CN114813818A - System for researching material rapid cooling and rapid heating properties - Google Patents
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- 238000010438 heat treatment Methods 0.000 title claims abstract description 87
- 239000000463 material Substances 0.000 title claims abstract description 48
- 238000001816 cooling Methods 0.000 title claims abstract description 31
- 230000007246 mechanism Effects 0.000 claims abstract description 28
- 238000012360 testing method Methods 0.000 claims abstract description 19
- GALOTNBSUVEISR-UHFFFAOYSA-N molybdenum;silicon Chemical compound [Mo]#[Si] GALOTNBSUVEISR-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052593 corundum Inorganic materials 0.000 claims description 18
- 239000010431 corundum Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 230000000171 quenching effect Effects 0.000 claims description 10
- 239000011261 inert gas Substances 0.000 claims description 8
- 238000010791 quenching Methods 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 4
- 230000032683 aging Effects 0.000 abstract description 3
- 230000003647 oxidation Effects 0.000 abstract description 2
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 230000035939 shock Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 7
- 238000010586 diagram Methods 0.000 description 3
- 230000002572 peristaltic effect Effects 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
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Abstract
Description
技术领域technical field
本发明涉及材料性质测试技术领域,具体为一种研究材料急冷急热性质的系统。The invention relates to the technical field of material property testing, in particular to a system for studying the rapid cooling and rapid heating properties of materials.
背景技术Background technique
在工业生产过程中,需要用到各式各样的化学材料,而不同化学材料的性质决定了它的用途,因此在化学材料的生产制备过程中,常常需要对其不同方面的性质进行研究、测试。In the process of industrial production, a variety of chemical materials need to be used, and the properties of different chemical materials determine their uses. test.
化学材料研究时,常常需要对其耐急冷急热的性质进行测试,而现有技术中研究材料急冷急热性质的方法较为复杂,且不方便对材料进行加热与冷却状态的快速转换。When researching chemical materials, it is often necessary to test their resistance to rapid cooling and rapid heating. However, the methods for studying the rapid cooling and rapid heating properties of materials in the prior art are relatively complicated, and it is inconvenient to rapidly switch the heating and cooling states of materials.
为此,我们提出一种研究材料急冷急热性质的系统。To this end, we propose a system to study the quenching and heating properties of materials.
发明内容SUMMARY OF THE INVENTION
本发明的目的在于提供一种研究材料急冷急热性质的系统,以解决上述背景技术中提出的问题。The purpose of the present invention is to provide a system for studying the quenching and heating properties of materials, so as to solve the problems raised in the above-mentioned background art.
为实现上述目的,本发明提供如下技术方案:一种研究材料急冷急热性质的系统,包括测试机构,所述测试机构上设置有加热机构和冷却机构,所述测试机构包括支撑架、固定在所述支撑架下方的电器箱、设置在所述电器箱内部的变压器、固定在所述支撑架上的控制屏,所述加热机构包括固定在所述支撑架上方的加热箱、设置在所述加热箱内部的硅钼棒、开设在所述加热箱顶部的出气孔、固定在所述加热箱内壁上的保温层、设置在所述加热箱侧壁上的水蒸气输入管、连接在所述加热箱侧壁上的惰性气体输入管、固定在所述加热箱侧壁上的注射泵、连接在所述水蒸气输入管上的预热组件、活动连接在所述加热箱底部的防火炉门、活动连接在所述防火炉门上的调节组件,所述冷却机构包括固定在所述电器箱内部的电动升降柱、固定在所述电动升降柱顶端的载物炉门、设置在所述载物炉门顶部的刚玉坩埚、固定在所述刚玉坩埚底部的刚玉垫板、固定在所述支撑架上的支撑板、设置在所述支撑板上的风机。In order to achieve the above object, the present invention provides the following technical solutions: a system for studying the rapid cooling and rapid heating properties of materials, including a testing mechanism, the testing mechanism is provided with a heating mechanism and a cooling mechanism, and the testing mechanism includes a support frame, which is fixed on the The electrical box below the support frame, the transformer arranged inside the electrical box, and the control panel fixed on the support frame, the heating mechanism includes a heating box fixed above the support frame, a heating box arranged on the The silicon molybdenum rod inside the heating box, the air outlet opening on the top of the heating box, the thermal insulation layer fixed on the inner wall of the heating box, the water vapor input pipe arranged on the side wall of the heating box, connected to the An inert gas input pipe on the side wall of the heating box, a syringe pump fixed on the side wall of the heating box, a preheating assembly connected to the water vapor input pipe, and a fireproof furnace door movably connected to the bottom of the heating box , an adjustment assembly movably connected to the fireproof furnace door, the cooling mechanism includes an electric lifting column fixed inside the electrical box, a loading furnace door fixed on the top of the electric lifting column, The corundum crucible on the top of the furnace door, the corundum backing plate fixed on the bottom of the corundum crucible, the support plate fixed on the support frame, and the fan arranged on the support plate.
