CN116370978B - Separation equipment of sodium carbonate - Google Patents

Separation equipment of sodium carbonate Download PDF

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Publication number
CN116370978B
CN116370978B CN202211648885.7A CN202211648885A CN116370978B CN 116370978 B CN116370978 B CN 116370978B CN 202211648885 A CN202211648885 A CN 202211648885A CN 116370978 B CN116370978 B CN 116370978B
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Prior art keywords
movable
fixedly connected
air pipe
ring
air
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CN202211648885.7A
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CN116370978A (en
Inventor
赵祥海
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Jiangsu Debang Xinghua Chemical Technology Co ltd
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Jiangsu Debang Xinghua Chemical Technology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00Carbonates of sodium, potassium or alkali metals in general
    • C01D7/22Purification
    • C01D7/24Crystallisation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/0011Heating features
    • B01D1/0041Use of fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/14Evaporating with heated gases or vapours or liquids in contact with the liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/30Accessories for evaporators ; Constructional details thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D19/00Degasification of liquids
    • B01D19/0042Degasification of liquids modifying the liquid flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0018Evaporation of components of the mixture to be separated
    • B01D9/0031Evaporation of components of the mixture to be separated by heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/02Crystallisation from solutions
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00Carbonates of sodium, potassium or alkali metals in general
    • C01D7/22Purification

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Degasification And Air Bubble Elimination (AREA)
  • Liquid Crystal (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The invention discloses separation equipment of sodium carbonate, relates to the technical field of separation equipment of sodium carbonate, and solves the problems that liquid close to the inner wall releases alkali crystals too fast to be easily out of line and molten, and comprises a machine body; the movable plate is fixedly communicated with a plurality of first air pipes, and the bottoms of the first air pipes are in rotary fit with second air pipes; the diffusion assembly is used for driving the plurality of second air pipes to diffuse and do circular rotation; the reciprocating assembly is used for matching with the movable plate to enable the mixed liquid level to be rippled; the defoaming component is used for carrying out elimination treatment on foam at the inner wall of the machine body by matching with the reciprocating component, and the second air pipe which moves circularly and rotates enables hot air to be fully sprayed on the liquid surface, so that the whole liquid surface is uniformly heated, and alkali crystals released in the mode sink into the bottom from the liquid surface, thereby avoiding the situation of excessive heating and melting of the crystals in the traditional mode.

Description

Separation equipment of sodium carbonate
Technical Field
The invention relates to the technical field of separation equipment of sodium carbonate, in particular to the separation equipment of sodium carbonate.
Background
Soda ash, also called sodium carbonate, is an inorganic compound of the formula Na2CO3, molecular weight 105.99, but classified as salt, not alkali, also known as soda or soda ash in international trade. Sodium carbonate is a white powder, odorless and odorless, is easy to dissolve in water, the aqueous solution is strong in alkalinity, can absorb moisture and agglomerate in humid air, and is partially changed into sodium bicarbonate, and the sodium carbonate can be prepared by a combined alkali preparation method, an ammonia alkali method, a Lu Bulan method and the like, and can also be processed and refined by natural alkali. In the process of separating sodium carbonate, the inner wall of the separating device is heated to evaporate the mixed liquid, so that the alkali releases crystals, the alkali released locally at first is easily heated excessively in this way, the alkali crystal part (the alkali near the inner wall) is molten, and the existing separating device for sodium carbonate is not provided with a way of releasing the alkali by contacting the heated gas with the liquid surface of the mixed liquid.
For this purpose, we propose a separation device for soda ash.
Disclosure of Invention
The invention aims to provide soda ash separation equipment for solving the problems in the background technology.
In order to achieve the above purpose, the present invention provides the following technical solutions: the soda ash separating equipment includes one body; the device is characterized by further comprising a movable plate, wherein the bottom of the movable plate is fixedly communicated with a plurality of first air pipes, and the bottom of the first air pipes is in rotary fit with second air pipes; the diffusion assembly is used for driving the second air pipes to diffuse and do circular rotation; the reciprocating assembly is used for matching with the movable plate to enable the mixed liquid level to ripple; and the defoaming component is used for matching with the reciprocating component to eliminate foam at the inner wall of the machine body.
