CN115414287A - Composition with oil control and moisture retention effects and application thereof - Google Patents
Composition with oil control and moisture retention effects and application thereof Download PDFInfo
- Publication number
- CN115414287A CN115414287A CN202211153723.6A CN202211153723A CN115414287A CN 115414287 A CN115414287 A CN 115414287A CN 202211153723 A CN202211153723 A CN 202211153723A CN 115414287 A CN115414287 A CN 115414287A
- Authority
- CN
- China
- Prior art keywords
- effects
- oil
- composition
- extract
- moisturizing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9717—Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Dermatology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a composition with oil control and moisture retention effects and application thereof. The invention creatively discovers that the composition consisting of the hydrolyzed red algae extract, the olive leaf extract, the mogrosia mackeri extract and the betaine has obvious moisturizing and oil controlling effects on skin, can obviously inhibit the reproduction of propionibacterium acnes, obviously reduces the occurrence of skin inflammation and accelerates the self-repairing capability of the skin. The fourth component has a certain synergistic effect on the effects, is very suitable for skin care products, is mild and non-irritant, and has good stability.
Description
Technical Field
The invention belongs to the technical field of cosmetics, relates to a composition with oil control and moisture retention effects and application thereof, and particularly relates to a composition with oil control and moisture retention effects and application thereof in preparation of cosmetics with oil control and moisture retention effects.
Background
Oily skin is a global problem, more common in men and adolescents, and is rooted in the exuberance of sebum secretion. Sebum from healthy skin plays an important role in protecting the skin barrier, protecting skin and hair from abrasion, regulating transepidermal water loss, maintaining skin biofilms, and delivering antioxidants. However, modern people face more stress and environmental pollution, sebum secretion may be disordered, oil secretion is excessive, and lipophilicity bacteria, fungi and parasitic bacteria are excessively bred, so that a series of skin problems are caused, such as inflammation, oily light, large pores, pore blockage, acne, skin thickening and darkness and the like.
In order to suppress excessive sebum secretion, many people increase the number of face washes, and even wash with facial cleanser each time, the more wash the skin feels more oily. When the face is washed for too many times, the secretion of sebum on the face can be stimulated, the oil output is increased, and the skin is dried more and more. The facial grease can be cleared away by washing the face with the facial cleanser in the morning and at night, but the secretion of the facial grease cannot be controlled, because the oil is produced on the surface of oily skin, but the internal part of the skin is seriously lack of water, and after the grease is removed, the effect of controlling the oil can be achieved only by replenishing water for the skin.
Most of the oil control related cosmetics on the market aim at inhibiting sebum secretion, or simply cleaning oil, or adding powder for instantly adsorbing oil, such as silicon powder, kaolin and the like into the product by adopting a physical adsorption method, although a certain effect is achieved, the effects of instantly getting rid of oil gloss, persistently controlling oil and improving skin quality which are required by consumers are not solved. The oily skin can be relieved to a certain extent but the skin can not really get rid of oily light by simply cleaning the oil or adding powder for instantly adsorbing the oil, such as silicon powder, kaolin and the like, into the product by adopting a physical adsorption method.
In order to solve the problems of vigorous sebum secretion and unbalanced sebum secretion of the face of people, reduce the daily oil-out phenomenon of the skin and radically solve the problems of oil-out and greasiness of the face, the development of an oil-control moisturizing skin care product is necessary.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a composition with oil control and moisture retention effects and application thereof, and particularly provides a composition with oil control and moisture retention effects and application thereof in preparing cosmetics with oil control and moisture retention effects.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the present invention provides a composition having oil-controlling and moisturizing effects comprising hydrolyzed red algae extract, olive leaf extract, moguissima extract and betaine.