进一步的,所述控制屏与电动升降柱、步进电机之间电性连接。Further, the control screen is electrically connected with the electric lifting column and the stepping motor.
进一步的,所述加热箱的内部固定连接有测温热电偶。Further, a temperature measuring thermocouple is fixedly connected to the inside of the heating box.
进一步的,所述预热组件包括连接在水蒸气输入管上的预热炉、连接在所述预热炉上的预热热电偶。Further, the preheating assembly includes a preheating furnace connected to the water vapor input pipe, and a preheating thermocouple connected to the preheating furnace.
进一步的,所述调节组件包括固定连接在所述支撑架上的三脚架、设置在所述三脚架上的导向杆、转动连接在所述三脚架上的滚珠丝杆、固定连接在所述防火炉门上的螺母套、固定在所述滚珠丝杆一端的步进电机。Further, the adjustment assembly includes a tripod fixedly connected to the support frame, a guide rod disposed on the tripod, a ball screw rotatably connected to the tripod, and fixedly connected to the fireproof furnace door. The nut sleeve and the stepping motor fixed at one end of the ball screw.
进一步的,所述导向杆的数量为两个,且防火门的两侧均开设有与导向杆相适配的导向孔。Further, the number of the guide rods is two, and both sides of the fire door are provided with guide holes adapted to the guide rods.
进一步的,所述螺母套的内部开设有与滚珠丝杆相适配的螺纹孔。Further, the inside of the nut sleeve is provided with a threaded hole adapted to the ball screw.
进一步的,所述电动升降柱与风机之间电性连接。Further, the electric lift column and the fan are electrically connected.
进一步的,所述风机的数量为两个,且两个风机左右对称固定在支撑板上。Further, the number of the fans is two, and the two fans are symmetrically fixed on the support plate from left to right.
本发明至少具备以下有益效果:The present invention at least has the following beneficial effects:
通过设置的加热箱、硅钼棒、预热组件等结构,能够对物料进行快速加热,通过设置的风机能够快速对物料进行冷却,且通过启动电动升降柱上下移动,能够使物料在加热与冷却两种状态下进行快速转换,便于对其进行多次重复急冷急热操作,操作简单,省时省力,不仅可以对物料进行热氧老化、热冲击循环等多种试验,还可以通过控制屏设置急冷急热的循环次数,进行连续作业,进一步提高了研究时的实用性。The material can be quickly heated by the set heating box, silicon molybdenum rod, preheating components and other structures, and the material can be quickly cooled by the set fan, and the material can be heated and cooled by starting the electric lifting column to move up and down. The rapid conversion between the two states is convenient for repeated rapid cooling and rapid heating operations. The operation is simple, time-saving and labor-saving. Not only can the material be subjected to various tests such as thermal oxygen aging, thermal shock cycle, etc., it can also be set through the control panel. The number of cycles of rapid cooling and rapid heating is performed continuously, which further improves the practicability during research.
当然,实施本发明的任一产品并不一定需要同时达到以上所述的所有优点。Of course, it is not necessary for any product embodying the present invention to achieve all of the advantages described above simultaneously.
附图说明Description of drawings
图1为本发明整体结构的立体示意图;Fig. 1 is the three-dimensional schematic diagram of the overall structure of the present invention;
图2为本发明整体结构的俯视图;Fig. 2 is the top view of the overall structure of the present invention;
图3为本发明A-A处结构的剖视图;Fig. 3 is the sectional view of the structure at A-A of the present invention;
图4为本发明整体结构的左视图;Fig. 4 is the left side view of the overall structure of the present invention;
图5为本发明整体结构的正视图;Fig. 5 is the front view of the overall structure of the present invention;
图6为本发明冷却状态的示意图;Fig. 6 is the schematic diagram of cooling state of the present invention;
图7为本发明加热状态的示意图。FIG. 7 is a schematic diagram of the heating state of the present invention.
