CN117551501A - Essence with jasmine tea characteristics, preparation method and application thereof - Google Patents
Essence with jasmine tea characteristics, preparation method and application thereof Download PDFInfo
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- CN117551501A CN117551501A CN202311778561.XA CN202311778561A CN117551501A CN 117551501 A CN117551501 A CN 117551501A CN 202311778561 A CN202311778561 A CN 202311778561A CN 117551501 A CN117551501 A CN 117551501A
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- parts
- tea
- jasmine
- essence
- absolute
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- 235000010254 Jasminum officinale Nutrition 0.000 title claims abstract description 113
- 244000269722 Thea sinensis Species 0.000 title claims abstract description 80
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 240000005385 Jasminum sambac Species 0.000 title 1
- 241000207840 Jasminum Species 0.000 claims abstract description 112
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 44
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 34
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 32
- KVWWIYGFBYDJQC-UHFFFAOYSA-N methyl dihydrojasmonate Chemical compound CCCCCC1C(CC(=O)OC)CCC1=O KVWWIYGFBYDJQC-UHFFFAOYSA-N 0.000 claims abstract description 32
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 30
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 claims abstract description 30
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 claims abstract description 30
- IAEGWXHKWJGQAZ-UHFFFAOYSA-N trimethylpyrazine Chemical compound CC1=CN=C(C)C(C)=N1 IAEGWXHKWJGQAZ-UHFFFAOYSA-N 0.000 claims abstract description 30
- DBZAKQWXICEWNW-UHFFFAOYSA-N 2-acetylpyrazine Chemical compound CC(=O)C1=CN=CC=N1 DBZAKQWXICEWNW-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000796 flavoring agent Substances 0.000 claims abstract description 20
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 17
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 17
- 229930007744 linalool Natural products 0.000 claims abstract description 17
- 244000188472 Ilex paraguariensis Species 0.000 claims abstract description 15
- 235000003368 Ilex paraguariensis Nutrition 0.000 claims abstract description 15
- XMLSXPIVAXONDL-PLNGDYQASA-N Jasmone Chemical compound CC\C=C/CC1=C(C)CCC1=O XMLSXPIVAXONDL-PLNGDYQASA-N 0.000 claims abstract description 15
- 229960002903 benzyl benzoate Drugs 0.000 claims abstract description 15
- IVLCENBZDYVJPA-ARJAWSKDSA-N cis-Jasmone Natural products C\C=C/CC1=C(C)CCC1=O IVLCENBZDYVJPA-ARJAWSKDSA-N 0.000 claims abstract description 15
- XMLSXPIVAXONDL-UHFFFAOYSA-N trans-jasmone Natural products CCC=CCC1=C(C)CCC1=O XMLSXPIVAXONDL-UHFFFAOYSA-N 0.000 claims abstract description 15
- AJKVQEKCUACUMD-UHFFFAOYSA-N 2-Acetylpyridine Chemical compound CC(=O)C1=CC=CC=N1 AJKVQEKCUACUMD-UHFFFAOYSA-N 0.000 claims abstract description 14
- VMUXSMXIQBNMGZ-UHFFFAOYSA-N 3,4-dihydrocoumarin Chemical compound C1=CC=C2OC(=O)CCC2=C1 VMUXSMXIQBNMGZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- DMSHWWDRAYHEBS-UHFFFAOYSA-N dihydrocoumarin Natural products C1CC(=O)OC2=C1C=C(OC)C(OC)=C2 DMSHWWDRAYHEBS-UHFFFAOYSA-N 0.000 claims abstract description 14
- 150000002576 ketones Chemical class 0.000 claims abstract description 13
- 241000220317 Rosa Species 0.000 claims abstract description 12
- 241000208125 Nicotiana Species 0.000 claims description 43
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 30
- 235000019504 cigarettes Nutrition 0.000 claims description 13
- 239000002994 raw material Substances 0.000 claims description 12
- 239000002904 solvent Substances 0.000 claims description 10
- 239000001674 (E)-1-(2,6,6-trimethyl-1-cyclohexenyl)but-2-en-1-one Substances 0.000 claims description 9