The seaweed polysaccharide and seaweed protein in the hydrolyzed red seaweed extract can form a protective film on the surface of skin through hydration, prevent water evaporation, help to strengthen and recover the moisture retention state of the skin, and can effectively relieve, repair and improve the skin through mineral elements, amino acids, active peptides and other active substances in the red seaweed penetrating into the skin bottom; the extract of folium Canarii albi (Canarium ALBUM) mainly contains secoiridoid and its glycoside, flavone and its glycoside, biflavone and its glycoside, low molecular tannin, etc., and secoiridoid is the main active ingredient, and has excellent effect on infectious and malignant microorganisms; the extract of Morganga madagascascariensis (HARUNGANA madagascacariensis) can eliminate spots, soothe and correct blemishes, and as a skin tone perfecting agent, provides significant blackhead reduction and pore minimization functions, and improves skin texture; betaine has unique moisture keeping and cell membrane protecting effects, and also has effects of improving moisture keeping ability of skin and hair, increasing solubility of active ingredients in water, and endowing skin and hair with feeling of moistening and smoothing.
The invention creatively discovers that the composition consisting of the hydrolyzed red algae extract, the olive leaf extract, the mogrosia mackeri extract and the betaine has obvious moisturizing and oil controlling effects on skin, can obviously inhibit the reproduction of propionibacterium acnes, obviously reduces the occurrence of skin inflammation and accelerates the self-repairing capability of the skin. The fourth component has a certain synergistic effect on the effects, is very suitable for skin care products, is mild and non-irritant, and has good stability.
Preferably, the mass ratio of the hydrolyzed red algae extract, the olive leaf extract, the motor garland harrenia extract and the betaine is (0.1-5): (0.01-1): (0.01-2): (0.1-5).
When the four components are combined according to a specific mass ratio, the skin moisturizing and oil controlling effects are more remarkable in the aspects of moisturizing and oil controlling of skin and inhibiting of the reproduction of propionibacterium acnes.
The specific point value in the above (0.1-5) may be selected from 0.1, 0.3, 0.5, 0.7, 1, 1.5, 2, 2.5, 3, 3.5, 4, 4.5, 5, etc.
The specific point value in (0.01-1) above may be selected from 0.01, 0.05, 0.08, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1, etc.
The specific point value in (0.01-2) above may be selected from 0.01, 0.05, 0.08, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1, 1.2, 1.5, 1.7, 1.8, 2, etc.
Other specific values within the above ranges can be selected, and are not described in detail herein.
In a second aspect, the present invention provides the use of the composition having oil-controlling and moisturizing effects according to the first aspect in the preparation of cosmetics.
Preferably, the cosmetic comprises essence water, lotion, milky lotion, cream, face toilet, or pack.
Preferably, the composition with oil-controlling and moisturizing effects is contained in the cosmetic in an amount of 0.5-20% by mass, such as 0.5%, 1%, 3%, 5%, 7%, 10%, 12%, 15%, 20%, etc., and other specific values within the numerical range can be selected, which is not described herein again.
In a third aspect, the invention provides an essence lotion with oil control and moisture retention effects, which comprises: the composition with the oil-controlling and moisture-retaining effects, the humectant, the thickener, the skin conditioner and the water in the first aspect.
Preferably, the essential water with oil control and moisturizing effects comprises the following components in parts by weight: 1-10 parts of composition with oil control and moisture retention effects, 1-10 parts of humectant, 0.1-2 parts of thickening agent, 0.1-2.5 parts of skin conditioner and water.
The weight parts of the composition can be selected from 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts and the like.
The humectant can be selected from 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts and the like in parts by weight.
The weight parts of the thickening agent can be selected from 0.1 part, 0.2 part, 0.3 part, 0.5 part, 0.8 part, 1 part, 1.2 parts, 1.5 parts, 1.8 parts, 2 parts and the like.
The parts by weight of the skin conditioner can be selected from 0.1 part, 0.2 part, 0.3 part, 0.5 part, 0.8 part, 1 part, 1.2 part, 1.5 part, 1.8 part, 2 parts, 2.5 parts and the like.
Other specific values within the above ranges can be selected, and are not described in detail herein.
