CN116726593A - Purification method of emamectin benzoate - Google Patents
Purification method of emamectin benzoate Download PDFInfo
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- CN116726593A CN116726593A CN202310710311.6A CN202310710311A CN116726593A CN 116726593 A CN116726593 A CN 116726593A CN 202310710311 A CN202310710311 A CN 202310710311A CN 116726593 A CN116726593 A CN 116726593A
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H17/00—Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
- C07H17/04—Heterocyclic radicals containing only oxygen as ring hetero atoms
- C07H17/08—Hetero rings containing eight or more ring members, e.g. erythromycins
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/62—Regenerating the filter material in the filter
- B01D29/64—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element
- B01D29/6469—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers
- B01D29/6484—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers with a translatory movement with respect to the filtering element
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/62—Regenerating the filter material in the filter
- B01D29/70—Regenerating the filter material in the filter by forces created by movement of the filter element
- B01D29/72—Regenerating the filter material in the filter by forces created by movement of the filter element involving vibrations
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/003—Filters in combination with devices for the removal of liquids
- B01D36/006—Purge means
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
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Abstract
Description
技术领域Technical field
本发明涉及甲维盐提取技术领域,具体为一种甲维盐的提纯方法。The present invention relates to the technical field of extracting emamectin salt, specifically a method for purifying emamectin salt.
背景技术Background technique
甲维盐一般指从发酵产品阿维菌素B1开始合成的一种新型高效半合成抗生素杀虫剂,它具有超高效、低毒(制剂近无毒)、低残留、无公害等生物农药的特点,广泛用于蔬菜、果树、棉花等农作物上的多种害虫的防治。Emamectin salt generally refers to a new type of high-efficiency semi-synthetic antibiotic pesticide synthesized from the fermentation product avermectin B1. It has the characteristics of ultra-high efficiency, low toxicity (the preparation is nearly non-toxic), low residue, and no pollution. Features, widely used in the prevention and control of various pests on vegetables, fruit trees, cotton and other crops.
现有的申请号为201610348559.2相关某项技术实施的过程中存在以下几个问题:The existing application number is 201610348559.2. There are the following problems in the implementation of a certain technology:
1.原文中所述取甲氨基阿维菌素提取液(浓度700mg/ml)500ml,升温至38±2℃,按15%(V/V)量加入氯化钠饱和溶液75ml,充分搅拌40分钟,静置20分钟,分水、过滤,过滤步骤中当过滤后滤网顶部杂质的处理方法一般为过滤结束后打开装置,去除滤网进行清洗处理,此专利中获取滤液结束后并未对杂质进行清理,常规处理方法使整个过程中滤网的损耗增加,在清洗滤网或者更换滤网时不仅费时费力,还要拆卸滤网,效率低下影响整个制备过程。1. As described in the original text, take 500 ml of mebamectin extract (concentration 700 mg/ml), heat it to 38±2°C, add 75 ml of saturated sodium chloride solution at 15% (V/V), and stir thoroughly for 40 minutes, let it stand for 20 minutes, separate water, and filter. In the filtration step, the method for dealing with impurities on the top of the filter after filtration is generally to open the device after filtration, remove the filter for cleaning. In this patent, there is no treatment after the filtrate is obtained. Impurities must be cleaned. Conventional treatment methods increase the loss of the filter during the entire process. Cleaning or replacing the filter is not only time-consuming and laborious, but also requires disassembly of the filter. This low efficiency affects the entire preparation process.
