CN115647097A - Extrusion Die and Manufacturing Method of Equiaxed Magnesium Alloy Rod - Google Patents
Extrusion Die and Manufacturing Method of Equiaxed Magnesium Alloy Rod Download PDFInfo
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Abstract
Description
技术领域technical field
本发明属于有色金属塑性成形技术领域,具体涉及一种等轴晶镁合金棒材的挤压模具和制造方法。The invention belongs to the technical field of plastic forming of nonferrous metals, and in particular relates to an extrusion die and a manufacturing method of equiaxed crystal magnesium alloy rods.
背景技术Background technique
随着轻量化进程的不断加快,镁合金得到了越来越广泛的关注。镁合金具有密度小、质量轻、导电导热性好、冲击韧性高、电磁屏蔽性能优良等诸多优点,被誉为“21世纪最具发展前景的绿色工程材料”。其中,镁合金型材已经广泛的应用于航空、航天、汽车制造、电子产品等领域。With the continuous acceleration of the lightweight process, magnesium alloys have received more and more attention. Magnesium alloy has many advantages such as low density, light weight, good electrical and thermal conductivity, high impact toughness, and excellent electromagnetic shielding performance. It is known as "the most promising green engineering material in the 21st century". Among them, magnesium alloy profiles have been widely used in aviation, aerospace, automobile manufacturing, electronic products and other fields.
此外,镁合金具有良好的生物相容性,且密度和弹性模量与人体骨骼相近,并能在人体内完全降解,在生物医疗领域得到了应用。由于HCP的特殊结构,在室温下镁合金只有三个滑移系可以开动,塑性变形能力差,加工难度大,当在225℃以上温度时,镁合金的锥面和棱柱面滑移系可以开动,塑性变形能力得到了提高。因此,目前主要通过热挤压的方式来制备镁合金型材。In addition, magnesium alloy has good biocompatibility, and its density and elastic modulus are similar to human bones, and can be completely degraded in the human body, so it has been applied in the field of biomedicine. Due to the special structure of HCP, only three slip systems can be activated in magnesium alloy at room temperature, the plastic deformation ability is poor, and the processing is difficult. When the temperature is above 225°C, the slip systems of the conical surface and prism surface of the magnesium alloy can be activated. , plastic deformation ability has been improved. Therefore, at present, magnesium alloy profiles are mainly prepared by hot extrusion.
目前,对于镁合金棒材的加工制造,主要的方法有半连续铸造工艺、普通正挤压、等径角正挤压、往复挤压、高压扭转工艺等。西南大学专利《一种镁合金棒材的加工方法》(申请号:201510029162.2,公开号:CN104498848A,公开日:2015.04.08),公开了镁合金棒材毛坯产生扭转塑性变形,通过调控切边量并结合热处理工艺,获得镁合金棒材。河南科技大学专利《一种高钆稀土镁合金棒材及其制备方法》(申请号:202110699449.1,公开号:CN113444903A,公开日:2021.09.28),公开了一种通过合金化和热处理工艺对合金进行调控,在通过等径角正挤压的方式实现镁合金棒材的大塑性变形制造。At present, for the processing and manufacturing of magnesium alloy rods, the main methods include semi-continuous casting process, ordinary forward extrusion, equal-diameter forward extrusion, reciprocating extrusion, high-pressure torsion process, etc. Southwest University's patent "A Processing Method for Magnesium Alloy Rods" (Application No.: 201510029162.2, Publication No.: CN104498848A, Publication Date: 2015.04.08), discloses that magnesium alloy bar blanks produce torsional plastic deformation, and by adjusting the trimming amount Combined with the heat treatment process, the magnesium alloy rod is obtained. Henan University of Science and Technology's patent "A High Gadolinium Rare Earth Magnesium Alloy Rod and Its Preparation Method" (Application No.: 202110699449.1, Publication No.: CN113444903A, Publication Date: 2021.09.28), discloses a process for alloying and heat treatment of alloys Controlled to realize the large plastic deformation manufacturing of magnesium alloy rods by means of equal radial angle forward extrusion.
