CN117563770A - Device for recycling rare earth oxide by utilizing rare earth magnetic material waste - Google Patents
Device for recycling rare earth oxide by utilizing rare earth magnetic material waste Download PDFInfo
- Publication number
- CN117563770A CN117563770A CN202311838460.7A CN202311838460A CN117563770A CN 117563770 A CN117563770 A CN 117563770A CN 202311838460 A CN202311838460 A CN 202311838460A CN 117563770 A CN117563770 A CN 117563770A
- Authority
- CN
- China
- Prior art keywords
- rare earth
- box
- magnetic
- magnetic suction
- leaching
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000002699 waste material Substances 0.000 title claims abstract description 34
- 229910052761 rare earth metal Inorganic materials 0.000 title claims abstract description 21
- 150000002910 rare earth metals Chemical class 0.000 title claims abstract description 20
- 239000000696 magnetic material Substances 0.000 title claims abstract description 18
- 229910001404 rare earth metal oxide Inorganic materials 0.000 title claims abstract description 18
- 238000004064 recycling Methods 0.000 title claims abstract description 11
- 238000002386 leaching Methods 0.000 claims abstract description 42
- 238000007885 magnetic separation Methods 0.000 claims abstract description 26
- 238000007599 discharging Methods 0.000 claims abstract description 17
- 238000004062 sedimentation Methods 0.000 claims abstract description 15
- 210000001503 joint Anatomy 0.000 claims abstract 4
- 238000003756 stirring Methods 0.000 claims description 30
- 230000005540 biological transmission Effects 0.000 claims description 13
- 239000007788 liquid Substances 0.000 claims description 12
- 230000007246 mechanism Effects 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 9
- 239000013049 sediment Substances 0.000 claims description 7
- 238000007789 sealing Methods 0.000 claims description 5
- 230000000903 blocking effect Effects 0.000 claims 3
- 230000005389 magnetism Effects 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 13
- 230000008569 process Effects 0.000 abstract description 10
- 239000002244 precipitate Substances 0.000 abstract description 3
- 230000010354 integration Effects 0.000 abstract description 2
- 238000000605 extraction Methods 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 25
- 229910052751 metal Inorganic materials 0.000 description 10
- 239000002184 metal Substances 0.000 description 10
- 238000010586 diagram Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 2
- 229910001172 neodymium magnet Inorganic materials 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C1/00—Magnetic separation
- B03C1/02—Magnetic separation acting directly on the substance being separated
- B03C1/10—Magnetic separation acting directly on the substance being separated with cylindrical material carriers
- B03C1/14—Magnetic separation acting directly on the substance being separated with cylindrical material carriers with non-movable magnets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C1/00—Magnetic separation
- B03C1/005—Pretreatment specially adapted for magnetic separation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Processing Of Solid Wastes (AREA)
Abstract
Description
技术领域Technical field
本发明涉及稀土废料回收技术领域,尤其涉及一种利用稀土磁性材料废料回收稀土氧化物的装置。The present invention relates to the technical field of rare earth waste recycling, and in particular to a device for recovering rare earth oxides from rare earth magnetic material waste.
背景技术Background technique
钕铁硼永磁材料因其优越的磁性性能,现已广泛应用于国防军工、航空航天、医疗器械、计算机、电子和新能源汽车工业等领域。现今全球每年生产的钕铁硼系永磁体在三十万吨以上,制造工序中将产生磁铁碎屑、切削屑、碾磨屑、超细粉等废料占投入物料比例的20~30%。还有随着时间的推移,作为各产品部件的永磁体也会逐渐到期报废。如何将其中所含的各种元素特别是稀土元素进行低成本、绿色回收成为当下重要的技术课题。NdFeB permanent magnet materials have been widely used in defense industry, aerospace, medical equipment, computers, electronics and new energy automobile industries due to their superior magnetic properties. Today, more than 300,000 tons of NdFeB permanent magnets are produced globally every year. Waste materials such as magnet chips, cutting chips, grinding chips, and ultrafine powder will be generated during the manufacturing process, accounting for 20 to 30% of the input materials. And as time goes by, the permanent magnets that are components of each product will gradually expire and be scrapped. How to low-cost and green recycle the various elements contained in it, especially rare earth elements, has become an important technical issue at the moment.
目前从稀土磁性废料中回收稀土氧化物的过程一般经过磁选、浸出、沉淀和煅烧过程,但是现有的回收设备大多为单一设备,设备与设备之间需要转运或者架设输送设备,占地面积大,并且磁选设备存在磁吸不彻底的情况。At present, the process of recovering rare earth oxides from rare earth magnetic waste generally goes through magnetic separation, leaching, precipitation and calcination. However, most of the existing recovery equipment is a single equipment, which requires transfer or erection of conveying equipment between equipment, which occupies an area of Large, and the magnetic separation equipment has incomplete magnetic suction.
