CN115430162A - Ethanol quick separation device for ethanol tantalum production - Google Patents
Ethanol quick separation device for ethanol tantalum production Download PDFInfo
- Publication number
- CN115430162A CN115430162A CN202211401578.9A CN202211401578A CN115430162A CN 115430162 A CN115430162 A CN 115430162A CN 202211401578 A CN202211401578 A CN 202211401578A CN 115430162 A CN115430162 A CN 115430162A
- Authority
- CN
- China
- Prior art keywords
- fixedly connected
- ethanol
- separation device
- plate
- shell
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 129
- 238000000926 separation method Methods 0.000 title claims abstract description 47
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- JVOQKOIQWNPOMI-UHFFFAOYSA-N ethanol;tantalum Chemical compound [Ta].CCO JVOQKOIQWNPOMI-UHFFFAOYSA-N 0.000 title abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 67
- 239000007788 liquid Substances 0.000 claims abstract description 34
- NGCRLFIYVFOUMZ-UHFFFAOYSA-N 2,3-dichloroquinoxaline-6-carbonyl chloride Chemical compound N1=C(Cl)C(Cl)=NC2=CC(C(=O)Cl)=CC=C21 NGCRLFIYVFOUMZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000010521 absorption reaction Methods 0.000 claims description 27
- 230000003014 reinforcing effect Effects 0.000 claims description 13
- 238000004321 preservation Methods 0.000 claims description 10
- 230000005540 biological transmission Effects 0.000 claims description 8
- 229920000742 Cotton Polymers 0.000 claims description 4
- 238000005192 partition Methods 0.000 claims description 4
- 238000011084 recovery Methods 0.000 claims 2
- 230000000694 effects Effects 0.000 abstract description 23
- 238000009835 boiling Methods 0.000 abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 8
- 238000001704 evaporation Methods 0.000 abstract description 4
- 230000000903 blocking effect Effects 0.000 description 10
- 238000000034 method Methods 0.000 description 7
- 238000010622 cold drawing Methods 0.000 description 5
- 210000003437 trachea Anatomy 0.000 description 4
- 239000011259 mixed solution Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 206010053615 Thermal burn Diseases 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/0011—Heating features
- B01D1/0041—Use of fluids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/30—Accessories for evaporators ; Constructional details thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
- B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a rapid ethanol separation device for ethanol tantalum production, which relates to the technical field of ethanol separation and comprises a separation device and an output device, wherein the outer surface of the separation device is fixedly connected to the surface of the output device, the output device comprises a base, the surface of the outer side of the base is fixedly connected with an air conveying tank, the air conveying tank achieves the effect of heating ethanol mixed liquid in a heating cup, meanwhile, the temperature of hot air can be kept above the boiling point of ethanol and below the boiling point of water all the time, so that the effect of evaporating ethanol into gas and facilitating separation and collection is achieved, and a lower ring is sleeved on the side end face of the base. This ethanol quick separation device is used in tantalum ethoxide production reaches the quick separation to the mixed liquid of ethanol to and the effect to the mixed liquid secondary separation of ethanol, utilize the mode that cold and hot meets to collect ethanol vapour, still play the control to intraductal temperature to and the effect of heat pressure release.
Description
Technical Field
The invention relates to the technical field of ethanol separation, in particular to a rapid ethanol separation device for producing tantalum ethanol.
Background
The separation apparatus is a device that implements the separation process.
The tower can be divided into a plate tower and a packed tower according to the structure, and commonly used bubble column, float valve tower, sieve plate tower, leaching plate tower, packed tower and the like are applied to operations such as distillation, absorption, extraction, adsorption and the like.
When the conventional ethanol separation device is used for heating and separating an ethanol mixture, a high-temperature and high-pressure environment is formed while the ethanol mixture is heated by hot gas so as not to lift a heating cup, and the evaporated residual solution is collected or separated for the second time. Meanwhile, the traditional method for forming ethanol liquid by contacting ethanol vapor with a condensing plate is low in efficiency, the separation of ethanol is influenced by uncontrollable heat in the process of heating the ethanol mixture, and excessive accumulation of heat can damage instruments and even cause problems such as explosion and the like.