- BGTBFNDXYDYBEY-UHFFFAOYSA-N 1-(2,6,6-trimethylcyclohexen-1-yl)but-2-en-1-one Chemical compound CC=CC(=O)C1=C(C)CCCC1(C)C BGTBFNDXYDYBEY-UHFFFAOYSA-N 0.000 claims description 9
- POIARNZEYGURDG-UHFFFAOYSA-N beta-damascenone Natural products CC=CC(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-UHFFFAOYSA-N 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 235000019505 tobacco product Nutrition 0.000 claims description 4
- 241000628997 Flos Species 0.000 claims description 2
- 235000006236 Paraguay tea Nutrition 0.000 claims description 2
- 235000011449 Rosa Nutrition 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 239000003571 electronic cigarette Substances 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 82
- 244000061176 Nicotiana tabacum Species 0.000 abstract 1
- 235000013616 tea Nutrition 0.000 description 69
- 238000011156 evaluation Methods 0.000 description 17
- 238000004458 analytical method Methods 0.000 description 9
- 230000001953 sensory effect Effects 0.000 description 9
- 235000019634 flavors Nutrition 0.000 description 7
- 239000000779 smoke Substances 0.000 description 7
- 239000000203 mixture Substances 0.000 description 6
- 235000013599 spices Nutrition 0.000 description 6
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 4
- 235000019506 cigar Nutrition 0.000 description 4
- 235000009508 confectionery Nutrition 0.000 description 4
- 229910052709 silver Inorganic materials 0.000 description 4
- 239000004332 silver Substances 0.000 description 4
- 244000046052 Phaseolus vulgaris Species 0.000 description 3
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 239000012046 mixed solvent Substances 0.000 description 3
- 239000000178 monomer Substances 0.000 description 3
- 230000000638 stimulation Effects 0.000 description 3
- 239000000341 volatile oil Substances 0.000 description 3
- SIKJAQJRHWYJAI-UHFFFAOYSA-N Indole Chemical compound C1=CC=C2NC=CC2=C1 SIKJAQJRHWYJAI-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- -1 aromatic organic compounds Chemical class 0.000 description 2
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- IFYYFLINQYPWGJ-UHFFFAOYSA-N gamma-decalactone Chemical compound CCCCCCC1CCC(=O)O1 IFYYFLINQYPWGJ-UHFFFAOYSA-N 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- UWKAYLJWKGQEPM-LBPRGKRZSA-N linalyl acetate Chemical compound CC(C)=CCC[C@](C)(C=C)OC(C)=O UWKAYLJWKGQEPM-LBPRGKRZSA-N 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- VAMXMNNIEUEQDV-UHFFFAOYSA-N methyl anthranilate Chemical compound COC(=O)C1=CC=CC=C1N VAMXMNNIEUEQDV-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- FQTLCLSUCSAZDY-UHFFFAOYSA-N (+) E(S) nerolidol Natural products CC(C)=CCCC(C)=CCCC(C)(O)C=C FQTLCLSUCSAZDY-UHFFFAOYSA-N 0.000 description 1
- GEWDNTWNSAZUDX-WQMVXFAESA-N (-)-methyl jasmonate Chemical compound CC\C=C/C[C@@H]1[C@@H](CC(=O)OC)CCC1=O GEWDNTWNSAZUDX-WQMVXFAESA-N 0.000 description 1
- WUOACPNHFRMFPN-SECBINFHSA-N (S)-(-)-alpha-terpineol Chemical compound CC1=CC[C@@H](C(C)(C)O)CC1 WUOACPNHFRMFPN-SECBINFHSA-N 0.000 description 1
- FQTLCLSUCSAZDY-ATGUSINASA-N Nerolidol Chemical compound CC(C)=CCC\C(C)=C\CC[C@](C)(O)C=C FQTLCLSUCSAZDY-ATGUSINASA-N 0.000 description 1
- OVKDFILSBMEKLT-UHFFFAOYSA-N alpha-Terpineol Natural products CC(=C)C1(O)CCC(C)=CC1 OVKDFILSBMEKLT-UHFFFAOYSA-N 0.000 description 1
- 229940088601 alpha-terpineol Drugs 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229940007550 benzyl acetate Drugs 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- IFYYFLINQYPWGJ-VIFPVBQESA-N gamma-Decalactone Natural products CCCCCC[C@H]1CCC(=O)O1 IFYYFLINQYPWGJ-VIFPVBQESA-N 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- PZOUSPYUWWUPPK-UHFFFAOYSA-N indole Natural products CC1=CC=CC2=C1C=CN2 PZOUSPYUWWUPPK-UHFFFAOYSA-N 0.000 description 1