Preferably, the humectant comprises any one or a combination of at least two of hydroxyethyl urea, polyglycerol-10, propylene glycol, inositol, dipropylene glycol, tremella polysaccharide, or sodium PCA; preferably a combination of hydroxyethyl urea, polyglycerol-10 and tremella polysaccharide.
When the humectant selects the specific optimal combination mode, the moisturizing and oil control effects of the product can be further improved, and the hydroxyethyl urea, the polyglycerol-10 and the tremella polysaccharide also have a certain synergistic effect on the effects.
Preferably, the thickener comprises any one of carbomer, glycerol polyacrylate, sodium polyacrylate or Sclerotinia sclerotiorum or a combination of at least two of the same.
Preferably, the skin conditioning agent comprises any one of or a combination of at least two of maltitol, lactobacillus/rice fermentation product, amino acid, dipotassium glycyrrhizinate, niacinamide, beta-glucan, hydrolyzed collagen, or polyglutamic acid.
Preferably, the essence water further comprises any one of or a combination of at least two of a chelating agent, a preservative, a pH regulator and a fragrance.
In a fourth aspect, the invention provides a preparation method of the essence water with oil control and moisturizing effects according to the third aspect, wherein the preparation method comprises the following steps:
mixing humectant, thickener, skin conditioner and water at 40-70 deg.C (such as 40 deg.C, 50 deg.C, 60 deg.C, 70 deg.C, etc.), homogenizing, cooling to 15-40 deg.C (such as 15 deg.C, 20 deg.C, 25 deg.C, 30 deg.C, 35 deg.C, 40 deg.C, etc.), and mixing the mixed matrix with the composition with oil controlling and moisturizing effects of claim 1 or 2.
Other specific point values within the above numerical ranges can be selected, and are not described in detail herein.
Compared with the prior art, the invention has the following beneficial effects:
the invention creatively discovers that the composition consisting of the hydrolyzed red algae extract, the olive leaf extract, the mogrosia mackeri extract and the betaine has obvious moisturizing and oil controlling effects on skin, can obviously inhibit the reproduction of propionibacterium acnes, obviously reduces the occurrence of skin inflammation and accelerates the self-repairing capability of the skin. The fourth component has a certain synergistic effect on the effects, is very suitable for skin care products, is mild and non-irritant, and has good stability.
Detailed Description
To further illustrate the technical means and effects of the present invention, the following further describes the technical solution of the present invention with reference to the preferred embodiments of the present invention, but the present invention is not limited to the scope of the embodiments.
The hydrolyzed red algae extracts referred to in the following examples, comparative examples, application examples, and comparative application examples are products available from Satipidae (Shanghai) specialty Chemicals, inc. under the trade name CONTACTICEL; the folium Canarii albi (Canarium ALBUM) extract is obtained from Zhaoquzhou Zhang JUANGJUN under the name of folium Canarii albi extract; the extract of Morganella madagascasii (Harungana madagascasiensis) is a product available from Spiaceae (Shanghai) specialty Chemicals, inc. under the trade name Subligana; betaine is a product of amino acid humectant purchased from Guanzhou City exhibition Biotechnology Co., ltd; the Beta-Glucan is a product of type AC Yeast Beta-Glucan Beta-Glucan purchased from Norran Biotech, guangzhou; the tremella polysaccharide is a product of tremella heteropolysaccharide (WSK) which is purchased from Shanghai Huiwen biotechnology, inc; the sodium polyacrylate is a product of CoVACRYL AC, which is purchased from Zhenbang daily chemical Co., ltd.
Example 1
The embodiment provides a composition with oil control and moisture retention effects, which comprises the following components in parts by weight: 1 part of hydrolyzed red algae extract, 0.5 part of olive leaf extract, 0.6 part of mogas crabaena extract and 0.8 part of betaine.
Example 2
The embodiment provides a composition with oil control and moisture retention effects, which comprises the following components in parts by weight: 0.6 part of hydrolyzed red algae extract, 0.3 part of olive leaf extract, 0.5 part of mogas crabaena extract and 1.5 parts of betaine.
