaded grooves.
As a preferred implementation mode of the invention, the outer side wall of the cylinder is fixedly connected with a cooling shell, the reaction kettle body is positioned in the cooling shell, the bottom end of the outer side wall of the cooling shell is fixedly connected with a water outlet pipe which is communicated with the cooling shell, and a valve is arranged in the water outlet pipe.
As a preferable implementation mode of the invention, the bottom end of the inner wall of the cooling shell is rotatably connected with a group of round rods, the top ends of the outer walls of the group of round rods are fixedly connected with gears nine, the group of gears nine are mutually meshed with the annular rack I, and the outer side walls of the round rods are fixedly connected with a group of rotating plates.
Compared with the prior art, the invention has the beneficial effects that:
1. When the auxiliary plate rotates, the auxiliary plate drives the reciprocating rotating rod II and the gear five on the reciprocating rotating rod II to rotate, and the gear five is meshed with the annular rack four, and the annular rack four does not rotate, so that the gear five rotates through the annular rack four, the reciprocating rotating rod II is driven to rotate, the reciprocating rotating rod is driven to rotate, the cleaning block is driven to reciprocate, the cleaning block is used for cleaning bristles, residues are not easy to adhere to the bristles, the bristles cannot clean the reaction kettle body more, and the reaction kettle body is dirty more, so that the cleanliness of the bristles is guaranteed.
2. Through connecting rod, brush hair along with the accessory plate when rotating, gear four on the connecting rod is followed and is rotated, because of gear four and four intermeshing of annular rack, and annular rack is four not rotated, makes gear four through four autorotations of annular rack to drive connecting rod and brush hair and rotate, increase the clearance effect to the reation kettle body when making the brush hair rotate, make this device's clearance effect better.
Drawings
The present invention is further described below with reference to the accompanying drawings for the convenience of understanding by those skilled in the art.
FIG. 1 is a main block diagram of the present invention;
FIG. 2 is a partial block diagram of the body of the present invention;
FIG. 3 is an exploded view of the reaction vessel of the present invention with an agitator plate, a heating device and a second annular rack;
FIG. 4 is a block diagram of the stirring plate, cleaning plate, seal housing and annular rack II of the present invention;
FIG. 5 is a block diagram of a motor, rotating shaft, annular post, stirring plate and reciprocating rotary rod of the present invention;
FIG. 6 is an exploded view of the mounting base and stirring blade of the present invention;
FIG. 7 is an exploded view of the seal housing and the purge plate and auxiliary plate of the present invention;
FIG. 8 is an exploded view of the cleaning block and bristles of the present invention;
FIG. 9 is a block diagram of a cooling shell, outlet pipe, rotating plate and annular rack I of the present invention;
1, a base, 2, a cylinder, 3, a reaction kettle body, 4, a heating device, 5, a discharging pipe, 6, a feeding hole, 7, a sealing plate, 8, a support column, 9, a motor, 10, a rotating shaft, 11, a ring column, 12, a stirring plate, 13, a ring rack I, 14, a rotating rod, 15, a first gear, 16, a sprocket I, 17, a chain I, 301, a round shell, 302, a cover plate, 18, a connecting column, 19, a ring rack II, 20, a reciprocating rotating rod I, 21, a cleaning plate, 22, a gear II, 23, a gear III, 24, an auxiliary plate, 25, a ring rack III, 26, a connecting rod, 27, bristles, 28, a ring rack IV, 29, a gear IV, 30, a reciprocating rotating rod II, 31, a cleaning block, 32, a guide rod, 33, a gear V, 34, 35, a sealing shell, 36, a reciprocating rotating rod III, 37, a gear V, 38, a ring V, 121, a fixing seat, 122, a stirring blade, 39, a placing groove, 40, a screw groove, 41, 42, a cooling shell, 43, a water outlet pipe, a rotating rod, 45, a round rack 46.