- RKJUIXBNRJVNHR-UHFFFAOYSA-N indolenine Natural products C1=CC=C2CC=NC2=C1 RKJUIXBNRJVNHR-UHFFFAOYSA-N 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- UWKAYLJWKGQEPM-UHFFFAOYSA-N linalool acetate Natural products CC(C)=CCCC(C)(C=C)OC(C)=O UWKAYLJWKGQEPM-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229940102398 methyl anthranilate Drugs 0.000 description 1
- 210000004877 mucosa Anatomy 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- WASNIKZYIWZQIP-AWEZNQCLSA-N nerolidol Natural products CC(=CCCC(=CCC[C@@H](O)C=C)C)C WASNIKZYIWZQIP-AWEZNQCLSA-N 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention provides essence with jasmine tea characteristics, a preparation method and application thereof, and the essence comprises the following components in parts by mass: 0.5-1.5 parts of jasmine absolute; 0.15-0.25 part of jasmine absolute; 2-3 parts of methyl dihydrojasmonate; 0.5-1.5 parts of cis-jasmone; 0.1-0.2 part of phenethyl alcohol; 2-4 parts of linalool; 0.04-0.06 part of rose alcohol; 0.03-0.05 part of tea-flavor spirane; 0.8-1.2 parts of tea-scented ketone; 0.08-0.12 parts of yerba mate absolute; 0.8-1.2 parts of tree moss extract; 2.5-3.5 parts of benzyl benzoate; 0.04-0.06 part of 2,3, 5-trimethyl pyrazine; 0.005-0.015 part of 2-acetylpyrazine; 0.005-0.015 part of 2-acetylpyridine; 0.005-0.015 part of beta-dihydro damascone; 0.04-0.06 part of isophorone; 0.005-0.015 part of dihydrocoumarin; 0.018-0.022 parts of plum extract; 0.018-0.022 parts of Brazilian tobacco extract. The invention also discloses a preparation method and application of the essence formula. The essence formula provided by the invention has the characteristic of jasmine tea fragrance.
Description
Technical Field
The invention belongs to the field of essence and spice and food flavoring, and particularly relates to essence with jasmine tea characteristics, a preparation method thereof and application of essence in tobacco, wherein the essence has the jasmine tea characteristic fragrance.
Background
The disclosure of this background section is only intended to increase the understanding of the general background of the invention and is not necessarily to be construed as an admission or any form of suggestion that this information forms the prior art already known to those of ordinary skill in the art.
The essence and spice are widely applied to the fields of tobacco, food, daily chemicals and the like. In the tobacco field, the essence and the spice not only can endow the cigarette product with unique style characteristics, but also can improve the sensory quality of the cigarette. Common flavor raw materials are tobacco essential oils, aromatic organic compounds, and the like. With the improvement of living standard, the requirements of people on the quality and taste of cigarettes are increasing. Jasmine tea is produced in Fujian Fuzhou, the producing area is wide, and the variety is rich. The tea fragrance and the jasmine fragrance are integrated, the fragrance is strong without flushing, the fragrance is durable, the fragrance is sharp, no peculiar smell is generated, and the nutritional value and the health care value are high.
The patent CN109393547A is a jasmine cigar, and the raw materials comprise: 100-150 parts of jasmine flower, 10-15 parts of mucosa protectant, 5-10 parts of flavoring agent, 3-8 parts of sodium bicarbonate or sodium carbonate, 5-10 parts of sweetener, 1-5 parts of tobacco flavor, 1-2 parts of antioxidant, 1-2 parts of preservative, 15-20 parts of tobacco extract, 5-10 parts of cigar type tobacco flavor, 20-30 parts of cigar material, 15-20 parts of deionized water, 0.5-1 part of compound vitamin, 5-8% of water content of finished product, 30-40 parts of propylene glycol, and the tobacco extract is absolute oil or essential oil of cloud tobacco, extract and/or Zimbabwe tobacco leaf oil or essential oil; cigar material is tobacco powder after crushing, grinding and sieving, and has granularity of 10-100 mesh.
