CN114767575A - Fluffy shampoo composition - Google Patents
Fluffy shampoo composition Download PDFInfo
- Publication number
- CN114767575A CN114767575A CN202210467197.4A CN202210467197A CN114767575A CN 114767575 A CN114767575 A CN 114767575A CN 202210467197 A CN202210467197 A CN 202210467197A CN 114767575 A CN114767575 A CN 114767575A
- Authority
- CN
- China
- Prior art keywords
- composition
- hair
- parts
- polyurethane
- fluffy
- Prior art date
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Links
- 239000000203 mixture Substances 0.000 title claims abstract description 59
- 239000002453 shampoo Substances 0.000 title claims abstract description 48
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 32
- 229920002635 polyurethane Polymers 0.000 claims abstract description 20
- 239000004814 polyurethane Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 244000068988 Glycine max Species 0.000 claims abstract description 15
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 15
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 15
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 8
- -1 pH regulator Substances 0.000 claims abstract description 8
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 6
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 6
- 239000002888 zwitterionic surfactant Substances 0.000 claims abstract description 6
- 239000003755 preservative agent Substances 0.000 claims abstract description 5
- 230000002335 preservative effect Effects 0.000 claims abstract description 5
- 239000002562 thickening agent Substances 0.000 claims abstract description 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 15
- 230000002040 relaxant effect Effects 0.000 claims description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 230000003750 conditioning effect Effects 0.000 claims description 5
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 4
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 4
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 claims description 3
- 229930182478 glucoside Natural products 0.000 claims description 3
- 150000002333 glycines Chemical class 0.000 claims description 3
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 108700004121 sarkosyl Proteins 0.000 claims description 3
- 210000000582 semen Anatomy 0.000 claims description 3
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 3
- 235000010234 sodium benzoate Nutrition 0.000 claims description 3
- 239000004299 sodium benzoate Substances 0.000 claims description 3
- 229960004025 sodium salicylate Drugs 0.000 claims description 3
- OYINQIKIQCNQOX-UHFFFAOYSA-M 2-hydroxybutyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCC(O)C[N+](C)(C)C OYINQIKIQCNQOX-UHFFFAOYSA-M 0.000 claims description 2
- 239000004475 Arginine Substances 0.000 claims description 2
- ODKSFYDXXFIFQN-BYPYZUCNSA-P L-argininium(2+) Chemical compound NC(=[NH2+])NCCC[C@H]([NH3+])C(O)=O ODKSFYDXXFIFQN-BYPYZUCNSA-P 0.000 claims description 2
- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims description 2
- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 claims description 2
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims 1
- 244000007835 Cyamopsis tetragonoloba Species 0.000 claims 1
- 229940079776 sodium cocoyl isethionate Drugs 0.000 claims 1
- 210000004209 hair Anatomy 0.000 abstract description 88
- 210000004761 scalp Anatomy 0.000 abstract description 34
- 230000000694 effects Effects 0.000 abstract description 26
- 230000000052 comparative effect Effects 0.000 description 33
- 238000012360 testing method Methods 0.000 description 27
- 239000004519 grease Substances 0.000 description 11
- 238000003756 stirring Methods 0.000 description 10
- 238000011156 evaluation Methods 0.000 description 9
- 230000003741 hair volume Effects 0.000 description 8
- 210000003128 head Anatomy 0.000 description 8
- 208000001840 Dandruff Diseases 0.000 description 6
- 239000000835 fiber Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 210000002374 sebum Anatomy 0.000 description 6
- 210000003491 skin Anatomy 0.000 description 6
- 239000002390 adhesive tape Substances 0.000 description 5
- 125000002091 cationic group Chemical group 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 150000001413 amino acids Chemical class 0.000 description 4
- 230000008859 change Effects 0.000 description 4
- 239000000428 dust Substances 0.000 description 4
- 230000028327 secretion Effects 0.000 description 4
- 229920002907 Guar gum Polymers 0.000 description 3
- ARIWANIATODDMH-UHFFFAOYSA-N Lauric acid monoglyceride Natural products CCCCCCCCCCCC(=O)OCC(O)CO ARIWANIATODDMH-UHFFFAOYSA-N 0.000 description 3