Detailed Description
The technical solutions of the present invention will be clearly and completely described in connection with the embodiments, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1
Referring to fig. 1-8, a temperature-controlled vitamin H bromination reaction kettle comprises a base 1; the top end of the outer wall of the base 1 is fixedly connected with a cylinder 2; the top end of the outer wall of the cylinder 2 is rotationally connected with a reaction kettle body 3; the bottom end of the inner wall of the reaction kettle body 3 is fixedly connected with a heating device 4, the bottom end of the outer wall of the reaction kettle body 3 is provided with a discharging pipe 5, an electric control valve is arranged in the discharging pipe 5, the top end of the outer wall of the reaction kettle body 3 is provided with a feeding hole 6, the top end of the outer wall of the reaction kettle body 3 is hinged with a sealing plate 7, the top end of the outer wall of a base 1 is fixedly connected with a supporting column 8, the supporting column 8 is U-shaped, the top end of the inner wall of the supporting column 8 is fixedly connected with a motor 9, the output end of the motor 9 is provided with a rotating shaft 10, the bottom end of the outer wall of the rotating shaft 10 extends into the reaction kettle body 3, the outer side wall of the rotating shaft 10 is provided with an annular column 11, the outer side wall of the annular column 11 is provided with a group of stirring plates 12, the outer side wall of the reaction kettle body 3 is fixedly connected with an annular rack 13, the inner wall top end of the supporting column 8 is rotatably connected with a rotating rod 14, the outer wall bottom end of the rotating rod 14 is fixedly connected with a first gear 15, the first gear 15 is meshed with the annular rack 13, the rotating rod 14 and the outer side walls of the rotating rod 10 are fixedly connected with a chain wheel 16, the pair of the chain 16 is connected with the rotating shaft 17, when the rotating shaft 10 is driven by the motor 6 to rotate the rotating shaft 10, the stirring plate 10 is driven by the rotating shaft 10, and the stirring plate 10, when the rotating shaft 10 is driven by the rotating shaft 10, and the rotating shaft 10, and the stirring plate 10 is driven by the rotating shaft 10, and the rotating device 10 and the rotating device 10 and the rotating device through the rotating shaft 11, the rotating rod 14 is enabled to drive the first gear 15 to rotate, the first gear 15 is enabled to drive the annular rack I13 and the reaction kettle body 3 to rotate, and the rotation direction of the reaction kettle body 3 is opposite to that of the stirring plate 12.
One end of the outer wall of the connecting rod 26 is rotationally connected to the outer side wall of the auxiliary plate 24, a plurality of groups of bristles 27 are fixedly connected to one end of the outer wall of the connecting rod 26 respectively, an annular rack four 28 is fixedly connected to the bottom end of the outer wall of the cleaning plate 21, a gear four 29 is fixedly connected to the outer side wall of the connecting rod 26, the gears four 29 are meshed with the annular rack four 28, when the connecting rod 26 and the bristles 27 rotate along with the auxiliary plate 24, the gears four 29 on the connecting rod 26 rotate, and the gears four 29 are meshed with the annular rack four 28, the annular rack four 28 does not rotate, so that the gears four 29 rotate through the annular rack four 28, the connecting rod 26 and the bristles 27 are driven to rotate, the cleaning effect on the reaction kettle body 3 is improved when the bristles 27 rotate, and the cleaning effect of the device is better.
The reaction kettle body 3 comprises a round shell 301 and a cover plate 302, the bottom end of the outer wall of the cover plate 302 is connected to the top end of the outer wall of the round shell 301 in a sealing and rotating mode, a connecting column 18 is fixedly connected to the top end of the outer wall of the cover plate 302, the top end of the outer wall of the connecting column 18 is fixedly connected to the top end of the inner wall of the supporting column 8, an annular rack II 19 is fixedly connected to the bottom end of the outer wall of the cover plate 302, a pair of first reciprocating rotating rods 20 are rotatably connected to the bottom end of the inner wall of the round shell 301, a cleaning plate 21 is arranged on the outer side wall of the first reciprocating rotating rods 20, the outer side walls of the cleaning plate 21 are in contact with the inner side walls of the round shell 301, a gear II 22 is fixedly connected to the top end of the outer wall of the first reciprocating rotating rods 20, the first reciprocating rotating rods 20 are meshed with the annular rack II 19, the first reciprocating rotating rods 22 are meshed with the annular rack II 19 respectively, the first reciprocating rotating rods 2 are meshed with the annular rack II 19 respectively, the top end of the outer wall of the cover plate 302 is connected to the top end of the outer wall of the round shell 301 in a sealing and rotating mode, the top end of the outer wall of the cover plate 302 is connected to the top end of the outer wall of the round shell 301 in a sealing and the top end of the outer wall of the round shell 301, when the round shell 301 rotates, the first reciprocating rods 20 is not rotating, the first reciprocating rods 20 and second reciprocating rotating, the first reciprocating rods 20 and second rotating round rods 20 and second rotating, the cleaning rods 20 are.