Patent CN104371830a discloses a jasmine essence with natural jasmine flavor and a preparation method thereof. The raw materials comprise: jasmine treatment fluid, benzyl alcohol, phenethyl alcohol, linalool, alpha-terpineol, nerolidol, benzyl alcohol, linalool, cis-jasmone, methyl anthranilate, benzyl acetate, linalyl acetate, methyl dihydrojasmonate, gamma-decalactone, indole, jasmine absolute, ethanol, distilled water, jasmine fragrance base, and propylene glycol.
However, the essence does not have jasmine tea fragrance.
Disclosure of Invention
In order to solve the problems, the invention provides the essence with the jasmine tea characteristics, which shows a certain jasmine tea fragrance characteristic on the basis of guaranteeing the elegant and fragrant jasmine tea fragrance, and effectively avoids the defect of unstable quality caused by the addition of natural tea products. The jasmine tea essence formula adopted by the application is added into tobacco shreds, so that the prepared cigarette has the jasmine fragrance style of being evident and the taste is improved.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
the first aspect of the invention provides essence with jasmine tea characteristics, which comprises the following raw materials in parts by mass: 0.5-1.5 parts of jasmine absolute; 0.15-0.25 part of jasmine absolute; 2-3 parts of methyl dihydrojasmonate; 0.5-1.5 parts of cis-jasmone; 0.1-0.2 part of phenethyl alcohol; 2-4 parts of linalool; 0.04-0.06 part of rose alcohol; 0.03-0.05 part of tea-flavor spirane; 0.8-1.2 parts of tea-scented ketone; 0.08-0.12 parts of yerba mate absolute; 0.8-1.2 parts of tree moss extract; 2.5-3.5 parts of benzyl benzoate; 0.04-0.06 part of 2,3, 5-trimethyl pyrazine; 0.005-0.015 part of 2-acetylpyrazine; 0.005-0.015 part of 2-acetylpyridine; 0.005-0.015 part of beta-dihydro damascone; 0.04-0.06 part of isophorone; 0.005-0.015 part of dihydrocoumarin; 0.018-0.022 parts of plum extract; 0.018-0.022 parts of Brazilian tobacco extract.
Through long-term research and systematic experiment of various different jasmine fragrances and tea fragrances, the invention compounds various monomer fragrances with jasmine flower fragrance and tea fragrance, and is assisted with various other monomer fragrances, the obtained jasmine tea-characteristic essence formula is used in tobacco, can embody the fragrance of the jasmine tea-characteristic fragrance, coordinate the jasmine tea fragrance, flower fragrance and tobacco fragrance, enrich the tobacco fragrance, soften the smoke, coordinate the tobacco fragrance and reduce the stimulation, and obtain satisfactory sucking feeling.
In some embodiments, the composition comprises the following raw materials in parts by mass: 1 part of jasmine absolute; 0.2 parts of jasmine absolute; 2.5 parts of methyl dihydrojasmonate; 1 part of cis-jasmone; 0.15 parts of phenethyl alcohol; 3 parts of linalool; 0.05 parts of rose alcohol; 0.04 parts of tea-flavor spirane; 1 part of tea-scented ketone; 0.1 part of yerba mate absolute; 1 part of tree moss extract; 3 parts of benzyl benzoate; 0.05 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.05 parts of isophorone; 0.01 part of dihydrocoumarin; 0.02 part of plum extract; 0.02 part of Brazilian tobacco extract.
In some embodiments, the composition comprises the following raw materials in parts by mass: 0.8 parts of jasmine absolute; 0.4 parts of jasmine absolute; 2.5 parts of methyl dihydrojasmonate; 1.2 parts of cis-jasmone; 0.1 part of phenethyl alcohol; 3.3 parts of linalool; 0.04 parts of rose alcohol; 0.05 part of tea-flavor spirane; 1.2 parts of tea-scented ketone; 0.3 parts of yerba mate absolute; 1.5 parts of tree moss extract; 2 parts of benzyl benzoate; 0.03 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.02 parts of isophorone; 0.02 parts of dihydrocoumarin; 0.04 part of plum extract; 0.02 part of Brazilian tobacco extract.