2.将以上洗脱液,加入5000ml三口反应瓶,控制温度60±2°C,减压蒸馏,除去二氯乙烷,得到甲氨基阿维菌素浓缩物,在减压蒸馏过程中,会出现冷却过后的水蒸气凝结成的水滴,顺着蒸汽管回流进反应瓶中,使得到的溶液溶解度并不准确,影响整个制备过程,此专利中并未解决这一问题,一般采用专用蒸馏器进行蒸馏,但是蒸馏器价格昂贵,反应结束后预热依然会使水滴凝结在管口并滴落,造成制备的溶液溶解度不准确,在后续制备过程中容易影响甲维盐的提取,造成产品质量问题。2. Add the above eluate into a 5000ml three-neck reaction bottle, control the temperature to 60±2°C, distill under reduced pressure, remove the dichloroethane, and obtain the methylaminoavermectin concentrate. During the reduced pressure distillation process, The water vapor condenses into water droplets after cooling, and flows back into the reaction bottle along the steam pipe, making the solubility of the solution inaccurate and affecting the entire preparation process. This problem is not solved in this patent, and a special distiller is generally used. Distillation is carried out, but the distiller is expensive. Preheating after the reaction will still cause water droplets to condense on the mouth of the tube and drip, resulting in inaccurate solubility of the prepared solution. In the subsequent preparation process, it is easy to affect the extraction of emamectin salt and affect the quality of the product. question.
发明内容Contents of the invention
本发明的目的在于提供一种甲维盐的提纯方法,以解决上述背景技术中提出的问题。The object of the present invention is to provide a method for purifying emamectin salt to solve the problems raised in the above background technology.
为实现上述目的,本发明提供如下技术方案:一种甲维盐的提纯方法,包括装置主体,所述装置主体前端固定连接有过滤单元,所述过滤单元内部固定设置有清理单元,所述清理单元前端固定设置有震动单元,所述装置主体底端固定设置有三通容器,所述过滤单元后端固定设置有密封单元,所述密封单元后端固定设置有隔水单元,所述隔水单元顶端固定设置有蒸馏单元,所述三通容器底端固定设置有加热装置。In order to achieve the above object, the present invention provides the following technical solution: a method for purifying emamectin salt, including a device body, a filter unit fixedly connected to the front end of the device body, a cleaning unit fixedly provided inside the filter unit, and the cleaning unit A vibration unit is fixed at the front end of the unit, a three-way container is fixed at the bottom end of the device body, a sealing unit is fixed at the rear end of the filter unit, and a water-isolating unit is fixed at the rear end of the sealing unit. The water-isolating unit A distillation unit is fixedly installed at the top, and a heating device is fixedly installed at the bottom of the three-way container.
优选的,所述过滤单元包括外壳,所述外壳内部固定设置有流通底板,所述过滤单元顶端固定设置有入液口,所述流通底板底端固定连接有输液管。Preferably, the filter unit includes a shell, a circulation bottom plate is fixed inside the shell, a liquid inlet is fixed at the top of the filter unit, and an infusion tube is fixedly connected to the bottom end of the circulation bottom plate.
优选的,所述清理单元包括滤网,所述滤网顶端固定连接有圆弧顶,所述滤网内部顶端滑动连接有清理圆板,所述清理圆板顶端固定连接有横移滑板,所述横移滑板顶端滑动连接有清理电机,所述清理电机和横移滑板之间固定连接有清理弹簧,所述清理电机输出端固定连接有转动轮,所述转动轮外侧滑动连接有清理架,所述清理电机底端固定连接有伸缩电线,所述伸缩电线底端固定连接有杂质感应器,所述滤网底端转动设置有两块弹力挡板,所述弹力挡板底端固定设置有回收仓。Preferably, the cleaning unit includes a filter screen, a circular arc top is fixedly connected to the top of the filter screen, a cleaning circular plate is slidingly connected to the internal top of the filter screen, and a traverse slide plate is fixedly connected to the top of the cleaning circular plate, so A cleaning motor is slidingly connected to the top of the traversing sliding plate. A cleaning spring is fixedly connected between the cleaning motor and the traversing sliding plate. A rotating wheel is fixedly connected to the output end of the cleaning motor. A cleaning frame is slidingly connected to the outside of the rotating wheel. The bottom end of the cleaning motor is fixedly connected with a telescopic wire, and the bottom end of the telescopic wire is fixedly connected with an impurity sensor. The bottom end of the filter screen is rotated with two elastic baffles, and the bottom end of the elastic baffle is fixedly equipped with Recycling bin.
