CN117844572A - A waste animal and vegetable oil alcoholysis esterification device and its implementation method - Google Patents

A waste animal and vegetable oil alcoholysis esterification device and its implementation method Download PDF

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CN117844572A
CN117844572A CN202211638913.7A CN202211638913A CN117844572A CN 117844572 A CN117844572 A CN 117844572A CN 202211638913 A CN202211638913 A CN 202211638913A CN 117844572 A CN117844572 A CN 117844572A
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mixing drum
adsorption
fixedly connected
grease
inner cavity
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顾光阳
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Lianyungang Jinbaiyi Oil Co ltd
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Lianyungang Jinbaiyi Oil Co ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/10Refining fats or fatty oils by adsorption

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention provides an alcoholysis esterification device of waste animal and vegetable oil and a method for implementing the same, which belongs to the technical field of alcoholysis esterification of oil and vegetable oil, and comprises a mixing drum, wherein oil and methanol solution are added into an inner cavity of the mixing drum, a cover plate is arranged on the upper end surface of the mixing drum, and the upper end surface of the cover plate is communicated with a condenser pipe, and the device further comprises: the output shaft end of the driving motor penetrates through the mixing cylinder to be fixedly connected with a center rod, and a plurality of guide plates are annularly arranged on the side wall of the center rod; the side wall of each guide plate is provided with a stirring mechanism; the inner cavity of each guide plate is provided with a guide mechanism; the adsorption mechanism is arranged on the side wall of the mixing drum. According to the invention, the guiding mechanism and the adsorption mechanism are used for adsorbing the floating foam of the grease in the mixing drum, and the stirring mechanism is used for stirring the grease in the mixing drum.

Description

一种废动植物油脂醇解酯化装置及其实施方法A waste animal and vegetable oil alcoholysis esterification device and its implementation method

技术领域Technical Field

本发明涉及油脂醇解酯化技术领域,具体而言,涉及一种废动植物油脂醇解酯化装置及其实施方法。The invention relates to the technical field of alcoholysis and esterification of fats and oils, and in particular to a device for alcoholysis and esterification of waste animal and plant fats and oils and an implementation method thereof.

背景技术Background technique

随着餐厨垃圾越来越多,人们对餐厨垃圾处理的研究也越来越深入,利用餐厨垃圾的油脂生产生物柴油是餐厨垃圾再利用的典型,目前受到广泛的研究。现有技术中,生物柴油的制造方法主要可分为物理法和化学法两类。常规的物理法包括直接混合法和微乳化法,化学法包括裂解法、酯化法和酯交换法。酯化法是使脂肪酸与甲醇或乙醇在酸催化下,发生酯化反应制成脂酸甲(乙)酯。而采用油脂加工过程中产生的酸化油为原料,其中既含有脂肪酸,又含有脂肪酸甘油酯。反应一般在甲醇的回流温度下进行,也可在加压反应器中进行,反应过程中生成的甲酯很容易与水和硫酸分离,因此采用酸化油作为原料生产生物柴油时,一般还要继续进行酯交换反应。As the amount of food waste increases, people are more and more deeply involved in the treatment of food waste. The production of biodiesel using the oil from food waste is a typical example of food waste recycling and is currently being widely studied. In the prior art, the production methods of biodiesel can be mainly divided into two categories: physical method and chemical method. Conventional physical methods include direct mixing method and microemulsification method, and chemical methods include cracking method, esterification method and transesterification method. The esterification method is to make fatty acids react with methanol or ethanol under acid catalysis to produce fatty acid methyl (ethyl) ester. The acidified oil produced in the oil processing process is used as the raw material, which contains both fatty acids and fatty acid glycerides. The reaction is generally carried out at the reflux temperature of methanol, and can also be carried out in a pressurized reactor. The methyl ester generated during the reaction is easily separated from water and sulfuric acid. Therefore, when using acidified oil as a raw material to produce biodiesel, the transesterification reaction is generally continued.

然而目前现有的用于废动植物油脂醇解酯化装置在对油脂和甲醇进行混合时,通常都只是使用单个搅拌杆对其进行搅拌混合,无法有效的将处于混合筒外侧的溶液和内侧的溶液进行混合,搅拌效率较差,同时在油脂醇解酯化反应时,液面上部溶液积累大量的油脂浮沫,不及时对其收集处理时会影响油脂出料时的质量。因此,如何发明一种废动植物油脂醇解酯化装置及其实施方法来改善这些问题,成为了本领域技术人员亟待解决的问题。However, the existing waste animal and plant oil alcoholysis esterification devices usually only use a single stirring rod to stir and mix the oil and methanol when mixing them, and cannot effectively mix the solution on the outside of the mixing cylinder with the solution on the inside, and the stirring efficiency is poor. At the same time, during the oil alcoholysis esterification reaction, a large amount of oil foam accumulates in the upper liquid surface solution, which will affect the quality of the oil when it is discharged if it is not collected and processed in time. Therefore, how to invent a waste animal and plant oil alcoholysis esterification device and its implementation method to improve these problems has become a problem that needs to be solved urgently by those skilled in the art.

发明内容Summary of the invention

为了弥补以上不足,本发明提供了一种废动植物油脂醇解酯化装置及其实施方法,旨在改善现有的钢桶预制板易因自身的冲击力过大与油脂醇解酯化发生碰撞造成损坏以及在两个钢桶预制板滑动时因碎屑的存在将使钢桶预制板的表面存在划痕的问题。In order to make up for the above shortcomings, the present invention provides a waste animal and plant oil alcoholysis and esterification device and its implementation method, aiming to improve the problem that the existing steel drum prefabricated plates are easily damaged by collision with the oil alcoholysis and esterification due to their own excessive impact force, and the surface of the steel drum prefabricated plates will be scratched due to the presence of debris when two steel drum prefabricated plates slide.