Disclosure of Invention
In order to achieve the purpose, the invention is realized by the following technical scheme: the ethanol rapid separation device for producing the tantalum ethanol comprises a separation device and an output device, wherein the outer surface of the separation device is fixedly connected to the surface of the output device;
the output device comprises a base, wherein a gas conveying tank is fixedly connected to the surface of the outer side of the base, the gas conveying tank achieves the effect of heating the ethanol mixed liquid in the heating cup, meanwhile, the temperature of hot gas can be kept above the boiling point of ethanol and below the boiling point of water all the time, so that the effect of evaporating ethanol into gas to be convenient for separation and collection is achieved, a lower ring is sleeved on the side end face of the base, a reinforcing connecting plate is fixedly connected to the top of the lower ring, an upper ring is fixedly connected to the outer side of the upper half section of the reinforcing connecting plate, and the inner side of the upper half section of the reinforcing connecting plate is fixedly connected to the outer surface of the separation device;
the surface of the inner side of the base is inserted with an air control pipe, one end of the air control pipe close to the base is connected with the air delivery tank, one end of the air control pipe far away from the base is fixedly connected with an air pipe, one end of the air pipe far away from the air control pipe is fixedly connected with an air nozzle, the surface of the air nozzle is fixedly connected with a heat-proof pad, and the side face of the heat-proof pad is fixedly connected to the inner side of the bottom of the separation device;
the separating device comprises a heat-insulating shell, the outer surface of the heat-insulating shell is respectively and fixedly connected to the inner side surfaces of the lower ring and the reinforcing connecting plate, and the inner wall of the top of the heat-insulating shell is fixedly connected with a gas-liquid separator.
Preferably, the inner wall of the heat-insulating shell is fixedly connected with a slide rail, the upper half section of the slide rail is provided with an outflow hole, the outflow hole respectively penetrates through the surfaces of the slide rail and the heat-insulating shell, and the surface of the slide rail is slidably connected with a heating cup.
Preferably, the surface of the heating cup is provided with a blocking hole, the blocking hole is positioned at a position facing the slide rail, the bottom of the inner wall of the heating cup is fixedly connected with a connecting rod, one end of the connecting rod, far away from the heating cup, is fixedly connected with a sheath, the bottom of the sheath is fixedly connected with a secondary collector, and the inner side of the bottom of the heat preservation shell is fixedly connected to the side face of the heat-proof pad.
Preferably, the secondary collector is including collecting the shell, the top fixed connection who collects the shell is in the bottom of sheath, the inner wall of collecting the shell is fixedly connected with cold drawing and hot plate respectively, and wherein cold drawing and hot plate play the collection effect to ethanol vapour, the last fixed surface of cold drawing is connected with the baffle, and wherein the baffle plays and collects and isolated effect, fixedly connected with keeps apart the bag between cold drawing and the hot plate, and wherein keep apart the bag and then play the effect of separation hot plate and cold drawing.
Preferably, the air control pipe comprises a pipe shell, the top of the pipe shell is fixedly connected with a flower-shaped plate, the outer surface of the pipe shell is connected with a pressure relief device in a sliding mode, one end, far away from the pipe shell, of the flower-shaped plate is fixedly connected with a limiting block, and one end, far away from the flower-shaped plate, of the limiting block is fixedly connected with an expansion ball.
Preferably, the bottom of the expansion ball is fixedly connected with a heat absorption block, the upper surface of the heat absorption block is fixedly connected with a restoration strip, one end, far away from the heat absorption block, of the restoration strip is fixedly connected to the inner wall of the tube shell, the outer surface of the heat absorption block is fixedly connected with a spiral auger, the outer side of the lower half section of the spiral auger is fixedly connected with a moving plate, and the bottom of the moving plate is fixedly connected to the surface of the heat absorption block.
Preferably, pressure relief device includes the circulation board, the inner wall sliding connection of circulation board has the heart bucket of inlaying, and wherein gomphosis bucket and spiral auger and move the gomphosis between the board can play the effect that reduces the heat inflow, the surface sliding connection who inlays the heart bucket is on the surface of tube, the annular has been seted up on the surface of the heart bucket of inlaying, and wherein the annular plays the effect of heat circulation between tube and the circulation board to and play the effect of pressure release, the central part fixedly connected with cotton body of heart bucket of inlaying.
Preferably, the surface of the flower-shaped plate is connected with the output end of the gas transmission tank, and the outer surface of the flow plate is fixedly connected with the vent pipe.