优选的,所述震动单元包括震动顶板,所述震动顶板底端滑动连接有震动凸轮,所述震动凸轮侧面固定连接有重力弹簧杆,所述重力弹簧杆侧端固定连接有震动电机,所述重力弹簧杆内侧固定设置有震动齿轮,所述震动齿轮顶端固定连接有震动卡板。Preferably, the vibration unit includes a vibration top plate, a vibration cam is slidably connected to the bottom end of the vibration top plate, a gravity spring rod is fixedly connected to the side of the vibration cam, and a vibration motor is fixedly connected to the side end of the gravity spring rod. A vibration gear is fixed inside the gravity spring rod, and a vibration clamping plate is fixedly connected to the top of the vibration gear.
优选的,所述密封单元包括密封管,所述密封管顶部转动连接有密封扇叶,所述密封扇叶底端固定连接有扇叶伞齿,所述扇叶伞齿侧端啮合连接有传动伞齿,所述传动伞齿侧端固定连接有动力伞齿,所述动力伞齿侧端啮合连接有密封顶齿,所述密封顶齿底端固定连接有密封转板,所述密封转板底端转动连接有复位转杆,所述密封转板底面滑动连接有升降板,所述升降板底端转动连接有辅助板,所述辅助板底端转动连接有平衡转板,所述平衡转板侧端转动连接有浮力块,所述平衡转板中部转动连接有固定板,所述固定板底端固定连接在三通容器底部。Preferably, the sealing unit includes a sealing tube, the top of the sealing tube is rotatably connected to a sealing fan blade, the bottom end of the sealing fan blade is fixedly connected to a fan blade bevel gear, and the side end of the fan blade bevel gear is meshedly connected to a transmission. Bevel teeth, the side ends of the transmission bevel teeth are fixedly connected with power bevel teeth, the side ends of the power bevel teeth are meshed with sealing top teeth, the bottom end of the sealing top teeth is fixedly connected with a sealing rotating plate, the sealing rotating plate A reset rotating rod is rotatably connected to the bottom end, a lifting plate is slidingly connected to the bottom surface of the sealing rotary plate, an auxiliary plate is rotatably connected to the bottom end of the lifting plate, and a balance rotary plate is rotatably connected to the bottom end of the auxiliary plate. A buoyancy block is rotatably connected to the side end of the plate, a fixed plate is rotatably connected to the middle part of the balance rotating plate, and the bottom end of the fixed plate is fixedly connected to the bottom of the tee container.
优选的,所述隔水单元包括隔水盘,所述隔水盘中央固定设置有通气口,所述隔水盘外侧滑动连接有支撑外壁,所述隔水盘底端固定连接有滑动盘,所述滑动盘周围均匀地滑动连接有四个辅助圆柱,所述隔水盘底端固定连接有复位弹簧,所述隔水单元固定设置于三通容器和蒸馏单元之间。Preferably, the water barrier unit includes a water barrier, a vent is fixed in the center of the water barrier, a supporting outer wall is slidably connected to the outside of the water barrier, and a sliding plate is fixedly connected to the bottom end of the water barrier. Four auxiliary cylinders are evenly and slidingly connected around the sliding plate, a return spring is fixedly connected to the bottom end of the water-isolating plate, and the water-isolating unit is fixedly arranged between the tee container and the distillation unit.
(一)有益效果(1) Beneficial effects
与现有技术相比,本发明提供了一种甲维盐的提纯方法,具备以下有益效果:Compared with the existing technology, the present invention provides a method for purifying emamectin salt, which has the following beneficial effects:
1、该甲维盐的提纯方法,通过清理单元的工作,可以帮助过滤过程中的滤网在过滤完成后对滤网内部杂质进行清理,帮助滤网清理掉杂质的同时还能够恢复滤网的过滤功能,使操作人员不必停止过滤过程或者打开装置对滤网进行清理或者更换,就能够完成滤网清理,清理单元还可以延长滤网的使用寿命,减少维修成本。1. The purification method of emamectin salt can help the filter during the filtration process to clean the impurities inside the filter after the filtration is completed through the work of the cleaning unit. It can help the filter to clean up the impurities and also restore the filter's function. The filtration function allows operators to complete filter cleaning without stopping the filtration process or opening the device to clean or replace the filter. The cleaning unit can also extend the service life of the filter and reduce maintenance costs.
