CN117180963A - Composition with deodorizing and antibacterial effects and preparation method and application thereof - Google Patents
Composition with deodorizing and antibacterial effects and preparation method and application thereof Download PDFInfo
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- CN117180963A CN117180963A CN202311183114.XA CN202311183114A CN117180963A CN 117180963 A CN117180963 A CN 117180963A CN 202311183114 A CN202311183114 A CN 202311183114A CN 117180963 A CN117180963 A CN 117180963A
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- deodorizing
- hackberry
- deodorant
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- 239000000284 extract Substances 0.000 claims abstract description 68
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 30
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- GAWWVVGZMLGEIW-GNNYBVKZSA-L zinc ricinoleate Chemical compound [Zn+2].CCCCCC[C@@H](O)C\C=C/CCCCCCCC([O-])=O.CCCCCC[C@@H](O)C\C=C/CCCCCCCC([O-])=O GAWWVVGZMLGEIW-GNNYBVKZSA-L 0.000 claims abstract description 18
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Landscapes
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention discloses a composition with peculiar smell removal and antibacterial effects and a preparation method thereof. The composition comprises, by mass, 2-3% of green persimmon extract, 3-4% of zinc ricinoleate, 4-5% of ylang flower essential oil, 4-5% of rosemary oil, 1-2% of lavender essential oil, 2-3% of tea tree extract, 2-3% of hackberry leaf extract, 1-2% of scindapsus aureus flower extract, 1-2% of vitamin E and 71-80% of purified water. The composition provided by the invention has the advantages that the experiment effect proves that the composition has good deodorizing effect, can remove most of peculiar smell within 10min, still has good deodorizing effect after 24h, has antibacterial effect, can improve deodorizing effect, and has the advantages that the raw materials do not contain alcohol, essence and other components, the safety is good, and the application range is wide.
Description
Technical Field
The invention relates to a deodorant, in particular to a composition with deodorizing and antibacterial properties and a preparation method thereof.
Background
The air quality of the environment is one of the important factors affecting the health of human bodies and the thought and emotion, the smell of people is very sensitive, the odor can cause breathing disorder of people, headache, nausea, cardiovascular disease, nerve hypofunction and other diseases are induced, the health of people is greatly endangered, and the odor is mainly from places such as garbage transfer stations, garbage cans, garbage depositing points, garbage burning plants, sewage plants and the like in the daily life of people at present.
The deodorant in the market at present has various patterns, mainly comprises chemical deodorant, enzyme product deodorant, plant deodorant, microorganism deodorant and the like, and the first chemical deodorant represented by chlorine dioxide, hypochlorite, ferrous sulfate and the like has the main effects of oxidation sterilization, and the deodorization mechanism mainly comprises desulfurization, oxidation, condensation, addition reaction and the like of odor molecules. The bactericidal products have strong bactericidal effect, eradicate putrefying bacteria, and eradicate the root cause of odor generation, thereby assisting the function of serving as a deodorant, and being capable of treating the root cause. The disadvantage is that people contact the disinfectant closely, are easy to inhale into alveoli, can cause chronic injury, and have poor safety; the microbial deodorant adopts deodorant microorganisms obtained by screening to construct a composite microbial inoculum, has better control effect on malodor sources formed by perishable organic substances, has insignificant effect on deodorization and longer period; the plant deodorant is prepared by compounding an extract of oil, juice or extractum extracted from roots, stems, leaves or flowers of plants according to a certain formula, wherein effective molecules in the plant extract contain active groups such as chemical activity, biological activity, conjugated double bonds and the like, and can react with different peculiar smell substances such as acid-base reaction, catalytic oxidation reaction, lewis acid-base reaction, oxidation-reduction reaction and the like to promote the malodorous substances to change the original molecular structure and decompose into non-toxic and odorless micromolecules, thereby achieving the aim of thoroughly eradicating the odor.
The deodorant in the market has various patterns, and a large amount of deodorant can cover the odor on the pet body or in the environment by the fragrance emitted by the essence, so that the odor problem on the source head, especially the odor caused by biological spoilage and fermentation, can be solved, and the odor can be removed and maintained only for a temporary treatment but not for a permanent treatment. Some plant deodorant is added with natural components such as essential oil or extract obtained from plants, which can cause effect on part of odor molecules, but most of the effective components in the extract are small molecules, and zinc ricinoleate adsorbs odor and simultaneously adsorbs the extract components which should be used for deodorization.