The outer side wall of the auxiliary plate 24 is rotationally connected with a group of reciprocating rotating rods II 30, the outer side walls of the group of reciprocating rotating rods II 30 are respectively provided with cleaning blocks 31, the group of cleaning blocks 31 are respectively matched with a plurality of groups of bristles 27, the outer side wall of the auxiliary plate 24 is fixedly connected with a group of guide rods 32, the group of guide rods 32 respectively penetrate through the group of cleaning blocks 31, the group of guide rods 32 are respectively in sliding connection with the group of cleaning blocks 31, the outer side walls of the group of reciprocating rotating rods II 30 are respectively fixedly connected with a gear five 33, the group of gears five 33 are mutually meshed with a ring-shaped rack IV 28, when the auxiliary plate 24 rotates, the auxiliary plate 24 drives the reciprocating rotating rods II 30 and the gear five 33 on the reciprocating rotating rods II 30 to rotate, the ring-shaped rack IV 28 does not rotate, the gear five 33 rotates through the ring-shaped rack IV 28, the reciprocating rotating rods II 30 rotate, the reciprocating rotating rods 31 drive the rotating rods III, the cleaning blocks 31 reciprocate the cleaning blocks 27, residues are not easy to adhere to the cleaning blocks 27, and the bristles 3 do not pass through the cleaning blocks 27, and the cleaning blocks 3 can not rotate the cleaning blocks 32, and the bristles 32 can only clean the bristles 32, but also can not rotate the cleaning blocks 32 due to the fact that the bristles are clean the cleaning blocks 3 and the bristles are not clean the cleaning blocks.
The outer side wall of the first reciprocating rotating rod 20 is slidably connected with a third gear 23, the top end of the outer wall of the third gear 23 is rotatably connected to the bottom end of the outer wall of the cleaning plate 21, the bottom end of the outer wall of the cleaning plate 21 is rotatably connected with an auxiliary plate 24, the auxiliary plate 24 is in a ring shape, the inner side wall of the auxiliary plate 24 is fixedly connected with a third ring-shaped rack 25, the third ring-shaped rack 25 is meshed with a pair of the third gears 23, a plurality of groups of bristles 27 are arranged on the outer side wall of the auxiliary plate 24 through a group of connecting rods 26, when the cleaning plate 21 reciprocates, the third gear 23 is slidably connected to the outer side wall of the first reciprocating rotating rod 20, the top end of the outer wall of the third gear 23 is rotatably connected to the bottom end of the outer wall of the cleaning plate 21, the first reciprocating rotating rod 20 drives the third gear 23 to rotate, the upper and lower reciprocating motion of the third gear 23 drives the third gear 23 to move up and down, the third gear 23 is rotated, the rotation of the third gear 23 is driven to move, the third gear 23 is meshed with the third ring-shaped rack 25, the rotation of the third gear 23 is driven by the rotation of the third gear 23 and the third ring-shaped rack 25, the third ring-shaped rack 25 is driven to rotate the auxiliary plate 24, the third connecting rods 26 and the bristles 27 are driven to rotate, the third ring-shaped rack 3, and the upper and lower end of the bristles 27 are driven to rotate, and the upper and lower end of the ring-shaped rack 23 is further driven to rotate, and the third gear 23 and the upper and lower end of the ring-shaped rack 23 is always driven to move 3 and the upper and lower end and the lower end to and the lower end 23.