发明内容Contents of the invention
针对上述问题,本发明提供一种利用稀土磁性材料废料回收稀土氧化物的装置,该装置能够连续化的完成磁选、浸出和沉淀过程,一体化设置,结构紧凑,占地面积小,采用旋转磁选的方式,磁选彻底,并且可同步进行磁选、浸出液混合以及沉淀物排出的过程。In view of the above problems, the present invention provides a device for recovering rare earth oxides from rare earth magnetic material waste. The device can continuously complete the magnetic separation, leaching and precipitation processes. It is integrated, compact in structure, small in floor space, and adopts a rotating method. The magnetic separation method is thorough and can simultaneously carry out the processes of magnetic separation, leachate mixing and sediment discharge.
为解决上述问题,本发明所采用的技术方案是:In order to solve the above problems, the technical solution adopted by the present invention is:
一种利用稀土磁性材料废料回收稀土氧化物的装置,包括浸出箱,所述浸出箱的顶部固定安装有支架,浸出箱的一侧安装有沉淀箱,所述支架上转动连接有磁吸箱,所述磁吸箱的底部设有出料管,所述支架的顶部固定有顶板,所述顶板上固定连接有位于磁吸箱上方的料斗,所述料斗的底部设有下料管,所述磁吸箱的顶部设有与下料管对接的下料口,所述料斗的顶部转动连接有转轴,所述转轴的下端贯穿下料管、下料口、磁吸箱和出料管,转轴与下料口内壁间固定连接有多根连接臂,转轴上安装有两个开闭机构,两个所述开闭机构分别对应下料管和出料管,所述磁吸箱的周向内壁上嵌设有多根竖直设置的磁吸条,磁吸箱的底部设有多个与磁吸条一一对应的落料口,磁吸箱内安装有可将多根磁吸条上磁吸的废料推至落料口的环形推板,位于磁选箱内所述转轴的周向侧壁固定有多个错位设置的导料板,所述浸出箱的顶部设有与落料口对应的环形落料通道,所述浸出箱内安装有与转轴对接的搅拌组件,所述沉淀箱内设有可将浸出箱内的浸出液泵入沉淀箱内的泵液管。A device for recovering rare earth oxides from rare earth magnetic material waste, including a leaching box. A bracket is fixedly installed on the top of the leaching box. A sedimentation box is installed on one side of the leaching box. A magnetic suction box is rotatably connected to the bracket. The bottom of the magnetic box is provided with a discharge pipe, and the top of the bracket is fixed with a top plate. The top plate is fixedly connected with a hopper located above the magnetic box. The bottom of the hopper is provided with a discharge pipe. The top of the magnetic suction box is provided with a discharge port connected to the discharge pipe. The top of the hopper is rotatably connected to a rotating shaft. The lower end of the rotating shaft runs through the discharge pipe, the discharge port, the magnetic suction box and the discharge pipe. The rotating shaft There are multiple connecting arms fixedly connected to the inner wall of the unloading port. Two opening and closing mechanisms are installed on the rotating shaft. The two opening and closing mechanisms correspond to the unloading pipe and the discharging pipe respectively. The circumferential inner wall of the magnetic suction box There are multiple vertical magnetic strips embedded in it. The bottom of the magnetic box is equipped with multiple drop-out openings corresponding to the magnetic strips. The magnetic box is equipped with a magnetic strip that can put multiple magnetic strips on the magnetic strips. The sucked waste is pushed to the annular push plate of the blanking port. A plurality of staggered guide plates are fixed on the circumferential side wall of the rotating shaft in the magnetic separation box. The top of the leaching box is provided with a material corresponding to the blanking port. An annular blanking channel, a stirring assembly connected to the rotating shaft is installed in the leaching tank, and a pump liquid pipe is provided in the settling tank to pump the leaching liquid in the leaching tank into the settling tank.
优选地,所述环形推板的两侧顶部均固定连接有延伸出磁吸箱的抵杆,所述抵杆上套设有第一弹簧,抵杆的上端固定连接有环形抵板,所述顶板上安装有用于推动环形抵板下移的气缸。Preferably, the tops of both sides of the annular push plate are fixedly connected with support rods extending out of the magnetic suction box. The first spring is set on the support rod, and the upper end of the support rod is fixedly connected with an annular support plate. A cylinder is installed on the top plate for pushing the annular supporting plate downward.
优选地,所述料斗的顶部固定安装有电机,所述电机的输出端与转轴的上端间通过一对齿轮传动连接。Preferably, a motor is fixedly installed on the top of the hopper, and the output end of the motor is connected to the upper end of the rotating shaft through a pair of gear transmission.
优选地,所述开闭机构包括设置在转轴内的圆腔,所述圆腔内通过第二弹簧弹性连接有连接杆,所述圆腔的两侧均设有供连接杆对应端穿出的条形口,所述转轴的外壁套设有与连接杆固定连接的锥形挡料座,所述锥形挡料座适配下料管和出料管的管口,所述锥形挡料座的底部固定有套设在转轴上的密封套。Preferably, the opening and closing mechanism includes a circular cavity arranged in the rotating shaft, a connecting rod is elastically connected to the circular cavity through a second spring, and there are holes on both sides of the circular cavity for the corresponding ends of the connecting rod to pass through. The outer wall of the rotating shaft is equipped with a tapered stopper fixedly connected to the connecting rod. The tapered stopper is adapted to the nozzles of the feeding pipe and the discharge pipe. The tapered stopper is The bottom of the seat is fixed with a sealing sleeve set on the rotating shaft.