In chinese patent application CN108245449a published at 7 and 6 in 2018, a pet deodorant is disclosed, which contains linalool acetate, citronellol, phenethyl alcohol, parachlorometaxylenol, lauryl methacrylate, linalool extract, polysorbate, citric acid, essence, alcohol, deionized water. The deodorant can be directly sprayed on pets, has remarkable deodorizing effect and long duration, and has sterilizing effect. However, the deodorizing essence added in the deodorizing agent can only cover the smell, and the preparation process is complex, so that the production cost is increased.
A deodorant with antibacterial effect is disclosed in Chinese patent application CN114831137A published at 8/2022. The composition comprises hydrogen peroxide solution with the concentration of 12-18 g/L, protocatechuic acid solution with the concentration of 0.1-2.6 g/L, a photocatalyst with the concentration of 0.01-0.3 g/L, dopamine solution with the concentration of 1.9-5.1 g/L and zinc ricinoleate with the concentration of 2-12 g/L. The deodorant has remarkable sterilizing and deodorizing effects, and can be used for sterilizing and eliminating odor. However, the disinfecting effect of the deodorant is not ensured in terms of safety because of the addition of chemical disinfecting components.
Therefore, development of a composition having an odor-removing and antibacterial effect, which can not only make efficient use of the components of the odor remover for a long period of time, but also sterilize indoor spaces and eradicate putrefying bacteria, has become an urgent need.
Disclosure of Invention
The invention aims to: in order to solve the problems in the background technology, the invention provides a deodorant which can remove the odor for a long time and has a sterilization function. The invention can solve the problems of bad deodorizing effect, temporary treatment, no permanent treatment, no sterilizing effect and the like of the market deodorizing products, can improve deodorizing effect, promote sterilizing quality, eradicate spoilage bacteria, and is suitable for market popularization.
The technical scheme is as follows: in order to achieve the above object, the present invention adopts the following technical scheme:
a composition with the effects of removing peculiar smell and resisting bacteria comprises the following raw materials in percentage by weight: 2-3% of green persimmon extract, 3-4% of zinc ricinoleate, 4-5% of ylang flower essential oil, 4-5% of rosemary oil, 1-2% of lavender essential oil, 2-3% of tea tree extract, 2-3% of hackberry leaf extract, 1-2% of scindapsus aureus extract, 1-2% of vitamin E and 71-80% of purified water.
The preparation method of the composition with the effects of removing peculiar smell and resisting bacteria comprises the following steps:
s1, mixing a green persimmon extract, a tea tree extract, a hackberry leaf extract, a scindapsus aureus extract and zinc ricinoleate according to weight percentage, and uniformly stirring by using a glass rod;
s1, mixing a green persimmon extract, a tea tree extract, a hackberry leaf extract, a scindapsus aureus extract and zinc ricinoleate according to weight percentage, and uniformly stirring by using a glass rod;
s2, transferring the mixture into a high-speed dispersion homogenizer, adding rosemary oil, ylang-orchid essential oil, lavender essential oil, vitamin E and purified water according to weight percentage, and dispersing and emulsifying at 40-60 ℃ for 2000-3000 r/min to obtain transparent liquid after 30-60 min;
s3, finally adding purified water to the specified mass to obtain the water-based paint.
As a preferred scheme, the magnolia leaf extract comprises flavone, polyphenol and triterpene, wherein the content of the flavone is 8-10%, the content of the polyphenol is 11-14%, the content of the triterpene is 7-9%, and the preparation method of the magnolia leaf extract comprises the following steps:
(1) Drying fresh leaves of Magnolia officinalis in a 45 deg.C drying oven for 48 hr to obtain dried leaves of Magnolia officinalis, pulverizing the dried leaves of Magnolia officinalis, and sieving with 60 mesh sieve;
(2) Mixing the powder with methanol at a feed-liquid ratio of 1:10 (g/mL), leaching at 60deg.C, stirring for 4 hr under electric power, centrifuging, and collecting supernatant (4000 r/min,15 min). Concentrating the supernatant at 40deg.C under vacuum, and recovering methanol to obtain folium Magnoliae officinalis extract.