The inner side wall of the annular column 11 is in sliding connection with the outer side wall of the rotating shaft 10, the outer side wall of the rotating shaft 10 is rotationally connected with a reciprocating rotating rod III 36 through a first square plate, the bottom end of the outer wall of the reciprocating rotating rod III 36 penetrates through the annular column 11, the reciprocating rotating rod III 36 is matched with the annular column 11, the top end of the outer wall of the reciprocating rotating rod III 36 is fixedly connected with a gear VI 37, the bottom end of the outer wall of the cover plate 302 is fixedly connected with an annular rack VI 38, the annular rack VI 38 is meshed with the gear VI 37, when the rotating shaft 10 drives the annular column 11 and the stirring plate 12 to rotate, the rotating shaft 10 drives the reciprocating rotating rod III 36 to rotate through the first square plate, the reciprocating rotating rod III 36 drives the gear VI 37 to rotate, and the cover plate 302 and the annular rack VI 38 are meshed with the annular rack VI, the gear VI rotates through the annular rack VI 38 when the gear VI rotates, the reciprocating rotating rod III 36 drives the annular column 11 and the stirring plate 12 to move up and down, the stirring range of the stirring plate 12 is increased, the stirring mode of the device is more flexible, the vitamin H bromination reaction efficiency is improved, and the bromination reaction efficiency is improved.
The stirring plate 12 comprises a fixed seat 121 and stirring blades 122, one end of the outer wall of the fixed seat 121 is fixedly connected to the outer side wall of the annular column 11, the top end and the bottom end of the outer wall of the fixed seat 121 are respectively provided with a placing groove 39, one side of the inner wall of the pair of placing grooves 39 is respectively provided with a threaded groove 40, the outer side walls of the pair of stirring blades 122 are respectively and slidably placed on the inner side walls of the pair of placing grooves 39, one end of the outer wall of the pair of stirring blades 122 is respectively in threaded connection with a bolt 41, the pair of bolts 41 penetrate through the pair of stirring blades 122, the pair of bolts 41 are respectively matched with the pair of threaded grooves 40, and the stirring plate 12 comprises the fixed seat 121 and the stirring blades 122.
The top end of the outer wall of the cleaning plate 21 is in threaded connection with a threaded rod 34, the bottom end of the outer wall of the threaded rod 34 penetrates through the cleaning plate 21, the bottom end of the outer wall of the threaded rod 34 is rotationally connected with a sealing shell 35, the outer side wall of the sealing shell 35 is in contact with the inner side wall of the round shell 301, the sealing shell 35 is matched with the auxiliary plate 24 and forms a sealing space with bristles 27, the threaded rod 34 is rotationally connected with the cleaning plate 21, the threaded rod 34 drives the threaded rod 34 to move up and down due to the threaded rod 34 being in threaded connection with the threaded rod 21, the threaded rod 34 drives the sealing shell 35 to move up and down, when bristles 27 are not needed to clean, the sealing shell 35 is rotated to move up through the threaded rod 34, at the moment, the sealing shell 35 and the auxiliary plate 24 form a sealing space, raw materials are not easy to adhere to the bristles 27 when mixed, and therefore raw material waste is reduced, when the reaction kettle body 3 needs cleaning, the inner side wall of the reaction kettle body 3 is reversely rotated, the sealing space is opened, the bristles 27 are enabled to clean the inner side wall of the reaction kettle body 3, and the cleaning efficiency of the reaction kettle body 3 is accelerated.
Example 2
Referring to fig. 1 and 9, a cooling shell 42 is fixedly connected to the outer side wall of the cylinder 2, the reaction kettle body 3 is located in the cooling shell 42, a water outlet pipe 43 is fixedly connected to the bottom end of the outer side wall of the cooling shell 42, the water outlet pipe 43 is communicated with the cooling shell 42, a valve is arranged in the water outlet pipe 43, when the bromination and mixing reaction of vitamin H is completed, the heating device 4 is closed at the moment, then water is poured into the cooling shell 42, the water in the cooling shell 42 absorbs heat in the reaction kettle body 3, the raw materials are cooled, after the temperature in the reaction kettle body 3 is reduced to a certain degree, the stirring motor 9 is stopped, then an electric control valve at the discharge pipe 5 is opened, and the brominated vitamin H is taken out.
The inner wall bottom end of the cooling shell 42 is rotationally connected with a group of round rods 44, the top ends of the outer walls of the group of round rods 44 are fixedly connected with gears nine 45, the group of gears nine 45 are meshed with the annular rack I13, the outer side wall of the round rod 44 is fixedly connected with a group of rotating plates 46, when water in the cooling shell 42 absorbs heat in the reaction kettle body 3, the annular rack I13 and the round shell 301 are meshed with the group of gears nine 45 through rotation of the annular rack I13, the annular rack I13 rotates to drive the group of gears nine 45 and the round rod 44 to rotate, the round rod 44 drives the rotating plates 46 to rotate, the rotating plates 46 stir the water in the cooling shell 42, heat dissipation is carried out on water faster, waste of water resources is reduced, the water can be rapidly dissipated, the heat in the reaction kettle body 3 is absorbed, and therefore the vitamin H bromination mixing reaction efficiency is further improved.