The invention provides a rapid ethanol separation device for tantalum ethanol production. The method has the following beneficial effects:
1. this ethanol quick separation device is used in tantalum ethanol production, through defeated gas pitcher to the intraductal steam of carrying of accuse gas, make steam follow jet-propelled head blowout steam through the breather pipe that is connected with the accuse gas pitcher, steam will be at the top of heat protection pad afterwards, the inner wall of heat preservation shell and the space that the bottom of heating cup constitutes form and pile up, in order to reach the effect of heating the mixed liquid of ethanol of heating cup inside, the temperature of steam can keep always more than the boiling point of ethanol and below the boiling point of water, in order to reach the effect of evaporating into gaseous separation of being convenient for and collecting with ethanol.
2. The device for quickly separating the ethanol for producing the tantalum ethanol comprises a heating cup, wherein the heating cup is heated, so that the volume of liquid in an ethanol mixed solution is reduced, hot gas accumulated in a space formed by the top of a heat-proof pad, the inner wall of a heat-preservation shell and the bottom of the heating cup can push the heating cup to enable the heating cup to move upwards along a sliding rail, when the heating cup moves to a blocking hole formed in the surface of the heating cup and an outflow hole formed in the surface of the sliding rail, the liquid in the heating cup can flow out from the junction of two ports, then the required new ethanol mixed solution can be separated again or the outflow mixed solution can be separated for the second time, the blocking hole is always blocked by the sliding rail before being overlapped with the outflow hole, finally, when the top of the heating cup reaches the bottom of a gas-liquid separator, the hot gas can also flow out from the outflow hole, and meanwhile, a gas conveying tank is closed, so that the heating is slowly restored to the original position along the sliding rail.
3. The ethanol rapid separation device for producing the ethanol tantalum comprises a heating cup, wherein a heating cup is arranged in the heating cup, a hot plate is arranged at the bottom of the heating cup, the ethanol vapor enters a secondary collector, the ethanol vapor is divided into two parts, one part of the ethanol vapor touches the hot plate at the bottom of the heating cup, the ethanol vapor is changed into liquid again and enters a collecting shell along the hot plate, the ethanol vapor cannot be adhered to the hot plate when the surface of the hot plate is fully paved with the liquid, but enters a next component along the hot plate, the other part of the ethanol vapor enters a cold plate and simultaneously contacts the hot plate at the upper layer, therefore, one part of the ethanol vapor on the hot plate at the upper layer enters the collecting shell, and the other part of the ethanol vapor forms water drops through cold and hot confluence generated between the hot plate and the cold plate and drops on the cold plate for collection. Wherein the partition plate functions as a collecting and insulating function, and the insulating bladder functions as a separating function of the hot plate and the cold plate.
4. This ethanol quick separation device for ethanol tantalum production makes steam rush into the flower-shaped board through opening the gas transmission jar, steam will pass through the tube shell and enter into pressure relief device along spiral auger afterwards, steam can contact the heat absorption piece at the in-process that spiral auger flows, when the temperature of steam rises, the heat absorption piece also can slowly scald and make the expansion ball who fixes at its top slowly grow, will promote heat absorption piece and spiral auger to move downwards when the expansion ball is big and supports the stopper, at this moment the bottom of spiral auger and move the board will with the inner wall looks gomphosis of gomphosis bucket, in order to reach the effect that reduces the heat inflow, when the heat reaches certain degree, spiral auger and move the board will drive the gomphosis bucket and move downwards along the inner wall of flow plate and the surface of tube shell, make the annular groove of gomphosis bucket surface open, wherein the annular groove forms sealedly with the bottom of tube shell at first, in order to reach the effect that the heat circulates between tube shell and the flow plate, and play the effect of pressure relief.
Drawings
FIG. 1 is a schematic structural diagram of a rapid ethanol separation device for tantalum ethoxide production according to the present invention;
FIG. 2 is a schematic top view of an output device according to the present invention;
FIG. 3 is a schematic bottom view of the output device of the present invention;
FIG. 4 is a schematic structural front view of the separating apparatus of the present invention;
FIG. 5 is a schematic top view of the separating apparatus of the present invention;
FIG. 6 is a schematic view of a secondary collector of the present invention;
FIG. 7 is a schematic view of a gas control tube structure according to the present invention;
FIG. 8 is a schematic cross-sectional view of the gas control tube according to the present invention;
fig. 9 is a schematic view of a pressure relief device according to the present invention.