As a preferred scheme, the tea tree extract comprises tea polyphenol, theanine and tea polysaccharide, wherein the content of the tea polyphenol is 18-30%, the content of the theanine is 2-3%, the content of the tea polysaccharide is 5-10%, and the preparation method of the tea tree extract comprises the following steps:
(1) Crushing tea leaves, adding the crushed tea leaves into an acid solution with the volume percentage of 10-20% for treatment for 30-35 min, adding sodium chloride, glutamic acid, tyrosine and gallate, reacting for 4h at the temperature of 80-100 ℃, and filtering after the reaction is finished;
(2) Distilling the filtrate obtained in the step (1) under reduced pressure, and controlling the temperature to be not higher than 60 ℃ to obtain the tea extract.
As a preferred scheme, the scindapsus aureus flower extract comprises scindapsus aureus flavone, wherein the scindapsus aureus flavone content is 15-18%, and the preparation method of the scindapsus aureus flower extract comprises the following steps:
(1) And (3) carrying out vacuum freeze drying on the cleaned scindapsus aureus flower in a light-proof environment, and crushing the dried scindapsus aureus flower in the vacuum environment to obtain scindapsus aureus pollen powder.
(2) Extracting with 80% ethanol solution at a feed-liquid ratio of 1:10 (g/mL) for 2 hr, centrifuging, and collecting supernatant (4000 r/min,15 min). Concentrating the supernatant at 40deg.C under vacuum, and recovering ethanol to obtain scindapsus aureus flower extract.
Preferably, the pH regulator is citric acid or sodium citrate or a combination thereof.
Through component screening, the composition of the invention is a novel safe and green deodorant which is prepared by taking green persimmon extract, tea tree extract, hackberry leaf extract and scindapsus aureus extract as main active components and ylang flower essential oil, rosemary oil and lavender essential oil as aroma components and being assisted by a pH value regulator through a scientific formula, and is stable, synchronous and efficient in sterilization and deodorization, free of irritation and convenient to use. The pH regulator is citric acid or sodium citrate or their combination
The green persimmon extract comprises green persimmon tannin, wherein the content of the green persimmon tannin is 5-8%. The green persimmon tannin is a polyphenol substance, has good antioxidant activity, has strong deodorization performance and strong deodorization performance on trimethylamine.
The tea tree extract comprises tea polyphenol, theanine and tea polysaccharide, wherein the content of the tea polyphenol is 18-30%, the content of the theanine is 2-3%, and the content of the tea polysaccharide is 5-10%. Tea polyphenols in tea tree extract have odor component methyl mercaptan (CH) generated by oral microorganism 3 SH) has good scavenging effect. The polysaccharide component of tea tree extract has a very strong affinity for ammonia and binds readily to it, thereby inhibiting the deleterious effects of ammonia and converting it to harmless nitrides. The scindapsus aureus flower extract comprises scindapsus aureus flavone, wherein the scindapsus aureus flavone content is 15-18%. The scindapsus aureus flavone has obvious antibacterial, bactericidal and antioxidant effects, and can eradicate putrefying bacteria from the source.
The hackberry leaf extract comprises 8-10% of flavone, 11-14% of polyphenol and 7-9% of triterpene. The polyphenol structure of the hackberry extract can react with proteins, polysaccharides, alkaloids and the like to change the physicochemical behaviors of the hackberry extract, so that the hackberry extract has unique advantages in the aspect of microbial inhibition. The zinc ricinoleate has the greatest advantages of low absorption toxicity through skin, mouth and respiratory tract, safe and reliable use, and can effectively eliminate main odor components of ammonia gas, hydrogen sulfide and organic sulfide and obviously reduce odor intensity.
Compared with the prior art, the invention has the following beneficial effects:
1. the deodorant provided by the invention has good deodorizing property on odor molecules, does not use chemical essence, and does not harm the smell of animals. The odor is mainly divided into ammonia gas, hydrogen sulfide, methyl mercaptan and the like, and various deodorizing components contained in the deodorant can effectively remove odor molecules through different action mechanisms such as capturing, adsorption and the like, so that the deodorizing efficiency is remarkably improved;
2. the deodorant spray of the invention has bactericidal properties and can radically remove odor. The flavonoid and phenolic compounds in various plant extracts contained in the deodorant have obvious antibacterial, sterilizing, antioxidant and antiseptic effects.