优选地,所述转轴的上端侧壁固定有两个导电环,两个所述导电环分别与两个第二弹簧电性连接,导电环外接电刷,所述电刷外接控制开关。Preferably, two conductive rings are fixed on the upper end side wall of the rotating shaft. The two conductive rings are electrically connected to the two second springs respectively. The conductive rings are externally connected to brushes, and the brushes are externally connected to the control switch.
优选地,所述磁吸箱的底部设有与对应落料口连通的伸缩槽,所述伸缩槽内通过第三弹簧弹性连接有延伸至落料口内的弧形挡板。Preferably, the bottom of the magnetic suction box is provided with a telescopic groove connected with the corresponding discharge opening, and an arc-shaped baffle extending into the discharge opening is elastically connected in the telescopic groove through a third spring.
优选地,所述支架上固定安装有套设在磁吸箱外围的环形导电轨,所述磁吸箱的周向侧壁固定有多个与环形导电轨抵触的导电滑块,所述导电滑块与对应第三弹簧电性连接,所述环形导电轨外接控制开关。Preferably, the bracket is fixedly mounted with an annular conductive rail sleeved around the periphery of the magnetic suction box, and a plurality of conductive sliders that conflict with the annular conductive rail are fixed on the circumferential side walls of the magnetic suction box. The block is electrically connected to the corresponding third spring, and the annular conductive rail is connected to an external control switch.
优选地,所述搅拌组件包括转动连接在浸出箱内的搅拌轴,所述搅拌轴上固定有多个混液板,搅拌轴的上端延伸出浸出箱并与转轴的下端间通过离合器对接。Preferably, the stirring assembly includes a stirring shaft rotatably connected in the leaching box. A plurality of liquid mixing plates are fixed on the stirring shaft. The upper end of the stirring shaft extends out of the leaching box and is connected to the lower end of the rotating shaft through a clutch.
优选地,所述沉淀箱的底部设有用于排出沉淀的排出通道,所述排出通道内转动连接有螺旋输送叶,所述浸出箱的底部内设有传动腔,所述螺旋输送叶的输送轴末端延伸至传动腔内,所述搅拌轴的下端延伸至传动腔内并与所述输送轴之间通过锥齿轮副传动连接。Preferably, the bottom of the sedimentation tank is provided with a discharge channel for discharging sediment, a spiral conveyor blade is rotatably connected in the discharge channel, a transmission cavity is provided in the bottom of the leaching tank, and the conveyor shaft of the spiral conveyor blade The end extends into the transmission cavity, and the lower end of the stirring shaft extends into the transmission cavity and is connected to the transmission shaft through a bevel gear pair.
优选地,所述转轴位于料斗内的一段侧壁上固定有搅拌叶。Preferably, a stirring blade is fixed on a side wall of the rotating shaft located in the hopper.
本发明的有益效果为:The beneficial effects of the present invention are:
1.通过安装料斗、磁选箱、浸出箱和沉淀箱,稀土磁性材料废料研磨成粉后倒入料斗内,即可自动化完成磁选、浸出以及沉淀过程,一体化设置,结构紧凑,占地面积小,并且可同步进行磁选、浸出液混合以及沉淀物排出的过程。1. By installing the hopper, magnetic separation box, leaching box and sedimentation box, the rare earth magnetic material waste is ground into powder and poured into the hopper, and the magnetic separation, leaching and sedimentation processes can be automatically completed. The integrated setting has a compact structure and occupies an area The area is small, and the processes of magnetic separation, leachate mixing and sediment discharge can be carried out simultaneously.
2.通过安装磁选箱、磁吸条、转轴、导料板以及环形推板,粉状废料通过下料管和下料口落入磁选箱内,转轴带动多个导料板以及磁选箱转动,粉末废料经多个导料板周向甩出,甩至磁选箱内壁,并随其转动,周向设置的多根磁吸条可将粉末废料中可被磁吸的金属粉末磁吸住,周向转动实现均匀磁吸,磁吸彻底,磁吸完毕后,启动气缸,通过环形抵板以及抵杆带动环形推板下移,即可将多根磁吸条上磁吸的金属粉末刮下。2. By installing the magnetic separation box, magnetic strips, rotating shaft, guide plate and annular push plate, the powdery waste falls into the magnetic selection box through the discharge pipe and the discharge port, and the rotating shaft drives multiple guide plates and magnetic separation The box rotates, and the powder waste is thrown out circumferentially through multiple guide plates, thrown to the inner wall of the magnetic separation box, and rotates with it. The multiple magnetic strips arranged circumferentially can magnetically absorb the metal powder in the powder waste. Suction, circumferential rotation achieves uniform magnetic suction, and the magnetic suction is complete. After the magnetic suction is completed, start the cylinder, drive the annular push plate downward through the annular resisting plate and the resisting rod, and then the metal magnetically attracted by the multiple magnetic strips can be Scrape off the powder.