上述方法虽然在一定程度上可以实现晶粒细化,但每次细化的程度都不足原始晶粒的二分之一,若要获得超细晶粒的镁合金棒材,则需要多道次的挤压来实现,工艺过程过于繁琐,生产周期长,且组织不均匀,在生产高性能镁合金棒材时存在一定的局限性。Although the above method can achieve grain refinement to a certain extent, the degree of refinement each time is less than half of the original grain. To obtain ultra-fine grain magnesium alloy rods, multiple passes are required. Extrusion to achieve, the process is too cumbersome, the production cycle is long, and the organization is uneven, there are certain limitations in the production of high-performance magnesium alloy rods.
有鉴于此,特提出本发明。In view of this, the present invention is proposed.
发明内容Contents of the invention
针对现有技术存在的问题和/或不足,本发明的目的在于提供一种镁合金棒材的挤压模具。该挤压模具,采用变径角挤压,进行有效的焊合,能够高效、快速的制造出超细等轴晶镁合金棒材,大大地提升了镁合金棒材的强度和塑性等,有效地拓展了镁合金的应用范围和使用领域。In view of the problems and/or deficiencies in the prior art, the object of the present invention is to provide an extrusion die for magnesium alloy rods. The extrusion die adopts variable-diameter angular extrusion for effective welding, and can efficiently and quickly manufacture ultra-fine equiaxed magnesium alloy rods, which greatly improves the strength and plasticity of magnesium alloy rods, effectively The scope of application and the field of use of magnesium alloys have been greatly expanded.
本发明提供的一种镁合金棒材挤压模具,它包括:下模具(1)、上模具(2)、内挤压筒(3)、外挤压筒(4)、加热圈(6)和热电偶(8);A magnesium alloy rod extrusion die provided by the present invention comprises: a lower die (1), an upper die (2), an inner extrusion cylinder (3), an outer extrusion cylinder (4), and a heating ring (6) and thermocouple (8);
其中,in,
所述内挤压筒(3)嵌套在外挤压筒(4)的内部;The inner extrusion cylinder (3) is nested inside the outer extrusion cylinder (4);
所述外挤压筒(4)的内部或外部设置有加热圈(6);A heating ring (6) is arranged inside or outside the outer extruding cylinder (4);
所述热电偶(8)插入到外挤压筒(4)和内挤压筒(3)之间连通的孔内;The thermocouple (8) is inserted into the hole communicated between the outer extrusion cylinder (4) and the inner extrusion cylinder (3);
所述内挤压筒(3)为上下贯通的中空结构;The inner extruding barrel (3) is a hollow structure that penetrates up and down;
所述上模具(2)从内挤压筒(3)顶部安装在内挤压筒(3)的中空结构内;The upper mold (2) is installed in the hollow structure of the inner extrusion barrel (3) from the top of the inner extrusion barrel (3);
所述下模具(1)从内挤压筒(3)底部安装在内挤压筒(3)的中空结构内。The lower die (1) is installed in the hollow structure of the inner extrusion barrel (3) from the bottom of the inner extrusion barrel (3).
进一步的,further,
在上述任一技术方案(镁合金棒材挤压模具)中,所述上模具(2)为倒置圆锥台结构,或者,所述上模具(2)为顶部带圆柱的倒置圆锥台结构;In any of the above technical solutions (magnesium alloy rod extrusion die), the upper die (2) is an inverted truncated conical structure, or, the upper die (2) is an inverted truncated conical structure with a column on the top;
所述上模具(2)的顶部设置有3~30个(例如,3个、6个、9个、12个、15个、18个、21个、24个等)直径相等的圆孔(201);所述上模具(2)的底部设置有半圆孔(202),每一个半圆孔(202)都有一个相对应的圆孔(201)相连通,所述半圆孔(202)的直径与圆孔(201)的直径相等。The top of the upper mold (2) is provided with 3 to 30 (for example, 3, 6, 9, 12, 15, 18, 21, 24, etc.) circular holes (201) with equal diameters. ); the bottom of the upper mold (2) is provided with semicircular holes (202), and each semicircular hole (202) has a corresponding circular hole (201) to communicate with each other, and the diameter of the semicircular hole (202) is the same as The diameters of the circular holes (201) are equal.