附图标记:Reference number:
100、测试机构;101、支撑架;102、电器箱;103、变压器;104、控制屏;100, testing organization; 101, support frame; 102, electrical box; 103, transformer; 104, control panel;
200、加热机构;201、加热箱;202、硅钼棒;203、出气孔;204、保温层;205、水蒸气输入管;206、惰性气体输入管;207、注射泵;208、预热组件;2081、预热炉;2082、预热热电偶;209、防火炉门;210、调节组件;2101、三脚架;2102、导向杆;2103、滚珠丝杆;2104、螺母套;2105、步进电机;200, heating mechanism; 201, heating box; 202, silicon molybdenum rod; 203, air outlet; 204, insulation layer; 205, water vapor input pipe; 206, inert gas input pipe; 207, syringe pump; 208, preheating component ;2081, preheating furnace; 2082, preheating thermocouple; 209, fireproof furnace door; 210, adjusting component; 2101, tripod; 2102, guide rod; 2103, ball screw; 2104, nut sleeve; 2105, stepping motor ;
300、冷却机构;301、电动升降柱;302、载物炉门;303、刚玉坩埚;304、刚玉垫板;305、支撑板;306、风机。300, cooling mechanism; 301, electric lift column; 302, load furnace door; 303, corundum crucible; 304, corundum backing plate; 305, support plate; 306, fan.
具体实施方式Detailed ways
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, but not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.
请参阅图1-7,本发明提供一种技术方案:一种研究材料急冷急热性质的系统,包括:包括测试机构100,所述测试机构100上设置有加热机构200和冷却机构300,所述测试机构100包括支撑架101、固定在所述支撑架101下方的电器箱102、设置在所述电器箱102内部的变压器103、固定在所述支撑架101上的控制屏104,控制屏104与电动升降柱301、步进电机2105之间电性连接,利用测试机构100能够对物料上下调节,使之向上移动至加热箱201内即可进行加热操作,向下移动至风机306处即可进行冷却操作,以此方式对物料重复多次加热与冷却,便于对其进行热氧老化实验,而加热机构200则通过硅钼棒202、测温热电偶等结构对物料进行加热操作,冷却机构300则可以对物料进行快速冷却。Referring to FIGS. 1-7, the present invention provides a technical solution: a system for studying the quenching and quenching properties of materials, including: a
所述加热机构200包括固定在所述支撑架101上方的加热箱201,加热箱201的内部固定连接有测温热电偶,可以对加热箱201内部的温度进行实时监测、设置在所述加热箱201内部的硅钼棒202,可以给加热箱201进行加热,最高可加热至1600°、开设在所述加热箱201顶部的出气孔203、固定在所述加热箱201内壁上的保温层204、设置在所述加热箱201侧壁上的水蒸气输入管205、连接在所述加热箱201侧壁上的惰性气体输入管206、固定在所述加热箱201侧壁上的注射泵207,利用注射泵207,能够将惰性气体注入惰性气体输入管206内,使其通入加热箱201内、连接在所述水蒸气输入管205上的预热组件208、活动连接在所述加热箱201底部的防火炉门209,利用防火炉门209,可以防止加热箱201内走火和其内部温场稳定、活动连接在所述防火炉门209上的调节组件210。The
需要说明的是,水蒸气输入管205外部连接有蠕动泵(现有设备,图中未示意),利用蠕动泵能够将水注入预热组件208内进行加热。It should be noted that a peristaltic pump (existing equipment, not shown in the figure) is externally connected to the water
进一步的,预热组件208包括连接在水蒸气输入管205上的预热炉2081、连接在所述预热炉2081上的预热热电偶2082,利用预热组件208,能够对蠕动泵输入的水进行加热,便于使之变成饱和水蒸气,通入加热箱201内。Further, the
另一方面,调节组件210包括固定连接在所述支撑架101上的三脚架2101、设置在所述三脚架2101上的导向杆2102,导向杆2102的数量为两个,且防火门的两侧均开设有与导向杆2102相适配的导向孔、转动连接在所述三脚架2101上的滚珠丝杆2103、固定连接在所述防火炉门209上的螺母套2104,螺母套2104的内部开设有与滚珠丝杆2103相适配的螺纹孔、固定在所述滚珠丝杆2103一端的步进电机2105,步进电机2105与控制屏104之间电性连接,通过控制屏104启动步进电机2105带动滚珠丝杆2103转动,能够带动螺母套2104转动,以此便于带动防火炉门209左右移动对加热箱201进行开启或关闭。On the other hand, the