3.通过设置开闭机构,每隔一段时间需要向磁选箱内加料时,或者需要将磁选箱内未被磁吸的废料排出时,只需通过控制开关、电刷以及导电环为对应第二弹簧通电,使其通电收缩,通过连接杆带动锥形挡料座上移,即可打开下料管或者出料管,此种打开的方式,下料管和出料管内部均未设置部件,下料速度快,并且料斗内的粉料能够通过通过下料管均匀的落入磁选箱内,保证磁选效果。3. By setting up the opening and closing mechanism, when you need to add materials to the magnetic selection box at regular intervals, or when you need to discharge the waste materials that are not magnetically attracted in the magnetic selection box, you only need to control the switch, brush and conductive ring accordingly. The second spring is energized, causing it to shrink when it is energized, and drives the conical stopper to move upward through the connecting rod, thereby opening the unloading pipe or the discharging pipe. In this way of opening, there are no internal settings in the discharging pipe or the discharging pipe. Components, the unloading speed is fast, and the powder in the hopper can evenly fall into the magnetic separation box through the unloading tube to ensure the magnetic separation effect.
4.通过设置搅拌组件、螺旋输送叶、离合器以及锥齿轮副,在离合器的控制下,转轴可同步带动搅拌轴转动,进而带动混液板转动,实现磁选后的粉料与浸出液混合过程,通过锥齿轮副带动螺旋输送叶转动,即可将沉淀箱内通过沉淀剂沉淀的底泥排出,一体化程度高。4. By setting up the stirring assembly, screw conveyor blade, clutch and bevel gear pair, under the control of the clutch, the rotating shaft can synchronously drive the stirring shaft to rotate, and then drive the mixing plate to rotate, realizing the mixing process of powder and leachate after magnetic separation. The bevel gear pair drives the spiral conveyor blade to rotate, which can discharge the sediment precipitated by the sedimentation agent in the sedimentation tank, with a high degree of integration.
附图说明Description of the drawings
图1为本发明的结构示意图;Figure 1 is a schematic structural diagram of the present invention;
图2为图1中的A处结构放大示意图;Figure 2 is an enlarged schematic diagram of the structure at point A in Figure 1;
图3为本发明提出的伸缩槽剖视图;Figure 3 is a cross-sectional view of the expansion tank proposed by the present invention;
图4为本发明提出的环形推板推料状态示意图;Figure 4 is a schematic diagram of the annular push plate pushing state proposed by the present invention;
图5为本发明提出的开闭机构打开状态示意图。Figure 5 is a schematic diagram of the open state of the opening and closing mechanism proposed by the present invention.
图中:1浸出箱、2锥齿轮副、3混液板、4搅拌轴、5泵液管、6沉淀箱、7排出通道、8螺旋输送叶、9离合器、10出料管、11环形落料通道、12磁吸箱、13落料口、14磁吸条、15环形导电轨、16导电滑块、17环形推板、18开闭机构、19转轴、20支架、21抵杆、22第一弹簧、23料斗、24顶板、25气缸、26电机、27齿轮、28导电环、29下料管、30锥形挡料座、31连接杆、32条形口、33第二弹簧、34圆腔、35密封套、36下料口、37连接臂、38弧形挡板、39第三弹簧、40伸缩槽、41导料板。In the picture: 1 leaching tank, 2 bevel gear pair, 3 mixing plate, 4 stirring shaft, 5 pump liquid pipe, 6 sedimentation tank, 7 discharge channel, 8 screw conveyor blade, 9 clutch, 10 discharge pipe, 11 annular blanking Channel, 12 magnetic box, 13 blanking port, 14 magnetic strip, 15 ring conductive rail, 16 conductive slider, 17 ring push plate, 18 opening and closing mechanism, 19 rotating shaft, 20 bracket, 21 supporting rod, 22 first Spring, 23 hopper, 24 top plate, 25 cylinder, 26 motor, 27 gear, 28 conductive ring, 29 discharge pipe, 30 tapered stopper, 31 connecting rod, 32 strip mouth, 33 second spring, 34 round cavity , 35 sealing sleeve, 36 unloading port, 37 connecting arm, 38 arc baffle, 39 third spring, 40 telescopic groove, 41 guide plate.
具体实施方式Detailed ways
为使本发明的上述目的、特征和优点能够更加明显易懂,下面结合附图对本发明的具体实施方式做详细的说明。在下面的描述中阐述了很多具体细节以便于充分理解本发明。但是本发明能够以很多不同于在此描述的其它方式来实施,本领域技术人员可以在不违背本发明内涵的情况下做类似改进,因此本发明不受下面公开的具体实施的限制。In order to make the above objects, features and advantages of the present invention more obvious and easy to understand, the specific embodiments of the present invention will be described in detail below with reference to the accompanying drawings. In the following description, numerous specific details are set forth in order to provide a thorough understanding of the invention. However, the present invention can be implemented in many other ways different from those described here. Those skilled in the art can make similar improvements without departing from the connotation of the present invention. Therefore, the present invention is not limited to the specific implementation disclosed below.