进一步的,further,
在上述任一技术方案(镁合金棒材挤压模具)中,所述圆孔(201)的设置为均匀分布。In any of the above technical solutions (magnesium alloy rod extrusion die), the circular holes (201) are arranged to be evenly distributed.
进一步的,further,
在上述任一技术方案(镁合金棒材挤压模具)中,所述下模具(1)通过螺纹结构从内挤压筒(3)底部安装在内挤压筒(3)的中空结构内。In any of the above technical solutions (magnesium alloy rod extrusion die), the lower die (1) is installed in the hollow structure of the inner extrusion barrel (3) from the bottom of the inner extrusion barrel (3) through a threaded structure.
进一步的,further,
在上述任一技术方案(镁合金棒材挤压模具)中,In any of the above-mentioned technical schemes (magnesium alloy rod extrusion die),
所述下模具(1)的上部设置有中空的倒置圆锥台结构(101);The upper part of the lower mold (1) is provided with a hollow inverted truncated cone structure (101);
所述上模具(2)的倒置圆锥台结构与下模具(1)中空的倒置圆锥台结构(101)具有相同的锥面角度,优选所述的锥面角度为90°~150°(例如,90°、120°、135°、150°等);The inverted truncated cone structure (101) of the upper mold (2) and the hollow inverted truncated cone structure (101) of the lower mold (1) have the same cone angle, preferably the cone angle is 90 ° ~ 150 ° (for example, 90°, 120°, 135°, 150°, etc.);
所述下模具(1)的中部设置有与倒置圆锥台结构(101)底部相连通的焊合室(102);The middle part of the lower mold (1) is provided with a welding chamber (102) communicating with the bottom of the inverted truncated conical structure (101);
所述下模具(1)的下部设置有与焊合室(102)底部相连通的挤出口(103)。The lower part of the lower mold (1) is provided with an extrusion port (103) communicating with the bottom of the welding chamber (102).
进一步的,further,
在上述任一技术方案(镁合金棒材挤压模具)中,所述挤出口(103)的内径大于焊合室(102)的内径;优选地,所述挤出口(103)的内径比焊合室(102)的内径大3mm~5mm。In any of the above technical solutions (magnesium alloy rod extrusion die), the inner diameter of the extrusion port (103) is greater than the inner diameter of the welding chamber (102); preferably, the inner diameter of the extrusion port (103) is larger than the welding chamber (102); The inner diameter of the combined chamber (102) is 3mm-5mm larger.
本发明还提供了一种镁合金棒材的制造方法,它包括以下步骤:The present invention also provides a kind of manufacturing method of magnesium alloy rod, it comprises the following steps:
①、将前述任意一项所述的镁合金棒材挤压模具放到挤压机工作台上,将去除表皮的镁合金坯料放入内挤压筒(3)里面,挤压杆(5)放入内挤压筒内(3)与镁合金坯料相接触,并在挤压机的作用下施加2~5MPa的预压力;①. Put the magnesium alloy rod extrusion die described in any one of the foregoing items on the extruder workbench, put the magnesium alloy billet with the skin removed into the inner extrusion cylinder (3), and extrude the rod (5) Put it into the inner extrusion cylinder (3) contact with the magnesium alloy billet, and apply a pre-pressure of 2 to 5 MPa under the action of the extruder;
②、通过加热圈(6)将挤压模具和镁合金坯料加热到250~450℃,热电偶(8)监测挤压模具的温度;②. Heat the extrusion die and the magnesium alloy billet to 250-450°C through the heating ring (6), and the thermocouple (8) monitors the temperature of the extrusion die;
③、当挤压模具的温度加热到所需温度时,保温5~15min,开始挤压,在挤压机的作用下挤压杆(5)推动镁合金坯料先通过上模具(2)的圆孔(201),经半圆孔(202)流出,进入下模具(1)的焊合室(102)内进行焊合,最后经挤出口(103)挤出,即得镁合金棒材。③. When the temperature of the extrusion die is heated to the required temperature, keep it warm for 5 to 15 minutes, and start extrusion. Under the action of the extruder, the extrusion rod (5) pushes the magnesium alloy billet through the circle of the upper die (2) first. The hole (201) flows out through the semicircular hole (202), enters the welding chamber (102) of the lower mold (1) for welding, and finally extrudes through the extrusion port (103) to obtain a magnesium alloy rod.