2、该甲维盐的提纯方法,通过密封单元和隔水单元的相互配合,可以在装置蒸馏的过程中防止顶部液化的水滴回流到容器内部,同时也能防止容器口凝结出水滴,避免液化的水滴回流造成溶液溶解度不准确,最终导致准备的产物质量产生偏差的问题。2. The purification method of the emamectin salt, through the cooperation of the sealing unit and the water isolation unit, can prevent the liquefied water droplets at the top from flowing back into the container during the distillation process of the device, and can also prevent water droplets from condensing out of the container mouth and avoid liquefaction. The reflux of water droplets causes inaccurate solubility of the solution, which ultimately leads to deviations in the quality of the prepared product.
3、该甲维盐的提纯方法,在制备过程中,通过震动单元的工作,将滤网内部无法被清理单元清理的残留的少量杂质进行震动清理,是这种特殊情况下,能够保持滤网进一步清洁,提高滤网的过滤功能和使用时限,进一步帮助减少更换维修的成本。3. The purification method of the emamectin salt, during the preparation process, uses the work of the vibration unit to vibrate and clean the small amount of residual impurities inside the filter that cannot be cleaned by the cleaning unit. In this special case, the filter can be maintained Further cleaning improves the filtration function and service life of the filter, further helping to reduce the cost of replacement and maintenance.
附图说明Description of drawings
下面结合附图和实施例对本发明进一步说明。The present invention will be further described below in conjunction with the accompanying drawings and examples.
图1为正侧面立体结构图。Figure 1 is a front and side perspective structural view.
图2为侧面立体结构图。Figure 2 is a side perspective structural view.
图3为过滤单元立体结构图。Figure 3 is a three-dimensional structural diagram of the filter unit.
图4为图3中A处的局部放大图。Figure 4 is a partial enlarged view of position A in Figure 3.
图5为密封单元立体结构图。Figure 5 is a three-dimensional structural view of the sealing unit.
图6为图5中B处的局部放大图图。Figure 6 is a partial enlarged view of position B in Figure 5.
图7为隔水单元立体结构图。Figure 7 is a three-dimensional structural diagram of the water isolation unit.
图8为震动单元立体结构图。Figure 8 is a three-dimensional structural diagram of the vibration unit.
图9为震动单元正面平面图。Figure 9 is a front plan view of the vibration unit.
图中:1、装置主体;101、三通容器;102、蒸馏单元;103、加热装置;2、过滤单元;201、外壳;202、流通底板;203、入液口;204、输液管;3、清理单元;301、滤网;302、圆弧顶;303、清理圆板;304、横移滑板;305、清理电机;306、清理弹簧;307、转动轮;308、清理架;309、伸缩电线;310、杂质感应器;311、弹力挡板;312、回收仓;4、震动单元;401、震动顶板;402、震动凸轮;403、重力弹簧杆;404、震动电机;405、震动齿轮;406、震动卡板;5、密封单元;501、密封管;502、密封扇叶;503、扇叶伞齿;504、传动伞齿;505、动力伞齿;506、密封顶齿;507、密封转板;508、复位转杆;509、升降板;510、辅助板;511、平衡转板;512、浮力块;513、固定板;6、隔水单元;601、隔水盘;602、通气口;603、支撑外壁;604、滑动盘;605、辅助圆柱;606、复位弹簧。In the figure: 1. Main body of the device; 101. Three-way container; 102. Distillation unit; 103. Heating device; 2. Filtration unit; 201. Shell; 202. Circulation bottom plate; 203. Liquid inlet; 204. Infusion tube; 3 , cleaning unit; 301, filter; 302, arc top; 303, cleaning disc; 304, traverse slide; 305, cleaning motor; 306, cleaning spring; 307, rotating wheel; 308, cleaning frame; 309, telescopic Wire; 310, impurity sensor; 311, elastic baffle; 312, recovery bin; 4, vibration unit; 401, vibration top plate; 402, vibration cam; 403, gravity spring rod; 404, vibration motor; 405, vibration gear; 406. Vibration card plate; 5. Sealing unit; 501. Sealing tube; 502. Sealing fan blade; 503. Fan blade bevel gear; 504. Transmission bevel gear; 505. Power bevel gear; 506. Sealing top gear; 507. Sealing Rotary plate; 508, reset rotary rod; 509, lifting plate; 510, auxiliary plate; 511, balance rotating plate; 512, buoyancy block; 513, fixed plate; 6, water isolation unit; 601, water isolation plate; 602, ventilation mouth; 603, support outer wall; 604, sliding plate; 605, auxiliary cylinder; 606, return spring.