- 239000003599 detergent Substances 0.000 description 3
- 230000002708 enhancing effect Effects 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 239000000665 guar gum Substances 0.000 description 3
- 229960002154 guar gum Drugs 0.000 description 3
- 235000010417 guar gum Nutrition 0.000 description 3
- 229940049964 oleate Drugs 0.000 description 3
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 description 2
- AJBZENLMTKDAEK-UHFFFAOYSA-N 3a,5a,5b,8,8,11a-hexamethyl-1-prop-1-en-2-yl-1,2,3,4,5,6,7,7a,9,10,11,11b,12,13,13a,13b-hexadecahydrocyclopenta[a]chrysene-4,9-diol Chemical compound CC12CCC(O)C(C)(C)C1CCC(C1(C)CC3O)(C)C2CCC1C1C3(C)CCC1C(=C)C AJBZENLMTKDAEK-UHFFFAOYSA-N 0.000 description 2
- 201000004384 Alopecia Diseases 0.000 description 2
- 235000003880 Calendula Nutrition 0.000 description 2
- 240000001432 Calendula officinalis Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000000686 essence Substances 0.000 description 2
- 230000029142 excretion Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000005189 flocculation Methods 0.000 description 2
- 230000016615 flocculation Effects 0.000 description 2
- 210000001061 forehead Anatomy 0.000 description 2
- 210000003780 hair follicle Anatomy 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 229920002545 silicone oil Polymers 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 238000002834 transmittance Methods 0.000 description 2
- 238000011282 treatment Methods 0.000 description 2
- 229910002012 Aerosil® Inorganic materials 0.000 description 1
- YDNKGFDKKRUKPY-JHOUSYSJSA-N C16 ceramide Natural products CCCCCCCCCCCCCCCC(=O)N[C@@H](CO)[C@H](O)C=CCCCCCCCCCCCCC YDNKGFDKKRUKPY-JHOUSYSJSA-N 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- 244000303965 Cyamopsis psoralioides Species 0.000 description 1
- 102000016942 Elastin Human genes 0.000 description 1
- 108010014258 Elastin Proteins 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- 102000011782 Keratins Human genes 0.000 description 1
- 108010076876 Keratins Proteins 0.000 description 1
- BACYUWVYYTXETD-UHFFFAOYSA-N N-Lauroylsarcosine Chemical compound CCCCCCCCCCCC(=O)N(C)CC(O)=O BACYUWVYYTXETD-UHFFFAOYSA-N 0.000 description 1
- CRJGESKKUOMBCT-VQTJNVASSA-N N-acetylsphinganine Chemical compound CCCCCCCCCCCCCCC[C@@H](O)[C@H](CO)NC(C)=O CRJGESKKUOMBCT-VQTJNVASSA-N 0.000 description 1
- 241000580938 Sapindus Species 0.000 description 1
- 240000003377 Shepherdia canadensis Species 0.000 description 1
- 235000018324 Shepherdia canadensis Nutrition 0.000 description 1
- 206010044625 Trichorrhexis Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 231100000360 alopecia Toxicity 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 229940106189 ceramide Drugs 0.000 description 1
- ZVEQCJWYRWKARO-UHFFFAOYSA-N ceramide Natural products CCCCCCCCCCCCCCC(O)C(=O)NC(CO)C(O)C=CCCC=C(C)CCCCCCCCC ZVEQCJWYRWKARO-UHFFFAOYSA-N 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000007405 data analysis Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000002612 dispersion medium Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 229920002549 elastin Polymers 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 239000013022 formulation composition Substances 0.000 description 1
- 229910021485 fumed silica Inorganic materials 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000003779 hair growth Effects 0.000 description 1
- 230000003676 hair loss Effects 0.000 description 1
- 208000024963 hair loss Diseases 0.000 description 1
- 208000021245 head disease Diseases 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 208000019622 heart disease Diseases 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- SUMDYPCJJOFFON-UHFFFAOYSA-N isethionic acid Chemical compound OCCS(O)(=O)=O SUMDYPCJJOFFON-UHFFFAOYSA-N 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- VVGIYYKRAMHVLU-UHFFFAOYSA-N newbouldiamide Natural products CCCCCCCCCCCCCCCCCCCC(O)C(O)C(O)C(CO)NC(=O)CCCCCCCCCCCCCCCCC VVGIYYKRAMHVLU-UHFFFAOYSA-N 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920003009 polyurethane dispersion Polymers 0.000 description 1
- 229920006264 polyurethane film Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000003658 preventing hair loss Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000007665 sagging Methods 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 229940057950 sodium laureth sulfate Drugs 0.000 description 1
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 description 1
- LADXKQRVAFSPTR-UHFFFAOYSA-M sodium;2-hydroxyethanesulfonate Chemical compound [Na+].OCCS([O-])(=O)=O LADXKQRVAFSPTR-UHFFFAOYSA-M 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 230000003813 thin hair Effects 0.000 description 1