3. According to the invention, through screening and proportioning tests, the zinc ricinoleate can adsorb small molecular substances, but the fragrance substances of the yland essential oil and the rosemary essential oil can not be excessively adsorbed on the zinc ricinoleate in a characteristic concentration range, so that the superposition and synergy of the effects of the two essential oils can be realized, the zinc ricinoleate and peculiar smell molecules in the air fully generate chemical building reaction, and the deodorizing effect is enhanced.
4. The deodorant provided by the invention has good deodorizing effect, the deodorizing rate reaches more than 80%, the deodorizing duration is long, and the deodorizing effect can be maintained for more than 24 hours.
5. The deodorant disclosed by the invention is a safe and environment-friendly green product. The deodorant provided by the invention is prepared from nontoxic, harmless and non-irritating raw materials, does not contain alcohol, essence and other components, can be safely used for household deodorization, and has no harm to people, pets and the environment.
6. The deodorant disclosed by the invention is wide in application range. The deodorant can not only eliminate various peculiar smell and odor in the air, but also eliminate peculiar smell generated in the oral cavity and the body of a pet, and can also inhibit bacteria and sterilize, so that the application range of the deodorant is wider.
7. The deodorant of the invention can be filled according to a conventional method to obtain spray and other different application occasions.
Detailed description of the preferred embodiments
The technical solutions of the present invention will be clearly and completely described below in conjunction with specific embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Examples
1. A composition with deodorizing and antibacterial effects comprises the following components in percentage by mass:
2g of green persimmon extract, namely 20g
Tea tree extract 2%, i.e. 20g
2g of the extract of the hackberry leaves, namely 20g
1g of scindapsus aureus flower extract, namely 10g
3g of zinc ricinoleate, namely 30g
4 g of rosemary oil, i.e. 40g
4 g of elvan essential oil, namely 40g
Lavender essential oil 1g, i.e. 10g
Vitamin E1%, i.e. 10g
80% purified water, 800g
2. The preparation method of the composition with deodorizing effect comprises the following steps:
s1, mixing the green persimmon extract, the tea tree extract, the hackberry leaf extract, the scindapsus aureus extract and the zinc ricinoleate according to mass percent, and uniformly stirring by using a glass rod.
S2, transferring the mixture into a high-speed dispersion homogenizer, adding rosemary oil, ylang-orchid essential oil, lavender essential oil, vitamin E and purified water according to weight percentage, and dispersing and emulsifying at 40-60 ℃ for 2000-3000 r/min to obtain transparent liquid after 30-60 min;
s3, adding purified water to the specified quality, and obtaining the composition with the effects of removing peculiar smell and resisting bacteria.
Examples
1. A composition with deodorizing and antibacterial effects comprises the following components in percentage by mass:
3g of green persimmon extract, namely 30g
3g of tea tree extract, namely 30g
3g of the extract of the hackberry leaves, namely 30g
2g of scindapsus aureus flower extract, namely 20g
4 g of zinc ricinoleate, namely 40g
Rosemary oil 5%, i.e. 50g
5 g of Epilobium essential oil, namely 50g
2g of lavender essential oil, namely 20g
Vitamin E2%, i.e. 20g
71 g of purified water, i.e. 710g
2. The preparation method of the composition with deodorizing effect comprises the following steps:
step 1, mixing the green persimmon extract, the tea tree extract, the hackberry leaf extract, the scindapsus aureus extract and the zinc ricinoleate according to the mass percentage, and uniformly stirring by using a glass rod.
S1, mixing the green persimmon extract, the tea tree extract, the hackberry leaf extract, the scindapsus aureus extract and the zinc ricinoleate according to mass percent, and uniformly stirring by using a glass rod.
S2, transferring the mixture into a high-speed dispersion homogenizer, adding rosemary oil, ylang-orchid essential oil, lavender essential oil, vitamin E and purified water according to weight percentage, and dispersing and emulsifying at 40-60 ℃ for 2000-3000 r/min to obtain transparent liquid after 30-60 min;
s3, adding purified water to the specified quality, and obtaining the composition with the effects of removing peculiar smell and resisting bacteria.