具体实施方式Detailed ways
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only some of the embodiments of the present invention, rather than all the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts fall within the scope of protection of the present invention.
请参阅图1,一种甲维盐的提纯方法,包括装置主体1,所述装置主体1前端固定连接有过滤单元2,所述过滤单元2内部固定设置有清理单元3,所述清理单元3前端固定设置有震动单元4,所述装置主体1底端固定设置有三通容器101,所述过滤单元2后端固定设置有密封单元5,所述密封单元5后端固定设置有隔水单元6,所述隔水单元6顶端固定设置有蒸馏单元102,所述三通容器101底端固定设置有加热装置103。Please refer to Figure 1. A method for purifying emamectin salt, including a device body 1. A filter unit 2 is fixedly connected to the front end of the device body 1. A cleaning unit 3 is fixedly provided inside the filter unit 2. The cleaning unit 3 A vibration unit 4 is fixedly installed at the front end, a three-way container 101 is fixedly installed at the bottom end of the device body 1, a sealing unit 5 is fixedly installed at the rear end of the filter unit 2, and a water isolation unit 6 is fixedly installed at the rear end of the sealing unit 5. , the distillation unit 102 is fixedly installed at the top of the water isolation unit 6, and the heating device 103 is fixedly installed at the bottom of the three-way container 101.
请参阅图2和图3,所述过滤单元2包括外壳201,所述外壳201内部固定设置有流通底板202,所述过滤单元2顶端固定设置有入液口203,所述流通底板202底端固定连接有输液管204。Please refer to Figures 2 and 3. The filter unit 2 includes a housing 201. A circulation bottom plate 202 is fixedly provided inside the housing 201. A liquid inlet 203 is fixedly provided at the top of the filter unit 2. The bottom of the circulation bottom plate 202 is fixed. An infusion tube 204 is fixedly connected.
请参阅图3和图4,所述清理单元3包括滤网301,所述滤网301顶端固定连接有圆弧顶302,所述滤网301内部顶端滑动连接有清理圆板303,所述清理圆板303顶端固定连接有横移滑板304,所述横移滑板304顶端滑动连接有清理电机305,所述清理电机305和横移滑板304之间固定连接有清理弹簧306,所述清理电机305输出端固定连接有转动轮307,所述转动轮307滑动连接有清理架,所述清理电机305底端固定连接有伸缩电线309,所述伸缩电线309底端固定连接有杂质感应器310,所述滤网301底端转动设置有两块弹力挡板311,所述弹力挡板311底端固定设置有回收仓312。Please refer to Figures 3 and 4. The cleaning unit 3 includes a filter 301. The top of the filter 301 is fixedly connected to an arc top 302. The top of the filter 301 is slidably connected to a cleaning circular plate 303. The top of the circular plate 303 is fixedly connected to a traversing slide plate 304. The top of the traversing slide plate 304 is slidingly connected to a cleaning motor 305. A cleaning spring 306 is fixedly connected between the cleaning motor 305 and the traversing slide plate 304. The cleaning motor 305 The output end is fixedly connected with a rotating wheel 307, and the rotating wheel 307 is slidingly connected with a cleaning frame. The bottom end of the cleaning motor 305 is fixedly connected with a telescopic wire 309, and the bottom end of the telescopic wire 309 is fixedly connected with an impurity sensor 310, so Two elastic baffles 311 are rotatably provided at the bottom end of the filter screen 301, and a recovery bin 312 is fixedly provided at the bottom end of the elastic baffles 311.