本发明是这样实现的:The present invention is achieved in that:

本发明提供一种废动植物油脂醇解酯化装置及其实施方法,包括混合筒,所述混合筒的内腔添加有油脂及甲醇溶液,所述混合筒的上端面放置有盖板,所述盖板的上端面连通有冷凝管,还包括:The present invention provides a waste animal and plant oil alcoholysis esterification device and an implementation method thereof, comprising a mixing cylinder, the inner cavity of which is added with oil and methanol solution, a cover plate is placed on the upper end surface of the mixing cylinder, the upper end surface of the cover plate is connected with a condenser, and further comprising:

通过机架固定连接在混合筒下部的驱动电机,所述驱动电机的输出轴端贯穿混合筒固定连接有中心杆,所述中心杆的侧壁上环形阵列有多个导向板;A driving motor is fixedly connected to the lower part of the mixing cylinder through a frame, the output shaft end of the driving motor passes through the mixing cylinder and is fixedly connected to a center rod, and a plurality of guide plates are arranged in a circular array on the side wall of the center rod;

搅拌机构,每个所述导向板的侧壁上均设置有搅拌机构,搅拌机构用于对混合筒内的油脂进行搅拌;A stirring mechanism, wherein the side wall of each guide plate is provided with a stirring mechanism, and the stirring mechanism is used to stir the grease in the mixing barrel;

导向机构,每个所述导向板的内腔均设置有导向机构,导向机构用于对油脂上层的浮沫进行聚拢;A guide mechanism, wherein the inner cavity of each guide plate is provided with a guide mechanism, and the guide mechanism is used to gather the floating foam on the upper layer of the grease;

吸附机构,所述混合筒的侧壁上设置有吸附机构;吸附机构用于对混合筒内油脂的浮沫进行吸附。Adsorption mechanism: the side wall of the mixing cylinder is provided with an adsorption mechanism; the adsorption mechanism is used to adsorb the floating foam of grease in the mixing cylinder.

优选的,所述导向机构包括支撑架、导向叶轮、导流框与导流框,所述导向板与中心杆固定连接,所述导向板的内腔左侧设置有导流框,所述导流框的内腔侧壁前后两侧固定连接有支撑架,所述支撑架的内腔转动连接有导向叶轮。Preferably, the guide mechanism includes a support frame, a guide impeller, a guide frame and a guide frame, the guide plate is fixedly connected to the center rod, a guide frame is arranged on the left side of the inner cavity of the guide plate, the front and rear sides of the inner cavity side walls of the guide frame are fixedly connected to the support frame, and the inner cavity of the support frame is rotatably connected to the guide impeller.

通过采用上述技术方案,能够对漂浮在液面上的油脂浮沫向导流框处聚拢。By adopting the technical solution, the grease foam floating on the liquid surface can be gathered toward the guide frame.

优选的,所述导向板的前后侧壁设置有导流槽,所述导流槽在导向板上呈凹形设置,并在导流框处处于最低位置。Preferably, the front and rear side walls of the guide plate are provided with guide grooves, the guide grooves are arranged in a concave shape on the guide plate and are at the lowest position at the guide frame.

优选的,所述搅拌机构包括传动蜗杆、传动蜗轮、转动杆、搅拌叶片、刮除板与安装座,所述导向板的前端面上下两侧固定连接有安装座,上下两侧的所述安装座之间转动连接有转动杆,所述转动杆的下端面固定连接有搅拌叶片。Preferably, the stirring mechanism includes a transmission worm, a transmission worm wheel, a rotating rod, a stirring blade, a scraper plate and a mounting seat, the front end surface of the guide plate is fixedly connected to the mounting seat on the upper and lower sides, a rotating rod is rotatably connected between the mounting seats on the upper and lower sides, and the lower end surface of the rotating rod is fixedly connected to the stirring blade.

通过采用上述技术方案,能够使搅拌叶片在混合筒内转动,以实现对油脂及甲醇溶液混合。By adopting the above technical solution, the stirring blades can be rotated in the mixing barrel to achieve mixing of the grease and the methanol solution.

优选的,所述导向叶轮的前端面固定连接有传动蜗杆,所述转动杆的侧壁上固定连接有传动蜗轮,所述传动蜗轮与传动蜗杆啮合连接,所述导向板的下端面外侧固定连接有刮除板,所述刮除板的侧壁与混合筒的内侧壁相贴合。Preferably, the front end face of the guide impeller is fixedly connected to a transmission worm, the side wall of the rotating rod is fixedly connected to a transmission worm wheel, the transmission worm wheel is meshingly connected to the transmission worm, and the outer side of the lower end face of the guide plate is fixedly connected to a scraper plate, and the side wall of the scraper plate is in contact with the inner wall of the mixing barrel.

通过采用上述技术方案,能够对混合筒侧壁上粘连的油脂进行刮除,避免了影响油脂出料时的质量。By adopting the above technical solution, the grease adhering to the side wall of the mixing barrel can be scraped off, thereby avoiding affecting the quality of the grease when it is discharged.

优选的,所述混合筒为中空设置,且中空腔体的内腔底面固定安装有电加热盘,所述混合筒的中空腔体内填充有清水,所述混合筒的外侧壁上固定连接有加水管,且加水管与中空腔体相连通,所述混合筒的下端面固定且连通有出液管,所述出液管与混合筒的内腔相连通。Preferably, the mixing cylinder is hollow, and an electric heating plate is fixedly installed on the bottom surface of the inner cavity of the hollow cavity, the hollow cavity of the mixing cylinder is filled with clean water, a water adding pipe is fixedly connected to the outer wall of the mixing cylinder, and the water adding pipe is connected to the hollow cavity, and a liquid outlet pipe is fixed and connected to the lower end surface of the mixing cylinder, and the liquid outlet pipe is connected to the inner cavity of the mixing cylinder.

通过采用上述技术方案,使反应后的油脂能够从出液管处排出。By adopting the above technical solution, the reacted grease can be discharged from the liquid outlet pipe.

优选的,所述吸附机构包括吸附箱、活塞板、复位弹簧、活塞柱、收集球、吸附管、吸附罩与出气管,所述吸附箱的内腔上部滑动连接有活塞板,所述活塞板的下端面固定连接有活塞柱,所述活塞柱的外侧壁下部螺纹连接有收集球。Preferably, the adsorption mechanism includes an adsorption box, a piston plate, a return spring, a piston column, a collecting ball, an adsorption tube, an adsorption cover and an outlet pipe. The upper part of the inner cavity of the adsorption box is slidably connected to the piston plate, the lower end surface of the piston plate is fixedly connected to the piston column, and the lower part of the outer wall of the piston column is threadedly connected to the collecting ball.

通过采用上述技术方案,能够快速对收集球进行更换,提高了工人的工作效率。By adopting the above technical solution, the collecting balls can be quickly replaced, thereby improving the work efficiency of workers.