When the device is used, raw materials are placed into the reaction kettle body 3 from the feed inlet 6, then the sealing plate 7 is closed, at the moment, the motor 9 drives the rotating shaft 10 to rotate, so that the rotating shaft 10 drives the annular column 11 and the stirring plate 12 to rotate, raw materials are stirred, the heating device 4 heats the raw materials during stirring, the raw materials are subjected to mixed reaction, when the rotating shaft 10 rotates, the rotating shaft 10 drives the rotating rod 14 to rotate through the first chain wheel 16 and the first chain 17, the rotating rod 14 drives the first gear 15 to rotate, the first gear 15 drives the annular rack 13 and the reaction kettle body 3 to rotate, and the rotating direction of the reaction kettle body 3 is opposite to the rotating direction of the stirring plate 12.
When the rotating shaft 10 drives the annular column 11 and the stirring plate 12 to rotate, the rotation of the rotating shaft 10 drives the reciprocating rotating rod III 36 to rotate through the first square plate, so that the reciprocating rotating rod III 36 drives the gear six 37 to rotate, the gear six 37 and the annular rack six 38 are meshed with each other, the reaction kettle body 3 comprises a round shell 301 and a cover plate 302, the cover plate 302 and the annular rack six 38 are in a fixed state, the gear six 37 rotates through the annular rack six 38 when rotating, and accordingly the reciprocating rotating rod III 36 is driven to rotate, the reciprocating rotating rod III 36 drives the annular column 11 and the stirring plate 12 to move up and down, the stirring range of the stirring plate 12 is increased, and the stirring mode of the device is more flexible and various, so that the efficiency and the effect of vitamin H bromination mixing reaction are improved.
Because stirring board 12 includes fixing base 121 and stirring leaf 122, make this device need change when suitable stirring leaf 122 according to the mixing demand, through rotating bolt 41, make bolt 41 shift out thread groove 40, fixing base 121 and stirring leaf are removed fixedly this moment, take stirring leaf 122 this moment, install suitable stirring leaf 122 again, make this device can change suitable stirring leaf 122 according to different demands and circumstances, thereby make the stirring efficiency and the stirring effect of this device further promote, also make this device more nimble, and suitable stirring leaf 122 has not only improved stirring efficiency, also reduced the consumption of the energy, and stirring leaf 122 damage need change or when maintaining, also more convenient, swift.
When the bromination of vitamin H is completed, the heating device 4 is closed, then water is poured into the cooling shell 42, so that the water in the cooling shell 42 absorbs the heat in the reaction kettle body 3, the raw materials are cooled, after the temperature in the reaction kettle body 3 is reduced to a certain degree, the stirring motor 9 is stopped, then the electric control valve at the discharging pipe 5 is opened, and the brominated vitamin H is taken out.
When the water absorbs the heat in the reaction kettle body 3 in the cooling shell 42, the annular rack 13 and the round shell 301 are mutually meshed, so that the annular rack 13 rotates to drive the round rod 44 and the round rod 44 to rotate, the round rod 44 drives the rotating plate 46 to rotate, the rotating plate 46 agitates the water in the cooling shell 42, the water dissipates heat faster, the waste of water resources is reduced, the water can dissipate heat quickly, the heat in the reaction kettle body 3 is absorbed, and the bromination reaction efficiency of the vitamin H is further improved.
When the brominated vitamin H is taken out and cleaned in the reaction kettle, the first reciprocating rotating rod 20 rotates through the rotation of the round shell 301, so that the first reciprocating rotating rod 20 drives the second gear 22 to rotate, the second gear 22 is meshed with the second annular rack 19 and the second annular rack 19 is in a fixed state, the second gear 22 rotates through the second annular rack 19, the second gear 22 drives the first reciprocating rotating rod 20 to rotate, the first reciprocating rotating rod 20 drives the cleaning plate 21 to reciprocate up and down, the inner side wall of the reaction kettle body 3 is cleaned, the cleaning of the reaction kettle body 3 is more convenient and quicker, and raw materials are not easy to adhere to the inner side wall of the reaction kettle body 3 during the bromination mixing reaction of the vitamin H through the up and down movement of the cleaning plate 21, and the waste of the raw materials is reduced.