进一步的,further,
在上述任一技术方案(镁合金棒材的制造方法)中,所述的镁合金棒材为AZ31镁合金棒材、AZ91镁合金棒材、ZK61镁合金棒材或ZM5镁合金棒材。In any of the above technical solutions (manufacturing method of magnesium alloy rods), the magnesium alloy rods are AZ31 magnesium alloy rods, AZ91 magnesium alloy rods, ZK61 magnesium alloy rods or ZM5 magnesium alloy rods.
进一步的,further,
在上述任一技术方案(镁合金棒材的制造方法)中,步骤②中,加热的速率为10~20℃/min。In any of the above technical solutions (manufacturing method of magnesium alloy rods), in
进一步的,further,
在上述任一技术方案(镁合金棒材的制造方法)中,所述挤压杆(5)的运动速率为1~8m/min。In any of the above technical solutions (manufacturing method of magnesium alloy rods), the moving speed of the extrusion rod (5) is 1-8 m/min.
在挤压过程中,镁合金坯料流经1/2截面变径角挤压后,既得到了剧烈的剪切变形而获得大塑性变形,又在焊合室得到镦粗从而得到剧烈大塑性变形,此时被挤压材料的晶粒组织得到剪切、破碎、流动和翻转而成为细小的超细等轴晶(亚微米和纳米晶组织)。In the extrusion process, after the magnesium alloy billet flows through the 1/2 cross-section variable diameter angular extrusion, it not only obtains severe shear deformation to obtain large plastic deformation, but also obtains upsetting in the welding chamber to obtain severe large plastic deformation. At this time, the grain structure of the extruded material is sheared, broken, flowed and turned over to become a fine ultrafine equiaxed crystal (submicron and nanocrystalline structure).
本发明的有益效果,具体包括以下方面:The beneficial effects of the present invention specifically include the following aspects:
(1)本发明对镁合金棒材挤压模具做出了改进,采用变径角挤压,实现多通道的变径角挤压,在上模具以及下模具的焊合室进行有效的焊合,进而挤压成棒材;(1) The present invention has made improvement to magnesium alloy rod extruding die, adopts variable-diameter angular extrusion, realizes multi-channel variable-diameter angular extrusion, and effectively welds in the welding chamber of the upper mold and the lower mold , and then extruded into rods;
(2)在挤压过程中,镁合金处于三向应力作用下,通过一次挤压就可获得极大的累积应变和变形量,从而获得具有超细等轴晶的镁合金棒材,大大提升了镁合金棒材的强度与塑性,简化了工艺过程,降低了生产成本;(2) During the extrusion process, the magnesium alloy is under the action of three-dimensional stress, and a large cumulative strain and deformation can be obtained through one extrusion, thereby obtaining a magnesium alloy rod with ultrafine equiaxed crystals, which greatly improves The strength and plasticity of the magnesium alloy bar are improved, the process is simplified, and the production cost is reduced;
(3)本发明的镁合金棒材挤压模具,不仅适用于镁合金的塑性变形,同样也适用于铝合金、铜合金、钛合金、不锈钢等多种合金的塑性变形及其生产制造。(3) The magnesium alloy rod extrusion die of the present invention is not only suitable for plastic deformation of magnesium alloys, but also for plastic deformation and production of various alloys such as aluminum alloys, copper alloys, titanium alloys, and stainless steel.