In the figure: 1. a separation device; 2. an output device; 21. ring fitting; 22. a gas showerhead; 23. reinforcing the connecting plate; 24. a base; 25. a gas delivery tank; 26. a lower ring; 27. a heat-proof cushion; 28. a breather pipe; 29. a gas control pipe; 11. heating the cup; 12. a connecting rod; 13. a heat preservation shell; 14. a sheath; 16. a gas-liquid separator; 17. a secondary collector; 15. plugging the hole; 18. a slide rail; 19. an outflow hole; 171. collecting the shells; 172. a cold plate; 173. a partition plate; 174. an isolation capsule; 175. a hot plate; 291. a flower-shaped plate; 292. a pipe shell; 293. a pressure relief device; 294. an expansion ball; 295. a limiting block; 296. restoring the strips; 297. a heat absorbing block; 298. moving the plate; 299. a spiral auger; 2931. a ring groove; 2932. embedding a core barrel; 2933. a flow-through plate; 2934. a cotton body.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings and specific embodiments. The embodiments of the present invention have been presented for purposes of illustration and description, and are not intended to be exhaustive or limited to the invention in the form disclosed. Many modifications and variations will be apparent to those of ordinary skill in the art. The embodiment was chosen and described in order to best explain the principles of the invention and the practical application, and to enable others of ordinary skill in the art to understand the invention for various embodiments with various modifications as are suited to the particular use contemplated.
As shown in fig. 1 to 9, the present invention provides a technical solution: the ethanol rapid separation device for producing tantalum ethoxide comprises a separation device 1 and an output device 2, wherein the outer surface of the separation device 1 is fixedly connected to the surface of the output device 2; the output device 2 comprises a base 24, a gas transmission tank 25 is fixedly connected to the surface of the outer side of the base 24, a lower ring 26 is sleeved on the side end face of the base 24, a reinforcing connecting plate 23 is fixedly connected to the top of the lower ring 26, an upper ring 21 is fixedly connected to the outer side of the upper half section of the reinforcing connecting plate 23, and the inner side of the upper half section of the reinforcing connecting plate 23 is fixedly connected to the outer surface of the separation device 1; the inboard surface of base 24 is pegged graft and is had accuse trachea 29, the one end that accuse trachea 29 is close to base 24 is connected with gas transmission tank 25, the one end fixedly connected with breather pipe 28 that base 24 was kept away from to accuse trachea 29, the one end fixedly connected with jet head 22 that accuse trachea 29 was kept away from to breather pipe 28, the fixed surface of jet head 22 is connected with heat protection pad 27, heat protection pad 27's side fixed connection is on the inboard of separator 1 bottom. Hot gas is delivered into the gas control pipe 29 through the gas delivery tank 25, so that the hot gas is ejected from the gas nozzle 22 through the gas vent pipe 28 connected with the gas control pipe 29, and then the hot gas is accumulated in a space formed by the top of the heat-proof pad 27, the inner wall of the heat-insulating shell 13 and the bottom of the heating cup 11, wherein the temperature of the hot gas is always kept above the boiling point of ethanol and below the boiling point of water.
The separating device 1 comprises a heat-insulating shell 13, the outer surface of the heat-insulating shell 13 is fixedly connected to the surface of the inner side of a lower ring 26 and a reinforcing connecting plate 23 respectively, the inner wall of the top of the heat-insulating shell 13 is fixedly connected with a gas-liquid separator 16, the inner wall of the heat-insulating shell 13 is fixedly connected with a slide rail 18, the upper half section of the slide rail 18 is provided with a flow hole 19, the flow hole 19 is respectively penetrated through the surfaces of the slide rail 18 and the heat-insulating shell 13, the surface of the slide rail 18 is slidably connected with a heating cup 11, the surface of the heating cup 11 is provided with a blocking hole 15, the blocking hole 15 is positioned right opposite to the slide rail 18, the bottom of the inner wall of the heating cup 11 is fixedly connected with a connecting rod 12, the connecting rod 12 is far away from one end of the heating cup 11 and is fixedly connected with a sheath 14, the bottom of the sheath 14 is fixedly connected with a secondary collector 17, and the inner side of the bottom of the heat-insulating shell 13 is fixedly connected to the side face of a heat-proof pad 27. Through heating the heating cup 11, the volume of the liquid in the ethanol mixed liquid is reduced, so that the hot gas accumulated in the space formed by the top of the heat-proof pad 27, the inner wall of the heat-insulating shell 13 and the bottom of the heating cup 11 pushes the heating cup 11 to move the heating cup 11 upwards along the slide rail 18, when the heating cup 11 moves to a blocking hole 15 formed in the surface of the heating cup and an outflow hole 19 formed in the surface of the slide rail, the liquid in the heating cup 11 flows out from the junction of the two ports, then the required new ethanol mixed liquid can be separated again or the outflow mixed liquid can be separated for the second time, wherein the blocking hole 15 is always blocked by the slide rail 18 before coinciding with the outflow hole 19, and finally when the top of the heating cup 11 reaches the bottom of the gas-liquid separator 16, the hot gas can also flow out from the outflow hole 19, and the gas conveying tank 25 is closed to ensure that the heating cup 11 is slowly restored to the original position along the slide rail 18.