优选的,所述活塞板的上端面固定连接有复位弹簧,所述复位弹簧的另一端固定连接在吸附箱的内腔顶面,所述活塞柱与吸附箱滑动连接,所述活塞柱与收集球相连通,所述活塞柱为中空设置,所述活塞柱的侧壁上设置有多个弧形槽,所述弧形槽与活塞柱为中空腔体像连通,所述活塞柱处于最低时,弧形槽恰好处于吸附箱的下端面侧壁处,所述导向板的上端面右侧固定连接有半球体,所述半球体与收集球滑动连接。Preferably, a return spring is fixedly connected to the upper end surface of the piston plate, and the other end of the return spring is fixedly connected to the top surface of the inner cavity of the adsorption box. The piston column is slidably connected to the adsorption box, and the piston column is connected to the collecting ball. The piston column is hollow, and a plurality of arc grooves are provided on the side wall of the piston column. The arc grooves are connected to the piston column like a hollow cavity. When the piston column is at its lowest, the arc grooves are just at the side wall of the lower end surface of the adsorption box. A hemisphere is fixedly connected to the right side of the upper end surface of the guide plate, and the hemisphere is slidably connected to the collecting ball.

优选的,所述吸附箱的右侧壁上固定且连通有吸附管,所述吸附管与吸附箱的连通处设置有开口向吸附箱内腔的单向水阀,所述吸附管的下端面固定连接有吸附罩,所述吸附箱的前后端面左侧固定且连通有出气管,所述出气管与吸附箱连通处设置有出口向外界的单向气阀。Preferably, an adsorption tube is fixed on and connected to the right side wall of the adsorption box, a one-way water valve opening to the inner cavity of the adsorption box is provided at the connection point between the adsorption tube and the adsorption box, an adsorption cover is fixedly connected to the lower end face of the adsorption tube, an air outlet pipe is fixed on and connected to the left side of the front and rear end faces of the adsorption box, and a one-way air valve with an outlet to the outside is provided at the connection point between the air outlet pipe and the adsorption box.

一种废动植物油脂醇解酯化装置的实施方法,包括如下步骤:A method for implementing a waste animal and vegetable oil alcoholysis and esterification device comprises the following steps:

步骤一:通过使用外部水泵将适量清水从加水管向混合筒的中空腔体内加入后,再通过启动电加热盘将水温保持在60℃。Step 1: Use an external water pump to add an appropriate amount of clean water from the water supply pipe into the hollow cavity of the mixing barrel, and then start the electric heating plate to maintain the water temperature at 60°C.

步骤二:向混合筒的内腔加入适量的油脂及甲醇溶液,再启动驱动电机使中心杆带动搅拌机构在混合筒内转动,以促进油脂及甲醇溶液反应。Step 2: Add an appropriate amount of grease and methanol solution to the inner cavity of the mixing cylinder, and then start the drive motor to make the central rod drive the stirring mechanism to rotate in the mixing cylinder to promote the reaction of the grease and methanol solution.

步骤三:在搅拌机构对油脂及甲醇溶液混合搅拌的同时,通过导向机构与吸附机构能够对液面上层的油脂浮沫进行吸附保留。Step 3: While the stirring mechanism is mixing and stirring the grease and the methanol solution, the grease foam on the upper layer of the liquid surface can be adsorbed and retained through the guiding mechanism and the adsorption mechanism.

本发明的有益效果是:The beneficial effects of the present invention are:

当半球体与收集球接触后,半球体能够挤压收集球使活塞柱向吸附箱的内腔上部移动,此时活塞板也将得到向上移动,在吸附机构的配合下,此时浮在液面上的油脂浮沫将能够被吸附吸附箱的内腔,油脂浮沫在自身重力的作用下将发生沉淀,堆积在吸附箱的内腔底部,在当半球体与收集球脱离接触后,失去半球体的挤压力,此时复位弹簧将得到复位,使活塞柱向下移动,此时活塞柱上的弧形槽恰好处于吸附箱的内腔底部,沉积在吸附箱底部的油脂浮沫将能够从弧形槽处进入活塞柱的内腔,最终沉积在收集球内,而吸附箱内多余的空气将能够从出气管处排出,进而通过上述所述,本装置能够代替人工对漂浮在液面上的油脂浮沫进行去除,避免了排出油脂是油脂浮沫一同排出,影响到油脂的质量,提高了整个装置的实用性。When the hemisphere contacts the collecting ball, the hemisphere can squeeze the collecting ball to make the piston column move toward the upper part of the inner cavity of the adsorption box. At this time, the piston plate will also be moved upward. Under the cooperation of the adsorption mechanism, the grease foam floating on the liquid surface can be adsorbed into the inner cavity of the adsorption box. The grease foam will settle under the action of its own gravity and accumulate at the bottom of the inner cavity of the adsorption box. When the hemisphere is out of contact with the collecting ball, the squeezing force of the hemisphere is lost. At this time, the reset spring will be reset to make the piston column move downward. At this time, the arc groove on the piston column is just at the bottom of the inner cavity of the adsorption box. The grease foam deposited at the bottom of the adsorption box can enter the inner cavity of the piston column from the arc groove and finally be deposited in the collecting ball, while the excess air in the adsorption box can be discharged from the air outlet pipe. Then, through the above, the device can replace manual removal of the grease foam floating on the liquid surface, avoids the discharge of grease and the grease foam together, affects the quality of grease, and improves the practicality of the whole device.

附图说明BRIEF DESCRIPTION OF THE DRAWINGS

为了更清楚地说明本发明实施方式的技术方案,下面将对实施方式中所需要使用的附图作简单地介绍,应当理解,以下附图仅示出了本发明的某些实施例,因此不应被看作是对范围的限定,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他相关的附图。In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings required for use in the embodiments will be briefly introduced below. It should be understood that the following drawings only show certain embodiments of the present invention and therefore should not be regarded as limiting the scope. For ordinary technicians in this field, other related drawings can be obtained based on these drawings without paying creative work.