附图说明Description of drawings
图1是本发明镁合金棒材挤压模具的结构示意图;Fig. 1 is the structural representation of magnesium alloy rod extrusion die of the present invention;
图2是本发明上模具的三维结构示意图;Fig. 2 is the three-dimensional structure schematic diagram of upper mold of the present invention;
图3是本发明上模具的剖视结构示意图;Fig. 3 is the sectional structure schematic diagram of upper mold of the present invention;
图4是本发明下模具的剖视结构示意图;Fig. 4 is the sectional structure schematic diagram of lower mold of the present invention;
图中,1-下模具,2-上模具,3-内挤压筒,4-外挤压筒,5-挤压杆,6-加热圈,7-镁合金坯料,8-热电偶,101-中空的倒置圆锥台结构,102-焊合室,103-挤出口,201-圆孔,202-半圆孔。In the figure, 1-lower mold, 2-upper mold, 3-inner extrusion cylinder, 4-outer extrusion cylinder, 5-extrusion rod, 6-heating ring, 7-magnesium alloy billet, 8-thermocouple, 101 - hollow inverted conical structure, 102 - welding chamber, 103 - extrusion port, 201 - circular hole, 202 - semicircular hole.
具体实施方式Detailed ways
为了使本领域的技术人员更好地理解本发明的技术方案,下面通过实施例的方式对本发明作进一步的详细说明,但并不表示因此将本发明的保护范围限制在所述的实施例范围之内。基于本申请中的实施例,本领域普通技术人员在没有做出创造性劳动的情况下所获得的其它类同实施例,都应当属于本申请保护的范围。In order to enable those skilled in the art to better understand the technical solution of the present invention, the present invention will be further described in detail below by means of examples, but it does not mean that the protection scope of the present invention is therefore limited to the scope of the described examples. within. Based on the embodiments in this application, other similar embodiments obtained by persons of ordinary skill in the art without creative efforts shall all fall within the scope of protection of this application.
在本发明的描述中,需要说明的是,术语“中心”、“上”、“下”、“左”、“右”、“竖直”、“水平”、“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本发明和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本发明的限制。In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer" etc. The indicated orientation or positional relationship is based on the orientation or positional relationship shown in the drawings, and is only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the referred device or element must have a specific orientation, or in a specific orientation. construction and operation, therefore, should not be construed as limiting the invention.
除非另有明确的规定和限定,术语“相连”、“连接”“安装”、“设置”等应做广义理解;例如,可以是固定连接,也可以是可拆卸连接,或一体地连接;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通。对于本领域的普通技术人员而言,可以根据具体情况理解上述术语在本发明中的具体含义。Unless otherwise clearly stipulated and limited, the terms "connected", "connected", "installed", "set", etc. should be interpreted in a broad sense; for example, it can be fixed connection, detachable connection, or integral connection; It can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediary, and it can be the internal communication of two components. Those of ordinary skill in the art can understand the specific meanings of the above terms in the present invention according to specific situations.
本发明中,未注明具体条件者,按照常规条件或制造商建议的条件进行。In the present invention, those without specific conditions are carried out according to conventional conditions or conditions suggested by the manufacturer.
关于本发明中使用术语的定义,除非另有说明,本文中术语提供的初始定义适用于全文中的该术语;对于本文没有具体定义的术语,应当根据公开内容和/或上下文,给出本领域技术人员能够给予它们的含义。Regarding the definition of terms used in the present invention, unless otherwise stated, the initial definition provided by the term herein is applicable to the term throughout the text; for terms that are not specifically defined herein, it should be given according to the disclosure and/or context. A skilled person can give their meaning.