In some embodiments, the composition comprises the following raw materials in parts by mass: 1.2 parts of jasmine absolute; 0.2 parts of jasmine absolute; 2.3 parts of methyl dihydrojasmonate; 1.2 parts of cis-jasmone; 0.12 parts of phenethyl alcohol; 3.5 parts of linalool; 0.05 parts of rose alcohol; 0.04 parts of tea-flavor spirane; 1.2 parts of tea-scented ketone; 0.2 parts of yerba mate absolute; 1 part of tree moss extract; 2.5 parts of benzyl benzoate; 0.05 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.03 parts of isophorone; 0.01 part of dihydrocoumarin; 0.03 part of plum extract; 0.03 part of Brazilian tobacco extract.
In a second aspect, the invention provides a preparation method of essence with jasmine tea characteristics, which comprises the following steps:
mixing flos Jasmini sambac absolute, methyl dihydrojasmonate, cis-jasmone, phenethyl alcohol, linalool, rosa alcohol, tea-leaf nutraceutica, paraguay tea absolute, tree moss extract, benzyl benzoate, 2,3, 5-trimethyl pyrazine, 2-acetyl pyridine, beta-dihydro-damascenone, isophorone, dihydrocoumarin, plum extract, brazilian tobacco extract and solvent, and standing in shade.
In some embodiments, the solvent is selected from at least one of propylene glycol, water, and ethanol.
In some embodiments, the mass ratio of solvent to perfume is 86-87: 13 to 14.
In a third aspect, the invention provides an application of the essence with jasmine tea characteristics in preparing tobacco products, in particular: the jasmine tea is used for tobacco and has the characteristic fragrance of jasmine tea.
The beneficial effects of the invention are that
(1) The fragrance of the essence formula with the jasmine tea characteristics can show the fragrance characteristics of the jasmine tea under different varieties and process conditions; for example, the jasmine tea has more prominent fragrance and sweet fragrance; the tea fragrance before the bright has obvious fragrance characteristics of flowers.
(2) The components of the essence formula with jasmine tea characteristics are completely prepared by adopting commercial monomer perfume, natural products such as jasmine tea extract and the like are not added, and unstable product quality caused by batch-to-batch differences and raw material quality differences is reduced to the greatest extent.
(3) The essence formula with the jasmine tea characteristics of the invention shows the fragrance characteristics of the jasmine tea on the basis of ensuring the fragrance of the characteristics of green tea, and improves the quality and identification degree of the product.
(4) The invention can be used as an independent essence, can be used after being diluted by an external solvent, has wider solvent selection range, can be used by both hydrophilic solvent and non-aqueous solvent, can fully satisfy the actual application of various production scenes, and has wider application prospect.
(5) The jasmine tea-specific essence formula is used in tobacco, can reflect the characteristic fragrance of jasmine tea, coordinates the fragrance of jasmine tea, flower fragrance and tobacco fragrance, enriches the tobacco fragrance, softens smoke, coordinates the tobacco fragrance and reduces irritation, and obtains satisfactory smoking feeling.
(6) The invention takes the tea aroma and the jasmine aroma as the principle, and through long-term research and experimental investigation on the fusion effect of different tea aroma, flower aroma and tobacco aroma, the invention discovers that: the tea aroma formed by tea aroma spirane, tea aroma ketone and yerba mate absolute can be well blended with jasmine aroma of jasmine absolute, small flower jasmine absolute, methyl dihydrojasmonate and cis-jasmonate, phenethyl alcohol, linalool and rosol with flower aroma, and tobacco herbal aroma generated by Brazil tobacco extract, isophorone and beta-dihydro damascone is coordinated by 2,3, 5-trimethyl pyrazine and 2-acetyl pyrazine; benzyl benzoate and the smoked plum extract soften smoke and reduce stimulation, and the effects of highlighting tea fragrance and jasmine fragrance, softening smoke, coordinating smoke fragrance and reducing stimulation can be achieved. The preparation method is simple, has strong practicability and is easy to popularize.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the invention.
Fig. 1 is a fragrance radar chart of a fragrance formulation featuring jasmine tea in the state of example 1.
Fig. 2 is a fragrance radar chart of the essence formulation featuring the pekoe jasmine tea of example 2.
Fig. 3 is a fragrance radar chart of the fragrance formulation featuring the silver needle jasmine tea of example 3.