Comparative example 1
The comparative example provides a composition with deodorizing effect and a preparation method thereof, which are different in that the composition does not contain a green persimmon extract (the content of which is complemented by vitamin E), and the other conditions are exactly the same as in example 1.
Comparative example 2
The comparative example provides a composition with deodorizing effect and a preparation method thereof, which are different in that the composition does not contain tea tree extract (the content of which is complemented by vitamin E), and the other conditions are exactly the same as in example 1.
Comparative example 3
The comparative example provides a composition with deodorizing effect and a preparation method thereof, which are different in that the composition does not contain the hackberry leaf extract (the content of which is complemented by vitamin E), and the other conditions are exactly the same as those of example 1.
Comparative example 4
The comparative example provides a composition with deodorizing effect and a preparation method thereof, which are different in that the composition does not contain scindapsus aureus extract (the content of which is complemented by vitamin E), and the rest conditions are exactly the same as those of example 1.
Comparative example 5
The comparative example provides a composition with deodorizing effect and a preparation method thereof, wherein the composition does not contain zinc ricinoleate (the content of which is complemented by vitamin E), and the rest conditions are exactly the same as those of example 1.
Comparative example 6
The comparative example provides a composition with deodorizing effect and a preparation method thereof, which are different in that rosemary oil (the content of which is complemented by vitamin E) is not contained in the composition, and the other conditions are exactly the same as in example 1.
Comparative example 7
The comparative example provides a composition with deodorizing effect and a preparation method thereof, wherein the composition does not contain ylang flower essential oil (the content of which is complemented by vitamin E), and the rest conditions are exactly the same as those of example 1.
Comparative example 8
The comparative example provides a composition with deodorizing effect and a preparation method thereof, which are different in that the composition does not contain lavender essential oil (the content of which is complemented by vitamin E), and the other conditions are exactly the same as in example 1.
Appearance inspection test of the deodorant, check whether the appearance of the deodorant is uniform, and whether layering or precipitation exists.
And (3) shaking the deodorant of examples 1 and 2 and comparative examples 1-8 in a primary packaging container fully and uniformly, taking not less than 500ml of primary liquid, taking 100m1 of primary liquid of the deodorant, placing the primary liquid of the deodorant in a 100ml cylinder with a stopper, and observing the appearance of the primary liquid of the deodorant spray after placing the primary liquid of the deodorant at 15-35 ℃ for 24 hours. The results of the appearance inspection test of the deodorant are shown in Table 1, and as can be seen from Table 1, the appearance properties of the deodorant of examples 1 and 2 and the deodorant of comparative examples 1 to 8 are uniform, and no delamination or precipitation occurs, and all meet the appearance inspection standards of liquids.
Table 1 visual inspection results for different formulations
| Different formulations | Appearance inspection |
| Example 1 | Uniform, free of delamination and precipitation |
| Example 2 | Uniform, free of delamination and precipitation |
| Comparative example 1 | Uniform, free of delamination and precipitation |
| Comparative example 2 | Uniform, free of delamination and precipitation |
| Comparative example 3 | Uniform, free of delamination and precipitation |
| Comparative example 4 | Uniform, free of delamination and precipitation |
| Comparative example 5 | Uniform, free of delamination and precipitation |
| Comparative example 6 | Uniform, free of delamination and precipitation |
| Comparative example 7 | Uniform, free of delamination and precipitation |
| Comparative example 8 | Uniform, free of delamination and precipitation |
And (3) detecting the PH value of the deodorant stock solution by a PH value investigation test of the deodorant.
The deodorant of examples 1 and 2 and comparative examples 1-8 are sufficiently and uniformly shaken in an original packaging container, a certain amount of deodorant stock solution is taken, the pH value of the deodorant spray stock solution is tested by a pH meter under the room temperature condition (25+/-2 ℃), the pH value is accurate to 0.1pH unit, the test results are shown in table 2, and the pH values of the deodorant stock solutions of examples 1 and 2 and comparative examples 1-8 are all neutral and are safe to use, have no corrosiveness and can be safely used for spraying oral cavities, bodies and environments as shown in table 2.