请参阅图8和图9,所述震动单元4包括震动顶板401,所述震动顶板401底端滑动连接有震动凸轮402,所述震动凸轮402侧面固定连接有重力弹簧杆403,所述重力弹簧杆403侧端固定连接有震动电机404,所述重力弹簧杆403内侧固定设置有震动齿轮405,所述震动齿轮405顶端固定连接有震动卡板406。Please refer to Figures 8 and 9. The vibration unit 4 includes a vibration top plate 401. A vibration cam 402 is slidably connected to the bottom end of the vibration top plate 401. A gravity spring rod 403 is fixedly connected to the side of the vibration cam 402. The gravity spring A vibration motor 404 is fixedly connected to the side end of the rod 403, a vibration gear 405 is fixed to the inside of the gravity spring rod 403, and a vibration clamping plate 406 is fixedly connected to the top of the vibration gear 405.
请参阅图5和图6,所述密封单元5包括密封管501,所述密封管501顶部转动连接有密封扇叶502,所述密封扇叶502底端固定连接有扇叶伞齿503,所述扇叶伞齿503侧端啮合连接有传动伞齿504,所述传动伞齿504侧端固定连接有动力伞齿505,所述动力伞齿505侧端啮合连接有密封顶齿506,所述密封顶齿506底端固定连接有密封转板507,所述密封转板507底端转动连接有复位转杆508,所述密封转板507底面滑动连接有升降板509,所述升降板509底端转动连接有辅助板510,所述辅助板510底端转动连接有平衡转板511,所述平衡转板511侧端转动连接有浮力块512,所述平衡转板511中部转动连接有固定板513,所述固定板513底端固定连接在三通容器101底部。Please refer to Figures 5 and 6. The sealing unit 5 includes a sealing tube 501. The top of the sealing tube 501 is rotatably connected to a sealing fan blade 502. The bottom end of the sealing fan blade 502 is fixedly connected to a fan blade bevel tooth 503. Therefore, The side ends of the fan blade bevel teeth 503 are meshed with transmission bevel teeth 504, the side ends of the transmission bevel teeth 504 are fixedly connected with power bevel teeth 505, and the side ends of the power bevel teeth 505 are meshed with sealing top teeth 506. The bottom end of the sealing top tooth 506 is fixedly connected to a sealing rotating plate 507. The bottom end of the sealing rotating plate 507 is rotatably connected to a reset rotating rod 508. The bottom surface of the sealing rotating plate 507 is slidingly connected to a lifting plate 509. The bottom of the lifting plate 509 An auxiliary plate 510 is rotatably connected to one end of the auxiliary plate 510, a balance rotating plate 511 is rotatably connected to the bottom end of the auxiliary plate 510, a buoyancy block 512 is rotatably connected to the side end of the balance rotating plate 511, and a fixed plate is rotatably connected to the middle of the balance rotating plate 511. 513, the bottom end of the fixed plate 513 is fixedly connected to the bottom of the tee container 101.
请参阅图7,所述隔水单元6包括隔水盘601,所述隔水盘601中央固定设置有通气口602,所述隔水盘601外侧滑动连接有支撑外壁603,所述隔水盘601底端固定连接有滑动盘604,所述滑动盘604周围均匀地滑动连接有四个辅助圆柱605,所述隔水盘601底端固定连接有复位弹簧606,所述隔水单元6固定设置于三通容器101和蒸馏单元102之间。Please refer to Figure 7. The water barrier unit 6 includes a water barrier 601. A vent 602 is fixedly provided in the center of the water barrier 601. A supporting outer wall 603 is slidably connected to the outside of the water barrier 601. The water barrier 601 is A sliding plate 604 is fixedly connected to the bottom of 601, and four auxiliary cylinders 605 are evenly and slidingly connected around the sliding plate 604. A return spring 606 is fixedly connected to the bottom of the water isolation plate 601, and the water isolation unit 6 is fixedly installed. Between the three-way container 101 and the distillation unit 102.