The secondary collector 17 comprises a collecting shell 171, the top of the collecting shell 171 is fixedly connected to the bottom of the jacket 14, the inner wall of the collecting shell 171 is fixedly connected with a cold plate 172 and a hot plate 175 respectively, the upper surface of the cold plate 172 is fixedly connected with a partition 173, and an isolating bag 174 is fixedly connected between the cold plate 172 and the hot plate 175. By heating the mixed liquid in the heating cup 11, a part of the ethanol vapor enters the secondary collector 17, and then the ethanol vapor is divided into two parts, wherein one part of the ethanol vapor contacts the bottommost hot plate 175, so that the ethanol vapor is changed into liquid again and enters the collecting shell 171 along the hot plate 175, when the surface of the hot plate 175 is full of liquid, the ethanol vapor does not adhere to the hot plate 175 and enters the next component along the hot plate 175, the other part of the ethanol vapor enters the cold plate 172 and contacts the hot plate 175 in the previous layer, therefore, the ethanol vapor in the hot plate 175 in the previous layer enters the collecting shell 171, and the other part of the ethanol vapor forms water drops through the cold and hot confluence generated between the hot plate 175 and the cold plate 172 and falls on the cold plate 172 for collection.
The air control pipe 29 comprises a pipe shell 292, a flower-shaped plate 291 is fixedly connected to the top of the pipe shell 292, a pressure relief device 293 is slidably connected to the outer surface of the pipe shell 292, a limiting block 295 is fixedly connected to one end, far away from the pipe shell 292, of the flower-shaped plate 291, an expansion ball 294 is fixedly connected to one end, far away from the flower-shaped plate 291, of the limiting block 295, a heat absorption block 297 is fixedly connected to the bottom of the expansion ball 294, a restoration strip 296 is fixedly connected to the upper surface of the heat absorption block 297, one end, far away from the heat absorption block 297, of the restoration strip 296 is fixedly connected to the inner wall of the pipe shell 292, a spiral auger 299 is fixedly connected to the outer surface of the heat absorption block 297, a moving plate 298 is fixedly connected to the outer side of the lower half section of the spiral auger 299, and the bottom of the moving plate 298 is fixedly connected to the surface of the heat absorption block 297.
The pressure relief device 293 comprises a circulation plate 2933, an embedded barrel 2932 is connected to the inner wall of the circulation plate 2933 in a sliding manner, the outer surface of the embedded barrel 2932 is connected to the surface of the pipe shell 292 in a sliding manner, a ring groove 2931 is formed in the surface of the embedded barrel 2932, a cotton body 2934 is fixedly connected to the center of the embedded barrel 2932, the surface of the flower-shaped plate 291 is connected to the output end of the gas transmission tank 25, and the outer surface of the circulation plate 2933 is fixedly connected to the gas transmission pipe 28. When the gas transmission tank 25 is opened, hot gas flows into the flower-shaped plate 291, then the hot gas passes through the pipe shell 292 and enters the pressure relief device 293 along the spiral auger 299, the hot gas contacts the heat absorption block 297 in the flowing process of the spiral auger 299, when the temperature of the hot gas rises, the heat absorption block 297 can slowly scald and the expansion ball 294 fixed at the top of the heat absorption block becomes gradually larger, when the expansion ball 294 is large and abuts against the limiting block 295, the heat absorption block 297 and the spiral auger 299 can be pushed to move downwards, at the moment, the bottom of the spiral auger 299 and the moving plate 298 can be embedded with the inner wall of the embedded barrel 2932, and when the heat reaches a certain degree, the spiral auger 299 and the moving plate 298 can drive the embedded barrel 2932 to move downwards along the inner wall of the flow plate 2933 and the outer surface of the pipe shell 292, so that the annular groove 2931 formed in the surface of the embedded barrel 2932 is opened.