Detailed Description
It should be noted that the following detailed description is exemplary and is intended to provide further explanation of the invention. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
The invention will now be described in further detail with reference to the following specific examples, which should be construed as illustrative rather than limiting.
In the examples below, each of the monomeric fragrances and solvents are commercially available products.
Example 1:
the essence formula with the jasmine tea characteristics comprises the following components in parts by mass: 1 part of jasmine absolute; 0.2 parts of jasmine absolute; 2.5 parts of methyl dihydrojasmonate; 1 part of cis-jasmone; 0.15 parts of phenethyl alcohol; 3 parts of linalool; 0.05 parts of rose alcohol; 0.04 parts of tea-flavor spirane; 1 part of tea-scented ketone; 0.1 part of yerba mate absolute; 1 part of tree moss extract; 3 parts of benzyl benzoate; 0.05 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.05 parts of isophorone; 0.01 part of dihydrocoumarin; 0.02 part of plum extract; 0.02 part of Brazilian tobacco extract. The components are weighed according to the proportion, added into a propylene glycol and 95% alcohol mixed solvent (the propylene glycol accounts for 30%, the alcohol accounts for 56.78%, and the total content of other spices accounts for 13.22% by mass), evenly mixed and placed at a shady and cool place for more than one week.
The jasmine tea characteristic essence of the embodiment has the characteristic aroma of the jasmine tea in Suzhou. The odor evaluation and classification table is shown in table 1 according to the classification of the odor and fragrance notes of jasmine tea essence. The final evaluation of each note gave the average of scores to 10 sensory evaluators. The evaluation was carried out by the flavor profile method with reference to the method specified in general theory of sensory analysis methods of GB/T10220-2012/ISO6658-2005, and the final evaluation analysis results are shown in FIG. 1.
As can be seen from the analysis result of the radar chart for evaluating the fragrance profile of the jasmine tea essence in fig. 1, the jasmine tea special essence of the embodiment has stronger floral fragrance (score of 6.5 points) and faint scent (score of 6.5 points), and also has obvious sweet fragrance (score of 4.5 points), baking fragrance (score of 3.5 points) and green fragrance (score of 3 points), and slightly fruit fragrance and bean fragrance. The characteristic essence note distribution characteristics of the jasmine tea accord with the note characteristics of the jasmine tea in Suzhou.
Table 1 odor evaluation scoring table
Note that: the minimum score unit was 0.5 points.
Example 2:
the essence formula with the jasmine tea characteristics comprises the following components in parts by mass: 0.8 parts of jasmine absolute; 0.4 parts of jasmine absolute; 2.5 parts of methyl dihydrojasmonate; 1.2 parts of cis-jasmone; 0.1 part of phenethyl alcohol; 3.3 parts of linalool; 0.04 parts of rose alcohol; 0.05 part of tea-flavor spirane; 1.2 parts of tea-scented ketone; 0.3 parts of yerba mate absolute; 1.5 parts of tree moss extract; 2 parts of benzyl benzoate; 0.03 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.02 parts of isophorone; 0.02 parts of dihydrocoumarin; 0.04 part of plum extract; 0.02 part of Brazilian tobacco extract. The components are weighed according to the proportion, added into a propylene glycol and 95% alcohol mixed solvent (the propylene glycol accounts for 30%, the alcohol accounts for 56.78%, and the total content of other spices accounts for 13.22% by mass), evenly mixed and placed at a shady and cool place for more than one week.
The jasmine tea characteristic essence provided by the embodiment has characteristic fragrance of pekoe jasmine tea. The evaluation of the odor and fragrance of jasmine tea essence is classified according to the odor and fragrance, and the classification table is the same as that of example 1, table 1. The final evaluation of each note gave the average of scores to 10 sensory evaluators. The evaluation was carried out by the flavor profile method with reference to the method specified in general theory of sensory analysis methods of GB/T10220-2012/ISO6658-2005, and the final evaluation analysis results are shown in FIG. 2.
As can be seen from the analysis result of the radar chart for evaluating the fragrance profile of the jasmine tea essence in fig. 2, the jasmine tea feature essence of the embodiment has strong fragrance (score 7 points) and floral fragrance (score 6 points), and has obvious sweet fragrance (score 5 points), baking fragrance (score 4 points) and green fragrance (3.5 points), and slightly fruity fragrance and bean fragrance. The characteristic essence note distribution characteristics of the jasmine tea accord with the note characteristics of the pekoe jasmine tea.