TABLE 2 pH detection results for different formulations
| Different formulations | PH value |
| Example 1 | 7.0 |
| Example 2 | 7.1 |
| Comparative example 1 | 7.1 |
| Comparative example 2 | 6.9 |
| Comparative example 3 | 7.2 |
| Comparative example 4 | 7.1 |
| Comparative example 5 | 6.8 |
| Comparative example 6 | 7.0 |
| Comparative example 7 | 7.2 |
| Comparative example 8 | 6.9 |
Deodorizing effect test of deodorizing spray the deodorizing effect of each of the deodorizing agent formulations of examples 1 and 2 and comparative examples 1-8 was evaluated by deodorizing effects on several common odor molecules.
The test reagents used in the deodorization effect test of the deodorization spray are ammonia water, hydrogen sulfide, methyl mercaptan, dimethyl sulfide and dimethyl disulfide. The test instruments used in the deodorant effect test of the deodorant are ammonia, a hydrogen sulfide gas detection tube, an HP5840A gas chromatograph, a 5.5L glass bottle and a syringe.
Odor instrument analysis method
Ammonia gas, hydrogen sulfide and 3 organic sulfides with different concentrations are respectively prepared in a 5.5L glass bottle, the deodorizing effect is evaluated by absorbing and fixing the ammonia gas with boric acid, and the deodorizing effect of the deodorizing spray on the hydrogen sulfide, methyl mercaptan, dimethyl sulfide and dimethyl disulfide is evaluated by a headspace gas phase chromatography. Gas chromatography conditions: column DB-1, sample inlet temperature 170 ℃, column temperature 40 ℃, tester 250 ℃, ammonia gas (60 ml/min) and other gases, hydrogen gas as fuel, pressure 1kg/cm 2 Air supporting combustion, pressure 1.5kg/cm 2 . 0.01g of sample is weighed and dissolved in a headspace bottle with 1ml of water, a certain amount of odor substances are injected in a sealing way, and the mixture is left for 1h to suck 1ml of headspace sample. The concentration of each gas before and after 1 hour of action was measured, the elimination rate was calculated, and the test was performed as a blank (purified water).
As shown in Table 3, the deodorizing effects of the single odor molecules are shown in Table 3, and examples 1 and 2 can effectively and rapidly remove the odors such as ammonia, hydrogen sulfide, methyl mercaptan, methyl sulfide, dimethyl disulfide and the like, so that the eliminating rate of the 5 single odor molecules can reach more than 82%, and the deodorizing effects are superior to those of comparative examples 1-8, which shows that the cooperation of the components of the invention has good synergistic deodorizing effects.
Table 3 deodorant effect of different formulations on 5 malodors alone
The collected pollution sources such as saliva and feces of the pets are sprayed respectively by using the above examples 1 and 2 and comparative examples 1-8, and 10 normal-smell panelists are selected to score after 10min and 24h, and the score is classified as qualified at 60-80, and the score is classified as good at 80-90, and the score is excellent at 90 or more, and the score is disqualified at less than 60, and the disqualification is regarded as bad deodorizing effect, and the specific experimental results are shown in table 4 and table 5. From the sensory experiments, the effect of the example 2 is optimal in the experiments of acting on the pollution source for 10min and 24h, and most of the odor can be removed in 10min in the examples 1 and 2, and even after 24h, the example 2 still has good deodorizing effect, so that the deodorizing effect is proved to be rapid and long-lasting; through the comparison experiment, the deodorizing effect is reduced when any component in the composition components is absent.
TABLE 4 evaluation score after 10min of the Effect of deodorant on contamination Source
TABLE 5 evaluation score Table after 24h of deodorant effect on contamination source
| Evaluation person | No. 1 | No. 2 | No. 3 | No. 4 | No. 5 | No. 6 | No. 7 | No. 8 | No. 9 | No. 10 |
| Example 1 | 90 | 88 | 86 | 83 | 83 | 87 | 85 | 83 | 84 | 83 |
| Example 2 | 91 | 90 | 88 | 84 | 85 | 90 | 86 | 95 | 86 | 85 |
| Comparative example 1 | 86 | 83 | 81 | 80 | 78 | 84 | 81 | 75 | 80 | 80 |
| Comparative example 2 | 83 | 84 | 82 | 78 | 80 | 80 | 79 | 76 | 75 | 80 |
| Comparative example 3 | 82 | 84 | 82 | 76 | 74 | 83 | 81 | 80 | 76 | 79 |
| Comparative example 4 | 87 | 84 | 84 | 78 | 79 | 82 | 80 | 75 | 76 | 81 |
| Comparative example 5 | 76 | 77 | 78 | 72 | 71 | 76 | 73 | 70 | 71 | 70 |
| Comparative example 6 | 87 | 82 | 80 | 78 | 76 | 76 | 77 | 73 | 71 | 70 |
| Comparative example 7 | 82 | 81 | 78 | 74 | 75 | 76 | 75 | 72 | 74 | 71 |
| Comparative example 8 | 85 | 86 | 81 | 80 | 79 | 81 | 82 | 80 | 76 | 80 |
The antibacterial and bacteriostatic effects of the composition were tested by referring to the QB/T2738-2012 evaluation method, and the test bacteria were staphylococcus aureus, escherichia coli and staphylococcus albus.