When the cleaning plate 21 reciprocates, the outer side wall of the first reciprocating rotating rod 20 is slidably connected with the third gear 23, the top end of the outer wall of the third gear 23 is rotationally connected to the bottom end of the outer wall of the cleaning plate 21, so that the first reciprocating rotating rod 20 rotates to drive the third gear 23 to rotate, and the cleaning plate 21 reciprocates up and down to drive the third gear 23 to move while rotating, and the third gear 23 and the third annular rack 25 are meshed with each other, so that the rotation of the third gear 23 drives the third annular rack 25 to rotate, the third annular rack 25 drives the auxiliary plate 24 to rotate, the auxiliary plate 24 drives the connecting rod 26 and the bristles 27 to rotate, the bristles 27 clean the inner side wall of the reaction kettle body 3, so that the cleaning efficiency and the cleaning effect of the reaction kettle body 3 are further improved, and the third gear 23 and the third annular rack 25 always keep a meshed state through the up and down movement of the third annular rack 25.
When the connecting rod 26 and the brush hair 27 rotate along with the auxiliary plate 24, the gear IV 29 on the connecting rod 26 rotates along with the rotation, and the gear IV 29 is meshed with the annular rack IV 28, and the annular rack IV 28 does not rotate, so that the gear IV 29 rotates through the annular rack IV 28, the connecting rod 26 and the brush hair 27 are driven to rotate, the cleaning effect on the reaction kettle body 3 is increased when the brush hair 27 rotates, and the cleaning effect of the device is better.
When the auxiliary plate 24 rotates, the auxiliary plate 24 drives the second reciprocating rotating rod 30 and the fifth gear 33 on the second reciprocating rotating rod 30 to rotate, and the fifth gear 33 is meshed with the fourth annular rack 28, and the fourth annular rack 28 does not rotate, so that the fifth gear 33 rotates through the fourth annular rack 28, the second reciprocating rotating rod 30 is driven to rotate, the cleaning block 31 is driven to reciprocate by the rotation of the second reciprocating rotating rod, the cleaning block 31 cleans the bristles 27, residues are not easy to adhere to the bristles 27, the bristles 27 cannot clean the reaction kettle body 3 more, the reaction kettle body 3 is dirty more, and cleanliness of the bristles 27 is guaranteed.
Through rotating threaded rod 34, because of threaded rod 34 and clearance board 21 threaded connection, the rotation that makes threaded rod 34 drive threaded rod 34 reciprocates, make threaded rod 34 drive seal shell 35 reciprocate, when making not needing brush hair 27 to clear up, make seal shell 35 reciprocate through rotating threaded rod 34, make seal shell 35 and accessory plate 24 form sealed space this moment, when making the raw materials mix, be difficult for the adhesion on brush hair 27, thereby the waste of raw materials has been reduced, when the reactor body 3 needs the clearance, reverse threaded rod 34, open sealed space, make brush hair 27 clear up the inside wall of reactor body 3, accelerate the clearance efficiency of reactor body 3, make this device more nimble, conveniently.
The preferred embodiments of the invention disclosed above are intended only to assist in the explanation of the invention. The preferred embodiments are not intended to be exhaustive or to limit the invention to the precise form disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best understand and utilize the invention. The invention is limited only by the claims and the full scope and equivalents thereof.