Example 3:
the essence formula with the jasmine tea characteristics comprises the following components in parts by mass: 1.2 parts of jasmine absolute; 0.2 parts of jasmine absolute; 2.3 parts of methyl dihydrojasmonate; 1.2 parts of cis-jasmone; 0.12 parts of phenethyl alcohol; 3.5 parts of linalool; 0.05 parts of rose alcohol; 0.04 parts of tea-flavor spirane; 1.2 parts of tea-scented ketone; 0.2 parts of yerba mate absolute; 1 part of tree moss extract; 2.5 parts of benzyl benzoate; 0.05 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.03 parts of isophorone; 0.01 part of dihydrocoumarin; 0.03 part of plum extract; 0.03 part of Brazilian tobacco extract. The components are weighed according to the proportion, added into a propylene glycol and 95% alcohol mixed solvent (the propylene glycol accounts for 30%, the alcohol accounts for 56.78%, and the total content of other spices accounts for 13.22% by mass), evenly mixed and placed at a shady and cool place for more than one week.
The jasmine tea characteristic essence of the embodiment has the characteristic fragrance of the silver needle jasmine tea. The evaluation of the odor and fragrance of jasmine tea essence is classified according to the odor and fragrance, and the classification table is the same as that of example 1, table 1. The final evaluation of each note gave the average of scores to 10 sensory evaluators. The evaluation was carried out by the flavor profile method with reference to the method specified in general theory of sensory analysis methods of GB/T10220-2012/ISO6658-2005, and the final evaluation analysis results are shown in FIG. 3.
As can be seen from the analysis result of the radar chart for evaluating the fragrance profile of the jasmine tea essence in fig. 3, the jasmine tea feature essence of the embodiment has strong fragrance (score 7 points) and floral fragrance (score 6 points), and has obvious green fragrance (score 4.5 points), sweet fragrance (score 3 points) and baking fragrance (score 3 points), and slightly fruity fragrance and bean fragrance. The characteristic essence note distribution characteristics of the jasmine tea accord with the note characteristics of the silver needle jasmine tea.
Example 4: use in tobacco
The jasmine tea essence prepared in the examples 1-3 is diluted by ethanol according to the amount of 0.35 per mill of tobacco shred, then added into the tobacco shred uniformly, added with equal amount of ethanol in a control group, rolled into cigarettes by the added tobacco shred and the control tobacco shred, placed into a constant temperature and humidity box, balanced for 24 hours at the humidity of 60% +/-2 and the temperature of 22 ℃ +/-2, and subjected to sensory evaluation, wherein the evaluation result is shown in the table 2. As can be seen from the smoking evaluation results, compared with the control cigarettes (blank), the cigarettes added with the prepared jasmine tea characteristic essence in the embodiment 1, the embodiment 2 and the embodiment 3 respectively have obvious Suzhou jasmine tea characteristic fragrance characteristics, pekoe jasmine tea characteristic fragrance characteristics and silver needle jasmine tea characteristic, meanwhile, the cigarette fragrance richness is obviously increased, the smoke coordination is improved, the irritation is reduced, the oral comfort is good, and the comprehensive sense of cigarette smoke is obviously improved.
Table 2 sensory evaluation results of jasmine tea feature essence
The above description is only of the preferred embodiments of the present invention and is not intended to limit the present invention, but various modifications and variations can be made to the present invention by those skilled in the art. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. The essence with the jasmine tea characteristics is characterized by comprising the following raw materials in parts by mass: 0.5-1.5 parts of jasmine absolute; 0.15-0.25 part of jasmine absolute; 2-3 parts of methyl dihydrojasmonate; 0.5-1.5 parts of cis-jasmone; 0.1-0.2 part of phenethyl alcohol; 2-4 parts of linalool; 0.04-0.06 part of rose alcohol; 0.03-0.05 part of tea-flavor spirane; 0.8-1.2 parts of tea-scented ketone; 0.08-0.12 parts of yerba mate absolute; 0.8-1.2 parts of tree moss extract; 2.5-3.5 parts of benzyl benzoate; 0.04-0.06 part of 2,3, 5-trimethyl pyrazine; 0.005-0.015 part of 2-acetylpyrazine; 0.005-0.015 part of 2-acetylpyridine; 0.005-0.015 part of beta-dihydro damascone; 0.04-0.06 part of isophorone; 0.005-0.015 part of dihydrocoumarin; 0.018-0.022 parts of plum extract; 0.018-0.022 parts of Brazilian tobacco extract.