Example 3
The embodiment provides a composition with oil control and moisture retention effects, which comprises the following components in parts by weight: 1.2 parts of hydrolyzed red algae extract, 0.2 parts of olive leaf extract, 0.4 parts of mogas garbona extract and 1.1 parts of betaine.
Comparative example 1
This comparative example provides a composition which differs from example 1 only in that: the extract is not extracted from hydrolyzed red algae, and is distributed proportionally to the weight of olive leaf extract, magalda extract and betaine.
Comparative example 2
This comparative example provides a composition which differs from example 1 only in that: the olive leaf extract is not contained, and the weight parts of the olive leaf extract are proportionally distributed into the weight parts of the hydrolyzed red algae extract, the motor gasharringtonia extract and the betaine.
Comparative example 3
This comparative example provides a composition which differs from example 1 only in that: without the extract of mogas crabaena, the parts by weight were proportioned to the weight of olive leaf extract, hydrolyzed red algae extract and betaine.
Comparative example 4
This comparative example provides a composition which differs from example 1 only in that: without betaine, the weight parts are proportionally distributed to the weight of olive leaf extract, moguisia amansii extract and hydrolyzed red algae extract.
Application example 1
The application example provides essence water with oil control and moisture retention effects, and the formula of the essence water is as follows:
the preparation method comprises the following steps: mixing humectant, thickener, skin conditioner and water at 60 deg.C, homogenizing, cooling to 30 deg.C, and mixing the mixed matrix with the composition with oil controlling and moisture keeping effects.
Application example 2
The application example provides essence water with oil control and moisturizing effects, and the formula of the essence water is as follows:
the preparation method comprises the following steps: mixing humectant, thickener, skin conditioner and water at 50 deg.C, homogenizing, cooling to 20 deg.C, and mixing the mixed matrix with the composition with oil controlling and moisture keeping effects.
Application example 3
The application example provides essence water with oil control and moisturizing effects, and the formula of the essence water is as follows:
the preparation method comprises the following steps: mixing humectant, thickener, skin conditioner and water at 55 deg.C, homogenizing, cooling to 25 deg.C, and mixing the mixed matrix with the composition with oil controlling and moisture keeping effects.
Comparative application examples 1 to 4
Four kinds of essence lotions were provided, which were different from application example 1 only in that the compositions of example 1 were respectively replaced with the compositions of comparative examples 1 to 4 in equal amounts, and the other components and contents were maintained. The preparation method is the same as application example 1.
Comparative application examples 5 to 8
Four serum solutions were provided which differed from application example 1 only in that the composition of example 1 was replaced equally with a single 3% hydrolyzed red algae extract, olive leaf extract, mogas harrana extract and betaine, respectively, and the other ingredients and contents remained unchanged. Preparation method reference application example 1.
Application example 4
The application example provides essence water with oil control and moisturizing effects, and the formula of the essence water is different from that of the application example 1 only in the following components: and (3) the weight ratio of the non-hydroxyethyl urea to the weight of the polyglycerol-10 and the tremella polysaccharide is proportionally distributed.
Application example 5
The application example provides essence water with oil control and moisturizing effects, and the formula of the essence water is different from that of the application example 1 only in the following components: and (3) the weight ratio of the polyglycerol-10 to the weight of the hydroxyethyl urea and the tremella polysaccharide is proportionally distributed.
Application example 6
The application example provides essence water with oil control and moisturizing effects, and the formula of the essence water is different from that of the application example 1 only in the following components: and (3) distributing the weight ratio of the tremella polysaccharide to the weight of the polyglycerol-10 and the hydroxyethyl urea in proportion so as to avoid the tremella polysaccharide.
Application example 7
The application example provides essence water with oil control and moisturizing effects, and the formula of the essence water is different from that of the application example 1 only in the following components: inositol 2.5%, dipropylene glycol 2% and sodium PCA 1.5%.