需要说明的是,当元件被称为“固定于”另一个元件,它可以直接在另一个元件上或者也可以存在居中的元件。当一个元件被认为是“连接”另一个元件,它可以是直接连接到另一个元件或者可能同时存在居中元件。本文所使用的术语“垂直的”,“水平的”,“左”、“右”以及类似的表述只是为了说明的目的,并不表示是唯一的实施方式。It should be noted that when an element is referred to as being "fixed" to another element, it can be directly on the other element or intervening elements may also be present. When an element is said to be "connected" to another element, it can be directly connected to the other element or there may also be intervening elements present. The terms "vertical", "horizontal", "left", "right" and similar expressions used herein are for illustrative purposes only and do not represent the only implementation manner.
参照图1-5,一种利用稀土磁性材料废料回收稀土氧化物的装置,包括浸出箱1,浸出箱1的顶部固定安装有支架20,浸出箱1的一侧安装有沉淀箱6,支架20上转动连接有磁吸箱12,磁吸箱12的底部设有出料管10,支架20的顶部固定有顶板24,顶板24上固定连接有位于磁吸箱12上方的料斗23,料斗23的底部设有下料管29,磁吸箱12的顶部设有与下料管29对接的下料口36,料斗23的顶部转动连接有转轴19,转轴19的下端贯穿下料管29、下料口36、磁吸箱12和出料管10,转轴19与下料口36内壁间固定连接有多根连接臂37,料斗23的顶部固定安装有电机26,电机26的输出端与转轴19的上端间通过一对齿轮27传动连接。Referring to Figure 1-5, a device for recovering rare earth oxides from rare earth magnetic material waste includes a leaching box 1. A bracket 20 is fixedly installed on the top of the leaching box 1. A sedimentation tank 6 is installed on one side of the leaching box 1. The bracket 20 A magnetic suction box 12 is rotatably connected to the top. The bottom of the magnetic suction box 12 is provided with a discharge pipe 10. A top plate 24 is fixed on the top of the bracket 20. A hopper 23 located above the magnetic suction box 12 is fixedly connected to the top plate 24. The hopper 23 The bottom is provided with a discharge pipe 29. The top of the magnetic suction box 12 is provided with a discharge opening 36 which is connected to the discharge pipe 29. The top of the hopper 23 is rotatably connected to a rotating shaft 19, and the lower end of the rotating shaft 19 passes through the discharge pipe 29 and the discharge pipe. The opening 36, the magnetic box 12 and the discharge pipe 10, the rotating shaft 19 and the inner wall of the discharge opening 36 are fixedly connected with a plurality of connecting arms 37. A motor 26 is fixedly installed on the top of the hopper 23, and the output end of the motor 26 is connected to the rotating shaft 19. The upper ends are connected through a pair of gears 27.
转轴19上安装有两个开闭机构18,两个开闭机构18分别对应下料管29和出料管10,开闭机构18包括设置在转轴19内的圆腔34,圆腔34内通过第二弹簧33弹性连接有连接杆31,圆腔34的两侧均设有供连接杆31对应端穿出的条形口32,转轴19的外壁套设有与连接杆31固定连接的锥形挡料座30,锥形挡料座30适配下料管29和出料管10的管口,锥形挡料座30的底部固定有套设在转轴19上的密封套35,锥形挡料座30上移,密封套35同步上移挡住条形口32,避免粉末进入,转轴19的上端侧壁固定有两个导电环28,两个导电环28分别与两个第二弹簧33电性连接,导电环28外接电刷,电刷外接控制开关,通过控制开关、电刷以及导电环28为对应第二弹簧33通电,使其通电收缩,通过连接杆31带动锥形挡料座30上移,即可打开下料管29或者出料管10。Two opening and closing mechanisms 18 are installed on the rotating shaft 19. The two opening and closing mechanisms 18 correspond to the unloading pipe 29 and the discharging pipe 10 respectively. The opening and closing mechanisms 18 include a circular cavity 34 arranged in the rotating shaft 19. The circular cavity 34 passes through The second spring 33 is elastically connected to the connecting rod 31. Both sides of the circular cavity 34 are provided with strip-shaped openings 32 for the corresponding ends of the connecting rod 31 to pass through. The outer wall of the rotating shaft 19 is provided with a tapered hole fixedly connected to the connecting rod 31. The conical stopper seat 30 is adapted to the nozzles of the discharge pipe 29 and the discharge pipe 10. The bottom of the conical stopper seat 30 is fixed with a sealing sleeve 35 that is sleeved on the rotating shaft 19. The conical stopper seat 30 is The material seat 30 moves upward, and the sealing sleeve 35 moves upward simultaneously to block the strip opening 32 to prevent powder from entering. Two conductive rings 28 are fixed on the upper end side wall of the rotating shaft 19. The two conductive rings 28 are electrically connected to the two second springs 33 respectively. The conductive ring 28 is connected to a brush externally, and the brush is connected to a control switch externally. The corresponding second spring 33 is energized through the control switch, brush and conductive ring 28, so that it contracts when energized, and drives the cone-shaped stopper seat 30 through the connecting rod 31. Move it upward to open the discharge pipe 29 or the discharge pipe 10.