Preferably, the diffusion subassembly include with organism clearance fit's movable tube, the fly leaf in the activity of movable tube, movable tube surface fixedly connected with motor, the output shaft of motor penetrates in the movable tube and fixedly connected with rotor plate, a plurality of recesses have been seted up to rotor plate edge, the fly leaf is slope distribution, fly leaf bottom surface edge be circular matrix arrange fixedly connected with a plurality of with recess butt pressure post of butt pressure fit, a plurality of inside telescopic links that have elastic compression spare of fixedly connected with in the movable tube, the telescopic link tip with the fly leaf butt pressure fit, be equipped with spacing subassembly on the second trachea.
Preferably, the diffusion subassembly still include with first trachea with the hose that the second trachea is connected, first trachea with the equal fixedly connected with of second trachea surface is spacing, sliding fit has and is semicircular gag lever post in spacing frame, fly leaf middle part fixed intercommunication have with the third trachea of first trachea intercommunication, the third trachea is established with the transmission pipe box of transmission steam.
Preferably, the limiting component comprises a first fixed ring fixedly connected with the movable barrel, a second fixed ring is arranged above the first fixed ring, a plurality of connecting rods are fixedly connected between the first fixed ring and the second fixed ring, a movable groove is formed in the second fixed ring, a first movable open ring with a circular cross section is slidably matched on the second fixed ring, a limiting arc plate is fixedly connected with the inner wall of the first movable open ring and slidably matched with the movable groove, a second movable open ring fixedly connected with the second air pipe is rotatably connected at the side end of the first movable open ring, and a notch of the first movable open ring is movably matched with the connecting rods.
Preferably, the reciprocating assembly comprises a movable rod fixedly connected with the middle part of the bottom surface of the movable plate, a pressing plate is fixedly connected to the bottom of the movable rod, and a plurality of stirring plates are fixedly connected to the pressing plate.
Preferably, the defoaming assembly comprises a movable ring in sliding fit with the inner wall of the machine body, a plurality of connecting rods are fixedly connected between the movable ring and the movable rod, and a plurality of through grooves are formed in the outer surface of the movable ring.
Preferably, the edge of the top of the movable cylinder is connected with an air pressure lifting device connected with an external fixing frame, so that the second air pipe can move along with the descending liquid level, the distance between the second air pipe and the liquid level is ensured, and the heating effect is ensured.
Preferably, the arc angle of the second movable open ring is smaller than the arc angle of the first movable open ring, so that the second movable open ring is prevented from being in position conflict with the connecting rod when moving.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the invention, through the second air pipe which moves circularly and rotates, the hot air is fully sprayed on the liquid surface, so that the whole liquid surface is uniformly heated, and the released alkali crystals sink into the bottom from the liquid surface, thereby avoiding the situation of excessive heating and melting of the crystals in the traditional mode.
2. The movable second air pipe is matched with the pressing plate and the stirring plate which rotate and reciprocate up and down, so that the liquid level is rippling, on one hand, bubbles are eliminated, and on the other hand, the liquid is heated uniformly.
3. Bubbles accumulated on the inner wall of the machine body are eliminated through the movable ring, and alkali crystals are effectively prevented from adhering to the inner wall and not sinking into the bottom of the machine body.
Drawings
FIG. 1 is a schematic diagram of the overall structure of the present invention;
FIG. 2 is a schematic diagram illustrating the overall structure of the present invention;
FIG. 3 is a schematic side view of the partial structure of FIG. 2;
FIG. 4 is a schematic cross-sectional view of a portion of the structure of FIG. 3;
FIG. 5 is a schematic diagram of the structure of FIG. 4;
FIG. 6 is a schematic bottom view of the partial structure of FIG. 5;
FIG. 7 is a schematic diagram of the structure of FIG. 6 with portions of the array removed;
FIG. 8 is a schematic diagram illustrating the structure of FIG. 7 in a disassembled state;
FIG. 9 is a schematic view of the partial structure of FIG. 8;
FIG. 10 is a schematic side view of the structure of area A of FIG. 9;
fig. 11 is a schematic diagram illustrating the structure of fig. 10 in a disassembled state.