图1是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的混合筒内部结构示意图;FIG1 is a schematic diagram of the internal structure of a mixing barrel of a waste animal and vegetable oil alcoholysis and esterification device and an implementation method thereof provided in an embodiment of the present invention;

图2是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的中心杆与导向板连接处结构示意图;2 is a schematic structural diagram of the connection between the center rod and the guide plate of a waste animal and plant oil alcoholysis and esterification device and its implementation method provided in an embodiment of the present invention;

图3是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的图2中区域放大结构示意图;FIG3 is a schematic diagram of the enlarged structure of the region in FIG2 of a waste animal and plant oil alcoholysis and esterification device and its implementation method provided in an embodiment of the present invention;

图4是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的正视局部剖视结构示意图;4 is a schematic diagram of a partial cross-sectional structure of a waste animal and vegetable oil alcoholysis esterification device and an implementation method thereof provided in an embodiment of the present invention;

图5是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的结构示意图;5 is a schematic structural diagram of a waste animal and plant oil alcoholysis esterification device and an implementation method thereof provided in an embodiment of the present invention;

图6是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的仰视整体结构示意图;6 is a bottom-up schematic diagram of the overall structure of a waste animal and vegetable oil alcoholysis and esterification device and its implementation method provided in an embodiment of the present invention;

图7是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的吸附箱处展示结构示意图;7 is a schematic diagram showing the structure of an adsorption box of a waste animal and plant oil alcoholysis and esterification device and an implementation method thereof provided in an embodiment of the present invention;

图8是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的吸附箱处剖视结构示意图;8 is a schematic cross-sectional view of the adsorption box of a waste animal and plant oil alcoholysis and esterification device and its implementation method provided in an embodiment of the present invention;

图9是本发明实施方式提供的一种废动植物油脂醇解酯化装置及其实施方法的吸附箱处于不同状态下示意图。9 is a schematic diagram of an adsorption box in different states of a waste animal and plant oil alcoholysis and esterification device and an implementation method thereof provided in an embodiment of the present invention.

图中:1、混合筒;11、电加热盘;12、加水管;13、出液管;2、盖板;3、冷凝管;4、驱动电机;5、中心杆;6、导向板;61、半球体;7、搅拌机构;71、传动蜗杆;72、传动蜗轮;73、转动杆;74、搅拌叶片;75、刮除板;76、安装座;8、导向机构;81、支撑架;82、导向叶轮;83、导流槽;84、导流框;9、吸附机构;91、吸附箱;92、活塞板;93、复位弹簧;94、活塞柱;941、弧形槽;95、收集球;96、吸附管;97、吸附罩;98、出气管。In the figure: 1. mixing cylinder; 11. electric heating plate; 12. water supply pipe; 13. liquid outlet pipe; 2. cover plate; 3. condenser; 4. drive motor; 5. center rod; 6. guide plate; 61. hemisphere; 7. stirring mechanism; 71. transmission worm; 72. transmission worm gear; 73. rotating rod; 74. stirring blade; 75. scraper plate; 76. mounting seat; 8. guide mechanism; 81. support frame; 82. guide impeller; 83. guide groove; 84. guide frame; 9. adsorption mechanism; 91. adsorption box; 92. piston plate; 93. reset spring; 94. piston column; 941. arc groove; 95. collecting ball; 96. adsorption tube; 97. adsorption cover; 98. outlet pipe.

具体实施方式Detailed ways

为使本发明实施方式的目的、技术方案和优点更加清楚,下面将结合本发明实施方式中的附图,对本发明实施方式中的技术方案进行清楚、完整地描述,显然,所描述的实施方式是本发明一部分实施方式,而不是全部的实施方式。基于本发明中的实施方式,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施方式,都属于本发明保护的范围。In order to make the purpose, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

实施例Example

参照图1-9,一种废动植物油脂醇解酯化装置及其实施方法,包括混合筒1,混合筒1的内腔添加有油脂及甲醇溶液,混合筒1的上端面放置有盖板2,盖板2的上端面连通有冷凝管3,还包括:1-9, a waste animal and plant oil alcoholysis esterification device and its implementation method include a mixing barrel 1, the inner cavity of the mixing barrel 1 is added with oil and methanol solution, the upper end surface of the mixing barrel 1 is placed with a cover plate 2, the upper end surface of the cover plate 2 is connected with a condenser 3, and further includes:

通过机架固定连接在混合筒1下部的驱动电机4,驱动电机4的输出轴端贯穿混合筒1固定连接有中心杆5,中心杆5的侧壁上环形阵列有多个导向板6;A driving motor 4 is fixedly connected to the lower part of the mixing drum 1 through a frame, and an output shaft end of the driving motor 4 passes through the mixing drum 1 and is fixedly connected to a center rod 5, and a plurality of guide plates 6 are arranged in a circular array on the side wall of the center rod 5;

搅拌机构7,每个导向板6的侧壁上均设置有搅拌机构7,搅拌机构7用于对混合筒1内的油脂进行搅拌;A stirring mechanism 7, each guide plate 6 is provided with a stirring mechanism 7 on its side wall, and the stirring mechanism 7 is used to stir the grease in the mixing barrel 1;

导向机构8,每个导向板6的内腔均设置有导向机构8,导向机构8用于对油脂上层的浮沫进行聚拢;A guide mechanism 8, wherein the inner cavity of each guide plate 6 is provided with a guide mechanism 8, and the guide mechanism 8 is used to gather the floating foam on the upper layer of the grease;

吸附机构9,混合筒1的侧壁上设置有吸附机构9;吸附机构9用于对混合筒1内油脂的浮沫进行吸附。Adsorption mechanism 9 : An adsorption mechanism 9 is disposed on the side wall of the mixing cylinder 1 ; the adsorption mechanism 9 is used to absorb the floating foam of the grease in the mixing cylinder 1 .