综上所述本发明中先通过入液口203将药液倒入,药业先进行过滤,通过过滤单元2过滤的过程中,药液通过密封管501进入密封单元5,然后通过减压蒸馏进行蒸馏,在此过程中,经过多次过滤的积累,滤网301上会积累大量杂质,此时由于杂质的增加触碰到杂质感应器310,杂质感应器310控制清理电机305开始转动,进而使转动轮307转动,进而通过转动轮307在清理架308内部移动带动清理圆板303升降,清理电机305通过横移滑板304和清理弹簧306之间配合辅助清理电机305左右横移,通过清理圆板303升降对滤网301内部进行清理,通过底部弹力挡板311的开合使杂质通过弹力挡板311进入回收仓312。To sum up, in the present invention, the medicinal liquid is first poured into the liquid inlet 203, and the pharmaceutical industry first performs filtration. During the process of filtering through the filter unit 2, the medicinal liquid enters the sealing unit 5 through the sealing tube 501, and then is distilled under reduced pressure. Distillation is carried out. During this process, after multiple filtrations, a large amount of impurities will accumulate on the filter 301. At this time, due to the increase in impurities, they touch the impurity sensor 310. The impurity sensor 310 controls the cleaning motor 305 to start rotating, and then The rotating wheel 307 is rotated, and then the rotating wheel 307 moves inside the cleaning frame 308 to drive the cleaning disc 303 to rise and fall. The cleaning motor 305 cooperates with the lateral sliding plate 304 and the cleaning spring 306 to assist the cleaning motor 305 to move left and right. The plate 303 moves up and down to clean the inside of the filter screen 301, and the impurities enter the recovery bin 312 through the elastic baffle 311 through the opening and closing of the bottom elastic baffle 311.
本发明中在滤液通过密封管501的过程中,带动密封扇叶502转动,进而带动扇叶伞齿503转动,进而使传动伞齿504和动力伞齿505转动,进而带动密封顶齿506转动,进而带动密封转板507转动同时三通容器101内部减压蒸馏,此时密封转板507被气压吸住,当减压蒸馏结束后,内部三通容器101中的液体由于蒸馏作用液面下降,进而使浮力块512下降,进而带动平衡转板511转动,进而使升降板509将密封转板507顶起,密封转板507通过复位转杆508复位。In the present invention, when the filtrate passes through the sealing tube 501, the sealing fan blade 502 is driven to rotate, which in turn drives the fan blade bevel gear 503 to rotate, which in turn drives the transmission bevel gear 504 and the power bevel gear 505 to rotate, which in turn drives the sealing top gear 506 to rotate. Then the sealing rotating plate 507 is driven to rotate while the inside of the three-way container 101 is decompressed and distilled. At this time, the sealing rotating plate 507 is sucked by the air pressure. When the decompression distillation is completed, the liquid level in the internal three-way container 101 drops due to the distillation effect. Then the buoyancy block 512 is lowered, which drives the balance rotating plate 511 to rotate, and then the lifting plate 509 lifts the sealing rotating plate 507, and the sealing rotating plate 507 is reset through the reset rotating rod 508.
本发明中在蒸馏的过程中由于液滴会在入口端附着,使液滴回流,此时回流的液滴会在隔水盘601内部积累,进而使隔水盘601重力逐渐增加,当通气口602被隔水盘601完全封住时,蒸馏结束,此时隔水盘601下降使滑动盘604在辅助圆柱605的内部下降逐渐封住通气口602,蒸馏结束后去除整流单元后,清理掉隔水盘601内部的水,通过复位弹簧606隔水盘601复位。During the distillation process of the present invention, the liquid droplets will adhere to the inlet end, causing the liquid droplets to flow back. At this time, the refluxed liquid droplets will accumulate inside the water barrier plate 601, and the gravity of the water barrier plate 601 will gradually increase. When the ventilation opening When 602 is completely sealed by the water barrier plate 601, the distillation ends. At this time, the water barrier plate 601 descends so that the sliding plate 604 descends inside the auxiliary cylinder 605 and gradually seals the vent 602. After the distillation is completed, the rectification unit is removed, and the barrier is cleaned. The water inside the water pan 601 is reset to the water isolating pan 601 through the return spring 606 .