In the figure: 1-a machine body; 2-a movable plate; 3-a first trachea; 4-a second trachea; a 5-diffusion assembly; 6, a movable cylinder; 7-a motor; 8-rotating a plate; 9-grooves; 10-pressing the column; 11-a telescopic rod; 12-hose; 13, a limit frame; 14-a limit rod; 15-a third trachea; 16-a limiting assembly; 17-a first securing ring; 18-a second securing ring; 19-connecting rods; 20-a movable groove; 21-a first active open loop; 22-limiting arc plates; 23-a second active absence of loops; 24-a reciprocating assembly; 25-moving a rod; 26-pressing plate; 27-stirring plate; 28-a defoaming assembly; 29-a movable ring; 30-connecting rods; 31-through grooves; 32-an air pressure lifting device.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1
Referring to fig. 1 to 3, an apparatus for separating soda ash in the drawings includes a body 1; the device also comprises a movable plate 2, wherein the bottom of the movable plate 2 is fixedly communicated with a plurality of first air pipes 3, and the bottom of the first air pipes 3 is in rotary fit with a second air pipe 4; the diffusion component 5 is used for driving the plurality of second air pipes 4 to diffuse and do circular rotation; the reciprocating assembly 24, the reciprocating assembly 24 is used for cooperating with the movable plate 2 to make the mixed liquid level ripple; and the defoaming assembly 28, wherein the defoaming assembly 28 is used for carrying out elimination treatment on foam at the inner wall of the machine body 1 in cooperation with the reciprocating assembly 24.
Referring to fig. 4 and 7-8, the diffusion assembly 5 in the drawings comprises a movable cylinder 6 movably matched with the machine body 1, a movable plate 2 is movably arranged in the movable cylinder 6, a motor 7 is fixedly connected to the outer surface of the movable cylinder 6, an output shaft of the motor 7 penetrates into the movable cylinder 6 and is fixedly connected with a rotating plate 8, a plurality of grooves 9 are formed in the edge of the rotating plate 8, the movable plate 2 is obliquely distributed, a plurality of pressing columns 10 which are in pressing fit with the grooves 9 are fixedly connected to the edge of the bottom surface of the movable plate 2 in a circular matrix arrangement, a plurality of telescopic rods 11 with elastic compression members are fixedly connected in the movable cylinder 6, the end parts of the telescopic rods 11 are in pressing fit with the movable plate 2, and a limiting assembly 16 is arranged on the second air pipe 4.
Referring to fig. 5-6 and 9, the diffusion assembly 5 in the drawings further includes a hose 12 connected to the first air tube 3 and the second air tube 4, the outer surfaces of the first air tube 3 and the second air tube 4 are fixedly connected with a limiting frame 13, a semicircular limiting rod 14 is slidably matched with the limiting frame 13 in a sliding manner, a third air tube 15 communicated with the first air tube 3 is fixedly communicated with the middle portion of the movable plate 2, and the third air tube 15 is sleeved with a transmission tube for transmitting hot air. Referring to fig. 8-11, the limiting assembly 16 in the drawings includes a first fixed ring 17 fixedly connected with the movable tube 6, a second fixed ring 18 is disposed above the first fixed ring 17, a plurality of connecting rods 19 are fixedly connected between the first fixed ring 17 and the second fixed ring 18, a movable groove 20 is formed on the second fixed ring 18, a first movable open ring 21 with a circular cross section is slidably matched with the second fixed ring 18, a limiting arc plate 22 slidably matched with the movable groove 20 is fixedly connected with the inner wall of the first movable open ring 21, a second movable open ring 23 fixedly connected with the second air tube 4 is rotatably connected with the side end of the first movable open ring 21, and a notch of the first movable open ring 21 is movably matched with the connecting rods 19.
Wherein, the top edge of the movable cylinder 6 is connected with an air pressure lifting device 32 connected with an external fixing frame, and the arc angle of the second movable open ring 23 is smaller than that of the first movable open ring 21.
