CN118873983A - A kind of preparation equipment and method of garlic ajoene - Google Patents

Abstract

The invention discloses a preparation device and method of garlic ajoene, comprising a crushing device, an extraction tank, a centrifugal filter device, a recovery device, a mixing device and a chromatography column device, and also comprising: an ultrasonic probe, which is arranged inside the extraction tank; a screw drive assembly, which is arranged on one side of the extraction tank and is used to drive the ultrasonic probe to move up and down; a gear assembly, which is fixedly sleeved on the surface of the extraction tank and is used to drive the ultrasonic probe to rotate through the screw drive assembly. The invention relates to the technical field of garlic ajoene preparation. The preparation device and method of garlic ajoene drive the ultrasonic probe to move up and down inside the extraction tank through the screw drive assembly, and at the same time, under the drive of the gear assembly, the ultrasonic probe can be driven to rotate in the extraction tank through the screw drive assembly, thereby increasing the range of ultrasonic oscillation, making the oscillation more uniform, improving the extraction effect, and thus shortening the time spent on extraction.

Description

A kind of preparation equipment and method of garlic ajoene

Technical Field

The invention relates to the technical field of garlic ajoene preparation, in particular to a garlic ajoene preparation device and a method thereof.

Background Art

Garlic ajoene is an important bioactive ingredient and belongs to an allyl sulfoxide compound with a vinyl sulfide part. It is a sulfur-containing organic compound in garlic and has many health benefits, including the prevention of cardiovascular diseases such as stroke, coronary thrombosis and atherosclerosis, as well as physiological and pharmacological activities such as antibacterial, antiviral and immunity-enhancing.

Reference patent application number CN201710280554.5 is a method for preparing high-purity natural garlic ajoene. The prior art utilizes allinase contained in garlic for fermentation, extracts ajoene by ultrasonic wave, purifies ajoene by supercritical CO2 extraction technology, and finally prepares a high-purity ajoene product by industrial chromatography technology;

The existing preparation method usually uses ultrasound to extract garlic ajoene. However, during the current ultrasonic extraction, most of the probes are set at fixed positions, resulting in poor extraction effect and uneven oscillation, thereby extending the ultrasonic extraction time and reducing the extraction effect. At the same time, during ultrasonic extraction, the crushed garlic is easy to precipitate at the bottom and cannot be fully mixed with the ethanol solution, which will affect the extraction effect.

Summary of the invention

In view of the deficiencies in the prior art, the present invention provides a preparation device and method for garlic ajoene, which solves the problems that most of the probes are set at fixed positions during ultrasonic extraction, resulting in poor extraction effect and prolonged ultrasonic extraction time. At the same time, the crushed garlic is easily precipitated at the bottom during extraction and cannot be fully mixed with the ethanol solution, which affects the extraction effect.

To achieve the above objectives, the present invention is implemented by the following technical scheme: a preparation device for garlic ajoene, comprising a crushing device, an extraction tank, a centrifugal filter device, a recovery device, a mixing device and a chromatography column device, and also comprising:

An ultrasonic probe is arranged inside the extraction tank;

The screw drive assembly is arranged on one side of the extraction tank and is used to drive the ultrasonic probe to move up and down;

The gear assembly is fixedly sleeved on the surface of the extraction tank and is used to drive the ultrasonic probe to rotate through the screw drive assembly;

A mixing mechanism is rotatably arranged inside the extraction tank, and the mixing mechanism includes a stirring rod, a cavity is opened inside the stirring rod, an electric push rod is fixedly connected to the top of the inner wall of the cavity, and the output end of the electric push rod is fixedly connected to the vertical rod through a connecting block, a sleeve is movably sleeved on the surface of the stirring rod, and a horizontal plate is fixedly connected between the two sides of the inner wall of the sleeve, the bottom end of the vertical rod is fixedly connected to the top of the horizontal plate, through grooves adapted to the horizontal plate are opened on both sides of the stirring rod, and three flip blades are fixedly connected to the surface of the sleeve.

Preferably, the screw drive assembly includes a first motor, the output end of the first motor is fixedly connected to a screw, and the surface of the screw is threadedly connected to a movable block, the surface of the first motor is fixedly connected to a slide rail through a base plate, and the slide rail is fixedly connected to the surface of the movable block through a slider, one side of the movable block is fixedly connected to a bracket, and the bottom of the bracket is fixedly connected to a fixing rod, and the bottom end of the fixing rod is fixedly connected to the top of the ultrasonic probe.

Preferably, the gear assembly includes an annular shell fixedly mounted on the outside of the extraction tank, the bottom of the inner wall of the annular shell is fixedly connected to an annular slide rail, and the top of the annular slide rail is slidably connected to an annular sleeve plate through a fixed block, the outer side of the annular sleeve plate is fixedly connected to teeth, one side of the annular shell is fixedly connected to a shell, and the bottom of the shell is fixedly connected to a second motor, the output end of the second motor is fixedly connected to a rotating shaft, and the surface of the rotating shaft is fixedly connected to a gear meshing with the teeth.

Preferably, one side of the top of the annular sleeve is fixedly connected to the bottom of the screw drive assembly through a column, and a fixing groove adapted to the column is formed on the top of the annular shell.

Preferably, the mixing mechanism also includes a stirring motor, and one end of the stirring rod passes through the extraction tank and is threadedly connected to one end of the output shaft of the stirring motor by a bolt, stirring blades are fixedly connected to both sides of the surface of the stirring rod, and L-shaped scrapers are fixedly connected to the bottom of both sides of the stirring rod.

Preferably, a movable groove is opened at the top of the extraction tank, and lap plates are provided on both sides of the inner wall of the movable groove, a rubber sheet is bonded to one side of the lap plate located inside the movable groove, a screw is fixedly connected to the top of the extraction tank, and one end of the screw passes through the outside of the lap plate and is threadedly connected to a hand nut.

Preferably, a crushing motor is fixedly connected to the top of the crushing device, and a rotating rod is fixedly connected to the output end of the crushing motor, blades are fixedly connected to both sides of the surface of the rotating rod, a screen is fixedly connected to the bottom of the crushing device, and an outer shell is fixedly connected to the bottom of the crushing device, and the bottom of the outer shell is connected to the top of the extraction tank through a discharge pipe.

Preferably, a servo motor is fixedly connected to the front side of the shell, and the output end of the servo motor is fixedly connected to a rotating shaft rotatably connected to the inner wall of the shell, a plurality of support rods are fixedly connected to one side of the rotating shaft surface, and a knocking ball is fixedly connected to one end of the support rod.

The present invention also discloses a method for using a garlic ajoene preparation device, comprising the following steps:

S1. Crushing: First, the garlic is put into a crushing device for crushing, and the garlic particles with a target particle size fall below the screen and directly enter the extraction tank through the discharge pipe;

S2, extraction: the mixing mechanism stirs and turns the mixed solution, and drives the ultrasonic probe to move up and down and rotate through the screw drive assembly and the gear assembly to perform ultrasonic extraction on the mixed solution in the extraction tank;

S3, centrifugal filtration: the extracted solution is transported to a centrifugal filtration device, the garlic grains in the solution are centrifuged and filtered, and finally an extract is obtained;

S4, volatilization: transporting the extract from which the garlic grains have been removed to a recovery device, and volatilizing and removing the solvent in the extract under vacuum conditions to obtain a concentrated solution;

S5, mixing: the concentrated liquid is transported to a mixing device and mixed with rapeseed oil;

S6. Refining and separation: The mixed and processed solution is then put into a chromatography column device for separation, extraction and elution to finally obtain high-purity ajoene.

The present invention provides a preparation device and method of garlic ajoene, which has the following beneficial effects:

(1) The garlic ajoene preparation device and method thereof drive the ultrasonic probe to move up and down inside the extraction tank through the screw drive assembly. At the same time, under the drive of the gear assembly, the ultrasonic probe can be driven by the screw drive assembly to rotate inside the extraction tank, thereby increasing the range of ultrasonic oscillation, making the oscillation more uniform, improving the extraction effect, and thus shortening the extraction time.

(2) The preparation device and method of garlic ajoene, when the ultrasonic probe is oscillating, the stirring rod drives the stirring blade to rotate, so as to mix the crushed garlic with the ethanol solution. At the same time, the electric push rod drives the stirring blade to move up and down through the vertical rod, so as to prevent the garlic from settling at the bottom of the cylinder, improve the uniformity of mixing, make the extraction effect better, and improve the production efficiency.

(3) The garlic ajoene preparation device and method thereof, when the garlic is crushed, only the garlic grains reaching the target particle size can fall below the screen, so that the solvent can react with the garlic grains better, thereby extracting more ajoene. In addition, during the use of the screen, the servo motor drives the rotating shaft to rotate back and forth, and the support rod drives the knocking ball to move up and down, and the screen is continuously beaten, so that the garlic grains blocking the screen are shaken out, and the screen is automatically cleaned, thereby improving work efficiency.

BRIEF DESCRIPTION OF THE DRAWINGS

FIG1 is a flow chart of the preparation of the structure of the present invention;

FIG2 is a cross-sectional view of the extraction tank structure of the present invention;

FIG3 is a partial enlarged view of point A in FIG2 of the present invention;

FIG4 is a schematic diagram of the installation of the flap blade structure of the present invention;

FIG5 is a schematic diagram of the gear assembly structure of the present invention;

FIG6 is a partial enlarged view of the S position in FIG2 of the present invention;

FIG7 is a cross-sectional view of the structure of the pulverizing device of the present invention;

FIG8 is a cross-sectional view of the housing structure of the present invention;

FIG. 9 is a schematic diagram of the cleaning component structure of the present invention.

In the figure: 1, crushing device; 2, extraction tank; 3, centrifugal filter device; 4, recovery device; 5, mixing device; 6, chromatography column device; 7, ultrasonic probe; 8, mixing mechanism; 81, stirring rod; 82, cavity; 83, electric push rod; 84, vertical rod; 85, sleeve; 86, horizontal plate; 87, through groove; 88, flip blade; 89, stirring motor; 810, stirring blade; 811, L-shaped scraper; 9, first motor; 10, screw rod; 11, movable block; 12, slide rail; 13, bracket; 14, fixed Fixed rod; 15, annular shell; 16, annular slide rail; 17, annular sleeve; 18, teeth; 19, shell; 20, second motor; 21, rotating shaft; 22, gear; 23, column; 24, fixed groove; 25, movable groove; 26, lap plate; 27, rubber sheet; 28, screw; 29, hand nut; 30, crushing motor; 31, rotating rod; 32, blade; 33, screen; 34, shell; 35, discharge pipe; 36, servo motor; 37, rotating shaft; 38, support rod; 39, knocking ball.

DETAILED DESCRIPTION

The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

Embodiment 1

Referring to FIGS. 1 to 5 , the present invention provides a preparation device for garlic ajoene, comprising a crushing device 1, an extraction tank 2, a centrifugal filter device 3, a recovery device 4, a mixing device 5 and a chromatography column device 6. The extraction tank 2, the centrifugal filter device 3, the recovery device 4, the mixing device 5 and the chromatography column device 6 are all connected by a delivery pump and a pipeline, and are integrated to improve the preparation efficiency. The present invention also includes:

An ultrasonic probe 7 is arranged inside the extraction tank 2;

The screw drive assembly is arranged on one side of the extraction tank 2 and is used to drive the ultrasonic probe 7 to move up and down;

The gear assembly is fixedly sleeved on the surface of the extraction tank 2 and is used to drive the ultrasonic probe 7 to rotate through the screw drive assembly;

The mixing mechanism 8 is rotatably arranged inside the extraction tank 2. The mixing mechanism 8 includes a stirring rod 81. A cavity 82 is provided inside the stirring rod 81. An electric push rod 83 is fixedly connected to the top of the inner wall of the cavity 82, and the output end of the electric push rod 83 is fixedly connected to a vertical rod 84 through a connecting block. A sleeve 85 is movably sleeved on the surface of the stirring rod 81, and a horizontal plate 86 is fixedly connected between the two sides of the inner wall of the sleeve 85. The bottom end of the vertical rod 84 is fixedly connected to the top of the horizontal plate 86. Through grooves 87 adapted to the horizontal plate 86 are provided on both sides of the stirring rod 81. Three flip blades 88 are fixedly connected to the surface of the sleeve 85. The electric push rod 83 drives the flip blades 88 to move up and down through the vertical rod 84 to prevent the garlic from settling at the bottom of the cylinder and improve the uniformity of mixing.

The screw drive assembly includes a first motor 9, the output end of the first motor 9 is fixedly connected to a screw 10, and the surface of the screw 10 is threadedly connected to a movable block 11, the surface of the first motor 9 is fixedly connected to a slide rail 12 through a bottom plate, and the slide rail 12 is fixedly connected to the surface of the movable block 11 through a slider, one side of the movable block 11 is fixedly connected to a bracket 13, and the bottom of the bracket 13 is fixedly connected to a fixed rod 14, and the bottom end of the fixed rod 14 is fixedly connected to the top of the ultrasonic probe 7;

The gear assembly includes an annular shell 15 fixedly mounted on the outside of the extraction tank 2, an annular slide rail 16 is fixedly connected to the bottom of the inner wall of the annular shell 15, and an annular sleeve plate 17 is slidably connected to the top of the annular slide rail 16 through a fixed block, and teeth 18 are fixedly connected to the outer side of the annular sleeve plate 17, a shell 19 is fixedly connected to one side of the annular shell 15, and a second motor 20 is fixedly connected to the bottom of the shell 19, a rotating shaft 21 is fixedly connected to the output end of the second motor 20, and a gear 22 meshing with the teeth 18 is fixedly connected to the surface of the rotating shaft 21, one side of the top of the annular sleeve plate 17 is fixedly connected to the bottom of the screw drive assembly through a column 23, and a fixing groove 24 adapted to the column 23 is provided at the top of the annular shell 15.

Through the setting of the above-mentioned structure, the screw drive assembly drives the ultrasonic probe 7 to move up and down inside the extraction tank 2. At the same time, driven by the gear assembly, the screw drive assembly can drive the ultrasonic probe 7 to rotate inside the extraction tank 2, thereby increasing the range of ultrasonic oscillation, making the oscillation more uniform, improving the extraction effect, and thus shortening the time spent on extraction.

Embodiment 2

Based on the first embodiment, please refer to Figures 1 to 5, the specific improvements are as follows:

An ultrasonic probe 7 is arranged inside the extraction tank 2;

The screw drive assembly is arranged on one side of the extraction tank 2 and is used to drive the ultrasonic probe 7 to move up and down;

The gear assembly is fixedly sleeved on the surface of the extraction tank 2 and is used to drive the ultrasonic probe 7 to rotate through the screw drive assembly;

The mixing mechanism 8 is rotatably arranged inside the extraction tank 2. The mixing mechanism 8 includes a stirring rod 81. A cavity 82 is provided inside the stirring rod 81. An electric push rod 83 is fixedly connected to the top of the inner wall of the cavity 82. The output end of the electric push rod 83 is fixedly connected to a vertical rod 84 through a connecting block. A sleeve 85 is movably sleeved on the surface of the stirring rod 81. A horizontal plate 86 is fixedly connected between the two sides of the inner wall of the sleeve 85. The bottom end of the vertical rod 84 is fixedly connected to the top of the horizontal plate 86. A through groove 87 matching the horizontal plate 86 is provided on both sides of the stirring rod 81. Three flapping blades 88 are fixedly connected to the surface. The mixing mechanism 8 also includes a stirring motor 89, which is fixed to the top of the extraction tank 2 through a frame. One end of the stirring rod 81 passes through the extraction tank 2 and is threadedly connected to one end of the output shaft of the stirring motor 89 through bolts. The setting of the bolts makes it easy to separate the stirring motor 89 from the stirring rod 81 and to maintain the electric push rod 83 and other structures inside the stirring rod 81. Stirring blades 810 are fixedly connected to both sides of the surface of the stirring rod 81, and L-shaped scrapers 811 are fixedly connected to the bottom of both sides of the stirring rod 81.

Through the arrangement of the above structure, the mixing mechanism 8 drives the stirring blade 810 to rotate, so as to mix the crushed garlic with the ethanol solution. At the same time, the electric push rod 83 drives the flipping blade 88 to move up and down through the vertical rod 84, so as to prevent the garlic from settling at the bottom of the cylinder and improve the uniformity of mixing. With the ultrasonic probe 7 that can move up and down and rotate, the extraction effect is better and the production efficiency is improved.

Embodiment 3

In combination with Example 1 and Example 2, please refer to Figures 1, 2 and 6, the specific improvements are as follows: a movable groove 25 is opened on the top of the extraction tank 2, and lap plates 26 are provided on both sides of the inner wall of the movable groove 25. The lap plates 26 are made of polyethylene plastic material, and a rubber sheet 27 is bonded to one side of the lap plate 26 located inside the movable groove 25. A screw rod 28 is fixedly connected to the top of the extraction tank 2, and one end of the screw rod 28 that passes through the outside of the lap plate 26 is threadedly connected to a hand-tightened nut 29.

By setting the above structure, the rubber sheet 27 does not affect the activity of the ultrasonic probe 7 while sealing the extraction tank 2. In addition, when the ultrasonic probe 7 is moved out of the extraction tank 2, the garlic grains adhering to the fixed rod 14 and the surface of the ultrasonic probe 7 can be cleaned through friction with the rubber sheet 27. By setting the screw 28 and the hand nut 29, it is convenient to manually remove the lap plate 26 and the rubber sheet 27 from the movable groove 25, replace the structure, and extend its service life.

Embodiment 4

In combination with the first to third embodiments, please refer to FIG. 1 and FIG. 7 to FIG. 9 , the specific improvements are as follows: the top of the crushing device 1 is fixedly connected to a crushing motor 30, and the output end of the crushing motor 30 is fixedly connected to a rotating rod 31, and both sides of the surface of the rotating rod 31 are fixedly connected to blades 32, and the blades 32 are provided with multiple groups to improve the crushing effect, and the bottom of the crushing device 1 is fixedly connected to a screen 33, and the screen 33 is used for garlic grains crushed to 0.1 cm to pass through. The garlic grains crushed to the target particle size can be better reacted with the solvent, thereby extracting more ajoene, and the bottom of the crushing device 1 is fixedly connected to a shell 34, and the bottom of the shell 34 is connected to the top of the extraction tank 2 through a discharge pipe 35;

A servo motor 36 is fixedly connected to the front side of the shell 34. The stroke and rotation angle of the servo motor 36 are set in advance through an external control system to drive the knocking ball 39 to move up and down to tap the screen 33. The output end of the servo motor 36 is fixedly connected to a rotating shaft 37 rotatably connected to the inner wall of the shell 34. A plurality of support rods 38 are fixedly connected to one side of the surface of the rotating shaft 37, and a knocking ball 39 is fixedly connected to one end of the support rod 38.

Through the arrangement of the above structure, the servo motor 36 drives the rotating shaft 37 to rotate back and forth, and drives the knocking ball 39 to move up and down through the support rod 38, so as to continuously beat the screen 33, so as to shake out the garlic grains blocking the screen 33, and automatically clean the screen 33, thereby reducing the workload of the staff.

Embodiment 5

The present invention also discloses a method for using a garlic ajoene preparation device, comprising the following steps:

S1, crushing: firstly, garlic is put into the crushing device 1 for crushing, and the garlic particles crushed to the target particle size fall below the screen 33 and directly enter the extraction tank 2 through the discharge pipe 35;

S2, extraction: the mixing mechanism stirs and turns the mixed solution, and drives the ultrasonic probe to move up and down and rotate through the screw drive assembly and the gear assembly to perform ultrasonic extraction on the mixed solution in the extraction tank;

S3, centrifugal filtration: the extracted solution is transported to the centrifugal filtration device 3, the garlic grains in the solution are centrifuged and filtered, and finally an extract is obtained;

S4, volatilization: the extract from which the garlic grains are removed is transported to the recovery device 4, and the solvent in the extract is volatilized and removed under vacuum conditions to obtain a concentrated solution;

S5, mixing: the concentrated liquid is transported to the mixing device 5 and mixed with rapeseed oil;

S6, refining and separation: the mixed solution is then sent into the chromatography column device 6 for separation, extraction and elution, and finally high-purity ajoene is obtained.

Meanwhile, the contents not described in detail in this specification belong to the prior art known to those skilled in the art, and the model parameters of each electrical appliance are not specifically limited, and conventional equipment compatible with the equipment can be used.

When in use, garlic is put into the crushing device 1, and the crushing motor 30 drives the multiple blades 32 to rotate through the rotating rod 31 to crush the garlic. The garlic grains crushed to the target particle size fall below the screen 33 and directly enter the extraction tank 2 through the discharge pipe 35. The stirring motor 89 is started to drive the stirring rod 81 to rotate, and the stirring rod 81 drives the stirring blade 810 to rotate to mix the crushed garlic with the ethanol solution. The L-shaped scrapers 811 on both sides scrape off the garlic grains adhered to the inner wall. At the same time, the electric push rod 83 drives the vertical rod 84 to move up and down, and the vertical rod 84 drives the flipping blade 88 to move up and down through the horizontal plate 86 and the sleeve 85 to flip the garlic grains. , preventing the garlic from settling at the bottom of the extraction tank 2, improving the uniformity of mixing, while the ultrasonic probe 7 performs ultrasonic oscillation, and by starting the first motor 9, driving the screw 10 to rotate, under the guidance of the slider and the slide rail 12, the movable block 11 moves up and down on the screw 10, and the movable block 11 drives the ultrasonic probe 7 to move up and down in the extraction tank 2 through the bracket 13, and by starting the second motor 20, driving the gear 22 to rotate, the gear 22 drives the annular sleeve 17 to rotate on the annular slide rail 16 through the teeth 18, and the annular sleeve 17 can drive the ultrasonic probe 7 to rotate through the screw drive assembly, so as to facilitate the full extraction and processing of the solution and improve the extraction efficiency;

When the ultrasonic probe 7 moves up and down or rotates, the rubber sheet 27 in the movable groove 25 will be squeezed. The rubber sheet 27 seals the extraction tank 2 without affecting the movement of the ultrasonic probe 7. In addition, when the ultrasonic probe 7 moves upward out of the extraction tank 2, the garlic grains adhering to the fixed rod 14 and the surface of the ultrasonic probe 7 can be cleaned by friction with the rubber sheet 27. By screwing the hand nut 29 out of the screw rod 28, the lap plate 26 can be moved out of the movable groove 25, so that the rubber sheet 27 can be replaced easily, thereby extending the service life of the structure.

When the screen 33 is in use, the servo motor 36 is started to drive the rotating shaft 37 to rotate back and forth, and the rotating shaft 37 drives the knocking ball 39 to move up and down through the support rod 38, and the screen 33 is continuously beaten, so that the garlic grains blocking the screen 33 can be shaken out, and the screen 33 can be automatically cleaned;

After ultrasonic extraction, the solution is transported to a centrifugal filter device 3, and the garlic grains in the solution are centrifugally filtered to obtain an extract;

The extract is then transported to a recovery device 4, where the solvent in the extract is volatilized and removed under vacuum conditions;

The evaporated concentrated liquid is transported to the mixing device 5 and mixed with rapeseed oil;

The mixed solution then enters the chromatography column device 6, and is separated, extracted and eluted by utilizing the difference in the distribution capacity or adsorption capacity between the solid phase adsorbent and the liquid phase solvent of ajoene or other impurities, thereby finally obtaining high-purity ajoene.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims (9)

1. The utility model provides a preparation facilities of garlic ajoene, includes reducing mechanism (1), draws jar (2), centrifugal filter equipment (3), recovery unit (4), mixing apparatus (5) and chromatographic column device (6), its characterized in that: further comprises:

an ultrasonic probe (7) provided inside the extraction tank (2);

the screw rod driving assembly is arranged at one side of the extraction tank (2) and is used for driving the ultrasonic probe (7) to move up and down;

the gear assembly is fixedly sleeved on the surface of the extraction tank (2) and is used for driving the ultrasonic probe (7) to rotate through the screw rod driving assembly;

Mixing mechanism (8), rotate and set up the inside at extracting jar (2), mixing mechanism (8) are including puddler (81), cavity (82) have been seted up to the inside of puddler (81), the top fixedly connected with electric putter (83) of cavity (82) inner wall, and the output of electric putter (83) passes through connecting block fixedly connected with montant (84), the surface activity cover of puddler (81) is equipped with sleeve (85), and fixedly connected with diaphragm (86) between the both sides of sleeve (85) inner wall, the bottom of montant (84) and the top fixed connection of diaphragm (86), logical groove (87) with diaphragm (86) looks adaptation have all been seted up to the both sides of puddler (81), the surface fixedly connected with of sleeve (85) three stirring blade (88).

2. The preparation equipment and the preparation method of the alliance according to claim 1 are characterized in that: the screw rod driving assembly comprises a first motor (9), the output end of the first motor (9) is fixedly connected with a screw rod (10), the surface of the screw rod (10) is connected with a movable block (11) in a threaded manner, the surface of the first motor (9) is fixedly connected with a sliding rail (12) through a bottom plate, the sliding rail (12) is fixedly connected with the surface of the movable block (11) through a sliding block, one side of the movable block (11) is fixedly connected with a support (13), the bottom of the support (13) is fixedly connected with a fixing rod (14), and the bottom of the fixing rod (14) is fixedly connected with the top of the ultrasonic probe (7).

3. The preparation equipment and the preparation method of the alliance according to claim 1 are characterized in that: the gear assembly comprises an annular shell (15) fixedly sleeved outside the extraction tank (2), an annular slide rail (16) is fixedly connected to the bottom of the inner wall of the annular shell (15), an annular sleeve plate (17) is slidably connected to the top of the annular slide rail (16) through a fixing block, teeth (18) are fixedly connected to the outer side of the annular sleeve plate (17), a shell (19) is fixedly connected to one side of the annular shell (15), a second motor (20) is fixedly connected to the bottom of the shell (19), a rotary shaft (21) is fixedly connected to the output end of the second motor (20), and a gear (22) meshed with the teeth (18) is fixedly connected to the surface of the rotary shaft (21).

4. A preparation device and method of alliance according to claim 3, wherein: one side at the top of the annular sleeve plate (17) is fixedly connected with the bottom of the screw rod driving assembly through a stand column (23), and a fixing groove (24) matched with the stand column (23) is formed in the top of the annular shell (15).

5. The preparation equipment and the preparation method of the alliance according to claim 1 are characterized in that: mixing mechanism (8) still include agitator motor (89), the one end that puddler (81) runs through out extraction tank (2) passes through bolt threaded connection with the one end of agitator motor (89) output shaft, equal fixedly connected with stirring vane (810) in both sides on puddler (81) surface, equal fixedly connected with L type scraper blade (811) in the bottom of puddler (81) both sides.

6. The preparation equipment and the preparation method of the alliance according to claim 1 are characterized in that: the top of extracting jar (2) has seted up movable groove (25), and the both sides of movable groove (25) inner wall all are provided with lapping plate (26), one side that lapping plate (26) are located movable groove (25) inside bonds has sheet rubber (27), the top fixedly connected with screw rod (28) of extracting jar (2), screw rod (28) run through to the outside one end threaded connection of lapping plate (26) has hand to twist nut (29).

7. The preparation equipment and the preparation method of the alliance according to claim 1 are characterized in that: the top fixedly connected with smashing motor (30) of reducing mechanism (1), and smashing the output fixedly connected with dwang (31) of motor (30), the equal fixedly connected with blade (32) in both sides on dwang (31) surface, the bottom fixedly connected with screen cloth (33) of reducing mechanism (1), the bottom fixedly connected with shell (34) of reducing mechanism (1), and the bottom of shell (34) is linked together through ejection of compact pipeline (35) and the top of extracting pot (2).

8. The apparatus and method for preparing alliance according to claim 7, wherein: the front of shell (34) fixedly connected with servo motor (36), and servo motor (36) output fixedly connected with and shell (34) inner wall rotation connection's axis of rotation (37), one side fixedly connected with a plurality of bracing pieces (38) on axis of rotation (37) surface, and the one end fixedly connected with of bracing piece (38) strikes ball (39).

9. A method of using the garlic ajoene producing apparatus according to any one of claims 1 to 8, characterized in that: the method comprises the following steps:

S1, crushing: firstly, putting garlic into a crushing device (1) for crushing treatment, and enabling the garlic particles crushed to the target particle size to fall below a screen (33) and directly enter an extraction tank (2) through a discharge pipeline (35);

S2, extracting: the mixing mechanism stirs and turns the mixed solution, and drives the ultrasonic probe to move up and down and rotate through the screw rod driving assembly and the gear assembly, so as to ultrasonically extract the mixed solution in the extracting tank;

s3, centrifugally filtering: delivering the extracted solution into a centrifugal filter device (3), and performing centrifugal filtration treatment on garlic particles in the solution to obtain an extracting solution;

S4, volatilizing: conveying the extracting solution with garlic particles removed into a recovery device (4), volatilizing and removing the solvent in the extracting solution under the vacuum condition to obtain concentrated solution;

S5, mixing: the concentrated solution is conveyed to mixing equipment (5) and is mixed with rapeseed oil for processing;

s6, refining and separating: and (3) separating, extracting and eluting the mixed solution in a chromatographic column device (6) to finally obtain the high-purity ajoene.