Claims (6)
1. A temperature-control type vitamin H bromination reaction kettle comprises a base (1), wherein a column (2) is fixedly connected to the top end of the outer wall of the base (1), a reaction kettle body (3) is rotatably connected to the top end of the outer wall of the column (2), a heating device (4) is fixedly connected to the bottom end of the inner wall of the reaction kettle body (3), a discharging pipe (5) is arranged at the bottom end of the outer wall of the reaction kettle body (3), an electric control valve is arranged in the discharging pipe (5), a feed inlet (6) is formed in the top end of the outer wall of the reaction kettle body (3), a sealing plate (7) is hinged to the top end of the outer wall of the reaction kettle body (3), a supporting column (8) is fixedly connected to the top end of the outer wall of the base (1), a motor (9) is fixedly connected to the top end of the inner wall of the supporting column (8), a rotating shaft (10) is arranged at the output end of the motor (9), the outer bottom end of the rotating shaft (10) extends into the reaction kettle body (3), an annular column (11) is arranged on the outer side wall of one end of the rotating shaft (10) in the reaction kettle body (3), a set of annular column (11) is arranged on the outer side wall of the reaction kettle (12), the reaction kettle comprises a reaction kettle body (3), a first annular rack (13), a rotating rod (14), a first gear (15), a first sprocket (16), a first chain wheel (17) and a second sprocket (16), wherein the annular rack (13) is fixedly connected to the outer side wall of the reaction kettle body (3), the top end of the inner wall of a supporting column (8) is rotatably connected with the rotating rod, the bottom end of the outer wall of the rotating rod (14) is fixedly connected with the first gear (15), the first gear (15) is meshed with the first annular rack (13), the rotating rod (14) and the outer side wall of a rotating shaft (10) are fixedly connected with the first chain wheel (16), and the first chain wheel (16) is connected through the first chain (17);
The reaction kettle body (3) comprises a round shell (301) and a cover plate (302), wherein the bottom end of the outer wall of the cover plate (302) is connected to the top end of the outer wall of the round shell (301) in a sealing and rotating mode, a connecting column (18) is fixedly connected to the top end of the outer wall of the cover plate (302), the top end of the outer wall of the connecting column (18) is fixedly connected to the top end of the inner wall of a supporting column (8), an annular rack II (19) is fixedly connected to the bottom end of the outer wall of the cover plate (302), a pair of first reciprocating rotating rods (20) are rotatably connected to the bottom end of the inner wall of the round shell (301), annular cleaning plates (21) are arranged on the outer side walls of the first reciprocating rotating rods (20), the outer side walls of the cleaning plates (21) are in contact with the inner side walls of the round shell (301), two gears (22) are fixedly connected to the top ends of the outer walls of the first reciprocating rotating rods (20), and the two gears (22) are meshed with the annular rack II (19) respectively;
The outer side wall of the reciprocating rotating rod I (20) is slidably connected with a gear III (23), the top end of the outer wall of the gear III (23) is rotatably connected to the bottom end of the outer wall of the cleaning plate (21), the bottom end of the outer wall of the cleaning plate (21) is rotatably connected with an auxiliary plate (24), the auxiliary plate (24) is in an annular shape, the inner side wall of the auxiliary plate (24) is fixedly connected with an annular rack III (25), the annular rack III (25) is meshed with a pair of gears III (23), and the outer side wall of the auxiliary plate (24) is provided with a plurality of groups of bristles (27) through a group of connecting rods (26);
One end of the outer wall of the connecting rod (26) is rotationally connected to the outer side wall of the auxiliary plate (24), a plurality of groups of bristles (27) are fixedly connected to the other end of the outer wall of one group of connecting rods (26) respectively, an annular rack IV (28) is fixedly connected to the bottom end of the outer wall of the cleaning plate (21), a gear IV (29) is fixedly connected to the outer side wall of the connecting rod (26), and the gears IV (29) are meshed with the annular rack IV (28) mutually;
The outer side wall of the auxiliary plate (24) is rotationally connected with a group of second reciprocating rotating rods (30), the outer side walls of the group of second reciprocating rotating rods (30) are respectively provided with cleaning blocks (31), the group of cleaning blocks (31) are respectively matched with a plurality of groups of bristles (27), the outer side wall of the auxiliary plate (24) is fixedly connected with a group of guide rods (32), the group of guide rods (32) respectively penetrate through the group of cleaning blocks (31), the group of guide rods (32) are respectively connected with the group of cleaning blocks (31) in a sliding mode, the outer side walls of the group of second reciprocating rotating rods (30) are respectively fixedly connected with a gear five (33), and the group of gears five (33) are mutually meshed with the annular rack four (28).