In this embodiment, the hot air is continuously conveyed into the third air pipe 15 through the conveying pipe, and the third air pipe 15 moves the hot air from the movable plate 2, the first air pipe 3, the hose 12 and the second air pipe 4 in sequence, so that the hot air is sprayed onto the liquid surface, wherein the height of the second air pipe 4 can be adjusted along with the descending of the liquid surface through the air pressure lifting device 32;
the motor 7 is started to drive the rotating plate 8 to rotate, under the action of the grooves 9 and the pressing columns 10, the movable plate 2 rotates in the movable cylinder 6, and simultaneously, as a plurality of pressing rods are inclined in distribution, the movable plate 2 moves up and down along the movable cylinder 6 in a fluctuating manner by matching with the telescopic rods 11 with elastic compression pieces in the telescopic rods, so that the movable plate 2 reciprocates vertically while rotating horizontally in the movable cylinder 6, and the first air pipe 3 and the second air pipe 4 are driven to move up and down and rotate circumferentially;
the second air pipe 4 moves up and down and circumferentially rotates, the positions of the first fixed ring 17 and the second fixed ring 18 are unchanged, when the second air pipe 4 moves circumferentially, the second movable unfilled ring 23 and the first movable unfilled ring 21 are driven to rotate on the second fixed ring 18, wherein the first movable unfilled ring 21 only slides on the second fixed ring 18 and does not rotate due to the cooperation of the limiting arc plate 22 and the movable groove 20, so that the connecting rod 19 passes through a notch of the first movable unfilled ring 21, the first movable unfilled ring 21 is prevented from sliding on the second fixed ring 18, the second movable unfilled ring 23 rotates relative to the first movable unfilled ring 21, the second air pipe 4 is guaranteed to rotate, and under the action of the hose 12, the limiting frame 13 and the limiting rod 14, the second air pipe 4 rotates relative to the first air pipe 3, and the second air pipe 4 moves circumferentially and simultaneously reciprocates back and forth relative to the movable rod 25, so that the full-scale hot air injection liquid level is ensured to be uniform;
wherein, the machine body 1 is provided with a feed inlet, a discharge outlet and a release pipe for releasing gas.
Example two
In the second embodiment, referring to fig. 7-8, the reciprocating assembly 24 in the illustrated embodiment includes a moving rod 25 fixedly connected to the middle of the bottom surface of the movable plate 2, a pressing plate 26 is fixedly connected to the bottom of the moving rod 25, and a plurality of stirring plates 27 are fixedly connected to the pressing plate 26.
In this embodiment, the second air pipe 4 performs a circular motion and rotates relative to the first air pipe 3, so as to change the inclination angle of the second air pipe 4, thereby making the liquid level ripple, and the movable plate 2 that reciprocates up and down and rotates, makes the pressing plate 26 and the stirring plate 27 reciprocate up and down through the moving rod 25, so as to increase the ripple degree of the liquid level, eliminate foam, and facilitate the release of alkali reaction.
Example III
In the third embodiment, referring to fig. 2-3, the defoaming assembly 28 in the illustrated embodiment includes a movable ring 29 slidably engaged with the inner wall of the machine body 1, a plurality of connecting rods 30 are fixedly connected between the movable ring 29 and the movable rod 25, and a plurality of through grooves 31 are formed on the outer surface of the movable ring 29.
In this embodiment, the liquid surface of the ripple causes the excessive bubbles to accumulate on the inner wall of the machine body 1, and the bubbles on the inner wall of the machine body 1 are eliminated by cooperating with the grooves 9 under the action of the movable ring 29 which reciprocates up and down and rotates.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (4)

1. A soda ash separation apparatus comprising:
a machine body (1);
characterized by further comprising:
the movable plate (2), a plurality of first air pipes (3) are fixedly communicated with the bottom of the movable plate (2), and a second air pipe (4) is in running fit with the bottom of the first air pipe (3);
the diffusion assembly (5) is used for driving the second air pipes (4) to diffuse and do circular rotation;
a reciprocating assembly (24), wherein the reciprocating assembly (24) is used for matching the movable plate (2) to cause the mixed liquid level to ripple;
the defoaming component (28) is used for being matched with the reciprocating component (24) to eliminate foam at the inner wall of the machine body (1);