When the heating cup is used, hot gas is conveyed into the gas control pipe 29 through the gas conveying tank 25, so that the hot gas is sprayed out of the gas spraying head 22 through the gas pipe 28 connected with the gas control pipe 29, and then the hot gas can form accumulation in a space formed by the top of the heat-proof cushion 27, the inner wall of the heat-insulating shell 13 and the bottom of the heating cup 11, so that the effect of heating the ethanol mixed liquid in the heating cup 11 is achieved, and meanwhile, the temperature of the hot gas can be kept above the boiling point of ethanol and below the boiling point of water all the time, so that the effect of evaporating ethanol into gas and facilitating separation and collection is achieved.
Through heating the heating cup 11, the volume of the liquid in the ethanol mixed liquid is reduced, so that the hot gas accumulated in the space formed by the top of the heat-proof pad 27, the inner wall of the heat-insulating shell 13 and the bottom of the heating cup 11 pushes the heating cup 11 to move the heating cup 11 upwards along the slide rail 18, when the heating cup 11 moves to a blocking hole 15 formed in the surface of the heating cup and an outflow hole 19 formed in the surface of the slide rail, the liquid in the heating cup 11 flows out from the junction of the two ports, then the required new ethanol mixed liquid can be separated again or the outflow mixed liquid can be separated for the second time, wherein the blocking hole 15 is always blocked by the slide rail 18 before coinciding with the outflow hole 19, and finally when the top of the heating cup 11 reaches the bottom of the gas-liquid separator 16, the hot gas can also flow out from the outflow hole 19, and the gas conveying tank 25 is closed to ensure that the heating cup 11 is slowly restored to the original position along the slide rail 18.
By heating the mixed liquid in the heating cup 11, a part of the ethanol vapor enters the secondary collector 17, and then the ethanol vapor is divided into two parts, wherein one part of the ethanol vapor contacts the bottommost hot plate 175, so that the ethanol vapor is changed into liquid again and enters the collecting shell 171 along the hot plate 175, when the surface of the hot plate 175 is full of liquid, the ethanol vapor does not adhere to the hot plate 175 and enters the next component along the hot plate 175, the other part of the ethanol vapor enters the cold plate 172 and contacts the hot plate 175 in the previous layer, therefore, the ethanol vapor in the hot plate 175 in the previous layer enters the collecting shell 171, and the other part of the ethanol vapor forms water drops through the cold and hot confluence generated between the hot plate 175 and the cold plate 172 and falls on the cold plate 172 for collection. Wherein the separator plate 173 acts as a trap and an isolator bladder 174 acts as a separator between the hot plate 175 and the cold plate 172.
By opening the gas delivery tank 25, the hot gas gushes into the flower-shaped plate 291, and then the hot gas passes through the pipe shell 292 and enters the pressure relief device 293 along the spiral auger 299, the hot gas contacts the heat absorption block 297 in the flowing process of the spiral auger 299, when the temperature of the hot gas rises, the heat absorption block 297 also slowly warms and the expansion ball 294 fixed at the top of the heat absorption block becomes large, when the expansion ball 294 is large and abuts against the limit block 295, the heat absorption block 297 and the spiral auger 299 are pushed to move downwards, at this time, the bottom of the spiral auger 299 and the moving plate 298 are engaged with the inner wall of the embedded barrel 2932 to achieve the effect of reducing the inflow of the heat, when the heat reaches a certain degree, the spiral auger 299 and the moving plate 298 drive the embedded barrel 2932 to move downwards along the inner wall of the circulation plate 2933 and the outer surface of the pipe shell 292, so that the annular groove 2931 formed on the surface of the embedded barrel 2932 is opened, wherein the annular groove 2931 and the bottom of the pipe shell are initially sealed to achieve the effect of heat circulation between the pipe shell 2933 and the effect of pressure relief effect of the heat circulation plate 292.
It is to be understood that the described embodiments are merely a few embodiments of the invention, and not all embodiments. All other embodiments, which can be derived by one of ordinary skill in the art and related arts based on the embodiments of the present invention without any creative effort, shall fall within the protection scope of the present invention. Structures, devices, and methods of operation not specifically described or illustrated herein are generally practiced in the art without specific recitation or limitation.