磁吸箱12的周向内壁上嵌设有多根竖直设置的磁吸条14,位于磁选箱12内转轴19的周向侧壁固定有多个错位设置的导料板41,转轴19带动多个导料板41以及磁选箱12转动,粉末废料经多个导料板41周向甩出,甩至磁选箱12内壁,并随其转动,周向设置的多根磁吸条14可将粉末废料中可被磁吸的金属粉末磁吸住,周向转动实现均匀磁吸,磁吸彻底。A plurality of vertically arranged magnetic strips 14 are embedded in the circumferential inner wall of the magnetic selection box 12. A plurality of offset guide plates 41 are fixed on the circumferential side wall of the rotating shaft 19 in the magnetic selection box 12. The rotating shaft 19 The multiple guide plates 41 and the magnetic selection box 12 are driven to rotate, and the powder waste is thrown out circumferentially through the multiple guide plates 41, to the inner wall of the magnetic selection box 12, and rotates with it. Multiple magnetic strips are arranged circumferentially. 14. It can magnetically attract the metal powder that can be magnetically attracted in the powder waste, and rotate it in a circumferential direction to achieve uniform magnetic attraction and complete magnetic attraction.
磁吸箱12的底部设有多个与磁吸条14一一对应的落料口13,浸出箱1的顶部设有与落料口13对应的环形落料通道11,支架20上固定安装有套设在磁吸箱12外围的环形导电轨15,磁吸箱12的周向侧壁固定有多个与环形导电轨15抵触的导电滑块16,导电滑块16与对应第三弹簧39电性连接,环形导电轨15外接控制开关,通过控制开关为环形导电轨15供电,通过导电滑块16为对应的第三弹簧39通电,使其收缩拉动弧形挡板38进入伸缩槽40,即可打开落料口13,金属粉末通过环形落料通道11落入浸出箱1内。The bottom of the magnetic box 12 is provided with a plurality of blanking openings 13 corresponding to the magnetic strips 14. The top of the leaching box 1 is provided with an annular blanking channel 11 corresponding to the blanking openings 13. The bracket 20 is fixedly installed with The annular conductive rail 15 is sleeved on the periphery of the magnetic suction box 12. A plurality of conductive sliders 16 that conflict with the annular conductive rail 15 are fixed on the circumferential side wall of the magnetic suction box 12. The conductive sliders 16 are electrically connected to the corresponding third spring 39. Sexual connection, the annular conductive rail 15 is connected to an external control switch, and the annular conductive rail 15 is powered by the control switch, and the corresponding third spring 39 is energized through the conductive slider 16, so that it contracts and pulls the arc baffle 38 into the telescopic slot 40, that is, The blanking port 13 can be opened, and the metal powder falls into the leaching box 1 through the annular blanking channel 11 .
磁吸箱12内安装有可将多根磁吸条14上磁吸的废料推至落料口13的环形推板17,环形推板17的两侧顶部均固定连接有延伸出磁吸箱12的抵杆21,抵杆21上套设有第一弹簧22,抵杆21的上端固定连接有环形抵板41,顶板24上安装有用于推动环形抵板41下移的气缸25,启动气缸25,通过环形抵板41以及抵杆21带动环形推板17下移,即可将多根磁吸条14上磁吸的金属粉末刮下。The magnetic suction box 12 is equipped with an annular push plate 17 that can push the magnetically attracted waste materials on the multiple magnetic suction strips 14 to the discharge port 13. The tops of both sides of the annular push plate 17 are fixedly connected with the magnetic suction box 12 extending out. The butt rod 21 is provided with a first spring 22. The upper end of the butt rod 21 is fixedly connected with an annular butt plate 41. A cylinder 25 is installed on the top plate 24 for pushing the annular butt plate 41 to move downward. The cylinder 25 is started. , the annular push plate 17 is driven downward by the annular resisting plate 41 and the resisting rod 21, so that the metal powder magnetically attracted on the plurality of magnetic strips 14 can be scraped off.