实施例1Example 1
如图1~4所示,本发明的镁合金棒材挤压模具,包括:下模具1、上模具2、内挤压筒3、外挤压筒4、加热圈6和热电偶8;As shown in Figures 1 to 4, the magnesium alloy rod extrusion die of the present invention includes: a
其中,in,
内挤压筒3嵌套在外挤压筒4的内部;The
外挤压筒4的内部或外部设置有加热圈6;A
热电偶8插入到外挤压筒4和内挤压筒3之间连通的孔内;The
内挤压筒3为上下贯通的中空结构;The
上模具2从内挤压筒3顶部安装在内挤压筒3的中空结构内;The
上模具2为倒置圆锥台结构,或者,上模具2为顶部带圆柱的倒置圆锥台结构;The
上模具2的顶部设置有3~30个直径相等的圆孔201,优选圆孔201的设置为均匀分布;The top of the
上模具2的底部设置有半圆孔202,每一个半圆孔202都有一个相对应的圆孔201相连通,半圆孔202的直径与圆孔201的直径相等,可以实现1/2截面变径角挤压;The bottom of the
下模具1从内挤压筒3底部安装在内挤压筒3的中空结构内,优选为下模具1通过螺纹结构从内挤压筒3底部安装在内挤压筒3的中空结构内;The
下模具1的上部设置有中空的倒置圆锥台结构101;The upper part of the
上模具2的倒置圆锥台结构与下模具1中空的倒置圆锥台结构101具有相同的锥面角度,两者之间可以紧密贴合,优选所述的锥面角度为90°~150°;The inverted truncated cone structure of the
下模具1的中部设置有与倒置圆锥台结构101底部相连通的焊合室102;The middle part of the
下模具1的下部设置有与焊合室102底部相连通的挤出口103;The lower part of the
挤出口103的内径略大于焊合室102的内径,例如挤出口103的内径比焊合室102的内径大3mm~5mm。The inner diameter of the
工作过程,具体如下:The working process is as follows:
(1)装配:将内挤压筒3嵌套在外挤压筒4的内部,下模具1从内挤压筒3底部安装在内挤压筒3的中空结构内,上模具2从内挤压筒3顶部安装在内挤压筒3的中空结构内,外挤压筒4安装加热圈6,热电偶8插入到外挤压筒4和内挤压筒3之间连通的孔内,得到装配好的镁合金棒材挤压模具;(1) Assembling: the
(2)将装配好的镁合金棒材挤压模具放到挤压机工作台上,将去除表皮的镁合金坯料7放入内挤压筒3里面,挤压杆5放入内挤压筒内3与镁合金坯料7相接触,并在挤压机的作用下施加2~5MPa的预压力;(2) Put the assembled magnesium alloy rod extrusion die on the extruder workbench, put the magnesium alloy billet 7 with the skin removed into the
(3)通过加热圈6将挤压模具和镁合金坯料7加热到250~450℃,热电偶8监测挤压模具的温度;(3) heating the extrusion die and the magnesium alloy billet 7 to 250-450°C through the
(4)当挤压模具的温度加热到所需温度时,保温5~15min,开始挤压,在挤压机的作用下挤压杆5推动镁合金坯料7先通过上模具2的圆孔201,经半圆孔202流出,进入下模具1的焊合室102内进行焊合,最后经挤出口103挤出,从而实现等轴晶镁合金棒材的挤压生产。(4) When the temperature of the extrusion die is heated to the desired temperature, keep it warm for 5 to 15 minutes, and start extrusion. Under the action of the extruder, the
实施例2Example 2
一种AZ31镁合金棒材的制造方法,包括以下步骤:A method for manufacturing an AZ31 magnesium alloy rod, comprising the following steps:
(1)与实施例1相同,装配镁合金棒材挤压模具;(1) same as
(2)将装配好的镁合金棒材挤压模具放到挤压机工作台上,将去除表皮的镁合金坯料放入内挤压筒3里面,挤压杆5放入内挤压筒内3与镁合金坯料相接触,并在挤压机的作用下施加2MPa的预压力;(2) Put the assembled magnesium alloy rod extrusion die on the workbench of the extruder, put the magnesium alloy billet with the skin removed into the
(3)通过加热圈6将挤压模具和镁合金坯料加热到250℃,热电偶8监测挤压模具的温度;(3) The extrusion die and the magnesium alloy billet are heated to 250°C by the
(4)当挤压模具的温度加热到所需温度时,保温5min,开始挤压,在挤压机的作用下挤压杆5推动镁合金坯料先通过上模具2的圆孔201,经半圆孔202流出,进入下模具1的焊合室102内进行焊合,最后经挤出口103挤出,实现等轴晶镁合金棒材的挤压生产。在挤压过程中,挤压杆的运动速率为1m/min。(4) When the temperature of the extrusion die is heated to the required temperature, keep it warm for 5 minutes, and start extrusion. Under the action of the extruder, the