Test example 1
Chick embryo test (irritation test):
selecting chicken embryos: 35 fresh, clean and intact chick embryos with the mass of 50g-60g are selected and divided into 7 groups, and each group comprises 5 chick embryos. When the chick embryos are incubated to 9 days old, the chick embryos are checked according to eggs, the chick embryos which are not fertilized, have no activity or are defective are discarded, and the chick embryos which are seriously deformed, broken or thin-shelled are not used.
And (3) testing environment: the room temperature is 20-25 ℃, and the relative humidity is 45-70%. The hatching temperature is 37.5 +/-0.5 ℃, the relative humidity is 55-70 percent, and the frequency of the turntable is 3 times/h to 6 times/h. The 9-day-old chick embryos do not need to rotate when being hatched.
And (3) operation specification: performing egg-lighting inspection on 9-day-old chick embryos, and marking the positions of air chambers on the surfaces of the eggshells; the marked egg shell part (1 silicone rubber ring IS placed on the chorioallantoic membrane of each egg) IS stripped by dental zigzag forceps to expose white egg membrane, the egg membrane IS moistened by sucking and dripping a test substance by a suction pipe, after 5min, the vascular system condition of the egg IS observed by using an amplifying mirror lamp, the blood vessel congestion, the blood vessel bleeding and the blood coagulation vessel are stimulated reactions, and the IS value IS calculated according to a stimulation evaluation method in a cosmetic eye irritation/corrosivity chick embryo chorioallantoic membrane test SN/T2329-2009.
And (4) test conclusion: according to the conditions of observing the chick embryo blood vessel system and the IS value, the IS mean value tested by application examples 1-7 IS less than or equal to 1, and the condition of no stimulation IS adopted.
Test example 2
Propionibacterium acnes inhibition assay:
the bacteriostatic effects of the oil-controlling and moisturizing products prepared in application examples 1-7 and comparative application examples 1-8 on propionibacterium acnes were determined. Preparation of a culture medium: weighing lecithin-Tween nutrient agar culture medium 33g and liquid thioglycollate culture medium 29.3g, respectively, adding 1L ultrapure water, stirring, heating, boiling to dissolve completely, subpackaging, sterilizing at 121 deg.C under high pressure for 30min, cooling to 60 deg.C, and keeping warm in water bath.
Recovery of propionibacterium acnes and preparation of bacterial suspension: the method comprises the steps of melting an ampoule bottle of propionibacterium acnes freeze-dried powder under an alcohol lamp, adding 1mL of 0.85% normal saline, uniformly stirring, inoculating the mixture onto 3 plates containing a culture medium, and then culturing for 3 days under the anaerobic condition at 37 ℃. Scraping slant colony with inoculating ring, and diluting the bacterial suspension with normal saline to make its concentration be 10 6 CFU·mL -1 . Taking the bacterial suspension under aseptic operation, and uniformly smearing the bacterial suspension on a culture medium by using a coating rod. Then, the Oxford cup is lightly placed on the surface of the solidified culture medium by using sterile forceps, and the Oxford cup (the outer diameter is 8 mm) is lightly pressed to ensure good contact. Adding 200 mu L of test solution into the Oxford cup, adding deionized water as a blank control, culturing in an incubator at 37 ℃ for 48h, taking out, and measuring the diameter of the effective inhibition zone of the test solution in each culture dish. Each set of experiments was repeated 3 times, and two samples were taken for testing each time.
And (4) judging the standard: the diameter of the inhibition zone is more than 20mm, the obvious inhibition is realized, and the diameter of the inhibition zone is 10-20mm, the medium inhibition is realized; the diameter of the bacteriostatic circle is less than 10mm, and no bacteriostatic action is realized; the results are shown in table 1:
TABLE 1
As can be seen from the data in Table 1: the composition and the essence water thereof have good inhibition effect on propionibacterium acnes, and compared with products prepared in application examples 1-4, the composition and the essence water thereof have certain inhibition effect, but compared with application examples 5-8, the composition and the essence water thereof have almost no inhibition effect; and the four components of the hydrolyzed red algae extract, the olive leaf extract, the moguisinga nervosa extract and the betaine in the composition have certain synergistic effect on the effects, have a remarkable inhibiting effect on propionibacterium acnes, effectively control the propagation of the propionibacterium acnes and maintain the ecological balance of skin colonies.