浸出箱1内安装有与转轴19对接的搅拌组件,沉淀箱6内设有可将浸出箱1内的浸出液泵入沉淀箱6内的泵液管5,搅拌组件包括转动连接在浸出箱1内的搅拌轴4,搅拌轴4上固定有多个混液板3,搅拌轴4的上端延伸出浸出箱1并与转轴19的下端间通过离合器9对接,沉淀箱6的底部设有用于排出沉淀的排出通道7,排出通道7内转动连接有螺旋输送叶8,浸出箱1的底部内设有传动腔,螺旋输送叶8的输送轴末端延伸至传动腔内,搅拌轴4的下端延伸至传动腔内并与输送轴之间通过锥齿轮副2传动连接,在离合器9的控制下,转轴19可同步带动搅拌轴4转动,进而带动混液板3转动,实现磁选后的粉料与浸出液混合过程,通过泵液管5将浸出液泵入沉淀箱6内,加入沉淀剂,即可将金属沉淀物沉于排出通道7内,通过锥齿轮副2带动螺旋输送叶8转动,即可沉淀物排出。A stirring assembly connected to the rotating shaft 19 is installed in the leaching tank 1. A pump liquid pipe 5 is provided in the settling tank 6 to pump the leachate in the leaching tank 1 into the settling tank 6. The stirring assembly includes a stirring assembly that is rotatably connected in the leaching tank 1. The stirring shaft 4 has a plurality of liquid mixing plates 3 fixed on the stirring shaft 4. The upper end of the stirring shaft 4 extends out of the leaching tank 1 and is connected to the lower end of the rotating shaft 19 through the clutch 9. The bottom of the settling tank 6 is provided with a Discharge channel 7, a spiral conveyor blade 8 is rotatably connected in the discharge channel 7, a transmission cavity is provided at the bottom of the leaching box 1, the end of the conveyor shaft of the spiral conveyor blade 8 extends into the transmission cavity, and the lower end of the stirring shaft 4 extends to the transmission cavity The inner conveyor and the conveyor shaft are connected through a bevel gear pair 2. Under the control of the clutch 9, the rotating shaft 19 can synchronously drive the stirring shaft 4 to rotate, and then drive the mixing plate 3 to rotate, thereby realizing the mixing process of the powder and leachate after magnetic separation. , pump the leachate into the sedimentation tank 6 through the pump pipe 5, add the precipitant, and the metal precipitate will sink into the discharge channel 7. The bevel gear pair 2 will drive the spiral conveyor blade 8 to rotate, and the precipitate will be discharged.
此外,转轴19位于料斗23内的一段侧壁上固定有搅拌叶,转轴19同步带动搅拌叶转动,可搅动料斗内的粉末,易于下料。In addition, a stirring blade is fixed on a side wall of the rotating shaft 19 located in the hopper 23. The rotating shaft 19 drives the stirring blade to rotate synchronously, which can stir the powder in the hopper and make it easy to discharge the powder.
稀土磁性材料废料先经过粉碎设备研磨成粉后倒入料斗23内,粉状废料通过下料管29和下料口36落入磁选箱12内,启动电机26,通过一对齿轮27带动转轴19转动,转轴19带动多个导料板41以及磁选箱12转动,粉末废料经多个导料板41周向甩出,甩至磁选箱12内壁,并随其转动,周向设置的多根磁吸条14可将粉末废料中可被磁吸的金属粉末磁吸住,周向转动实现均匀磁吸,磁吸彻底,磁吸完毕后,启动气缸25,通过环形抵板41以及抵杆21带动环形推板17下移,即可将多根磁吸条14上磁吸的金属粉末刮下,通过控制开关为环形导电轨15供电,通过导电滑块16为对应的第三弹簧39通电,使其收缩拉动弧形挡板38进入伸缩槽40,即可打开落料口13,金属粉末通过环形落料通道11落入浸出箱1内。The rare earth magnetic material waste is first ground into powder by the crushing equipment and then poured into the hopper 23. The powdery waste material falls into the magnetic separation box 12 through the discharge pipe 29 and the discharge port 36. The motor 26 is started to drive the rotating shaft through a pair of gears 27. 19 rotates, the rotating shaft 19 drives the plurality of guide plates 41 and the magnetic separation box 12 to rotate, and the powder waste is thrown out circumferentially through the plurality of guide plates 41, to the inner wall of the magnetic separation box 12, and rotates with it, and the circumferentially arranged The multiple magnetic strips 14 can magnetically attract the metal powder that can be magnetically attracted in the powder waste, and the circumferential rotation can achieve uniform magnetic attraction and complete magnetic attraction. After the magnetic attraction is completed, the cylinder 25 is started, and the annular resisting plate 41 and the resisting force are used. The rod 21 drives the annular push plate 17 to move downward, which can scrape off the magnetically attracted metal powder on the multiple magnetic strips 14. The annular conductive rail 15 is powered through the control switch, and the corresponding third spring 39 is supplied through the conductive slider 16. Turn on the electricity and cause it to shrink and pull the arc baffle 38 into the telescopic groove 40, then the blanking port 13 can be opened, and the metal powder falls into the leaching box 1 through the annular blanking channel 11.