2. The essence with jasmine tea characteristics according to claim 1, which is characterized by comprising the following raw materials in parts by mass: 1 part of jasmine absolute; 0.2 parts of jasmine absolute; 2.5 parts of methyl dihydrojasmonate; 1 part of cis-jasmone; 0.15 parts of phenethyl alcohol; 3 parts of linalool; 0.05 parts of rose alcohol; 0.04 parts of tea-flavor spirane; 1 part of tea-scented ketone; 0.1 part of yerba mate absolute; 1 part of tree moss extract; 3 parts of benzyl benzoate; 0.05 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.05 parts of isophorone; 0.01 part of dihydrocoumarin; 0.02 part of plum extract; 0.02 part of Brazilian tobacco extract.
3. The essence with jasmine tea characteristics according to claim 1, which is characterized by comprising the following raw materials in parts by mass: 0.8 parts of jasmine absolute; 0.4 parts of jasmine absolute; 2.5 parts of methyl dihydrojasmonate; 1.2 parts of cis-jasmone; 0.1 part of phenethyl alcohol; 3.3 parts of linalool; 0.04 parts of rose alcohol; 0.05 part of tea-flavor spirane; 1.2 parts of tea-scented ketone; 0.3 parts of yerba mate absolute; 1.5 parts of tree moss extract; 2 parts of benzyl benzoate; 0.03 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.02 parts of isophorone; 0.02 parts of dihydrocoumarin; 0.04 part of plum extract; 0.02 part of Brazilian tobacco extract.
4. The essence with jasmine tea characteristics according to claim 1, which is characterized by comprising the following raw materials in parts by mass: 1.2 parts of jasmine absolute; 0.2 parts of jasmine absolute; 2.3 parts of methyl dihydrojasmonate; 1.2 parts of cis-jasmone; 0.12 parts of phenethyl alcohol; 3.5 parts of linalool; 0.05 parts of rose alcohol; 0.04 parts of tea-flavor spirane; 1.2 parts of tea-scented ketone; 0.2 parts of yerba mate absolute; 1 part of tree moss extract; 2.5 parts of benzyl benzoate; 0.05 part of 2,3, 5-trimethyl pyrazine; 0.01 part of 2-acetylpyrazine; 0.01 part of 2-acetyl pyridine; 0.01 part of beta-damascone; 0.03 parts of isophorone; 0.01 part of dihydrocoumarin; 0.03 part of plum extract; 0.03 part of Brazilian tobacco extract.
5. The preparation method of the essence with jasmine tea characteristics is characterized by comprising the following steps:
mixing flos Jasmini sambac absolute, methyl dihydrojasmonate, cis-jasmone, phenethyl alcohol, linalool, rosa alcohol, tea-leaf nutraceutica, paraguay tea absolute, tree moss extract, benzyl benzoate, 2,3, 5-trimethyl pyrazine, 2-acetyl pyridine, beta-dihydro-damascenone, isophorone, dihydrocoumarin, plum extract, brazilian tobacco extract and solvent, and standing in shade.
6. The jasmine tea-distinctive essence of claim 5, wherein the solvent is selected from at least one of propylene glycol, water and ethanol.
7. The jasmine tea-distinctive essence according to claim 5, wherein the mass ratio of the solvent to the essence is 86-87: 13 to 14.
8. The jasmine tea-distinctive essence prepared by the method of any one of claims 5-7.
9. Use of the essence with jasmine tea characteristics as defined in any one of claims 1-4 and 8 in the preparation of tobacco products.
10. The use of claim 9, wherein the tobacco product includes, but is not limited to: burning cigarettes, heating non-burning cigarettes or electronic cigarettes;
or, when preparing the tobacco product, applying jasmine tea special essence to one or more of the following objects:
tobacco shred, slice, cigarette paper, cigarette lining paper, filter stick and electronic cigarette liquid.
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