2. The temperature-controlled vitamin H bromination reaction kettle according to claim 1, wherein a threaded rod (34) is connected to the top end of the outer wall of the cleaning plate (21) in a threaded manner, the bottom end of the outer wall of the threaded rod (34) penetrates through the cleaning plate (21), a sealing shell (35) is rotatably connected to the bottom end of the outer wall of the threaded rod (34), the outer side wall of the sealing shell (35) is in contact with the inner side wall of the round shell (301), the sealing shell (35) is matched with the auxiliary plate (24) and bristles (27), and the sealing shell (35) and the auxiliary plate (24) form a sealing space.
3. The temperature-controlled vitamin H bromination reaction kettle is characterized in that the inner side wall of the annular column (11) is in sliding connection with the outer side wall of the rotating shaft (10), the outer side wall of the rotating shaft (10) is rotatably connected with a reciprocating rotary rod III (36) through a first square plate, the bottom end of the outer wall of the reciprocating rotary rod III (36) penetrates through the annular column (11) and is matched with the annular column (11), a gear VI (37) is fixedly connected to the top end of the outer wall of the reciprocating rotary rod III (36), an annular rack VI (38) is fixedly connected to the bottom end of the outer wall of the cover plate (302), and the annular rack VI (38) is meshed with the gear VI (37).
4. The temperature-controlled vitamin H bromination reaction kettle as claimed in claim 1, wherein the stirring plate (12) comprises a fixing seat (121) and stirring blades (122), one end of the outer wall of the fixing seat (121) is fixedly connected to the outer side wall of the annular column (11), the top end and the bottom end of the outer wall of the fixing seat (121) are respectively provided with a placing groove (39), one side of the inner wall of each placing groove (39) is respectively provided with a threaded groove (40), the outer side walls of the stirring blades (122) are respectively placed on the inner side walls of the placing grooves (39) in a sliding mode, one end of the outer wall of each stirring blade (122) is respectively connected with a bolt (41) in a threaded mode, the pair of bolts (41) penetrate through the stirring blades (122) respectively, and the pair of bolts (41) are respectively matched with the pair of threaded grooves (40).
5. The temperature-controlled vitamin H bromination reaction kettle disclosed by claim 1 is characterized in that a cooling shell (42) is fixedly connected to the outer side wall of a cylinder (2), a reaction kettle body (3) is positioned in the cooling shell (42), a water outlet pipe (43) is fixedly connected to the bottom end of the outer side wall of the cooling shell (42), the water outlet pipe (43) is communicated with the cooling shell (42), and a valve is arranged in the water outlet pipe (43).
6. The temperature-controlled vitamin H bromination reaction kettle is characterized in that a group of round rods (44) are rotatably connected to the bottom end of the inner wall of the cooling shell (42), gears nine (45) are fixedly connected to the top ends of the outer walls of the round rods (44), the gears nine (45) are meshed with the annular racks one (13), and a group of rotating plates (46) are fixedly connected to the outer side walls of the round rods (44).
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| CN202510261982.8A CN120094534B (en) | 2025-03-06 | 2025-03-06 | A temperature-controlled vitamin H bromination reactor |
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| CN202510261982.8A CN120094534B (en) | 2025-03-06 | 2025-03-06 | A temperature-controlled vitamin H bromination reactor |
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| CN112108474A (en) * | 2020-09-27 | 2020-12-22 | 张学梅 | Automatic high-efficient cleaning equipment of lubricating oil settling cask |
| CN118122241A (en) * | 2024-05-07 | 2024-06-04 | 山东欧迈机械股份有限公司 | Reaction kettle capable of preventing materials from adhering and application method |
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| CN217068838U (en) * | 2022-03-25 | 2022-07-29 | 开原化工机械容器有限公司 | Reation kettle for chemical production convenient to clean inner wall |
| CN221956850U (en) * | 2024-03-19 | 2024-11-05 | 华电新疆五彩湾北一发电有限公司 | Pressure water delivery tank |
| CN222287326U (en) * | 2024-12-04 | 2025-01-03 | 淄博新农基作物科学有限公司 | Micao smoke water aqua synthesis reaction kettle |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112108474A (en) * | 2020-09-27 | 2020-12-22 | 张学梅 | Automatic high-efficient cleaning equipment of lubricating oil settling cask |
| CN118122241A (en) * | 2024-05-07 | 2024-06-04 | 山东欧迈机械股份有限公司 | Reaction kettle capable of preventing materials from adhering and application method |
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