Claims (8)
1. The utility model provides a tantalum ethoxide production is with ethanol quick separation device, includes separator (1) and output device (2), its characterized in that: the outer surface of the separation device (1) is fixedly connected to the surface of the output device (2);
the output device (2) comprises a base (24), the surface of the outer side of the base (24) is fixedly connected with an air conveying tank (25), the side end face of the base (24) is sleeved with a lower ring (26), the top of the lower ring (26) is fixedly connected with a reinforcing connecting plate (23), the outer side of the upper half section of the reinforcing connecting plate (23) is fixedly connected with an upper ring (21), and the inner side of the upper half section of the reinforcing connecting plate (23) is fixedly connected to the outer surface of the separation device (1);
the surface of the inner side of the base (24) is inserted with a gas control pipe (29), one end of the gas control pipe (29) close to the base (24) is connected with the gas transmission tank (25), one end of the gas control pipe (29) far away from the base (24) is fixedly connected with a gas pipe (28), one end of the gas pipe (28) far away from the gas control pipe (29) is fixedly connected with a gas nozzle (22), the surface of the gas nozzle (22) is fixedly connected with a heat-proof pad (27), and the side face of the heat-proof pad (27) is fixedly connected to the inner side of the bottom of the separation device (1);
the separation device (1) comprises a heat preservation shell (13), the outer surface of the heat preservation shell (13) is fixedly connected to the inner surface of the lower ring (26) and the inner side of the reinforcing connecting plate (23) respectively, and the inner wall of the top of the heat preservation shell (13) is fixedly connected with a gas-liquid separator (16).
2. The ethanol rapid separation device for tantalum ethoxide production according to claim 1, wherein: the inner wall of the heat preservation shell (13) is fixedly connected with a sliding rail (18), the upper half section of the sliding rail (18) is provided with an outflow hole (19), the outflow hole (19) respectively penetrates through the surfaces of the sliding rail (18) and the heat preservation shell (13), and the surface of the sliding rail (18) is slidably connected with a heating cup (11).
3. The ethanol rapid separation device for tantalum ethoxide production according to claim 2, wherein: stifled hole (15) have been seted up on the surface of heating cup (11), stifled hole (15) are in the position that faces slide rail (18), bottom fixedly connected with connecting rod (12) of heating cup (11) inner wall, one end fixedly connected with sheath (14) of heating cup (11) are kept away from in connecting rod (12), the bottom fixedly connected with secondary collector (17) of sheath (14), inboard fixed connection in heat preservation shell (13) bottom is on the side of heat protection pad (27).
4. The ethanol rapid separation device for tantalum ethoxide production according to claim 3, wherein: the secondary collector (17) comprises a collecting shell (171), the top of the collecting shell (171) is fixedly connected to the bottom of the sheath (14), the inner wall of the collecting shell (171) is fixedly connected with a cold plate (172) and a hot plate (175) respectively, the upper surface of the cold plate (172) is fixedly connected with a partition plate (173), and an isolating bag (174) is fixedly connected between the cold plate (172) and the hot plate (175).
5. The ethanol rapid separation device for tantalum ethoxide production according to claim 1, wherein: the air control pipe (29) comprises a pipe shell (292), the top of the pipe shell (292) is fixedly connected with a flower-shaped plate (291), the outer surface of the pipe shell (292) is connected with a pressure relief device (293) in a sliding mode, one end, far away from the pipe shell (292), of the flower-shaped plate (291) is fixedly connected with a limiting block (295), and one end, far away from the flower-shaped plate (291), of the limiting block (295) is fixedly connected with an expansion ball (294).
6. The ethanol rapid separation device for tantalum ethoxide production according to claim 5, wherein: the bottom fixedly connected with heat absorption piece (297) of inflation ball (294), the last fixed surface of heat absorption piece (297) is connected with recovery strip (296), the one end fixed connection that heat absorption piece (297) was kept away from in recovery strip (296) is on the inner wall of shell (292), the surface fixed connection of heat absorption piece (297) has spiral auger (299), the outside fixedly connected with of half section down of spiral auger (299) moves board (298), the bottom fixed connection that moves board (298) is on the surface of heat absorption piece (297).
7. The ethanol rapid separation device for tantalum ethoxide production according to claim 5, wherein: the pressure relief device (293) comprises a circulation plate (2933), an embedded barrel (2932) is connected to the inner wall of the circulation plate (2933) in a sliding mode, the outer surface of the embedded barrel (2932) is connected to the surface of the pipe shell (292) in a sliding mode, a ring groove (2931) is formed in the surface of the embedded barrel (2932), and a cotton body (2934) is fixedly connected to the center of the embedded barrel (2932).
8. The ethanol rapid separation device for tantalum ethoxide production according to claim 7, wherein: the surface of the flower-shaped plate (291) is connected with the output end of the air delivery tank (25), and the outer surface of the circulation plate (2933) is fixedly connected with the air delivery pipe (28).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211401578.9A CN115430162B (en) | 2022-11-10 | 2022-11-10 | Ethanol quick separation device for ethanol tantalum production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211401578.9A CN115430162B (en) | 2022-11-10 | 2022-11-10 | Ethanol quick separation device for ethanol tantalum production |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115430162A true CN115430162A (en) | 2022-12-06 |
| CN115430162B CN115430162B (en) | 2023-02-07 |
Family
ID=84252726
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211401578.9A Active CN115430162B (en) | 2022-11-10 | 2022-11-10 | Ethanol quick separation device for ethanol tantalum production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115430162B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB150940A (en) * | 1920-02-03 | 1920-09-16 | Ariel Clyde Jewell | Improvements in stills |
| CN210612903U (en) * | 2019-08-23 | 2020-05-26 | 贵州苗药药业有限公司 | Novel ball-type concentrator is used in medicine subsides production |
| CN210933819U (en) * | 2019-10-14 | 2020-07-07 | 湖北省三鑫生物科技有限公司 | A evaporating pot for producing resveratrol |
| CN113593742A (en) * | 2021-08-15 | 2021-11-02 | 郭婷婷 | Environment-friendly nuclear wastewater treatment system |
-
2022
- 2022-11-10 CN CN202211401578.9A patent/CN115430162B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB150940A (en) * | 1920-02-03 | 1920-09-16 | Ariel Clyde Jewell | Improvements in stills |
| CN210612903U (en) * | 2019-08-23 | 2020-05-26 | 贵州苗药药业有限公司 | Novel ball-type concentrator is used in medicine subsides production |
| CN210933819U (en) * | 2019-10-14 | 2020-07-07 | 湖北省三鑫生物科技有限公司 | A evaporating pot for producing resveratrol |
| CN113593742A (en) * | 2021-08-15 | 2021-11-02 | 郭婷婷 | Environment-friendly nuclear wastewater treatment system |
Also Published As
| Publication number | Publication date |
|---|---|
| CN115430162B (en) | 2023-02-07 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP4762154B2 (en) | Vacuum extraction device used for extraction of Chinese medicine | |
| CN104399269A (en) | Boiler for preparing concentrated solution | |
| CN110835584B (en) | Simultaneous nitrogen-blowing extraction device and essential oil fidelity extraction method | |
| CN206103371U (en) | Spherical concentrator in vacuum | |
| CN201355161Y (en) | High-efficiency gas-liquid separator | |
| CN115430162B (en) | Ethanol quick separation device for ethanol tantalum production | |
| CN103992880B (en) | A high-efficiency extraction separator for volatile oil | |
| CN106139622A (en) | Liquid vacuum enrichment facility and method for concentration thereof | |
| CN211133067U (en) | Percolation extraction system | |
| CN104873100B (en) | One kind is without hot courage insulating pot | |
| CN104667570A (en) | Traditional Chinese medicine extraction equipment | |
| CN206001929U (en) | A kind of condenser assembly | |
| CN205925038U (en) | Continuous vaporization system of subcritical extract | |
| CN107178938A (en) | A kind of automatic exhaust system | |
| CN201202959Y (en) | Bellows air-discharging free floating ball type steam drain valve | |
| CN102144886A (en) | Miniature full-automatic kungfu tea making pot | |
| CN206887225U (en) | A kind of high vacuum unit for ion plating equipment | |
| CN205850302U (en) | There is the Multifunctional pot for extracting Chinese medicine pressing down foam function online | |
| CN217163267U (en) | Gas-liquid separator for polyurethane curing agent reaction | |
| CN208591558U (en) | A kind of economic benefits and social benefits vacuum concentrator | |
| CN204411770U (en) | A kind of Chinese medicine extractor | |
| CN107726627A (en) | A kind of gas and oil separating plant and its method of hot-oil circulation system | |
| CN214654743U (en) | Demulsifying aromatic oil recovery device | |
| CN208463634U (en) | A kind of energy-saving electric rice pot | |
| CN205412940U (en) | Reation kettle inhales useless liquid device that divides |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |