Disclosure of Invention
The invention aims to provide a preparation process of an antibacterial blended yarn, which aims to solve the problems in the background technology.
In order to achieve the aim, the invention provides the following technical scheme that the preparation process of the antibacterial blended yarn comprises the following steps of:
selecting blending raw materials, namely 30% by weight of bamboo pulp fibers, 20% by weight of natural fibrilia, specifically 10% by weight of flax fibers or jute fibers and modified polyester fibers, and 5% by weight of spandex fibers through special-shaped section design and ultraviolet resistance treatment;
Pretreating the blended raw material, namely mercerizing the blended raw material in a weak alkaline aqueous solution with the pH value of 8.5 for 60 minutes, adopting a plasma surface modification technology, wherein the treatment power is 80W, the treatment time is 45 seconds, the gas atmosphere is argon, and simultaneously introducing nano silicon dioxide particles, wherein the addition amount is 1.0% of the weight of the fiber;
And uniformly mixing the pretreated blending raw materials to obtain a blending fiber mixture.
Preferably, the method further comprises the step of feeding the blend into an intimate spinning apparatus for spinning at 4000 rpm, a spinning tension of 7 grams force/denier, a spinning temperature of 22 ℃, a relative humidity of 50%, and the step of introducing an air spinning technique.
Preferably, in the spinning process, the composite antibacterial agent is uniformly loaded on the blend fiber, the concentration of nano silver ions in the composite antibacterial agent is 1.0%, the concentration of natural plant extracts is 2.0%, the concentration of chitosan is 1.0%, and the spinning process is carried out by adopting an ultrasonic spraying and microwave treatment cooperative treatment technology, wherein the ultrasonic spraying power is 300W, the spraying time is 7 minutes, the microwave power is 800W, and the treatment time is 2 minutes.
Preferably, the method further comprises the step of carrying out post-treatment on the yarns, wherein the low-temperature dyeing temperature is 90 ℃, the shaping treatment temperature is 135 ℃, the anti-wrinkling treatment adopts an environment-friendly cross-linking agent, then the treatment time is 10 minutes by adopting an ultraviolet curing technology, the light source is an LED ultraviolet lamp, and the wavelength is 365nm.
Preferably, the method further comprises the step of carrying out on-line color mixing treatment on the blended raw materials before spinning, wherein the step is realized by a special color mixing device, the color mixing device comprises a color mixing chamber and a color homogenizing chamber, a stirrer is arranged in the color mixing chamber, the rotating speed is 120 revolutions per minute, a color homogenizing device is arranged in the color homogenizing chamber, and the color homogenizing time is 15 minutes.
Preferably, the method also comprises the step of introducing an intelligent monitoring system in the spinning process, wherein the system can monitor the quality parameters of the yarn in real time, the breaking strength is 10-50cN/tex, the elongation is 5-20% and the uniformity is less than or equal to 3%, and the spinning parameters such as spinning speed, tension and temperature are automatically adjusted according to the monitoring result.
Compared with the prior art, the invention has the beneficial effects that:
According to the preparation process of the antibacterial blended yarn, the raw materials such as the bamboo pulp fiber, the natural fibrilia, the modified polyester fiber and the spandex fiber are carefully selected, and the reasonable proportion is determined, so that the prepared yarn has excellent antibacterial performance, and good hygroscopicity, air permeability, elasticity and wear resistance are maintained.
And uniformly loading the composite antibacterial agent onto the blend fiber by adopting an ultrasonic spraying and microwave treatment cooperative treatment technology. The technology not only improves the loading efficiency of the antibacterial agent, but also ensures the uniform distribution of the antibacterial agent in the fiber, thereby improving the antibacterial performance of the yarn.
In the spinning and post-treatment processes, the quality and performance stability of the yarn are ensured by precisely controlling the spinning speed, tension, temperature, dyeing, shaping and other parameters. Meanwhile, an intelligent monitoring system is introduced to monitor quality parameters of the yarns in real time, spinning parameters are automatically adjusted according to monitoring results, and the accuracy and the intelligent level of the preparation process are further improved.
In the preparation process, the environment-friendly cross-linking agent and the LED ultraviolet lamp are adopted for crease-resist finishing and ultraviolet curing treatment, so that the emission of harmful substances is reduced, the energy consumption is reduced, and the requirements of sustainable development are met.
The prepared antibacterial blended yarn has the characteristics of excellent antibacterial property, hygroscopicity, air permeability, elasticity, wear resistance and the like, is suitable for a plurality of fields of medical treatment, sports, household and the like, and has wide market application prospect.
Detailed Description
In order to make the objects, technical solutions, and advantages of the present invention more apparent, the embodiments of the present invention will be further described in detail with reference to the accompanying drawings. It should be understood that the specific embodiments described herein are some, but not all, embodiments of the present invention, are intended to be illustrative only and not limiting of the embodiments of the present invention, and that all other embodiments obtained by persons of ordinary skill in the art without making any inventive effort are within the scope of the present invention.
Referring to fig. 1, the invention provides a preparation process of an antibacterial blended yarn, which comprises the following steps:
selecting blending raw materials, namely 30% by weight of bamboo pulp fibers, 20% by weight of natural fibrilia, specifically 10% by weight of flax fibers or jute fibers and modified polyester fibers, and 5% by weight of spandex fibers through special-shaped section design and ultraviolet resistance treatment;
Pretreating the blended raw material, namely mercerizing the blended raw material in a weak alkaline aqueous solution with the pH value of 8.5 for 60 minutes, adopting a plasma surface modification technology, wherein the treatment power is 80W, the treatment time is 45 seconds, the gas atmosphere is argon, and simultaneously introducing nano silicon dioxide particles, wherein the addition amount is 1.0% of the weight of the fiber;
uniformly mixing the pretreated blending raw materials to obtain a blending fiber mixture;
The spinning process comprises the steps of uniformly loading a composite antibacterial agent on the blend fiber, wherein the concentration of nano silver ions in the composite antibacterial agent is 1.0%, the concentration of natural plant extracts is 2.0%, the concentration of chitosan is 1.0%, the spinning process is carried out by an ultrasonic spraying and microwave treatment cooperative treatment technology, the ultrasonic spraying power is 300W, the spraying time is 7 minutes, the microwave power is 800W, and the treatment time is 2 minutes;
The method further comprises the step of performing post-treatment on the yarns, wherein the low-temperature dyeing temperature is 90 ℃, the shaping treatment temperature is 135 ℃, the anti-wrinkle finishing adopts an environment-friendly cross-linking agent, then an ultraviolet curing technology is adopted, the treatment time is 10 minutes, the light source is an LED ultraviolet lamp, and the wavelength is 365nm;
The method also comprises the step of carrying out on-line color mixing treatment on the blended raw materials before spinning, wherein the step is realized by a special color mixing device, the color mixing device comprises a color mixing chamber and a color homogenizing chamber, a stirrer is arranged in the color mixing chamber, the rotating speed is 120 r/min, a color homogenizing device is arranged in the color homogenizing chamber, and the color homogenizing time is 15 min;
The intelligent monitoring system is introduced in the spinning process, and can monitor the quality parameters of the yarn in real time, wherein the breaking strength is 10-50cN/tex, the elongation is 5-20% and the uniformity is less than or equal to 3%, and the spinning parameters such as spinning speed, tension and temperature are automatically adjusted according to the monitoring result.
Embodiment II, on the basis of embodiment I, a preparation process of the antibacterial blended yarn is provided
The raw materials are selected and proportioned, namely 30 percent by weight of bamboo pulp fiber, 20 percent by weight of natural fibrilia (flax fiber), 10 percent by weight of modified polyester fiber (subjected to special-shaped cross section design and ultraviolet resistance treatment) and 5 percent by weight of spandex fiber.
Pretreatment, namely placing the blended raw materials into a weak alkaline aqueous solution (pH value is 8.5) to carry out mercerization treatment, wherein the treatment time is 60 minutes. The plasma surface modification technology is adopted, the treatment power is 80W, the treatment time is 45 seconds, and the gas atmosphere is argon. In the modification process, nano silicon dioxide particles are simultaneously introduced, and the addition amount is 1.0 percent of the weight of the fiber.
Blending, namely uniformly mixing the pretreated blending raw materials to obtain a blend fiber mixture. Spinning, namely feeding the blend fiber mixture into compact spinning equipment for spinning, wherein the spinning speed is 4000 r/min, the spinning tension is 7 g/denier, the spinning temperature is 22 ℃, and the relative humidity is 50%. Air spinning technology is introduced to improve the strength and uniformity of the yarn.
And the antibacterial agent is loaded, namely the composite antibacterial agent is uniformly loaded on the blend fiber in the spinning process. The composite antibacterial agent contains nano silver ions (concentration is 1.0%), natural plant extracts (concentration is 2.0%) and chitosan (concentration is 1.0%). The ultrasonic spraying and microwave treatment cooperative treatment technology is adopted for loading, the ultrasonic spraying power is 300W, the spraying time is 7 minutes, the microwave power is 800W, and the treatment time is 2 minutes.
And (3) post-treatment, namely dyeing the yarn at a low temperature, wherein the dyeing temperature is 90 ℃. And (5) shaping treatment, wherein the shaping treatment temperature is 135 ℃. Adopts environment-friendly crosslinking the agent is subjected to crease-resistant finishing. Ultraviolet curing treatment was performed using an LED ultraviolet lamp (wavelength: 365 nm) for 10 minutes.
The third embodiment provides the materials comprising bamboo pulp fiber 30 wt%, natural fibrilia (flax fiber) 20 wt%, modified polyester fiber (with special section and uvioresistant treatment) 10 wt% and spandex fiber 5 wt% based on the second embodiment.
Pretreatment, namely placing the blended raw materials into a weak alkaline aqueous solution (pH value is 8.5) to carry out mercerization treatment, wherein the treatment time is 60 minutes. The plasma surface modification technology is adopted, the treatment power is 80W, the treatment time is 45 seconds, and the gas atmosphere is argon. In the modification process, nano silicon dioxide particles are simultaneously introduced, and the addition amount is 1.0 percent of the weight of the fiber.
Blending, namely uniformly mixing the pretreated blending raw materials to obtain a blend fiber mixture.
And (3) performing on-line color mixing treatment, namely performing on-line color mixing treatment on the blended raw materials before spinning. A specially adapted color mixing device is used, which comprises a color mixing chamber and a color homogenizing chamber. The color mixing chamber was equipped with a stirrer at a speed of 120 rpm to ensure uniform color mixing. The color homogenizing chamber is internally provided with a color homogenizing device, and the color homogenizing time is 15 minutes so as to further ensure the uniformity of the color.
Spinning, namely feeding the blend fiber mixture into compact spinning equipment for spinning, wherein the spinning speed is 4000 r/min, the spinning tension is 7 g/denier, the spinning temperature is 22 ℃, and the relative humidity is 50%. Air spinning technology is introduced to improve the strength and uniformity of the yarn.
And the antibacterial agent is loaded, namely the composite antibacterial agent is uniformly loaded on the blend fiber in the spinning process. The composite antibacterial agent contains nano silver ions (concentration is 1.0%), natural plant extracts (concentration is 2.0%) and chitosan (concentration is 1.0%). The ultrasonic spraying and microwave treatment cooperative treatment technology is adopted for loading, the ultrasonic spraying power is 300W, the spraying time is 7 minutes, the microwave power is 800W, and the treatment time is 2 minutes.
And (3) post-treatment, namely dyeing the yarn at a low temperature, wherein the dyeing temperature is 90 ℃. And (5) shaping treatment, wherein the shaping treatment temperature is 135 ℃. Adopts environment-friendly crosslinking the agent is subjected to crease-resistant finishing. Ultraviolet curing treatment was performed using an LED ultraviolet lamp (wavelength: 365 nm) for 10 minutes.
The fourth embodiment provides the materials comprising bamboo pulp fiber 30 wt%, natural fibrilia (flax fiber) 20 wt%, modified polyester fiber (with special section and uvioresistant treatment) 10 wt% and spandex fiber 5 wt%.
Pretreatment, namely placing the blended raw materials into a weak alkaline aqueous solution (pH value is 8.5) to carry out mercerization treatment, wherein the treatment time is 60 minutes. The plasma surface modification technology is adopted, the treatment power is 80W, the treatment time is 45 seconds, and the gas atmosphere is argon. In the modification process, nano silicon dioxide particles are simultaneously introduced, and the addition amount is 1.0 percent of the weight of the fiber.
Spinning, namely feeding the blend fiber mixture into compact spinning equipment for spinning, wherein the spinning speed is 4000 r/min, the spinning tension is 7 g/denier, the spinning temperature is 22 ℃, and the relative humidity is 50%.
Air spinning technology is introduced to improve the strength and uniformity of the yarn.
An intelligent monitoring system is introduced in the spinning process, and the system can monitor quality parameters of yarn in real time, including breaking strength (monitoring range is 10-50 cN/tex), elongation (monitoring range is 5% -20%) and uniformity (variation coefficient is less than or equal to 3%).
According to the monitoring result, spinning parameters such as spinning speed, tension and temperature are automatically adjusted to ensure stable quality of yarn.
And the antibacterial agent is loaded, namely the composite antibacterial agent is uniformly loaded on the blend fiber in the spinning process. The composite antibacterial agent contains nano silver ions (concentration is 1.0%), natural plant extracts (concentration is 2.0%) and chitosan (concentration is 1.0%). The ultrasonic spraying and microwave treatment cooperative treatment technology is adopted for loading, the ultrasonic spraying power is 300W, the spraying time is 7 minutes, the microwave power is 800W, and the treatment time is 2 minutes.
And (3) post-treatment, namely dyeing the yarn at a low temperature, wherein the dyeing temperature is 90 ℃. And (5) shaping treatment, wherein the shaping treatment temperature is 135 ℃. Adopts environment-friendly crosslinking the agent is subjected to crease-resistant finishing. Ultraviolet curing treatment was performed using an LED ultraviolet lamp (wavelength: 365 nm) for 10 minutes.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.