Test example 3
And (3) oil control effect testing:
respectively weighing 4g of the essence water of the application examples 1-7 and the comparative application examples 1-8, uniformly coating the essence water on a glass culture dish with the diameter of 60mm, placing the glass culture dish in a constant temperature box with the temperature of 30 ℃, standing for 48 hours, and then placing the glass culture dish at the temperature of 25 ℃ for 30 minutes; then, 40. Mu.l of oleic acid was dropped onto the middle position of the petri dish, and after standing for 30min, the diffusion area of oleic acid was observed, and the oil spot diameter was measured. Each product was made into 3 groups and the average was taken. The smaller the diameter of the oil spot is, the stronger the oil control capability of the product is. The results are shown in table 2:
TABLE 2
As can be seen from the data in Table 2: compared with a comparative application example, the composition and the essential water thereof have stronger oil adsorption capacity and better oil control effect; the four components of the hydrolyzed red algae extract, the olive leaf extract, the mogas canadensis harrenia extract and the betaine in the composition have certain synergistic effect on the effects, and the four components are matched but not matched; and the combination mode of the humectant also influences the oil control effect of the product to a certain extent.
Test example 4
And (4) testing the moisture retention performance:
the essences prepared in application examples 1 to 7 and comparative application examples 1 to 8 were compared with the change in skin moisture content before and after use (consistency of use), and subjects had 150 volunteers among them: 120 men, 30 men, between 20 and 40 years of age, with a mean age of 28 years, randomly divided into 15 groups of 8 women and 2 men.
Cleaning forearm of the testee, sitting at a set humidity for 30min, and selecting 3 × 3cm of forearm of the testee 2 The water content of each experimental part is detected by a Corneometer CM825 and repeated for 3 times, and the average value is obtained and recorded.
The skin hydration rate is calculated as:
the average skin hydration results for the subjects 2 hours after using the samples are shown in table 3:
TABLE 3
| Group of | Rate of skin hydration |
| Application example 1 | 43.6％ |
| Application example 2 | 41.3％ |
| Application example 3 | 43.5％ |
| Application example 4 | 34.4％ |
| Application example 5 | 31.9％ |
| Application example 6 | 35.7％ |
| Application example 7 | 31.6％ |
| Comparative application example 1 | 18.3％ |
| Comparative application example 2 | 24.8％ |
| Comparative application example 3 | 26.5％ |
| Comparative application example 4 | 20.1％ |
| Comparative application example 5 | 15.4％ |
| Comparative application example 6 | 8.4％ |
| Comparative application example 7 | 7.9％ |
| Comparative application example 8 | 17.2％ |
As can be seen from the data in Table 3: compared with a comparative application example, the composition and the essence water thereof have stronger moisturizing effect; the four components of the hydrolyzed red algae extract, the olive leaf extract, the mogas canadensis harrenia extract and the betaine in the composition have certain synergistic effect on the effects, and the four components are matched but not matched; and the combination mode of the humectant further influences the moisturizing effect of the product obviously.
The applicant states that the present invention is illustrated by the above examples, but the present invention is not limited to the above examples, i.e. it does not mean that the present invention must be implemented by the above examples. It should be understood by those skilled in the art that any modification of the present invention, equivalent substitutions of the raw materials of the product of the present invention, addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.
The preferred embodiments of the present invention have been described in detail, however, the present invention is not limited to the specific details of the above embodiments, and various simple modifications may be made to the technical solution of the present invention within the technical idea of the present invention, and these simple modifications are within the protective scope of the present invention.
It should be noted that, in the above embodiments, the various features described in the above embodiments may be combined in any suitable manner, and in order to avoid unnecessary repetition, the present invention does not separately describe various possible combinations.
Claims (10)
1. A composition with oil controlling and moisturizing effects is characterized by comprising hydrolyzed red algae extract, olive leaf extract, moguissima harrana extract and betaine.