(1) Preparation of test bacterial suspensions
(1) Taking freeze-dried strain, adding a proper amount of nutrient broth by a capillary suction tube, and gently blowing and sucking for several times to melt and disperse the strain. Taking a test tube containing 5.0mL of nutrient broth culture medium, dripping a little strain suspension, and culturing at 37 ℃ for 24 hours; inoculating the bacterial suspension of the 1 st generation culture on a nutrient agar culture medium plate by streaking, and culturing for 24 hours at 37 ℃; picking a typical colony in the 2 nd generation culture, inoculating the typical colony to a nutrient agar inclined plane, and culturing for 24 hours at 37 ℃ to obtain a 3 rd generation culture;
(2) taking a 3 rd generation fresh culture, sucking 3-5 mL by a suction pipe, adding into a test tube, repeatedly blowing and sucking to wash lawn, then transferring the washing liquid into another sterile test tube by the suction pipe, mixing for 20s by an electric mixer, or vibrating on the palm for 80 times to uniformly suspend bacteria;
(3) the bacterial suspension prepared preliminarily is subjected to rough measurement on the bacterial concentration, then diluted to the required concentration for use, and stored in a refrigerator at 4 ℃ for standby.
(4) Diluting the test bacterial suspension with PBS, and recovering bacterial count to 1×10 4 ~9x10 4 cfu/mL；
(2) Determination of the bacteriostatic Rate
The test samples of the present invention (examples 1 and 2, comparative examples 1 to 8) were diluted with water for injection to a prescribed concentration (0.01 mg/mL), and then 5.0mL of the test sample stock solution was sucked and placed in a sterilized test tube, and the temperature was kept constant at 30℃for 5 minutes. Then sucking 0.1mL of test bacterial liquid, adding the test bacterial liquid into a test tube containing 5.0mL of sample stock solution, quickly and uniformly mixing, and timing immediately; after 3min of action, 0.5mL of mixed solution is taken and added into a PBS test tube containing 4.5mL of sterilized PBS, the mixture is fully and uniformly mixed, after 10min of standing, 1mL of sample solution is sucked, the sample solution is placed into a sterilization plate, 15mL of nutrient agar medium cooled to 40-45 ℃ is used as pouring, the plate is rotated to be fully and uniformly, the plate is turned over after agar solidification, after 48h of culture at 37 ℃, viable bacteria colony counting is carried out, and the bacteriostasis rate is calculated. The test sample was replaced with PBS solution, and the procedure was followed as described above to serve as a control. The results of the antibacterial performance test are shown in table 2, and indicate that the antibacterial effect of examples 1 and 2 is higher than that of comparative examples 1 to 8, and the antibacterial effect of example 2 is better than that of example 1.
Experiments were repeated 3 times and averaged.
TABLE 6 antibacterial Property test results
While the invention has been described in detail in the general context and with reference to specific embodiments thereof, it will be apparent to one skilled in the art that modifications and improvements can be made thereto. Such modifications and improvements are therefore intended to be within the scope of this invention as claimed.
Claims (9)
1. The composition with the effects of removing peculiar smell and resisting bacteria is characterized by comprising the following raw materials in percentage by weight: 2-3% of green persimmon extract, 3-4% of zinc ricinoleate, 4-5% of ylang flower essential oil, 4-5% of rosemary oil, 1-2% of lavender essential oil, 2-3% of tea tree extract, 2-3% of hackberry leaf extract, 1-2% of scindapsus aureus extract, 1-2% of vitamin E and 71-80% of purified water.