本实施例中,上模具2均匀分布30个直径相等的圆孔201,上模具2的倒置圆锥台结构与下模具1中空的倒置圆锥台结构101具有相同的锥面角度,所述的锥面角度为150°,两者之间可以紧密贴合;结果显示,所制得的镁合金棒材,表面质量良好,尺寸精确,组织均匀、致密、无缺陷,其晶粒尺寸约500nm,抗拉强度为336MPa,伸长率为18%。In this embodiment, 30
实施例3Example 3
一种AZ91镁合金棒材的制造方法,包括以下步骤:A method for manufacturing an AZ91 magnesium alloy rod, comprising the following steps:
(1)与实施例1相同,装配镁合金棒材挤压模具;(1) same as
(2)将装配好的镁合金棒材挤压模具放到挤压机工作台上,将去除表皮的镁合金坯料放入内挤压筒3里面,挤压杆5放入内挤压筒内3与镁合金坯料相接触,并在挤压机的作用下施加4MPa的预压力;(2) Put the assembled magnesium alloy rod extrusion die on the workbench of the extruder, put the magnesium alloy billet with the skin removed into the
(3)通过加热圈6将挤压模具和镁合金坯料加热到450℃,热电偶8监测挤压模具的温度;(3) The extrusion die and the magnesium alloy billet are heated to 450° C. by the
(4)当挤压模具的温度加热到所需温度时,保温8min,开始挤压,在挤压机的作用下挤压杆5推动镁合金坯料先通过上模具2的圆孔201,经半圆孔202流出,进入下模具1的焊合室102内进行焊合,最后经挤出口103挤出,实现等轴晶镁合金棒材的挤压生产。在挤压过程中,挤压杆的运动速率为1.5m/min。(4) When the temperature of the extrusion die is heated to the required temperature, keep it warm for 8 minutes and start extrusion. Under the action of the extruder, the
本实施例中,上模具2均匀分布3个直径相等的圆孔201,上模具2的倒置圆锥台结构与下模具1中空的倒置圆锥台结构101具有相同的锥面角度,所述的锥面角度为90°,两者之间可以紧密贴合;结果显示,所制得的镁合金棒材,表面质量良好,尺寸精确,组织均匀、致密、无缺陷,其晶粒尺寸约305nm,抗拉强度为286MPa,伸长率为16.4%。In this embodiment, three
实施例4Example 4
一种ZK61镁合金棒材的制造方法,包括以下步骤:A method for manufacturing a ZK61 magnesium alloy rod, comprising the following steps:
(1)与实施例1相同,装配镁合金棒材挤压模具;(1) same as
(2)将装配好的镁合金棒材挤压模具放到挤压机工作台上,将去除表皮的镁合金坯料放入内挤压筒3里面,挤压杆5放入内挤压筒内3与镁合金坯料相接触,并在挤压机的作用下施加3MPa的预压力;(2) Put the assembled magnesium alloy rod extrusion die on the workbench of the extruder, put the magnesium alloy billet with the skin removed into the
(3)通过加热圈6将挤压模具和镁合金坯料加热到330℃,热电偶8监测挤压模具的温度;(3) The extrusion die and the magnesium alloy billet are heated to 330°C by the
(4)当挤压模具的温度加热到所需温度时,保温12min,开始挤压,在挤压机的作用下挤压杆5推动镁合金坯料先通过上模具2的圆孔201,经半圆孔202流出,进入下模具1的焊合室102内进行焊合,最后经挤出口103挤出,实现等轴晶镁合金棒材的挤压生产。在挤压过程中,挤压杆的运动速率为2.5m/min。(4) When the temperature of the extrusion die is heated to the desired temperature, keep it warm for 12 minutes, and start extrusion. Under the action of the extruder, the
本实施例中,上模具2均匀分布9个直径相等的圆孔201,上模具2的倒置圆锥台结构与下模具1中空的倒置圆锥台结构101具有相同的锥面角度,所述的锥面角度为120°,两者之间可以紧密贴合;结果显示,所制得的镁合金棒材,表面质量良好,尺寸精确,组织均匀、致密、无缺陷,其晶粒尺寸约412nm,抗拉强度为368MPa,伸长率为24.5%。In this embodiment, the
实施例5Example 5
一种AZ31镁合金棒材的制造方法,包括以下步骤:A method for manufacturing an AZ31 magnesium alloy rod, comprising the following steps:
(1)与实施例1相同,装配镁合金棒材挤压模具;(1) same as