每隔一段时间需要向磁选箱12内加料时,或者需要将磁选箱12内未被磁吸的废料排出时,只需通过控制开关、电刷以及导电环28为对应第二弹簧33通电,使其通电收缩,通过连接杆31带动锥形挡料座30上移,即可打开下料管29或者出料管10,此种打开的方式,下料管29和出料管10内部均未设置部件,下料速度快,并且料斗23内的粉料能够通过下料管29周向均匀的落入磁选箱12内,保证磁选效果。When it is necessary to add materials to the magnetic selection box 12 at regular intervals, or when it is necessary to discharge the waste materials that are not magnetically attracted in the magnetic selection box 12, it is only necessary to energize the corresponding second spring 33 through the control switch, brush and conductive ring 28. , causing it to shrink when it is energized, and the conical stopper seat 30 is driven upward through the connecting rod 31, and the discharge pipe 29 or the discharge pipe 10 can be opened. In this way of opening, the insides of the discharge pipe 29 and the discharge pipe 10 are both No components are provided, the unloading speed is fast, and the powder in the hopper 23 can evenly fall into the magnetic separation box 12 through the unloading pipe 29 circumferentially, ensuring the magnetic separation effect.
向浸出箱1内注入浸出液,在离合器9的控制下,转轴19可同步带动搅拌轴4转动,进而带动混液板3转动,实现磁选后的粉料与浸出液混合过程,通过泵液管5将浸出液泵入沉淀箱6内,加入沉淀剂,即可将金属沉淀物沉于排出通道7内,通过锥齿轮副2带动螺旋输送叶8转动,即可沉淀物排出,排出后经过过滤后送入煅烧炉中即可得到稀土氧化物。Inject the leaching liquid into the leaching tank 1. Under the control of the clutch 9, the rotating shaft 19 can synchronously drive the stirring shaft 4 to rotate, and then drive the mixing plate 3 to rotate, realizing the mixing process of the magnetically separated powder and the leaching liquid, and pumping the liquid through the pump pipe 5 The leachate is pumped into the sedimentation tank 6, and the precipitant is added to sink the metal sediment into the discharge channel 7. The bevel gear pair 2 drives the spiral conveyor blade 8 to rotate, and the sediment is discharged. After being discharged, it is filtered and sent to Rare earth oxides can be obtained in the calciner.
以上所述仅为本发明的较佳实施例,并不用以限制本发明,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above are only preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention shall be included in the protection of the present invention. within the range.
Claims (10)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311838460.7A CN117563770A (en) | 2023-12-28 | 2023-12-28 | Device for recycling rare earth oxide by utilizing rare earth magnetic material waste |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311838460.7A CN117563770A (en) | 2023-12-28 | 2023-12-28 | Device for recycling rare earth oxide by utilizing rare earth magnetic material waste |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN117563770A true CN117563770A (en) | 2024-02-20 |
Family
ID=89861061
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202311838460.7A Withdrawn CN117563770A (en) | 2023-12-28 | 2023-12-28 | Device for recycling rare earth oxide by utilizing rare earth magnetic material waste |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN117563770A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118293703A (en) * | 2024-06-04 | 2024-07-05 | 河北鸿科碳素有限公司 | Material distribution crown block for petroleum coke calcination |
-
2023
- 2023-12-28 CN CN202311838460.7A patent/CN117563770A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118293703A (en) * | 2024-06-04 | 2024-07-05 | 河北鸿科碳素有限公司 | Material distribution crown block for petroleum coke calcination |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106834672A (en) | High efficiency rare-earth extraction equipment is used in a kind of rare earth processing | |
| CN117563770A (en) | Device for recycling rare earth oxide by utilizing rare earth magnetic material waste | |
| CN115814674A (en) | Material mixing device | |
| CN110127393B (en) | Neodymium iron boron powder discharging device and discharging method | |
| CN114574717B (en) | Device and method for recycling praseodymium-neodymium oxide in sections from neodymium-iron-boron waste | |
| CN211913717U (en) | Tombarthite oxalic acid precipitate filter equipment | |
| CN219807874U (en) | Sludge impurity separation device | |
| CN217247109U (en) | Separator is used in extraction of hydrolysate | |
| CN108358415B (en) | Ultrasonic-enhanced supercritical petroleum oil sludge extraction equipment | |
| CN107051261A (en) | One kind, which is smelted, uses ore batch mixer | |
| CN207887315U (en) | Automatic charging equipment with demagnetizer | |
| CN212018083U (en) | A permanent magnet iron removing device for feed processing | |
| CN208648967U (en) | A kind of sludge concentrator | |
| CN211016757U (en) | A NdFeB permanent magnet material smelting device | |
| CN209254188U (en) | A kind of dissolution slot structure extracted for ore | |
| CN219377484U (en) | Rare earth permanent magnet material impurity separating device | |
| CN221937232U (en) | A mixing device for processing rubber additives | |
| CN222093261U (en) | Reaction kettle with impurity filtering function | |
| CN215389948U (en) | Magnetic separator for recovering metallurgical waste residues | |
| CN223329363U (en) | Waste recycling device for rare earth metal production | |
| CN222196560U (en) | A storage mixing tank | |
| CN222930878U (en) | Construction waste recycling treatment equipment | |
| CN221003160U (en) | Needle Jiao Shuijiao separates and uses sediment stuff pump | |
| CN205761752U (en) | A kind of iron ore tailings ore-dressing plant | |
| CN214635840U (en) | Porous solid-liquid material mixing device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20240220 |
|
| WW01 | Invention patent application withdrawn after publication |