the diffusion assembly (5) comprises a movable barrel (6) movably matched with the machine body (1), the movable plate (2) moves in the movable barrel (6), a motor (7) is fixedly connected to the outer surface of the movable barrel (6), an output shaft of the motor (7) penetrates into the movable barrel (6) and is fixedly connected with a rotating plate (8), a plurality of grooves (9) are formed in the edge of the rotating plate (8), the movable plate (2) is obliquely distributed, a plurality of pressing columns (10) which are in pressing fit with the grooves (9) are fixedly connected to the edge of the bottom surface of the movable plate (2) in a circular matrix arrangement, a plurality of telescopic rods (11) with elastic compression pieces are fixedly connected in the movable barrel (6), the end parts of the telescopic rods (11) are in pressing fit with the movable plate (2), and a limiting assembly (16) is arranged on the second air pipe (4);
the diffusion assembly (5) further comprises a hose (12) connected with the first air pipe (3) and the second air pipe (4), the outer surfaces of the first air pipe (3) and the second air pipe (4) are fixedly connected with a limiting frame (13), a semicircular limiting rod (14) is slidably matched in the limiting frame (13), a third air pipe (15) communicated with the first air pipe (3) is fixedly communicated in the middle of the movable plate (2), and the third air pipe (15) is sleeved with a transmission pipe for transmitting hot air;
the top edge of the movable cylinder (6) is connected with an air pressure lifting device (32) connected with an external fixing frame;
the limiting component (16) comprises a first fixed ring (17) fixedly connected with the movable barrel (6), a second fixed ring (18) is arranged above the first fixed ring (17), a plurality of connecting rods (19) are fixedly connected between the first fixed ring (17) and the second fixed ring (18), movable grooves (20) are formed in the second fixed ring (18), a first movable open ring (21) with a circular cross section is slidably matched on the second fixed ring (18), limiting arc plates (22) slidably matched with the movable grooves (20) are fixedly connected to the inner wall of the first movable open ring (21), second movable open rings (23) fixedly connected with the second air pipe (4) are rotatably connected to the side ends of the first movable open ring (21), and gaps of the first movable open ring (21) are movably matched with the connecting rods (19).
2. The soda ash separation device according to claim 1, characterized in that: the reciprocating assembly (24) comprises a movable rod (25) fixedly connected with the middle part of the bottom surface of the movable plate (2), a pressing plate (26) is fixedly connected to the bottom of the movable rod (25), and a plurality of stirring plates (27) are fixedly connected to the pressing plate (26).
3. The soda ash separation device according to claim 2, characterized in that: the defoaming assembly (28) comprises a movable ring (29) which is in sliding fit with the inner wall of the machine body (1), a plurality of connecting rods (30) are fixedly connected between the movable ring (29) and the movable rod (25), and a plurality of through grooves (31) are formed in the outer surface of the movable ring (29).
4. The soda ash separation device according to claim 1, characterized in that: the arc angle of the second movable open ring (23) is smaller than that of the first movable open ring (21).
CN202211648885.7A 2022-12-21 2022-12-21 Separation equipment of sodium carbonate Active CN116370978B (en)

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CN113546553A (en) * 2021-08-03 2021-10-26 吴易仁 Textile processing is with printing and dyeing liquid agent mixing device
CN113828470A (en) * 2021-11-02 2021-12-24 无锡牧宇自动化科技有限公司 Automatic glue brushing device and method for annular part
CN114042334A (en) * 2021-11-18 2022-02-15 黑龙江职业学院(黑龙江省经济管理干部学院) Traditional Chinese medicine microwave extraction device
CN216456939U (en) * 2021-11-23 2022-05-10 福建中锦新材料有限公司 Evaporation tower for caprolactam production
CN216497484U (en) * 2021-11-27 2022-05-13 山东谊源药业股份有限公司 A even concentrated canning of being heated device for animal remedy liquid
CN217015438U (en) * 2022-01-08 2022-07-22 山东峰泉新材料有限公司 Defoaming device of evaporative crystallizer
CN217312043U (en) * 2022-04-20 2022-08-30 山东高密高源化工有限公司 Preparation sodium chlorite crystal is with concentrated cauldron
CN217139277U (en) * 2022-04-28 2022-08-09 宁夏派可威生物科技有限公司 Dry crystallization device is used in production of second naphthyl methyl ether
CN217567464U (en) * 2022-06-01 2022-10-14 安徽尖峰北卡药业有限公司 Production of hydrochloric acid moxifloxacin is with effectively guaranteeing decompression concentration device of defoaming
CN217854577U (en) * 2022-07-18 2022-11-22 哈德逊(苏州)水技术有限公司 Acid-base recovery device

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