(2)将装配好的镁合金棒材挤压模具放到挤压机工作台上,将去除表皮的镁合金坯料放入内挤压筒3里面,挤压杆5放入内挤压筒内3与镁合金坯料相接触,并在挤压机的作用下施加5MPa的预压力;(2) Put the assembled magnesium alloy rod extrusion die on the workbench of the extruder, put the magnesium alloy billet with the skin removed into the
(3)通过加热圈6将挤压模具和镁合金坯料加热到350℃,热电偶8监测挤压模具的温度;(3) The extrusion die and the magnesium alloy billet are heated to 350°C by the
(4)当挤压模具的温度加热到所需温度时,保温10min,开始挤压,在挤压机的作用下挤压杆5推动镁合金坯料先通过上模具2的圆孔201,经半圆孔202流出,进入下模具1的焊合室102内进行焊合,最后经挤出口103挤出,实现等轴晶镁合金棒材的挤压生产。在挤压过程中,挤压杆的运动速率为5m/min。(4) When the temperature of the extrusion die is heated to the desired temperature, keep it warm for 10 minutes, and start extrusion. Under the action of the extruder, the
本实施例中,上模具2均匀分布12个直径相等的圆孔201,上模具2的倒置圆锥台结构与下模具1中空的倒置圆锥台结构101具有相同的锥面角度,所述的锥面角度为135°,两者之间可以紧密贴合;结果显示,所制得的镁合金棒材,表面质量良好,尺寸精确,组织均匀、致密、无缺陷,其晶粒尺寸约352nm,抗拉强度为357MPa,伸长率为17.2%。In this embodiment, 12
实施例6Example 6
一种ZM5镁合金棒材的制造方法,包括以下步骤:A kind of manufacture method of ZM5 magnesium alloy rod, comprises the following steps:
(1)与实施例1相同,装配镁合金棒材挤压模具;(1) same as
(2)将装配好的镁合金棒材挤压模具放到挤压机工作台上,将去除表皮的镁合金坯料放入内挤压筒3里面,挤压杆5放入内挤压筒内3与镁合金坯料相接触,并在挤压机的作用下施加3MPa的预压力;(2) Put the assembled magnesium alloy rod extrusion die on the workbench of the extruder, put the magnesium alloy billet with the skin removed into the
(3)通过加热圈6将挤压模具和镁合金坯料加热到400℃,热电偶8监测挤压模具的温度;(3) The extrusion die and the magnesium alloy billet are heated to 400°C by the
(4)当挤压模具的温度加热到所需温度时,保温15min,开始挤压,在挤压机的作用下挤压杆5推动镁合金坯料先通过上模具2的圆孔201,经半圆孔202流出,进入下模具1的焊合室102内进行焊合,最后经挤出口103挤出,实现等轴晶镁合金棒材的挤压生产。在挤压过程中,挤压杆的运动速率为3m/min。(4) When the temperature of the extrusion die is heated to the desired temperature, keep it warm for 15 minutes, and start extrusion. Under the action of the extruder, the
本实施例中,上模具2均匀分布6个直径相等的圆孔201,上模具2的倒置圆锥台结构与下模具1中空的倒置圆锥台结构101具有相同的锥面角度,所述的锥面角度为120°,两者之间可以紧密贴合;结果显示,所制得的镁合金棒材,表面质量良好,尺寸精确,组织均匀、致密、无缺陷,其晶粒尺寸约415nm,抗拉强度为429MPa,伸长率为14.4%。In this embodiment, six
应当理解,虽然本说明书按照实施方式加以描述,但并非每个实施方式仅包含一个独立的技术方案,说明书的这种叙述方式仅仅是为清楚起见,本领域技术人员应当将说明书作为一个整体,各实施例中的技术方案也可以经适当组合,形成本领域技术人员可以理解的其他实施方式。It should be understood that although this description is described according to implementation modes, not each implementation mode only contains an independent technical solution, and this description in the description is only for clarity, and those skilled in the art should take the description as a whole, and each The technical solutions in the embodiments can also be properly combined to form other implementations that can be understood by those skilled in the art.
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