参照图1-9,进一步地;导向机构8包括支撑架81、导向叶轮82、导流槽83与导流框84,导向板6与中心杆5固定连接,导向板6的内腔左侧设置有导流框84,导流框84的内腔侧壁前后两侧固定连接有支撑架81,支撑架81的内腔转动连接有导向叶轮82,导向板6的前后侧壁设置有导流槽83,导流槽83在导向板6上呈凹形设置,并在导流框84处处于最低位置,搅拌机构7包括传动蜗杆71、传动蜗轮72、转动杆73、搅拌叶片74、刮除板75与安装座76,导向板6的前端面上下两侧固定连接有安装座76,上下两侧的安装座76之间转动连接有转动杆73,转动杆73的下端面固定连接有搅拌叶片74,导向叶轮82的前端面固定连接有传动蜗杆71,转动杆73的侧壁上固定连接有传动蜗轮72,传动蜗轮72与传动蜗杆71啮合连接,导向板6的下端面外侧固定连接有刮除板75,刮除板75的侧壁与混合筒1的内侧壁相贴合。Referring to Figures 1-9, further; the guide mechanism 8 includes a support frame 81, a guide impeller 82, a guide groove 83 and a guide frame 84, the guide plate 6 is fixedly connected to the center rod 5, a guide frame 84 is provided on the left side of the inner cavity of the guide plate 6, and the inner cavity side walls of the guide frame 84 are fixedly connected to the support frame 81 on both sides, and the inner cavity of the support frame 81 is rotatably connected to the guide impeller 82, and the front and rear side walls of the guide plate 6 are provided with a guide groove 83, which is concavely arranged on the guide plate 6 and is at the lowest position at the guide frame 84, and the stirring mechanism 7 includes a transmission worm 71, a transmission worm wheel 72, a rotation The movable rod 73, the stirring blade 74, the scraper plate 75 and the mounting seat 76, the front end surface of the guide plate 6 is fixedly connected with the mounting seat 76 on the upper and lower sides, the rotating rod 73 is rotatably connected between the mounting seats 76 on the upper and lower sides, the lower end surface of the rotating rod 73 is fixedly connected with the stirring blade 74, the front end surface of the guide impeller 82 is fixedly connected with the transmission worm 71, the side wall of the rotating rod 73 is fixedly connected with the transmission worm gear 72, the transmission worm gear 72 is meshed with the transmission worm 71, the outer side of the lower end surface of the guide plate 6 is fixedly connected with the scraper plate 75, and the side wall of the scraper plate 75 is in contact with the inner wall of the mixing barrel 1.

需要说明的是:导向叶轮82将带动传动蜗杆71转动,由于传动蜗轮72与传动蜗杆71啮合连接,从而此时转动杆73将能够带动搅拌叶片74在混合筒1的内腔转动,从而此时搅拌叶片74能够沿着中心杆5做公转搅拌的同时自身得到自转,能够有效的将处于混合筒1外侧的油脂及甲醇溶液流入混合筒1的中,进而此时整个装置及实现了提高搅拌效果的功能;It should be noted that: the guide impeller 82 will drive the transmission worm 71 to rotate. Since the transmission worm wheel 72 is meshed and connected with the transmission worm 71, the rotating rod 73 can drive the stirring blade 74 to rotate in the inner cavity of the mixing barrel 1. At this time, the stirring blade 74 can rotate along the central rod 5 while performing orbital stirring, and can effectively flow the grease and methanol solution on the outside of the mixing barrel 1 into the mixing barrel 1, so that the whole device can achieve the function of improving the stirring effect.

于此同时,在导向板6沿着中心杆5做公转运动的同时,通过导向板6前后侧壁设置导流槽83的配合,此时浮在液面上的油脂浮沫将能够向导流框84处一定,在导流框84处形成一个圆周轨迹。At the same time, when the guide plate 6 revolves along the center rod 5, the guide grooves 83 are arranged on the front and rear side walls of the guide plate 6, so that the grease foam floating on the liquid surface can be moved to the guide frame 84 to form a circular track.

参照图1-9,进一步地;混合筒1为中空设置,且中空腔体的内腔底面固定安装有电加热盘11,混合筒1的中空腔体内填充有清水,混合筒1的外侧壁上固定连接有加水管12,且加水管12与中空腔体相连通,混合筒1的下端面固定且连通有出液管13,出液管13与混合筒1的内腔相连通。Referring to Figures 1-9, further; the mixing cylinder 1 is hollow, and an electric heating plate 11 is fixedly installed on the bottom surface of the inner cavity of the hollow cavity, the hollow cavity of the mixing cylinder 1 is filled with clean water, a water adding pipe 12 is fixedly connected to the outer wall of the mixing cylinder 1, and the water adding pipe 12 is connected to the hollow cavity, the lower end surface of the mixing cylinder 1 is fixed and connected with a liquid outlet pipe 13, and the liquid outlet pipe 13 is connected to the inner cavity of the mixing cylinder 1.

需要说明的是:通过使用外部水泵将适量清水从加水管12向混合筒1的中空腔体内加入后,再通过启动电加热盘11将水温保持在60℃,向混合筒1的内腔加入适量的油脂及甲醇溶液后,通过启动驱动电机4使中心杆5带动导向板6在混合筒1的内腔转动,需要说明的是:此时导向板6恰好处于液面的下部;在导向板6发生转动时,在混合筒1内部油脂及甲醇溶液的阻力作用下,导向叶轮82将发生转动,简单的实现对小区域的油脂及甲醇溶液进行混合功能。It should be noted that: after using an external water pump to add an appropriate amount of clean water from the water adding pipe 12 into the hollow cavity of the mixing barrel 1, and then starting the electric heating plate 11 to maintain the water temperature at 60°C, after adding an appropriate amount of grease and methanol solution to the inner cavity of the mixing barrel 1, the driving motor 4 is started to drive the center rod 5 to drive the guide plate 6 to rotate in the inner cavity of the mixing barrel 1. It should be noted that: at this time, the guide plate 6 is just below the liquid surface; when the guide plate 6 rotates, under the resistance of the grease and methanol solution inside the mixing barrel 1, the guide impeller 82 will rotate, thereby simply realizing the mixing function of the grease and methanol solution in a small area.