本发明中当清理单元3清理结束后,滤网301的网孔中依然会残留少量杂质,使用时间增长后杂质的重量也会增加,这种特殊情况需要震动单元4进行处理,正常情况下震动单元4的震动齿轮405与震动卡板406啮合进而使重力弹簧杆403静止不动,当滤网301内部中立达到一定极限时,重力弹簧杆403下沉并转动,进而使震动齿轮405脱离震动卡板406转动,进而带动震动凸轮402转动,进而使滤网301震动将网孔中的杂质震动清理掉,当杂质去除后,重力弹簧杆403复位,重力齿轮重新和震动卡板406啮合静止。In the present invention, after cleaning by the cleaning unit 3 is completed, a small amount of impurities will still remain in the mesh of the filter 301, and the weight of the impurities will also increase as the use time increases. This special situation requires the vibration unit 4 to handle it. Under normal circumstances, vibration The vibration gear 405 of unit 4 meshes with the vibration clamping plate 406 to make the gravity spring rod 403 stationary. When the neutrality inside the filter 301 reaches a certain limit, the gravity spring rod 403 sinks and rotates, thereby causing the vibration gear 405 to break away from the vibration clamp. The plate 406 rotates, which in turn drives the vibration cam 402 to rotate, which in turn causes the filter screen 301 to vibrate and clean out the impurities in the mesh. When the impurities are removed, the gravity spring rod 403 resets, and the gravity gear engages with the vibration clamping plate 406 again.
在本发明的描述中,除非另有明确的规定和限定,属于“设置”、“安装”、“相连”、“连接”、“固定”应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或成一体;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通或两个元件的相互作用关系。对于本领域的普通技术人员而言,可以具体情况理解上述属于在本发明中的具体含义。In the description of the present invention, unless otherwise expressly stipulated and limited, the words "setting", "installation", "connecting", "connecting" and "fixing" should be understood in a broad sense. For example, it can be a fixed connection or a fixed connection. It can be detachably connected or integrated; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium; it can be an internal connection between two elements or an interaction between two elements. For those of ordinary skill in the art, the above-mentioned specific meanings in the present invention can be understood in specific situations.
本发明使用到的标准零件均可以从市场上购买,异形件根据说明书的和附图的记载均可以进行定制。The standard parts used in the present invention can be purchased from the market, and the special-shaped parts can be customized according to the instructions and drawings.
以上,仅为本发明较佳的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,根据本发明的技术方案及其发明构思加以等同替换或改变,都应涵盖在本发明的保护范围之内。The above are only preferred specific embodiments of the present invention, but the protection scope of the present invention is not limited thereto. Any person familiar with the technical field can, within the technical scope disclosed in the present invention, use the technical solutions of the present invention and its Equivalent substitutions or changes of the inventive concept shall be included in the protection scope of the present invention.
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| CN117185444A (en) * | 2023-09-19 | 2023-12-08 | 吉水金诚新材料加工有限公司 | Method for treating oxalic acid precipitation wastewater and ammonia nitrogen wastewater of rare earth separation plant and simultaneously recycling rare earth |
| CN117263208A (en) * | 2023-10-20 | 2023-12-22 | 江西欧氏化工有限公司 | Recovery method of by-product ammonium chloride in kresoxim-methyl production process |
| CN117619009A (en) * | 2023-11-27 | 2024-03-01 | 吉水金诚新材料加工有限公司 | Shower method for producing high-purity praseodymium neodymium oxide by using neodymium iron boron smelting slag |
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| CN112456664A (en) * | 2020-11-12 | 2021-03-09 | 陈时云 | Sewage treatment plant convenient to get rid of residue |
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