2. The composition with effects of controlling oil and preserving moisture as claimed in claim 1, wherein the mass ratio of the hydrolyzed red algae extract, the olive leaf extract, the moguisagana extract and the betaine is (0.1-5): 0.01-1): 0.01-2): 0.1-5.
3. Use of the composition with oil-controlling and moisturizing effects according to claim 1 or 2 in the preparation of cosmetics.
4. The use according to claim 3, wherein the cosmetic comprises an essence, a lotion, an emulsion, a cream, a face lotion or a mask;
preferably, the composition with the effects of controlling oil and moisturizing is 0.5-20% of the cosmetic by mass.
5. The essence water with the effects of controlling oil and preserving moisture is characterized by comprising the following components in parts by weight: composition, moisturizer, thickener, skin conditioner, water with oil control and moisturizing effects according to claim 1 or 2.
6. The essence water with oil control and moisturizing effects as claimed in claim 5, wherein the essence water with oil control and moisturizing effects comprises the following components in parts by weight: the composition with the effects of controlling oil and moisturizing as claimed in claim 1 or 2, 1-10 parts of moisturizer, 0.1-2 parts of thickener, 0.1-2.5 parts of skin conditioner and water.
7. The essence lotion with oil control and moisture retention efficacy according to claim 5 or 6, wherein the moisture retention agent comprises any one or a combination of at least two of hydroxyethyl urea, polyglycerol-10, propylene glycol, inositol, dipropylene glycol, tremella polysaccharide or sodium PCA; preferably a combination of hydroxyethyl urea, polyglycerol-10 and tremella polysaccharide.
8. The essential water with the effects of controlling oil and moisturizing as claimed in claim 5 or 6, wherein the thickener comprises any one or a combination of at least two of carbomer, glycerol polyacrylate, sodium polyacrylate or sclerotium rolfsii;
preferably, the skin conditioning agent comprises any one of or a combination of at least two of maltitol, lactobacillus/rice fermentation product, amino acid, dipotassium glycyrrhizinate, niacinamide, beta-glucan, hydrolyzed collagen or polyglutamic acid.
9. The essence lotion with oil control and moisture retention effects according to any one of claims 5 to 8, wherein the essence lotion further comprises any one or a combination of at least two of a chelating agent, a preservative, a pH regulator and a fragrance.
10. The preparation method of essential water with oil control and moisture retention effects according to any one of claims 5-8, characterized by comprising the following steps:
mixing humectant, thickener, skin conditioner and water at 40-70 deg.C, homogenizing, cooling to 15-40 deg.C, and mixing the mixed matrix with the composition with oil controlling and moisturizing effects of claim 1 or 2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211153723.6A CN115414287B (en) | 2022-09-21 | 2022-09-21 | Composition with oil control and moisturizing effects and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211153723.6A CN115414287B (en) | 2022-09-21 | 2022-09-21 | Composition with oil control and moisturizing effects and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115414287A true CN115414287A (en) | 2022-12-02 |
| CN115414287B CN115414287B (en) | 2023-07-07 |
Family
ID=84203514
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211153723.6A Active CN115414287B (en) | 2022-09-21 | 2022-09-21 | Composition with oil control and moisturizing effects and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115414287B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117045578A (en) * | 2023-09-12 | 2023-11-14 | 广东科盈科技有限公司 | Acne-removing and oil-controlling composition containing motor Gastrodia elata extract and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106860067A (en) * | 2015-12-08 | 2017-06-20 | 巴斯夫美容护理法国公司 | The cosmetic of Madagascar's Ha Lunjiana extracts and/or dermatological use |
| CN109069563A (en) * | 2016-04-21 | 2018-12-21 | 化工产品开发公司Seppic | For treating and/or preventing Madagascar's Ha Lunjiana leaf extract of acne |