参照图1-8,进一步地;吸附机构9包括吸附箱91、活塞板92、复位弹簧93、活塞柱94、收集球95、吸附管96、吸附罩97与出气管98,吸附箱91的内腔上部滑动连接有活塞板92,活塞板92的下端面固定连接有活塞柱94,活塞柱94的外侧壁下部螺纹连接有收集球95,活塞板92的上端面固定连接有复位弹簧93,复位弹簧93的另一端固定连接在吸附箱91的内腔顶面,活塞柱94与吸附箱91滑动连接,活塞柱94与收集球95相连通,活塞柱94为中空设置,活塞柱94的侧壁上设置有多个弧形槽941,弧形槽941与活塞柱94为中空腔体像连通,活塞柱94处于最低时,弧形槽941恰好处于吸附箱91的下端面侧壁处,导向板6的上端面右侧固定连接有半球体61,半球体61与收集球95滑动连接,吸附箱91的右侧壁上固定且连通有吸附管96,吸附管96与吸附箱91的连通处设置有开口向吸附箱91内腔的单向水阀,吸附管96的下端面固定连接有吸附罩97,吸附箱91的前后端面左侧固定且连通有出气管98,出气管98与吸附箱91连通处设置有出口向外界的单向气阀。1-8, further; the adsorption mechanism 9 includes an adsorption box 91, a piston plate 92, a return spring 93, a piston column 94, a collecting ball 95, an adsorption tube 96, an adsorption cover 97 and an exhaust pipe 98, the piston plate 92 is slidably connected to the upper part of the inner cavity of the adsorption box 91, the lower end surface of the piston plate 92 is fixedly connected to the piston column 94, the lower part of the outer wall of the piston column 94 is threadedly connected to the collecting ball 95, the upper end surface of the piston plate 92 is fixedly connected to the return spring 93, the other end of the return spring 93 is fixedly connected to the top surface of the inner cavity of the adsorption box 91, the piston column 94 is slidably connected to the adsorption box 91, the piston column 94 is connected to the collecting ball 95, the piston column 94 is hollow, and the side wall of the piston column 94 is provided with a There are multiple arc grooves 941, and the arc grooves 941 are connected to the piston column 94 as a hollow cavity. When the piston column 94 is at the lowest position, the arc grooves 941 are just at the side wall of the lower end surface of the adsorption box 91. A hemisphere 61 is fixedly connected to the right side of the upper end surface of the guide plate 6, and the hemisphere 61 is slidably connected to the collecting ball 95. An adsorption tube 96 is fixed and connected to the right side wall of the adsorption box 91. A one-way water valve opening to the inner cavity of the adsorption box 91 is provided at the connection between the adsorption tube 96 and the adsorption box 91. An adsorption cover 97 is fixedly connected to the lower end surface of the adsorption tube 96. An air outlet pipe 98 is fixed on the left side of the front and rear end surfaces of the adsorption box 91 and is connected. A one-way air valve with an outlet to the outside is provided at the connection between the air outlet pipe 98 and the adsorption box 91.

需要说明的是:当半球体61与收集球95接触后,半球体61能够挤压收集球95使活塞柱94向吸附箱91的内腔上部移动(如图8所示),此时活塞板92也将得到向上移动,复位弹簧93处于压缩状态,吸附箱91内腔下部的总容量将得到变大,内部压强将得到变小,在吸附管96处设置的单向水阀作用下,此时浮在液面上的油脂浮沫将能够被吸附吸附箱91的内腔,此时在油脂浮沫自身重力的作用下将发生沉淀,堆积在吸附箱91的内腔底部;在当半球体61与收集球95脱离接触后,失去半球体61的挤压力,此时复位弹簧93将得到复位,使活塞柱94向下移动(如图9所示),此时活塞柱94上的弧形槽941恰好处于吸附箱91的内腔底部,沉积在吸附箱91底部的油脂浮沫将能够从弧形槽941处进入活塞柱94的内腔,最终沉积在收集球95内,于此同时,随着吸附箱91内腔下部的总容量将得到变小,内部压强将得到变大,此时吸附箱91内多余的空气将能够从出气管98处排出,需要说明的是,由于此时油脂浮沫是沉积在吸附箱91的内腔底部,从出气管98处排出的气体并不足以能克服油脂浮沫的重力带动其从出气管98处喷出;进而通过上述所述,本装置能够代替人工对漂浮在液面上的油脂浮沫进行去除,避免了排出油脂是油脂浮沫一同排出,影响到油脂的质量,同时,大大提高了工人的工作效率。It should be noted that: when the hemispherical body 61 contacts the collecting ball 95, the hemispherical body 61 can squeeze the collecting ball 95 to make the piston column 94 move toward the upper part of the inner cavity of the adsorption box 91 (as shown in FIG8 ). At this time, the piston plate 92 will also move upward, and the return spring 93 will be in a compressed state. The total capacity of the lower part of the inner cavity of the adsorption box 91 will be increased, and the internal pressure will be reduced. Under the action of the one-way water valve provided at the adsorption tube 96, the grease foam floating on the liquid surface will be able to be adsorbed into the inner cavity of the adsorption box 91. At this time, the grease foam will precipitate under the action of its own gravity and accumulate at the bottom of the inner cavity of the adsorption box 91. When the hemispherical body 61 is out of contact with the collecting ball 95, the squeezing force of the hemispherical body 61 is lost. At this time, the return spring 93 will be reset, so that the piston column 94 moves downward (as shown in FIG9 ). At this time, the arc on the piston column 94 The groove 941 is just at the bottom of the inner cavity of the adsorption box 91. The grease foam deposited at the bottom of the adsorption box 91 will be able to enter the inner cavity of the piston rod 94 from the arc groove 941, and finally deposited in the collecting ball 95. At the same time, as the total capacity of the lower part of the inner cavity of the adsorption box 91 will be reduced, the internal pressure will be increased, and the excess air in the adsorption box 91 will be able to be discharged from the outlet pipe 98. It should be noted that, since the grease foam is deposited at the bottom of the inner cavity of the adsorption box 91 at this time, the gas discharged from the outlet pipe 98 is not enough to overcome the gravity of the grease foam and drive it to be ejected from the outlet pipe 98; furthermore, through the above, the present device can replace manual removal of the grease foam floating on the liquid surface, avoiding the discharge of the grease and the grease foam together, which affects the quality of the grease, and at the same time, greatly improves the work efficiency of the workers.