- 238000002054 transplantation Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Biophysics (AREA)
- Molecular Biology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a fluffy shampoo composition which comprises the following components in parts by weight: 0.05-10 parts of polyurethane, 0.05-10 parts of silica disilicide and 0.05-10 parts of wild soybean seed extract; the composition comprises the following components in addition to the three components: anionic surfactant, nonionic surfactant, zwitterionic surfactant, conditioner, pearlizing agent, thickening agent, preservative, pH regulator, essence and water. The fluffy shampoo composition is mild, does not stimulate the scalp, has strong oil control capability, and can endow hair with good fluffy effect.
Description
Technical Field
The invention belongs to the field of daily chemical articles, and relates to a fluffy shampoo composition.
Background
In recent years, the reduction of hair size has become a heart and head disease in more and more people, and the phenomenon of hair loss has a tendency to be younger. The effectiveness of a plurality of hair loss prevention and hair growth promoting products on the market is questioned; the hair transplantation operation has high investment and certain risk. However, if the hair is sufficiently fluffy, the amount of hair can be visually increased significantly. Fluffy hair is formed and dressed by the hair, and the hair is very layered and has gaps instead of clinging and collapsing. According to 2021 scalp health white paper, the efficacy of controlling oil and fluffiness becomes a popular trend, and the proportion of people who consume the oil-control fluffy washing and caring product is increased year by year after 95; and the consumption level of the population after 95 is almost the same as that of the population before 80. The oil-control fluffy product has huge market and wide prospect.
Healthy hair is tough, but keratin in hair is easily damaged by excessive physicochemical treatments such as combing, blowing heat, dyeing, and perming, resulting in rough hair, loss of luster, and thus reduced softness and flexibility, and it is difficult to finish hair due to increased friction, resulting in broken hair or split ends, and hair becomes thin, loses elasticity, and loses vitality and sagging, and thus loses a fluffy feeling. The shampoo is used for cleaning human body oil, sweat stain, cells dropped from the scalp, foreign dust, microorganism, residues of styling products, and bad smell etc. adhered to the scalp and hair, keeping the scalp and hair clean and beautiful. However, shampoos with various additional functions have been increasingly popular due to the diversification of people's needs.
Most of the shampoos in the market today use cationic conditioning agents to induce hair volume, which is generally achieved by cationic charge repulsion to keep the hair repulsive. The cationic conditioner is adsorbed on the surface of hair through the action of electric charges, has stronger accumulation than silicone oil, and is easy to adsorb more dust particles when the hair is contacted with the outside air, continuously stimulates the scalp to secrete grease, and the grease is mixed with the dust to form grease, so that the greasiness of the hair is aggravated. The frequency of use is increased continuously, the more cations are accumulated, pores are tightly wrapped by accumulated matters, the breath of hair follicles is blocked, oxygen permeation is insufficient, hair papilla is gradually shrunk, and then alopecia occurs. Good hair care effects such as softness can be realized in a short period, but the long-term use of the shampoo can reduce the cleaning power of the shampoo, deteriorate the oil control and fluffy effects and increase the oil output of scalp.
Chinese patent application CN 109419643 a discloses a shampoo composition containing aqueous polyurethane, comprising aqueous polyurethane, detersive surfactant, conditioner and carrier; the shampoo composition has the characteristics of good film-forming elasticity, high glossiness, good toughness and non-sticky and greasy hand feeling by unique design of polyurethane molecules in the aqueous polyurethane dispersion, and brings a brand-new natural and plump effect to washed hair. However, the composition improves the hair bulkiness through the water-based polyurethane film forming, and is easy to deposit on the hair in the continuous use process for many times, so that the hair becomes heavier and the bulking effect is influenced. And has no effect on hair collapse caused by scalp oil discharge, and the fluffy effect is not durable.
Chinese patent application CN 109620754 a discloses a low-irritation hair shampoo composition for volumizing hair, which comprises the following components by mass percent: 0.5-1.5% of nonionic surfactant, 9-25% of anionic surfactant, 0.5-5% of zwitterionic surfactant, 0.05-5% of cationic conditioner, 0.05-11.5% of grease, 0.01-10% of suspending agent, 0.01-5% of higher fatty alcohol and the balance of pure water. The hair conditioner adopts mild surfactant and reasonable conditioner matching, and has the effects of small irritation and remarkable increase of hair volume after washing. However, the shampoo composition achieves the effect of voluminous hair by reducing the electrostatic adsorption of the hair through the flocculation deposition of cationic guar gum, polyquaternium-10, a silicone oil conditioner and the like. Has no effect on the collapse of hair caused by the oil on the scalp, and the fluffy effect is not durable.
Therefore, there is a need for a shampoo composition with high cleansing power, high oil control, and good lathering benefits.
Disclosure of Invention
The invention provides a shampoo composition capable of enhancing a fluffy effect, aiming at the problem that fluffy shampoos generally have a fluffy effect in the market. The composition has low irritation and good oil control effect, and can reduce hair static and dandruff.
In order to realize the purpose, the technical scheme adopted by the invention is as follows:
first, a composition is provided, the composition comprising the following components: polyurethane, silica disilicide, and extract of semen glycines.
Further, the composition comprises the following components in parts by weight: 0.05-10 parts of polyurethane, 0.05-10 parts of silica disilicide and 0.05-10 parts of wild soybean seed extract.
Further, the weight ratio of the polyurethane, the silica disilicide and the wild soybean seed extract in the composition is 1-5:0.1-5: 0.1-3.
Further, the weight percentage of the polyurethane in the composition is 1-5%, the weight percentage of the silica disilicide in the composition is 0.1-5%, and the weight percentage of the wild soybean seed extract in the composition is 0.1-3%.
The polyurethane can form a soft film on the surface of hair, so that the hair is provided with stronger toughness, and the hair is reduced in soft collapse. The film can permanently ensure the fluffy effect of hair, can also play a good shape-keeping effect under the condition of high humidity, and has good anti-dandruff performance. The polyurethane can protect hair under high temperature (such as a hair drier), reduce heat injury of hair, has certain anti-frizzy effect, and reduces bifurcation.
The silica disilicide is one of fumed silica, and has good effects of improving fullness and combing property of hair; can control oil continuously, reduce greasiness, and prevent greasy hair from collapse.
The wild soybean seed extract is an oil-in-water emulsifier with HLB up to 14.9, and has strong emulsifying property; has higher charge density, can reduce the interfacial tension between the particles and a dispersion medium, wraps micro particles, prevents flocculation/coagulation caused by steric hindrance and static electricity, can enhance the stability of a product, and is beneficial to reducing the sticky feeling of a system. The wild soybean seed extract also has excellent moisturizing performance, can obviously reduce the percutaneous water loss of skin, moisturizes and simultaneously increases the generation of ceramide, and also has the promotion effect on the synthesis of collagen and elastin; the characteristic enables the hair care composition to provide sufficient nutrition for the skin of the head when being added into the hair care composition, and simultaneously endows the hair with good moisture retention performance, thereby reducing the oil production of the scalp and enhancing the oil control capability of the shampoo.
The wild soybean extract has a chemical structural formula:
further, the composition also comprises the following components: anionic surfactant, nonionic surfactant, zwitterionic surfactant, conditioning agent, pearlizing agent, thickening agent, preservative, pH regulator, essence and water.
Further, the anionic surfactant comprises one or two of cocoyl hydroxyethyl sulfonate sodium and lauroyl sarcosine sodium.
Further, the nonionic surfactant comprises one or more of cocamide MEA, cocamide methyl MEA, and lauric acid monoglyceride.
Further, the zwitterionic surfactant comprises cocamidopropyl betaine, the conditioning agent comprises guar hydroxypropyltrimonium chloride, and the thickening agent comprises PEG-120 glycerol glucoside trioleate.
Further, the preservative comprises one or more of benzyl alcohol, sodium benzoate and sodium salicylate, and the pH regulator comprises one or two of citric acid and arginine.
Further, the composition is applied to the preparation of a fluffy shampoo.
In some embodiments, the method for preparing a relaxing shampoo composition comprises the following steps (the components are added according to the formula amount):
(1) adding guar gum hydroxypropyl trimethyl ammonium chloride into cold water under stirring, adding citric acid after stirring and dispersing, and stirring and dissolving uniformly;
(2) sequentially adding cocamidopropyl betaine, sodium cocoyl hydroxyethyl sulfonate, sodium lauroyl sarcosinate, cocamidomethyl MEA, glycerol laurate and PEG-120 glycerol glucoside trioleate, stirring, heating to 80-85 ℃, uniformly dissolving, keeping the temperature for 5min, and beginning to cool;
(3) cooling to 45 deg.C, sequentially adding benzyl alcohol, sodium salicylate, sodium benzoate, essence, citric acid, polyurethane, semen glycines seed extract, and silica disilicide, and stirring to obtain shampoo.
Compared with the prior art, the invention has the following beneficial effects:
(1) the fluffy shampoo composition belongs to a nonionic composition, has no strong accumulation and deposition, and does not adsorb dust particles with negative charges like cations;
(2) the fluffy shampoo composition is mild, does not stimulate the scalp, and has strong oil control capability;
(3) the fluffy shampoo composition can remove oil, continuously control the oil, keep the hair style and endow hair with a good fluffy effect.
Detailed Description
It should be noted that the raw materials used in the present invention are all common commercial products, and the sources thereof are not particularly limited.
The following reagent sources are exemplary: extract of Glycine max seed (LysoCore Biotech, lysoft) and polyurethane (polyurethane)
C1010 scientific polymer (China) Inc.), disilylated silica (AEROSIL R972 With specialty Chemicals (Shanghai) Inc.), polyglycerol-10 oleate from Kashibai, comparative example 10, from Longsha (China) IncJinhuahuosheng full amino acid shampoo (3474636612475), plant amino acid calendula oil control shampoo (6970197302031) of comparative example 11, and sapindus oil control light shampoo (6944750437713) of comparative example 12.
First, shampoo formulation composition
Examples 1 to 3
Table 1 shows the compositions of the shampoo formulations of examples 1-3.
TABLE 1
Note: in the above table, To 100 represents that the sum of the parts by weight of water and the parts by weight of the other components is 100 parts.
Comparative examples 1 to 9
Table 2 shows the compositions of the shampoo formulations of comparative examples 1-9.
TABLE 2
Note: in the above table, To 100 represents that the sum of the parts by weight of water and the parts by weight of the other components is 100 parts.
Comparative examples 10 to 12
Comparative example 10 is a caribbean platinum revitalizing and plumping amino acid shampoo, comparative example 11 is a plant amino acid calendula oil-control shampoo, and comparative example 12 is a nourishing soapberry oil-control and light shampoo.
The preparation method of the shampoo comprises the following steps:
(1) adding guar gum hydroxypropyl trimethyl ammonium chloride into cold water under stirring, adding citric acid after stirring and dispersing, and stirring and dissolving uniformly;
(2) adding the phase B raw materials one by one according to the sequence in tables 1 and 2, stirring and heating to 80-85 ℃, dissolving uniformly, preserving heat for 5min, and beginning to cool;
(3) cooling to 45 deg.C, sequentially adding the C phase raw materials in the order of Table 1 and 2, and stirring to obtain shampoo.
The physicochemical indexes and the sanitation indexes of the shampoos prepared in examples 1-3 and comparative examples 1-9 are within the requirements of GB/T29679-2013.
Second, test
1. Hair volume change before and after shampoo application
The volume of hair is related to the total combined volume of hair fibers on the head rather than the volume of individual fibers. Depending on the style and length of the hair, individual fibers of the hair contact and help support other fibers, thereby maintaining the structure of the hair as a whole. All hair fibers in the hair braid are fixed at one end, rather than each being fixed at thousands of points on the scalp, and the hair fibers in the hair braid cannot be seen as a space-filling structure as in actual hair, but rather the hairs should support each other to create volume. Therefore, a human body model volume measuring method is used, which is closer to the real human hair, and the test is more reliable.
The dummy heads used in the volume experiments were purchased from amazon, RYHAIR Store, USA and were rinsed with a detergent solution containing 20% sodium laureth sulfate and 5% cocamidopropyl betaine prior to treatment. To reduce tangling, the detergent was brought to the hair with a vent brush (vent brush) and the head was rinsed with running water at 38 ℃ until the rinse water was clear. The model heads were washed twice with 5mL of detergent solution each time, followed by 2.5mL of solution, and after washing, the hair was combed straight with a brush. The hair is then allowed to dry overnight and must be combed as flat as possible so that the intrinsic volume V measured at this point(front)The impact of the hairstyle is minimal.
In the volume experiment, first, the hair was wetted with 38 ℃ water, then 3mL of shampoo was rubbed into the hair for 30 seconds, and then rinsed with 38 ℃ water for more than 60 seconds until the rinse water was clear and transparent. Volume measurements were performed after one administration and five replicates were tested. Apparent changes in the manikin head were measured using a Zeiss Kontron image analyzer connected to a SonyXC-77CE miniature camera (with a 60mm Nikon AF Micro-Nikkor lens). Human body modelThe image is shot by a camera and processed by a computer to obtain the hair volume V of the manikin head(rear)。
The rate of change in volume V% is 100% × [ V ](rear)－V(front)]/V(front)
The data was validated using statistical p-values, with p-values greater than 0.05 indicating that the data was not statistically significant at a 95% confidence level. Note that the data are the average of at least 5 evaluations.
TABLE 3 Hair volume Change with different shampoos
The volume increases reported in table 3 are all statistically significant p <0.05, with a magnitude of 7.7-39.5% of the volume increase, indicating that the compositions of the present invention are very effective in providing a significant increase in hair volume, as compared to examples 1-3 and comparative example 1, where a significant increase in hair volume is observed with a composition containing a relaxing composition (referred to herein as polyurethane, silica disilicide, and glycine seed extract), confirming that the relaxing effect is from the relaxing composition; comparing examples 1-3 with comparative examples 2-8, the volumizing effect of hair is most pronounced when the three components of polyurethane, silica disilicide and wild soybean seed extract are used in combination in a certain ratio, and the effect is worsened in the absence of either or both of these components; comparative example 9 based on example 1, using polyglycerol-10 oleate instead of the extract of the soybean seeds, the rate of change in volume of hair of example 1 was almost twice that of comparative example 9, and comparative example 9 was slightly less effective in relaxing than example 1; comparing examples 1-3 with comparative examples 10-12, the hair volume enhancing effect of the volumizing shampoo compositions of the present invention was found to be superior to that of the commercial products.
2. Evaluation of oil control in human body test
Equipment and equipment use: grease bars (CK, Germany), Meibometer
MB560 scalp oil tester (CK, Germany), skin pencil, rubber band, stopwatch timer, hair dryer.
The test is based on the principle of a grease test photometer, an adhesive tape strip used in a skin grease test method Sebumeter method is coiled into a ring to be contacted with a scalp, the transparency of the test adhesive tape is changed by lipid (grease) in the scalp, then the test adhesive tape strip is placed into a sliding block of an instrument after being flattened, and the sliding block is pushed into the instrument. The light transmittance distribution curve of the adhesive tape can be obtained by testing through a photoelectric tube in an instrument, the peak value of the light transmittance curve distribution represents the content of lipid compounds, namely grease, in the scalp, and the annular top end of the adhesive tape strip is just the part which is in contact with the scalp completely during the test.
90 volunteers with abundant scalp grease secretion are recruited, the age is 20-30 years, the hair is not washed in the evening before the test, the grease secreted by scalp sebaceous glands is easier to stick to hair roots under the condition of comb hair, and the volunteers are required to comb hair as little as possible in the test interval. Examples 1-3 and comparative examples 1-12, 15 shampoos were used, 6 volunteers of each shampoo were randomly drawn for testing.
Before testing, volunteers should sit still for 30min in a room with a temperature of 20-22 deg.C and a humidity of 40-65%, during which time they cannot drink water and beverages. The test part is exposed and placed in a test state to be kept relaxed. The test time points were immediately before and immediately after the sample application, 6 hours after the sample application, and 8 hours after the sample application. The test site was a 1cm x 1cm square drawn on the test area by a skin pen, using a forehead-vertex 5cm area. When the sample is used, the oil content is tested for three times at the test part for analysis. When washing hair, the same person washes hair for volunteers by the same method, and the hair of the volunteers is dried by middle-grade hot air of a blower.
Because scalp oil secretion is a dynamic and continuous process, there is a difference in scalp oil content at different times after shampooing. The evaluation of the oil control effect of the washing and care product actually measures the temporary sebum level of the scalp, namely the content of oil overflowing to the hair follicle after sebum secretion. If the oil on the skin surface is removed, the sebum will be excreted at a very rapid rate, which may take about 4 hours to return to a temporary level, entering the sebum excretion phase. If only the excretion of sebum, not the secretion of sebum is measured after 3-4 hours after shampooing. Therefore, the oil content determination time point of the scalp oil control test should be greater than 4 hours.
And (3) performing data analysis by using SPSS19.0 statistical software, comparing data differences before and after sample comparison, immediately after sample comparison, 6 hours after sample comparison and 8 hours after sample comparison by using T-test or rank sum test, and performing significance analysis.
TABLE 4 sample forehead scalp oil content
| Formulation(s) | Scalp oil content (μ g/cm) before use2) (mean. + -. standard deviation) |
| Example 1 | 450.7±125.1 |
| Example 2 | 473.4±108.1 |
| Example 3 | 455.6±123.6 |
| Comparative example 1 | 453.3±127.6 |
| Comparative example 2 | 490.3±129.6 |
| Comparative example 3 | 469.3±138.9 |
| Comparative example 4 | 468.3±113.7 |
| Comparative example 5 | 444.9±126.9 |
| Comparative example 6 | 479.6±119.6 |
| Comparative example 7 | 465.3±126.4 |
| Comparative example 8 | 461.7±130.4 |
| Comparative example 9 | 477.9±109.6 |
| Comparative example 10 | 459.6±117.5 |
| Comparative example 11 | 478.3±123.6 |
The data in table 4 show that there is no significant difference in the scalp oil content of the test groups as the base value of the study before the samples were used, which also ensures the scientificity and stringency of the subsequent tests.
TABLE 5 forehead scalp oil content at different time periods after sampling
Scalp oil content was tested over the test period for 90 volunteers and the results are shown in table 5. Comparing the scalp oil content data of examples 1-3 and comparative examples 1-12 at 6 and 8 hours after the sample, the scalp oil content is lower when the three components of polyurethane, silica disilicide and wild soybean seed extract in the fluffy composition are used together, and either one or two of the components are lacked or replaced, so that the scalp oil content is increased and the effect is better when the scalp oil content is set within a certain proportion range; at the same time, the relaxing shampoo compositions of the present invention (i.e., examples 1-3) had lower scalp oil content than the commercial products.
3. Human body sensory evaluation
150 volunteers with few hairs and soft and thin hairs are selected, the phenomena of hair collapse, lack of fluffiness and the like in different degrees exist at ordinary times, meanwhile, the symptoms of hair oil and dandruff are accompanied, and before the product is tried, sensory evaluation and hair image evaluation are carried out on the scalps of patients so as to ensure that the volunteers meet the requirements of the test.
Examples 1-3 and comparative examples 1-12, 15 shampoos were used, 10 volunteers of each shampoo were randomly drawn for testing.
The volunteers used the samples once a day for two weeks. In the trial process, the hair flattening degree and the hair fluffiness are respectively recorded, and the comprehensive scoring is carried out after two weeks, which is shown in the following table.
The higher the score the better the effect, the better the score before and after the use of the volunteer.
1-2: invalid, evaluating the bulkiness of the hair after each shampoo, wherein the flat and collapsed state and the fluffy state of the hair are the same as those before use;
2-3: the evaluation of the hair bulkiness is carried out after each shampoo, so that the flat and collapsed state of the hair and the fluffy state of the scurf are improved;
3-5: the evaluation of the bulkiness of the hair after each shampooing is strong, the flat and collapsed state of the hair and the fluffy state of the scurf are improved, the hair becomes relatively thick and fluffy and can last for 24 hours, the head oil is obviously reduced, and the scurf is reduced along with the reduction.
The results of sensory evaluation of the volunteers using the inventive and comparative examples are shown in Table 6.
TABLE 6
As can be seen from the data in table 6, the number of sensibly strong volunteers was higher and the number of sensibly ineffective were lower for examples 1-3, and the absence of any one or two of the components in the fluffy compositions of comparative examples 2-8, and the use of polyglycerol-10 oleate in place of the extract from the soybean seeds of comparative example 9 resulted in a reduction in the number of sensibly strong volunteers, an increase in the number of sensibly ineffective individuals, and a better effect of the fluffy composition at a given rate.
Finally, it should be noted that the above-mentioned contents are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, and that the simple modifications or equivalent substitutions of the technical solutions of the present invention by those of ordinary skill in the art can be made without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. A composition, comprising the following components: polyurethane, silica disilicide, and extract of semen glycines.
2. The composition according to claim 1, characterized in that it comprises the following components in parts by weight: 0.05-10 parts of polyurethane, 0.05-10 parts of silica disilicide and 0.05-10 parts of wild soybean seed extract.
3. The composition of claim 1, wherein the weight ratio of polyurethane, silica disilicide, and extract of glycine soja seeds in said composition is from 1-5:0.1-5: 0.1-3.
4. The composition as claimed in claim 1, wherein the weight percentage of said polyurethane in the composition is 1-5%, the weight percentage of said silica disilicide in the composition is 0.1-5%, and the weight percentage of said extract of the seeds of the wild soybean in the composition is 0.1-3%.
5. The composition according to any one of claims 1 to 3, wherein the composition further comprises the following components: anionic surfactant, nonionic surfactant, zwitterionic surfactant, conditioning agent, pearlizing agent, thickening agent, preservative, pH regulator, essence and water.
6. The composition of claim 5, wherein the anionic surfactant comprises one or both of sodium cocoyl isethionate and sodium lauroyl sarcosinate.
7. The composition according to claim 5, wherein the nonionic surfactant comprises one or more of cocamide MEA, cocamide methyl MEA, and lauric monoglyceride.
8. The composition of claim 5, wherein the zwitterionic surfactant comprises cocamidopropyl betaine, the conditioning agent comprises guar hydroxypropyltrimonium chloride, and the thickening agent comprises PEG-120 glycerol glucoside trioleate.
9. The composition as claimed in claim 5, wherein the preservative comprises one or more of benzyl alcohol, sodium benzoate and sodium salicylate, and the pH regulator comprises one or two of citric acid and arginine.
10. Use of a composition according to any of claims 1 to 9 in the preparation of a relaxing shampoo.
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| CN104207950A (en) * | 2013-06-05 | 2014-12-17 | 上海家化联合股份有限公司 | Application of gas silicon dioxide in increasing amount of hair |
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| CN112842937A (en) * | 2019-11-12 | 2021-05-28 | 万华化学集团股份有限公司 | Hair conditioner containing aqueous nonionic polyurethane dispersion |
| CN114364363A (en) * | 2019-04-16 | 2022-04-15 | 自然进化公司 | Silk hair care composition |
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| KR20110092971A (en) * | 2010-02-11 | 2011-08-18 | 웅진코웨이주식회사 | Mixture extracts having anti-oxidation activity and anti-inflammatory activity and cosmetic composition comprising the same |
| CN104207950A (en) * | 2013-06-05 | 2014-12-17 | 上海家化联合股份有限公司 | Application of gas silicon dioxide in increasing amount of hair |
| CN108096173A (en) * | 2017-12-28 | 2018-06-01 | 广州蜜妆生物科技有限公司 | Mild amino acid shampoo of a kind of green and preparation method thereof |
| CN114364363A (en) * | 2019-04-16 | 2022-04-15 | 自然进化公司 | Silk hair care composition |
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