2. A method for preparing the composition with deodorizing and antibacterial effects according to claim 1, characterized by comprising the following steps:
s1, mixing a green persimmon extract, a tea tree extract, a hackberry leaf extract, a scindapsus aureus extract and zinc ricinoleate according to weight percentage, and uniformly stirring by using a glass rod;
s2, transferring the mixture into a high-speed dispersion homogenizer, adding rosemary oil, ylang-orchid essential oil, lavender essential oil, vitamin E and purified water according to weight percentage, and dispersing and emulsifying at 40-60 ℃ for 2000-3000 r/min to obtain transparent liquid after 30-60 min;
s3, finally adding purified water to the specified mass to obtain the water-based paint.
3. The composition with deodorizing and antibacterial effects according to claim 1, wherein the preparation method of the green persimmon extract is as follows:
(1) Soaking and cleaning the green persimmons which are not turned into yellow with warm water at the temperature of 30-40 ℃ to remove impurities;
(2) Taking a certain amount of green persimmons, stirring with a stirrer, adding ethanol with a certain proportion as an extraction solvent, homogenizing, placing in a constant-temperature water bath, heating, refluxing for extraction, filtering to obtain filtrate, and vacuum concentrating to obtain the green persimmons extract.
4. The composition with deodorizing and antibacterial effects according to claim 1, wherein the process for preparing the extract of the hackberry leaves is as follows:
(1) Drying fresh hackberry leaves in a drying oven at 40-45 ℃ for 24-48 hours to obtain dried hackberry leaves, crushing the dried hackberry leaves and sieving the crushed hackberry leaves with a 60-mesh sieve;
(2) Mixing the powder of the leaf of Magnolia officinalis with methanol at a feed-liquid ratio of 1:10, leaching at 60deg.C, stirring electrically for 4 hr, centrifuging to collect supernatant, vacuum concentrating the supernatant at 40deg.C, and recovering methanol to obtain leaf extract.
5. The composition with deodorizing and antibacterial effects according to claim 1, wherein the tea tree extract is prepared by the following method:
(1) Crushing tea leaves, adding the crushed tea leaves into an acid solution with the volume percentage of 10-20% for treatment for 30-35 min, adding sodium chloride, glutamic acid, tyrosine and gallate, reacting for 4h at the temperature of 80-100 ℃, and filtering after the reaction is finished;
(2) Distilling the filtrate obtained in the step (1) under reduced pressure, and controlling the temperature to be not higher than 60 ℃ to obtain the tea tree extract.
6. The composition with deodorizing and antibacterial effects according to claim 1, wherein the preparation method of the scindapsus aureus extract is as follows:
(1) Vacuum freeze drying cleaned scindapsus aureus flower in a dark environment, and pulverizing in a vacuum environment to obtain scindapsus aureus pollen powder;
(2) Reflux-extracting with 80% ethanol solution at a ratio of 1:10 for 2 hr, centrifuging to collect supernatant, vacuum concentrating the supernatant at 40deg.C, and recovering ethanol to obtain scindapsus aureus flower extract.
7. Use of the composition of claim 1 for the preparation of a deodorant.
8. Use according to claim 8, of a composition for the preparation of a deodorant for the removal of hydrogen sulphide, ammonia or methyl mercaptan (ether).
9. Use of the composition of claim 1 for the preparation of an antibacterial agent.
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| CN117180963A true CN117180963A (en) | 2023-12-08 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN120531849A (en) * | 2025-07-28 | 2025-08-26 | 广东工业大学 | Composition with synergistic antibacterial and deodorizing functions and its application |
| CN120771096A (en) * | 2025-08-28 | 2025-10-14 | 赛维泰(广州)健康药业有限公司 | Composition for repairing oral soft tissue injury |
-
2023
- 2023-09-14 CN CN202311183114.XA patent/CN117180963A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN120531849A (en) * | 2025-07-28 | 2025-08-26 | 广东工业大学 | Composition with synergistic antibacterial and deodorizing functions and its application |
| CN120771096A (en) * | 2025-08-28 | 2025-10-14 | 赛维泰(广州)健康药业有限公司 | Composition for repairing oral soft tissue injury |
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