该一种废动植物油脂醇解酯化装置及其实施方法的工作原理:The working principle of the waste animal and vegetable oil alcoholysis esterification device and its implementation method:

通过使用外部水泵将适量清水从加水管12向混合筒1的中空腔体内加入后,再通过启动电加热盘11将水温保持在60℃,向混合筒1的内腔加入适量的油脂及甲醇溶液后,通过启动驱动电机4使中心杆5带动导向板6在混合筒1的内腔转动,需要说明的是:此时导向板6恰好处于液面的下部;在导向板6发生转动时,在混合筒1内部油脂及甲醇溶液的阻力作用下,导向叶轮82将发生转动,简单的实现对小区域的油脂及甲醇溶液进行混合功能;After adding a proper amount of clean water from the water adding pipe 12 into the hollow cavity of the mixing barrel 1 by using an external water pump, the water temperature is maintained at 60°C by starting the electric heating plate 11, and after adding a proper amount of grease and methanol solution into the inner cavity of the mixing barrel 1, the driving motor 4 is started to drive the central rod 5 to drive the guide plate 6 to rotate in the inner cavity of the mixing barrel 1. It should be noted that: at this time, the guide plate 6 is just below the liquid surface; when the guide plate 6 rotates, under the resistance of the grease and methanol solution inside the mixing barrel 1, the guide impeller 82 will rotate, thereby simply achieving the function of mixing the grease and methanol solution in a small area;

于此同时,导向叶轮82将带动传动蜗杆71转动,由于传动蜗轮72与传动蜗杆71啮合连接,从而此时转动杆73将能够带动搅拌叶片74在混合筒1的内腔转动,从而此时搅拌叶片74能够沿着中心杆5做公转搅拌的同时自身得到自转,能够有效的将处于混合筒1外侧的油脂及甲醇溶液流入混合筒1的中,进而此时整个装置及实现了提高搅拌效果的功能;At the same time, the guide impeller 82 will drive the transmission worm 71 to rotate. Since the transmission worm wheel 72 is meshed with the transmission worm 71, the rotating rod 73 can drive the stirring blade 74 to rotate in the inner cavity of the mixing barrel 1. At this time, the stirring blade 74 can rotate along the central rod 5 while stirring, and can effectively flow the grease and methanol solution outside the mixing barrel 1 into the mixing barrel 1. At this time, the whole device realizes the function of improving the stirring effect.

于此同时,在导向板6沿着中心杆5做公转运动的同时,通过导向板6前后侧壁设置导流槽83的配合,此时浮在液面上的油脂浮沫将能够向导流框84处一定,在导流框84处形成一个圆周轨迹;At the same time, when the guide plate 6 revolves along the center rod 5, the grease foam floating on the liquid surface can be moved to the guide frame 84 to form a circular track at the guide frame 84 through the cooperation of the guide grooves 83 provided on the front and rear side walls of the guide plate 6.

当半球体61与收集球95接触后,半球体61能够挤压收集球95使活塞柱94向吸附箱91的内腔上部移动(如图8所示),此时活塞板92也将得到向上移动,复位弹簧93处于压缩状态,吸附箱91内腔下部的总容量将得到变大,内部压强将得到变小,在吸附管96处设置的单向水阀作用下,此时浮在液面上的油脂浮沫将能够被吸附吸附箱91的内腔,此时在油脂浮沫自身重力的作用下将发生沉淀,堆积在吸附箱91的内腔底部;When the hemispherical body 61 contacts the collecting ball 95, the hemispherical body 61 can squeeze the collecting ball 95 to move the piston column 94 toward the upper part of the inner cavity of the adsorption box 91 (as shown in FIG. 8 ). At this time, the piston plate 92 will also move upward, and the return spring 93 will be in a compressed state. The total capacity of the lower part of the inner cavity of the adsorption box 91 will be increased, and the internal pressure will be reduced. Under the action of the one-way water valve provided at the adsorption tube 96, the grease foam floating on the liquid surface will be able to be adsorbed into the inner cavity of the adsorption box 91. At this time, the grease foam will settle under the action of its own gravity and accumulate at the bottom of the inner cavity of the adsorption box 91.

在当半球体61与收集球95脱离接触后,失去半球体61的挤压力,此时复位弹簧93将得到复位,使活塞柱94向下移动(如图9所示),此时活塞柱94上的弧形槽941恰好处于吸附箱91的内腔底部,沉积在吸附箱91底部的油脂浮沫将能够从弧形槽941处进入活塞柱94的内腔,最终沉积在收集球95内,于此同时,随着吸附箱91内腔下部的总容量将得到变小,内部压强将得到变大,此时吸附箱91内多余的空气将能够从出气管98处排出,需要说明的是,由于此时油脂浮沫是沉积在吸附箱91的内腔底部,从出气管98处排出的气体并不足以能克服油脂浮沫的重力带动其从出气管98处喷出;When the hemispherical body 61 is out of contact with the collecting ball 95, the squeezing force of the hemispherical body 61 is lost, and the reset spring 93 is reset to make the piston column 94 move downward (as shown in FIG. 9 ). At this time, the arc groove 941 on the piston column 94 is just at the bottom of the inner cavity of the adsorption box 91. The grease foam deposited at the bottom of the adsorption box 91 can enter the inner cavity of the piston column 94 from the arc groove 941 and finally deposit in the collecting ball 95. At the same time, as the total capacity of the lower part of the inner cavity of the adsorption box 91 is reduced, the internal pressure is increased, and the excess air in the adsorption box 91 can be discharged from the outlet pipe 98. It should be noted that, since the grease foam is deposited at the bottom of the inner cavity of the adsorption box 91 at this time, the gas discharged from the outlet pipe 98 is not enough to overcome the gravity of the grease foam and drive it to be ejected from the outlet pipe 98.

进而通过上述所述,本装置能够代替人工对漂浮在液面上的油脂浮沫进行去除,避免了排出油脂是油脂浮沫一同排出,影响到油脂的质量,同时,大大提高了工人的工作效率。Furthermore, through the above, the device can replace manual work to remove the grease foam floating on the liquid surface, avoiding the discharge of grease and grease foam together, which affects the quality of the grease, and at the same time, greatly improves the work efficiency of workers.

搅拌机构7在混合筒1内转动,以促进油脂及甲醇溶液反应。The stirring mechanism 7 rotates in the mixing barrel 1 to promote the reaction between the oil and the methanol solution.

需要说明的是,电机具体的型号规格需根据该装置的实际规格等进行选型确定,具体选型计算方法采用本领域现有技术,故不再详细赘述。It should be noted that the specific model and specifications of the motor need to be selected and determined based on the actual specifications of the device, and the specific selection calculation method adopts the existing technology in this field, so it will not be described in detail.

以上所述仅为本发明的优选实施方式而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. For those skilled in the art, the present invention may have various modifications and variations. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.

Claims (10)

1. The utility model provides a useless animal and plant grease alcoholysis esterification apparatus, includes mixing drum (1), the inner chamber of mixing drum (1) has added grease and methanol solution, apron (2) have been placed to the up end of mixing drum (1), the up end intercommunication of apron (2) has condenser pipe (3), its characterized in that still includes:
the device comprises a driving motor (4) fixedly connected to the lower part of a mixing drum (1) through a frame, wherein a central rod (5) is fixedly connected to the output shaft end of the driving motor (4) penetrating through the mixing drum (1), and a plurality of guide plates (6) are annularly arranged on the side wall of the central rod (5);
the stirring mechanisms (7) are arranged on the side walls of the guide plates (6), and the stirring mechanisms (7) are used for stirring the grease in the mixing drum (1);
the inner cavity of each guide plate (6) is provided with a guide mechanism (8), and the guide mechanisms (8) are used for gathering floating foam on the upper layer of grease;
the adsorption mechanism (9) is arranged on the side wall of the mixing drum (1); the adsorption mechanism (9) is used for adsorbing the floating foam of the grease in the mixing drum (1).
2. The device for alcoholysis esterification of waste animal and vegetable oil according to claim 1, characterized in that the guiding mechanism (8) comprises a supporting frame (81), a guiding impeller (82), a guiding groove (83) and a guiding frame (84), the guiding plate (6) is fixedly connected with the central rod (5), the guiding frame (84) is arranged on the left side of the inner cavity of the guiding plate (6), the supporting frame (81) is fixedly connected on the front side and the rear side of the inner cavity side wall of the guiding frame (84), and the guiding impeller (82) is rotatably connected in the inner cavity of the supporting frame (81).
3. The device for alcoholysis esterification of waste animal and vegetable oil according to claim 2, wherein guide grooves (83) are formed in the front and rear side walls of the guide plate (6), and the guide grooves (83) are concavely formed in the guide plate (6) and are located at the lowest position at the guide frame (84).
4. The device for alcoholysis esterification of waste animal and vegetable oil according to claim 2, characterized in that the stirring mechanism (7) comprises a transmission worm (71), a transmission worm wheel (72), a rotating rod (73), stirring blades (74), scraping plates (75) and mounting seats (76), wherein the mounting seats (76) are fixedly connected to the upper side and the lower side of the front end surface of the guide plate (6), the rotating rod (73) is rotatably connected between the mounting seats (76) on the upper side and the lower side, and the stirring blades (74) are fixedly connected to the lower end surface of the rotating rod (73).
5. The device for alcoholysis esterification of waste animal and vegetable oil according to claim 4, characterized in that the front end surface of the guide impeller (82) is fixedly connected with a transmission worm (71), a transmission worm wheel (72) is fixedly connected to the side wall of the rotating rod (73), the transmission worm wheel (72) is meshed with the transmission worm (71), a scraping plate (75) is fixedly connected to the outer side of the lower end surface of the guide plate (6), and the side wall of the scraping plate (75) is attached to the inner side wall of the mixing drum (1).
6. The device for alcoholysis esterification of waste animal and vegetable oil according to claim 1, characterized in that the mixing drum (1) is hollow, an electric heating disc (11) is fixedly installed on the bottom surface of the inner cavity of the hollow cavity, clear water is filled in the hollow cavity of the mixing drum (1), a water adding pipe (12) is fixedly connected to the outer side wall of the mixing drum (1), the water adding pipe (12) is communicated with the hollow cavity, a liquid outlet pipe (13) is fixedly and communicated with the lower end surface of the mixing drum (1), and the liquid outlet pipe (13) is communicated with the inner cavity of the mixing drum (1).
7. The device for alcoholysis esterification of waste animal and vegetable oil according to claim 1, wherein the adsorption mechanism (9) comprises an adsorption box (91), a piston plate (92), a return spring (93), a piston column (94), a collecting ball (95), an adsorption tube (96), an adsorption cover (97) and an air outlet tube (98), the piston plate (92) is slidably connected to the upper portion of an inner cavity of the adsorption box (91), the piston column (94) is fixedly connected to the lower end face of the piston plate (92), and the collecting ball (95) is screwed to the lower portion of an outer side wall of the piston column (94).
8. The device for alcoholysis esterification of waste animal and vegetable oil according to claim 7, characterized in that an upper end surface of the piston plate (92) is fixedly connected with a reset spring (93), the other end of the reset spring (93) is fixedly connected with the top surface of an inner cavity of the adsorption box (91), the piston column (94) is slidably connected with the adsorption box (91), the piston column (94) is communicated with the collecting ball (95), the piston column (94) is in a hollow arrangement, a plurality of arc grooves (941) are formed in the side wall of the piston column (94), the arc grooves (941) are communicated with the hollow cavity of the piston column (94), the arc grooves (941) are just located at the side wall of the lower end surface of the adsorption box (91) when the piston column (94) is at the lowest, a hemispherical body (61) is fixedly connected with the right side of the upper end surface of the guide plate (6), and the hemispherical body (61) is slidably connected with the collecting ball (95).
9. The device for alcoholysis esterification of waste animal and vegetable oil according to claim 7, characterized in that an adsorption pipe (96) is fixed on and communicated with the right side wall of the adsorption box (91), a one-way water valve with an opening to the inner cavity of the adsorption box (91) is arranged at the communication position of the adsorption pipe (96) and the adsorption box (91), an adsorption cover (97) is fixedly connected with the lower end face of the adsorption pipe (96), an air outlet pipe (98) is fixed on and communicated with the left side of the front end face and the rear end face of the adsorption box (91), and a one-way air valve with an outlet to the outside is arranged at the communication position of the air outlet pipe (98) and the adsorption box (91).
10. A method for implementing the apparatus for alcoholysis esterification of waste animal and vegetable fats and oils according to any one of claims 1 to 9, comprising the steps of:
step one: after a proper amount of clean water is added into the hollow cavity of the mixing drum (1) from the water adding pipe (12) by using an external water pump, the water temperature is kept at 60 ℃ by starting the electric heating disc (11);
step two: adding a proper amount of grease and methanol solution into the inner cavity of the mixing drum (1), and starting the driving motor (4) to drive the central rod (5) to drive the stirring mechanism (7) to rotate in the mixing drum (1) so as to promote the reaction of the grease and the methanol solution;
step three: the stirring mechanism (7) is used for mixing and stirring the grease and the methanol solution, and the guiding mechanism (80) and the adsorption mechanism (9) can be used for adsorbing and retaining grease foam on the upper layer of the liquid surface.
CN202211638913.7A 2022-12-20 2022-12-20 A waste animal and vegetable oil alcoholysis esterification device and its implementation method Pending CN117844572A (en)

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