CN115959701A - 一种3d自组装绣球花状硫化铟的制备方法及应用 - Google Patents
一种3d自组装绣球花状硫化铟的制备方法及应用 Download PDFInfo
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- CN115959701A CN115959701A CN202310136147.2A CN202310136147A CN115959701A CN 115959701 A CN115959701 A CN 115959701A CN 202310136147 A CN202310136147 A CN 202310136147A CN 115959701 A CN115959701 A CN 115959701A
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- indium sulfide
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- GKCNVZWZCYIBPR-UHFFFAOYSA-N sulfanylideneindium Chemical compound [In]=S GKCNVZWZCYIBPR-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 238000001338 self-assembly Methods 0.000 title claims abstract description 9
- 239000012467 final product Substances 0.000 claims abstract description 23
- 239000000463 material Substances 0.000 claims abstract description 18
- 238000010438 heat treatment Methods 0.000 claims abstract description 15
- 239000002244 precipitate Substances 0.000 claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- -1 polytetrafluoroethylene Polymers 0.000 claims abstract description 7
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims abstract description 7
- 239000004810 polytetrafluoroethylene Substances 0.000 claims abstract description 7
- YUKQRDCYNOVPGJ-UHFFFAOYSA-N thioacetamide Chemical compound CC(N)=S YUKQRDCYNOVPGJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- DLFVBJFMPXGRIB-UHFFFAOYSA-N thioacetamide Natural products CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910021617 Indium monochloride Inorganic materials 0.000 claims abstract description 4
- 238000001816 cooling Methods 0.000 claims abstract description 4
- APHGZSBLRQFRCA-UHFFFAOYSA-M indium(1+);chloride Chemical compound [In]Cl APHGZSBLRQFRCA-UHFFFAOYSA-M 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims abstract description 3
- 238000002156 mixing Methods 0.000 claims abstract description 3
- 238000005406 washing Methods 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 241000134970 Cornales Species 0.000 claims description 4
- 239000006227 byproduct Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 2
- 229910052717 sulfur Inorganic materials 0.000 abstract description 15
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract description 14
- 239000011593 sulfur Substances 0.000 abstract description 14
- 230000008859 change Effects 0.000 abstract description 7
- 238000011065 in-situ storage Methods 0.000 abstract description 7
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- 125000003396 thiol group Chemical class [H]S* 0.000 abstract description 3
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- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 30
- 239000000047 product Substances 0.000 description 29
- 239000007789 gas Substances 0.000 description 24
- 150000003573 thiols Chemical class 0.000 description 10
- 238000007306 functionalization reaction Methods 0.000 description 9
- 229910052976 metal sulfide Inorganic materials 0.000 description 8
- 239000007795 chemical reaction product Substances 0.000 description 7
- 239000013078 crystal Substances 0.000 description 6
- 241001092080 Hydrangea Species 0.000 description 5
- 235000014486 Hydrangea macrophylla Nutrition 0.000 description 5
- 239000002135 nanosheet Substances 0.000 description 5
- 238000000026 X-ray photoelectron spectrum Methods 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 125000000524 functional group Chemical group 0.000 description 4
- 239000003446 ligand Substances 0.000 description 4
- 239000002055 nanoplate Substances 0.000 description 4
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- 238000012512 characterization method Methods 0.000 description 3
- 229910052738 indium Inorganic materials 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
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- LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 description 2
- 238000003917 TEM image Methods 0.000 description 2
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 2
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- AGBQKNBQESQNJD-SSDOTTSWSA-N (R)-lipoic acid Chemical group OC(=O)CCCC[C@@H]1CCSS1 AGBQKNBQESQNJD-SSDOTTSWSA-N 0.000 description 1
- DGSQQLTUOHNCPG-UHFFFAOYSA-N 2-sulfanyltridecanoic acid Chemical compound CCCCCCCCCCCC(S)C(O)=O DGSQQLTUOHNCPG-UHFFFAOYSA-N 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
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- 150000002118 epoxides Chemical class 0.000 description 1
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- MHMNJMPURVTYEJ-UHFFFAOYSA-N fluorescein-5-isothiocyanate Chemical compound O1C(=O)C2=CC(N=C=S)=CC=C2C21C1=CC=C(O)C=C1OC1=CC(O)=CC=C21 MHMNJMPURVTYEJ-UHFFFAOYSA-N 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
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- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
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- 238000000024 high-resolution transmission electron micrograph Methods 0.000 description 1
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- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- AGBQKNBQESQNJD-UHFFFAOYSA-N lipoic acid Chemical compound OC(=O)CCCCC1CCSS1 AGBQKNBQESQNJD-UHFFFAOYSA-N 0.000 description 1
- 235000019136 lipoic acid Nutrition 0.000 description 1
- 230000000877 morphologic effect Effects 0.000 description 1
- 230000005693 optoelectronics Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000009832 plasma treatment Methods 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
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- 230000007847 structural defect Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 125000004434 sulfur atom Chemical group 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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- 229960002663 thioctic acid Drugs 0.000 description 1
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- 238000002371 ultraviolet--visible spectrum Methods 0.000 description 1
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- 239000012855 volatile organic compound Substances 0.000 description 1
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Citations (12)
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KR20050101802A (ko) * | 2004-04-20 | 2005-10-25 | 삼성전자주식회사 | 황 전구체로서 싸이올 화합물을 이용한 황화 금속나노결정의 제조방법 |
CN102335616A (zh) * | 2011-07-21 | 2012-02-01 | 北京工业大学 | 一种新型可见光光催化剂硫化铟的合成方法 |
CN104959151A (zh) * | 2015-06-02 | 2015-10-07 | 福州大学 | 一种硫化铟催化剂及其制备方法和应用 |
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KR20050101802A (ko) * | 2004-04-20 | 2005-10-25 | 삼성전자주식회사 | 황 전구체로서 싸이올 화합물을 이용한 황화 금속나노결정의 제조방법 |
CN102335616A (zh) * | 2011-07-21 | 2012-02-01 | 北京工业大学 | 一种新型可见光光催化剂硫化铟的合成方法 |
CN104959151A (zh) * | 2015-06-02 | 2015-10-07 | 福州大学 | 一种硫化铟催化剂及其制备方法和应用 |
CN105692688A (zh) * | 2016-02-23 | 2016-06-22 | 许昌学院 | 一种离子液体辅助制备花球状In2S3纳米材料的方法 |
CN106345494A (zh) * | 2016-10-14 | 2017-01-25 | 石家庄铁道大学 | 一种高效可见光降解剂纳米片状In2.77S4的制备方法 |
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CN112209369A (zh) * | 2019-07-12 | 2021-01-12 | 哈尔滨理工大学 | 一种氧化铟纳米片阵列/泡沫石墨烯电极的制备及应用 |
CN113461046A (zh) * | 2021-07-28 | 2021-10-01 | 四川恒瑞天成科技有限公司 | 一种梳状氮掺杂硫化铟气敏材料、制备方法及应用 |
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