具体的,如图7所示,使物料处于加热室内后,通过控制屏104启动硅钼棒202,对加热箱201内进行加热,加热至设定温度后进行恒温加热,然后在加热的过程中,启动注射泵207与预热组件208,还能够分别将惰性气体与饱和水蒸气输送到加热箱201内,通入惰性气体便于避免物料加热时被氧化,通入饱和水蒸气便于充当加热介质,使加热箱201内温度均匀。Specifically, as shown in FIG. 7, after the material is placed in the heating chamber, the silicon molybdenum rod 202 is activated through the
冷却机构300包括固定在所述电器箱102内部的电动升降柱301,控制屏104与电动升降柱301之间电性连接,方便通过控制屏104控制电动升降柱301上下移动、固定在所述电动升降柱301顶端的载物炉门302、设置在所述载物炉门302顶部的刚玉坩埚303,用来盛放物料、固定在所述刚玉坩埚303底部的刚玉垫板304,刚玉垫板304具有承重强、耐高温的性质,能够在加热时对物料进行支撑、固定在所述支撑架101上的支撑板305、设置在所述支撑板305上的风机306,风机306的数量为两个,且两个风机306左右对称固定在支撑板305上,利用风机306对物料进行快速降温。The
需要说明的是,风机306与电动升降柱301、控制屏104之间电性连接,通过控制屏104可以使电动升降柱301与风机306之间产生动作联动,当电动升降柱301向下移动带动载物炉门302随之下降时,风机306会自动打开对物料进行强制冷却,当电动升降柱301带动载物炉门302向上移动时,风机306便会自动停止。It should be noted that the
具体的,如图6所示,通过控制屏104启动电动升降柱301收缩,使其带动刚玉坩埚303向下移动,当刚玉坩埚303向下移动时,风机306即会自动启动对物料进行冷却,同时步进电机2105也会启动带动滚珠丝杆2103转动,并利用螺母套2104带动防火炉门209移动对加热箱201进行关闭,避免加热箱201走火。Specifically, as shown in FIG. 6, the
本发明的工作原理:如图3所示,首先将物料装入刚玉坩埚303内,然后启动电动升降柱301带动刚玉坩埚303向上移动,当刚玉坩埚303向上移动时,控制屏104会启动步进电机2105带动滚珠丝杆2103转动,并利用螺母套2104在滚珠丝杆2103上移动带动防火炉门209向左移动对加热箱201进行开启,然后电动升降柱301继续上升带动刚玉坩埚303进入到加热箱201内,此时启动硅钼棒202对物料进行加热处理,当加热完成后,再次启动电动升降柱301使其向下移动风机306处,在电动升降柱301向下移动的同时风机306会启动对物料进行快速冷却,以此往复,能够对物料进行重复加热与冷却,便于对物料进行耐急冷急热性质的实验。The working principle of the present invention: as shown in Figure 3, firstly, the material is loaded into the
需要说明的是,在本文中,诸如第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来,而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且,术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含,从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素,而且还包括没有明确列出的其他要素,或者是还包括为这种过程、方法、物品或者设备所固有的要素。It should be noted that, in this document, relational terms such as first and second are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any relationship between these entities or operations. any such actual relationship or sequence exists. Moreover, the terms "comprising", "comprising" or any other variation thereof are intended to encompass a non-exclusive inclusion such that a process, method, article or device that includes a list of elements includes not only those elements, but also includes not explicitly listed or other elements inherent to such a process, method, article or apparatus.
尽管已经示出和描述了本发明的实施例,对于本领域的普通技术人员而言,可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型,本发明的范围由所附权利要求及其等同物限定。Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, and substitutions can be made in these embodiments without departing from the principle and spirit of the invention and modifications, the scope of the present invention is defined by the appended claims and their equivalents.
Claims (9)
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