| CN112107533A (en) * | 2020-09-27 | 2020-12-22 | 广州妮趣化妆品有限公司 | Composition with effects of controlling oil, tendering skin and collecting fine pores and preparation method and application thereof |
| CN113018241A (en) * | 2021-04-08 | 2021-06-25 | 重庆灵方三帆医药贸易有限公司 | Formula for making rice vinegar shower gel |
| US20220211607A1 (en) * | 2019-04-11 | 2022-07-07 | Natura Cosméticos S.A. | Topical cosmetic composition and uses thereof |
-
2022
- 2022-09-21 CN CN202211153723.6A patent/CN115414287B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106860067A (en) * | 2015-12-08 | 2017-06-20 | 巴斯夫美容护理法国公司 | The cosmetic of Madagascar's Ha Lunjiana extracts and/or dermatological use |
| CN109069563A (en) * | 2016-04-21 | 2018-12-21 | 化工产品开发公司Seppic | For treating and/or preventing Madagascar's Ha Lunjiana leaf extract of acne |
| US20220211607A1 (en) * | 2019-04-11 | 2022-07-07 | Natura Cosméticos S.A. | Topical cosmetic composition and uses thereof |
| CN112107533A (en) * | 2020-09-27 | 2020-12-22 | 广州妮趣化妆品有限公司 | Composition with effects of controlling oil, tendering skin and collecting fine pores and preparation method and application thereof |
| CN113018241A (en) * | 2021-04-08 | 2021-06-25 | 重庆灵方三帆医药贸易有限公司 | Formula for making rice vinegar shower gel |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117045578A (en) * | 2023-09-12 | 2023-11-14 | 广东科盈科技有限公司 | Acne-removing and oil-controlling composition containing motor Gastrodia elata extract and application thereof |
| CN117045578B (en) * | 2023-09-12 | 2024-02-13 | 广东科盈科技有限公司 | Acne-removing and oil-controlling composition containing motor Gastrodia elata extract and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN115414287B (en) | 2023-07-07 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107019655B (en) | Oil control composition and application thereof | |
| CN110115704B (en) | Enzyme composition and application thereof in cosmetics with whitening function | |
| CN115414287B (en) | Composition with oil control and moisturizing effects and application thereof | |
| CN110478308B (en) | Cosmetic composition containing yeast fermentation product extract and preparation method thereof | |
| CN111407682A (en) | Cosmetic preservative and preparation method and application thereof | |
| CN102949460A (en) | Application of melaleuca alternifolia oil and preparation thereof | |
| CN111904909B (en) | Dandruff removing scalp essence containing rose fermentation liquor and preparation method thereof | |
| CN114767561B (en) | Anti-dandruff shampoo composition | |
| CN115414308B (en) | Acne-removing composition, preparation method and application | |
| CN116650351A (en) | Skin care lotion and preparation method thereof | |
| CN113797129B (en) | Antibacterial composition and preparation method and application thereof | |
| CN114788795A (en) | Acne-removing composition and preparation method and application thereof | |
| JPH03236319A (en) | Skin drug for external use | |
| CN112522150B (en) | Rice washing water plant fermentation product capable of long-acting removing dandruff and relieving itching and preparation method thereof | |
| CN111514053B (en) | Composition with acne removing effect and preparation method and application thereof | |
| CN107737062A (en) | A kind of hyaluronic acid BB frosts and preparation method with multi-efficiency | |
| CN113244140A (en) | Composition for regulating skin micro-ecological balance and application and preparation method thereof | |
| CN111467288A (en) | Hand-washing-free disinfectant and preparation method thereof | |
| CN116270291B (en) | Odor-removing skin care composition and application thereof | |
| CN116617356B (en) | Alopecia preventing composition, and preparation method and application thereof | |
| WO2017113263A1 (en) | Novel use of gluconacetobacter xylinus fermentation broth as cosmetic composition | |
| CN108498399B (en) | Compound plant extract with antiseptic effect and application thereof in cosmetic antiseptic | |
| CN112402455B (en) | Application of fermented yak milk extract | |
| KR20090001268A (en) | Cosmetic composition comprising thyme oil for treating acne vulgaris | |
| CN106753890A (en) | A kind of sterilization hand-guarding liquid detergent and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |